CN107033638A - A kind of anticorrosive paint and preparation method thereof - Google Patents
A kind of anticorrosive paint and preparation method thereof Download PDFInfo
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- CN107033638A CN107033638A CN201611218781.7A CN201611218781A CN107033638A CN 107033638 A CN107033638 A CN 107033638A CN 201611218781 A CN201611218781 A CN 201611218781A CN 107033638 A CN107033638 A CN 107033638A
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- anticorrosive paint
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- defoamer
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
A kind of anticorrosive paint that the present invention is provided and preparation method thereof, using water, ethylene glycol, titanium dioxide, kaolin, butyl ester and ethyl ester as major ingredient, add foam inhibitor, defoamer, dispersant, conditioning agent and wetting agent to be prepared from by stirring, heating and three big steps of cooling, simple in construction, configuration is convenient, cost is relatively low, non-hazardous, favorable anti-corrosion effect, it is not easy to produce the phenomenon of Paint Falling, overall security is effectively raised, the demand of producer can be more met.
Description
Technical field
The present invention relates to anticorrosive paint technology field, more particularly to a kind of anticorrosive paint and preparation method thereof.
Background technology
Anticorrosive paint, is generally divided into conventional anticorrosive paint and anticorrosive paint, is essential one kind in paint
Coating.Conventional anticorrosive paint is under general condition, etch-proof effect, the longevity that protection non-ferrous metal is used to be played to metal etc.
Life;Anticorrosive paint refers to for relatively conventional anticorrosive paint, can be applied in relatively harsh corrosive environment, and has and can reach
The class anticorrosive paint of protection period longer than conventional anticorrosive paint.But existing most of anticorrosive paints are used in long-time
Afterwards, by the phenomenon come off is easily produced after the erosion and shock of wind and rain, claimed metal is made to get rusty and corrosion
Phenomenon, can not meet the demand of user.
The content of the invention
It is an object of the invention to provide a kind of anticorrosive paint and preparation method thereof, solve existing most of anticorrosive paints and exist
After long-time use, by the phenomenon that comes off easily is produced after the erosion and shock of wind and rain, claimed metal is set to produce life
Rust and the phenomenon of corrosion, the problem of can not meet the demand of user.
The purpose of the present invention can be achieved through the following technical solutions;
A kind of anticorrosive paint and preparation method thereof, its preparation method is as follows:
(1)It is as follows that raw material are weighed by weight:100-300 parts of water, 5-15 parts of ethylene glycol, 45-135 parts of titanium dioxide, kaolinite
It is native 15-45 parts, 9-27 parts of butyl ester, 3-9 parts of ethyl ester, 1-2 parts of foam inhibitor, 1-2 parts of defoamer, 1-3 parts of dispersant, conditioning agent 1-3
Part, 1-3 parts of wetting agent;
(2)Stirring:First titanium dioxide is added with water and is stirred in mixer, temperature is 50 DEG C -60 DEG C, and mixing time is 10-
20min, then adds kaolin and continues to stir 5-15min;
(3)Heating:When temperature rises to 65 DEG C -70 DEG C, add ethylene glycol and continue to stir, when temperature rises to 75 DEG C -80 DEG C, plus
Enter butyl ester to continue to stir with ethyl ester, when temperature rises to 85 DEG C -90 DEG C, add dispersant and conditioning agent, continue to stir;
(4)Cooling:When temperature is down to 70 DEG C -80 DEG C, add foam inhibitor and defoamer, continue to stir, when temperature be down to 50 DEG C -
At 60 DEG C, wetting agent is added, 10-30min is stirred, you can.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described butyl ester and the weight fraction ratio of ethyl ester are 3:
1。
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the size of described kaolinic particle is 0.2-
0.5mm。
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the powder of described titanium dioxide is 300-500nm.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the model EFKA-526 of described foam inhibitor.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, during described defoamer dimethyl silicone polymer with
Silicone emulsion is mixed together, and its proportion of composing is 1:2.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the model H-3275 of described dispersant.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described conditioning agent is dimethylethanolamine.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described wetting agent is the NP-9 of Tao Shi chemical industry.
The beneficial effect of this programme:
A kind of anticorrosive paint that the present invention is provided and preparation method thereof, with water, ethylene glycol, titanium dioxide, kaolin, butyl ester and ethyl ester
For major ingredient, add foam inhibitor, defoamer, dispersant, conditioning agent and wetting agent and prepared by stirring, heating and the big step of cooling three
Form, simple in construction, configuration is convenient, and cost is relatively low, non-hazardous, favorable anti-corrosion effect, it is not easy to produce the phenomenon of Paint Falling, have
What is imitated improves overall security, can more meet the demand of producer.
Embodiment
Embodiment 1:A kind of anticorrosive paint and preparation method thereof, its preparation method is as follows:
(1)It is as follows that raw material are weighed by weight:100 parts of water, 5 parts of ethylene glycol, 45 parts of titanium dioxide, 15 parts of kaolin, butyl ester 9
Part, 3 parts of ethyl ester, 1 part of foam inhibitor, 1 part of defoamer, 1 part of dispersant, 1 part of conditioning agent, 1 part of wetting agent;
(2)Stirring:First titanium dioxide is added with water and is stirred in mixer, temperature is 50 DEG C, and mixing time is 10min, so
Kaolin is added afterwards to continue to stir 5min;
(3)Heating:When temperature rises to 65 DEG C, add ethylene glycol and continue to stir, when temperature rises to 75 DEG C, add butyl ester and second
Ester continues to stir, when temperature rises to 85 DEG C, adds dispersant and conditioning agent, continues to stir;
(4)Cooling:When temperature is down to 70 DEG C, foam inhibitor and defoamer are added, continues to stir, when temperature is down to 50 DEG C, plus
Enter wetting agent, stir 10min, you can.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described butyl ester and the weight fraction ratio of ethyl ester are 3:
1。
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the size of described kaolinic particle is 0.2mm.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the powder of described titanium dioxide is 300nm.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the model EFKA-526 of described foam inhibitor.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, during described defoamer dimethyl silicone polymer with
Silicone emulsion is mixed together, and its proportion of composing is 1:2.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the model H-3275 of described dispersant.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described conditioning agent is dimethylethanolamine.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described wetting agent is the NP-9 of Tao Shi chemical industry.
Embodiment 2:A kind of anticorrosive paint and preparation method thereof, its preparation method is as follows:
(1)It is as follows that raw material are weighed by weight:200 parts of water, 10 parts of ethylene glycol, 90 parts of titanium dioxide, 30 parts of kaolin, butyl ester
18 parts, 6 parts of ethyl ester, 1 part of foam inhibitor, 2 parts of defoamer, 2 parts of dispersant, 2 parts of conditioning agent, 2 parts of wetting agent;
(2)Stirring:First titanium dioxide is added with water and is stirred in mixer, temperature is 55 DEG C, and mixing time is 15min, so
Kaolin is added afterwards to continue to stir 10min;
(3)Heating:When temperature rises to 65 DEG C -70 DEG C, add ethylene glycol and continue to stir, when temperature rises to 77 DEG C, add fourth
Ester continues to stir with ethyl ester, when temperature rises to 88 DEG C, adds dispersant and conditioning agent, continues to stir;
(4)Cooling:When temperature is down to 75 DEG C, foam inhibitor and defoamer are added, continues to stir, when temperature is down to 55 DEG C, plus
Enter wetting agent, stir 20min, you can.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described butyl ester and the weight fraction ratio of ethyl ester are 3:
1。
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the size of described kaolinic particle is 0.3mm.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the powder of described titanium dioxide is 400nm.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the model EFKA-526 of described foam inhibitor.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, during described defoamer dimethyl silicone polymer with
Silicone emulsion is mixed together, and its proportion of composing is 1:2.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the model H-3275 of described dispersant.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described conditioning agent is dimethylethanolamine.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described wetting agent is the NP-9 of Tao Shi chemical industry.
Embodiment 3:A kind of anticorrosive paint and preparation method thereof, its preparation method is as follows:
(1)It is as follows that raw material are weighed by weight:300 parts of water, 15 parts of ethylene glycol, 135 parts of titanium dioxide, 45 parts of kaolin, fourth
27 parts of ester, 9 parts of ethyl ester, 2 parts of foam inhibitor, 2 parts of defoamer, 3 parts of dispersant, 3 parts of conditioning agent, 3 parts of wetting agent;
(2)Stirring:First titanium dioxide is added with water and is stirred in mixer, temperature is 60 DEG C, and mixing time is 20min, so
Kaolin is added afterwards to continue to stir 15min;
(3)Heating:When temperature rises to 65 DEG C -70 DEG C, add ethylene glycol and continue to stir, when temperature rises to 80 DEG C, add fourth
Ester continues to stir with ethyl ester, when temperature rises to 90 DEG C, adds dispersant and conditioning agent, continues to stir;
(4)Cooling:When temperature is down to 80 DEG C, foam inhibitor and defoamer are added, continues to stir, when temperature is down to 60 DEG C, plus
Enter wetting agent, stir 30min, you can.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described butyl ester and the weight fraction ratio of ethyl ester are 3:
1。
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the size of described kaolinic particle is 0.5mm.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the powder of described titanium dioxide is 500nm.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the model EFKA-526 of described foam inhibitor.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, during described defoamer dimethyl silicone polymer with
Silicone emulsion is mixed together, and its proportion of composing is 1:2.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, the model H-3275 of described dispersant.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described conditioning agent is dimethylethanolamine.
Above-mentioned a kind of anticorrosive paint and preparation method thereof, wherein, described wetting agent is the NP-9 of Tao Shi chemical industry.
A kind of anticorrosive paint that the present invention is provided and preparation method thereof, with water, ethylene glycol, titanium dioxide, kaolin, butyl ester with
Ethyl ester is major ingredient, adds foam inhibitor, defoamer, dispersant, conditioning agent and wetting agent by stirring, heating and three big steps of cooling
It is prepared from, simple in construction, configuration is convenient, and cost is relatively low, non-hazardous, favorable anti-corrosion effect, it is not easy to produce showing for Paint Falling
As effectively raising overall security, can more meet the demand of producer.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, the change or replacement that can be readily occurred in,
It should all cover within the scope of the present invention.Therefore, protection scope of the present invention should be with the protection domain of claims
It is defined.
Claims (9)
1. a kind of anticorrosive paint and preparation method thereof, it is characterized in that, its preparation method is as follows:
(1)It is as follows that raw material are weighed by weight:100-300 parts of water, 5-15 parts of ethylene glycol, 45-135 parts of titanium dioxide, kaolinite
It is native 15-45 parts, 9-27 parts of butyl ester, 3-9 parts of ethyl ester, 1-2 parts of foam inhibitor, 1-2 parts of defoamer, 1-3 parts of dispersant, conditioning agent 1-3
Part, 1-3 parts of wetting agent;
(2)Stirring:First titanium dioxide is added with water and is stirred in mixer, temperature is 50 DEG C -60 DEG C, and mixing time is 10-
20min, then adds kaolin and continues to stir 5-15min;
(3)Heating:When temperature rises to 65 DEG C -70 DEG C, add ethylene glycol and continue to stir, when temperature rises to 75 DEG C -80 DEG C, plus
Enter butyl ester to continue to stir with ethyl ester, when temperature rises to 85 DEG C -90 DEG C, add dispersant and conditioning agent, continue to stir;
(4)Cooling:When temperature is down to 70 DEG C -80 DEG C, add foam inhibitor and defoamer, continue to stir, when temperature be down to 50 DEG C -
At 60 DEG C, wetting agent is added, 10-30min is stirred, you can.
2. a kind of anticorrosive paint as claimed in claim 1 and preparation method thereof, it is characterized in that, described butyl ester and the weight of ethyl ester
It is 3 to measure score ratio:1.
3. a kind of anticorrosive paint as claimed in claim 1 and preparation method thereof, it is characterized in that, described kaolinic particle
Size is 0.2-0.5mm.
4. a kind of anticorrosive paint as claimed in claim 1 and preparation method thereof, it is characterized in that, the powder of described titanium dioxide is
300-500nm。
5. a kind of anticorrosive paint as claimed in claim 1 and preparation method thereof, it is characterized in that, the model of described foam inhibitor
EFKA-526。
6. a kind of anticorrosive paint as claimed in claim 1 and preparation method thereof, it is characterized in that, with poly- two during described defoamer
Methylsiloxane is mixed together with silicone emulsion, and its proportion of composing is 1:2.
7. a kind of anticorrosive paint as claimed in claim 1 and preparation method thereof, it is characterized in that, the model of described dispersant
H-3275。
8. a kind of anticorrosive paint as claimed in claim 1 and preparation method thereof, it is characterized in that, described conditioning agent is dimethyl
Monoethanolamine.
9. a kind of anticorrosive paint as claimed in claim 1 and preparation method thereof, it is characterized in that, described wetting agent is Tao Shiization
The NP-9 of work.
Priority Applications (1)
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CN201611218781.7A CN107033638A (en) | 2016-12-26 | 2016-12-26 | A kind of anticorrosive paint and preparation method thereof |
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CN201611218781.7A CN107033638A (en) | 2016-12-26 | 2016-12-26 | A kind of anticorrosive paint and preparation method thereof |
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Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102295864A (en) * | 2010-06-25 | 2011-12-28 | 苏州美亚美建筑涂料有限公司 | Styrene-acrylate emulsion sealing primer |
CN102796427A (en) * | 2012-08-10 | 2012-11-28 | 中山大桥化工企业集团中山智亨实业发展有限公司 | Aqueous high-performance monocomponent primer-topcoat anti-corrosion coating |
CN103319958A (en) * | 2013-05-31 | 2013-09-25 | 句容亿格纳米材料厂 | Titanium dioxide composite paint and preparation method therefor |
CN103725127A (en) * | 2013-12-12 | 2014-04-16 | 青岛海洋新材料科技有限公司 | Marine climate resistant high-strength coating and preparation process thereof |
CN104098972A (en) * | 2014-08-07 | 2014-10-15 | 江苏美亿晨新材料科技有限公司 | Water-based antirust and antiseptic paint for metal and preparation method thereof |
CN104449389A (en) * | 2014-11-10 | 2015-03-25 | 厦门防水博士建筑工程有限公司 | Metal roof coating and preparation method thereof |
CN104893499A (en) * | 2015-05-27 | 2015-09-09 | 芜湖县双宝建材有限公司 | Corrosion-resistant high-adhesive-force water-based metal paint |
-
2016
- 2016-12-26 CN CN201611218781.7A patent/CN107033638A/en active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102295864A (en) * | 2010-06-25 | 2011-12-28 | 苏州美亚美建筑涂料有限公司 | Styrene-acrylate emulsion sealing primer |
CN102796427A (en) * | 2012-08-10 | 2012-11-28 | 中山大桥化工企业集团中山智亨实业发展有限公司 | Aqueous high-performance monocomponent primer-topcoat anti-corrosion coating |
CN103319958A (en) * | 2013-05-31 | 2013-09-25 | 句容亿格纳米材料厂 | Titanium dioxide composite paint and preparation method therefor |
CN103725127A (en) * | 2013-12-12 | 2014-04-16 | 青岛海洋新材料科技有限公司 | Marine climate resistant high-strength coating and preparation process thereof |
CN104098972A (en) * | 2014-08-07 | 2014-10-15 | 江苏美亿晨新材料科技有限公司 | Water-based antirust and antiseptic paint for metal and preparation method thereof |
CN104449389A (en) * | 2014-11-10 | 2015-03-25 | 厦门防水博士建筑工程有限公司 | Metal roof coating and preparation method thereof |
CN104893499A (en) * | 2015-05-27 | 2015-09-09 | 芜湖县双宝建材有限公司 | Corrosion-resistant high-adhesive-force water-based metal paint |
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Application publication date: 20170811 |