CN107032472A - Portable over-saturation High Purity Hydrogen molecule water preparation apparatus and its application method - Google Patents
Portable over-saturation High Purity Hydrogen molecule water preparation apparatus and its application method Download PDFInfo
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- CN107032472A CN107032472A CN201710211781.2A CN201710211781A CN107032472A CN 107032472 A CN107032472 A CN 107032472A CN 201710211781 A CN201710211781 A CN 201710211781A CN 107032472 A CN107032472 A CN 107032472A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
- F17C1/00—Pressure vessels, e.g. gas cylinder, gas tank, replaceable cartridge
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
- F17C13/00—Details of vessels or of the filling or discharging of vessels
- F17C13/002—Details of vessels or of the filling or discharging of vessels for vessels under pressure
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
- F17C2201/00—Vessel construction, in particular geometry, arrangement or size
- F17C2201/01—Shape
- F17C2201/0104—Shape cylindrical
- F17C2201/0119—Shape cylindrical with flat end-piece
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
- F17C2201/00—Vessel construction, in particular geometry, arrangement or size
- F17C2201/03—Orientation
- F17C2201/035—Orientation with substantially horizontal main axis
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
- F17C2201/00—Vessel construction, in particular geometry, arrangement or size
- F17C2201/05—Size
- F17C2201/056—Small (<1 m3)
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
- F17C2203/00—Vessel construction, in particular walls or details thereof
- F17C2203/06—Materials for walls or layers thereof; Properties or structures of walls or their materials
- F17C2203/0634—Materials for walls or layers thereof
- F17C2203/0636—Metals
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
- F17C2221/00—Handled fluid, in particular type of fluid
- F17C2221/01—Pure fluids
- F17C2221/012—Hydrogen
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- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
- F17C2223/00—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
- F17C2223/01—Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the phase
- F17C2223/0107—Single phase
- F17C2223/0123—Single phase gaseous, e.g. CNG, GNC
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F17—STORING OR DISTRIBUTING GASES OR LIQUIDS
- F17C—VESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
- F17C2270/00—Applications
- F17C2270/05—Applications for industrial use
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/30—Hydrogen technology
- Y02E60/32—Hydrogen storage
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- General Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
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- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
Portable over-saturation High Purity Hydrogen molecule water preparation apparatus and its application method, belong to hydrogen molecule water preparing technical field, device is by alloy-type hydrogen-storage tank, semiconductor refrigerating seat, cup and hydrogen refining device etc. are constituted, apparatus structure is novel, prepared by hydrogen water and alloy-type hydrogen-storage tank is flushed with hydrogen two big steps, solve the hydrogen water existed in the past and prepare and there is accessory substance, other ions are introduced in water, the hydrogen molecule concentration actually drunk is low, can not be simple and efficient realize hydrogen water prepare, device structure complexity is huge, the shortcomings of being unfavorable for carrying, present invention dramatically reduces the volume of equipment, hydrogen water is substantially reduced to prepare and the distance between drink, operate simple and convenient, significantly improve the concentration of high-purity hydrogen in hydrogen water, obtain more preferably medical health effect.
Description
Technical field
The invention belongs to hydrogen molecule water preparing technical field, it is related to a kind of hydrogen molecule water Preparation equipment and application method,
Particularly relate to a kind of portable over-saturation High Purity Hydrogen molecule water preparation apparatus and its application method.
Background technology
A large amount of biological study evidences show that hydrogen has the work of selectivity neutralization hydroxyl radical free radical and nitrous acid anion
With this is the basis that hydrogen treats disease to anti-oxidative damage.Research shows that the disease type that hydrogen can be treated is very more, example
Such as encephalopathic, cerebral ischemia, senile dementia, Parkinson after malignant tumour, colitis, anthracemia.On November 30th, 2016, day
This MHLW " inhaling hydrogen treatment cardiac arrest syndrome " includes " the advanced medical B classes of Japan " system.There is scholar's comment to think,
Hydrogen inhalation therapy is a kind of：Allow heartbeat recover after patient's suction hydrogen, so as to play protection life and brain function, allow patient
Early recovery and the innovative treatment method for returning society.This is a kind of first official conducted a research on hydrogen as medicine
Certification, is included in medical item by hydrogen suction, has started new era of hydrogen medical research.
Hydrogen has been subjected to extensive concern and approved now as a kind of instrument of disease treatment.Japan and China are permitted
Many universities and medical institutions all carry out clinical research in succession.More than wherein comparing is to drink hydrogen water, injection hydrogen water and breathing hydrogen.
It is one of them critically important selection to drink hydrogen water.The conventional method of hydrogen water is manufactured mainly by the method for electrolysis water, due to electricity
Solution preocess easily produces certain accessory substance, is gradually either directly solubilised the technology substitution of hydrogen.In addition, also having using magnesium metal and water
The method of reaction manufacture hydrogen water, many hydrogen rods substantially belong to this principle on the market at present, but this process also can be in water
More magnesium ion is introduced, largely intake magnesium ion may be adversely affected to body for a long time as health-care drinking-water.In addition, city
Also a large amount of easy-to-draw pot hydrogen water sell on field, but hydrogen molecule is a kind of smallest molecule for being only second to helium, it spreads and oozed
Thoroughly very competent, for plastics and metal, hydrogen molecule can be easier the gap passed through and escape, therefore these are easy-to-draw
Pot hydrogen water is after transport and long-term preservation, the severity that its density of hydrogen can decline, it is impossible to play good health care
Effect.Therefore, the more reliable more preferable hydrogen water Preparation equipment of effect is developed very necessary.
The content of the invention
The present invention prepares to exist for the hydrogen water that existed in the past introduces other ions in accessory substance, water, the hydrogen actually drunk
Molecular concentration is low, it is impossible to which simple and efficient to realize prepared by hydrogen water, device structure complexity is huge, the shortcomings of being unfavorable for carrying there is provided
A kind of portable over-saturation High Purity Hydrogen molecule water preparation apparatus and its application method, it is a kind of efficient its object is to provide, it is easy
Quickly, safety, hydrogen gas dissolved water concentration are higher, the portable over-saturation High Purity Hydrogen molecular water Preparation equipment of compact conformation and its
Application method.
The technical scheme is that：Portable over-saturation High Purity Hydrogen molecule water preparation apparatus, it is characterised in that：The system
Standby device is made up of alloy-type hydrogen-storage tank, semiconductor refrigerating seat, cup and hydrogen refining device；
The alloy-type hydrogen-storage tank is made up of steel cylinder, powder, foam copper coin and multi-hole copper tube, and the foam copper coin is disposed on
The interior of steel bottle, the multi-hole copper tube is passed through in the middle of the foam copper coin and formed a fixed connection with foam copper plate, described
The tube wall of multi-hole copper tube is provided with stomata, and the stomata is communicated with foam copper coin, and the powder is placed between the foam copper coin
Every place；
The hydrogen refining device sinters refinement slices by air chamber, stainless steel and supporter is constituted, and the stainless steel sintering refinement slices are set
Put in the bottom of the air chamber；The hydrogen refining device is arranged on the bottom of the cup, and the top of the cup is provided with and water
The Drinking cup lid that cup is sealed and is fastenedly connected, the Drinking cup lid is provided with pressure releasing device, and the cup is integrally provided in the semiconductor
In refrigeration seat；
The outlet of the alloy-type hydrogen-storage tank is connected with needle-valve, and the pipeline of the needle-valve and alloy-type hydrogen-storage tank is provided with filtering
Piece, the needle-valve exit parallel connection is provided with pressure gauge and snap joint, and the outlet of the snap joint is passed through by stainless steel tube
It is connected after the Drinking cup lid with the hydrogen refining device, outer wall and the Drinking cup lid formation of the stainless steel tube are sealedly and fixedly connected.
The outer wall of the stainless steel tube is sealedly connected and fixed with Drinking cup lid by argon arc welding.
The Drinking cup lid is coordinated with cup by screw thread and silicagel pad tightens sealing.
The powder is La0.55Ce0.45Ni4Co hydrogen-storage alloy powders.
The foam copper coin and multi-hole copper tube are fixed by soldering connection, the porosity ranges of foam copper coin for 80%~
90%。
The pore-size distribution of the stainless steel sintering refinement slices is 50~500nm.
The application method of portable over-saturation High Purity Hydrogen molecule water preparation apparatus, it is characterised in that comprise the following steps：
(1) hydrogen water preparation process：
Cup is put into semiconductor refrigerating seat by (1-1) first；
(1-2) starts semiconductor refrigerating seat, starts refrigeration, drinking water is poured into cup；
Hydrogen refining device is put into the bottom of cup by (1-3), tightens Drinking cup lid；
(1-4) opens needle-valve and hydrogen is filled with into cup, and hydrogen flowing velocity is adjusted by needle-valve；
(1-5) treats that gauge hand is stable and points to 1MPa or so, closes needle-valve, waits 20~30 minutes；
(1-6) presses the hydrogen in pressure releasing device releasing cup, closes semiconductor refrigerating seat, outwards winding Drinking cup lid, obtains over-saturation high
Pure hydrogen molecule water, takes out cup and drinks hydrogen water；
(2) hydrogen of alloy-type hydrogen-storage tank fills step：
(2-1) looks first at gauge hand, when instruction pressure<0.8MPa, prepares to fill alloy-type hydrogen-storage tank progress hydrogen；
(2-2) closes needle-valve, and alloy-type hydrogen-storage tank, filter, pressure gauge, needle-valve are pulled out at snap joint as entirety；
(2-3) and then alloy-type hydrogen-storage tank, filter, pressure gauge, needle-valve are connected as entirety with the snap joint of hydrogen source, its
Middle hydrogen source is the Steel Cylinder for High-purity Hydrogen that commercially available purity is 99.999%, opens needle-valve, gas is flushed with hydrogen into alloy-type hydrogen-storage tank, is observed
Gauge hand, treats that gauge hand points to 1.5MPa, closes needle-valve；
(2-4) pulls out alloy-type hydrogen-storage tank, filter, pressure gauge, ball valve as entirety from hydrogen source snap joint, then will close
Metal type hydrogen-storage tank, filter, pressure gauge, needle-valve are as entirety from the quick of portable over-saturation High Purity Hydrogen molecular water Preparation equipment
Joint is connected.
Beneficial effects of the present invention are：Portable over-saturation High Purity Hydrogen molecule water preparation apparatus proposed by the present invention and its make
With method, device is made up of alloy-type hydrogen-storage tank, semiconductor refrigerating seat, cup and hydrogen refining device etc., and apparatus structure is novel, leads to
Cross the preparation of hydrogen water and alloy-type hydrogen-storage tank is flushed with hydrogen two big steps, solve the hydrogen water preparation existed in the past and exist in accessory substance, water
Other ions are introduced, the hydrogen molecule concentration actually drunk is low, it is impossible to which simple and efficient realizing is prepared by hydrogen water, device structure is complicated huge
Greatly, the shortcomings of being unfavorable for carrying, present invention dramatically reduces the volume of equipment, between substantially reducing the preparation of hydrogen water and drinking
Distance, operates simple and convenient, significantly improves the concentration of high-purity hydrogen in hydrogen water, obtains more preferably medical health effect.
Brief description of the drawings
Fig. 1 is the overall structure diagram of apparatus of the present invention.
Fig. 2 is alloy-type hydrogen-storage tank internal structure schematic diagram in the present invention.
Fig. 3 is hydrogen refining device structural representation in the present invention.
Fig. 4 is hydrogen molecule water preparation flow figure of the present invention.
The flow chart that Fig. 5 is flushed with hydrogen for the present invention to alloy-type hydrogen-storage tank.
In figure：Alloy-type hydrogen-storage tank 1, steel cylinder 1-1, foam copper coin 1-2, powder 1-3, porous steel pipe 1-4, stomata 1-5, mistake
Filter disc 2, needle-valve 3, pressure gauge 4, snap joint 5, semiconductor refrigerating seat 6, cup 7, Drinking cup lid 7-1, pressure releasing device 7-2, drinking water
8th, hydrogen refining device 9, stainless steel sintering refinement slices 9-1, supporter 9-2, air chamber 9-3.
Embodiment
The invention will be further described below in conjunction with the accompanying drawings：
As shown in figure 1, portable over-saturation High Purity Hydrogen molecule water preparation apparatus, alloy-type hydrogen-storage tank 1 is with filter 2 by stainless
Steel pipe and VCR joints are connected with filter 2, and filter 2 is connected by VCR joints and stainless steel tube with the entrance of needle-valve 3, needle-valve 3
Outlet be connected respectively with pressure gauge 4 and the entrance of snap joint 5 by stainless steel tube, snap joint 5 outlet pass through stainless steel tube
It is connected with hydrogen refining device 9, the outer wall of stainless steel tube is connected with Drinking cup lid 7-1 by argon arc welding simultaneously, and water 8 is housed in cup 7,
Hydrogen refining device 9 is placed on the bottom of cup 7, and Drinking cup lid 7-1 is coordinated with cup 7 by screw thread and silicagel pad to be tightened and seal, whole
Individual cup 7 is placed in semiconductor refrigerating seat 6, and pressure releasing device 7-2 is housed on Drinking cup lid 7-1.Cup 7, Drinking cup lid 7-1, tracheae, hydrogen
Refining device 9 is made of the stainless steel material of food-grade 304, and the silicagel pad of sealing is made of food grade silicone.Semiconductor
Refrigeration seat 6 can make the water cooling in cup to less than 5 DEG C.In low temperature, high pressure, be sufficiently mixed under conditions of, can make high-purity
Rapidly over-saturation is dissolved in the water hydrogen, greatly improves its medical health effect.
As shown in Fig. 2 including steel cylinder in portable over-saturation High Purity Hydrogen molecule water preparation apparatus, alloy-type hydrogen-storage tank 1
1-1, La0.55Ce0.45Ni4Co powder 1-3, foam copper coin 1-2, multi-hole copper tube 1-4.Multi-hole copper tube 1-4 is from foam copper coin 1-2's
Centre is passed through, and foam copper coin 1-2 and multi-hole copper tube 1-4 are connected by way of soldering in certain intervals, in link position
Between, the interval location that multi-hole copper tube 1-4 sides are provided between stomata 1-5, foam copper coin 1-2 is filled with La0.55Ce0.45Ni4Co powder
Last 1-3, wherein multi-hole copper tube 1-4 mainly realize the conveying of hydrogen, and foam copper coin 1-2 mainly realizes efficient heat and mass, together
When play the effect of filtering, prevent La0.55Ce0.45Ni4Co powder 1-3 scurries into multi-hole copper tube 1-4 and resulted in blockage.
La0.55Ce0.45Ni4Co is high capacity hydrogen storage alloy, ensure that and safely and efficiently preserves a large amount of high-purity hydrogens at room temperature, tool
There are good suction hydrogen desorption kineticses, hydrogen platform pressure is put in the 1MPa suctions that maintain that can stablize at room temperature.
As shown in figure 3, portable over-saturation High Purity Hydrogen molecule water preparation apparatus, hydrogen refining device includes air chamber 9-3, it is stainless
Steel sinters refinement slices 9-1, supporter 9-2.Stainless steel sintering refinement slices 9-1 can make high-purity hydrogen be refined into nano grade air bubbles, make
High-purity hydrogen and water are sufficiently mixed.The pore-size distribution of wherein stainless steel sintering refinement slices is 50~500nm.
As shown in figure 4, the application method of portable over-saturation High Purity Hydrogen molecule water preparation apparatus, is prepared super using the equipment
The flow of saturation High Purity Hydrogen molecular water：Cup 7 is put into semiconductor refrigerating seat 6 first, then starts semiconductor refrigerating seat 6,
Start refrigeration, drinking water 8 is poured into cup 7, hydrogen refining device 9 is put into the bottom of cup 7, Drinking cup lid 7-1 is tightened.Open
Needle-valve 3 is filled with hydrogen into cup 7, adjusts hydrogen flowing velocity by needle-valve 3 in this process.Treat that the pointer of pressure gauge 4 is steady
Surely 1MPa or so is pointed to, needle-valve is closed, waited 20~30 minutes, the hydrogen in pressure releasing device 7-2 releasing cups 7 is pressed, closes half
Conductor refrigeration seat 6, outwards winding Drinking cup lid 7-1, obtains over-saturation High Purity Hydrogen molecular water, takes out cup 7 and drinks hydrogen water.
As shown in figure 5, the application method of portable over-saturation High Purity Hydrogen molecule water preparation apparatus, alloy-type hydrogen-storage tank 1 is passed through
Cross after long-term use, the hydrogen of its inside storage is exhausted, it is necessary to be inflated it to reuse again, it mainly flows
Cheng Wei：The pointer of pressure gauge 4 is looked first at, when instruction pressure<0.8MPa, prepares to fill the progress hydrogen of alloy-type hydrogen-storage tank 1, closes
Needle-valve 3 is closed, by alloy-type hydrogen-storage tank 1, filter 2, pressure gauge 4, needle-valve 3 is pulled out as entirety at snap joint 5, then will
Alloy-type hydrogen-storage tank 1, filter 2, pressure gauge 4, needle-valve 3 is connected as overall with the snap joint of hydrogen source, and wherein hydrogen source is city
The Steel Cylinder for High-purity Hydrogen that purity is 99.999% is sold, needle-valve 3 is opened, gas is flushed with hydrogen into alloy-type hydrogen-storage tank 1, observation pressure gauge 4 refers to
Pin, treats that the pointer of pressure gauge 4 points to 1.5MPa, closes needle-valve 3.By alloy-type hydrogen-storage tank 1, filter 2, pressure gauge 4, ball valve 3 is made
Pulled out for entirety from hydrogen source snap joint, then by alloy-type hydrogen-storage tank 1, filter 2, pressure gauge 4, needle-valve 3 as it is overall from
Connected at the snap joint of portable over-saturation High Purity Hydrogen molecular water Preparation equipment.
Claims (7)
1. portable over-saturation High Purity Hydrogen molecule water preparation apparatus, it is characterised in that：The preparation facilities is by alloy-type hydrogen-storage tank
(1), semiconductor refrigerating seat (6), cup (7) and hydrogen refining device (9) composition；
The alloy-type hydrogen-storage tank (1) is by steel cylinder (1-1), powder (1-3), foam copper coin (1-2) and multi-hole copper tube (1-4) structure
The steel cylinder (1-1) is disposed on into, the foam copper coin (1-2) internal, the multi-hole copper tube (1-4) is from the foam copper
Pass through and formed a fixed connection with foam copper coin (1-2) in the middle of plate (1-2), the tube wall of the multi-hole copper tube (1-4) is provided with gas
Hole (1-5), the stomata (1-5) communicates with foam copper coin (1-2), and the powder (1-3) is placed in the foam copper coin (1-2)
Interval；
The hydrogen refining device (9) sinters refinement slices (9-1) by air chamber (9-3), stainless steel and supporter (9-2) is constituted, described
Stainless steel sintering refinement slices (9-1) are arranged on the air chamber (9-3) bottom；The hydrogen refining device (9) is arranged on the water
The bottom of cup (7), the top of the cup (7) is provided with the Drinking cup lid (7-1) for sealing and being fastenedly connected with cup (7), the water
Cup lid (7-1) is provided with pressure releasing device (7-2), and the cup (7) is integrally provided in the semiconductor refrigerating seat (6)；
The outlet of the alloy-type hydrogen-storage tank (1) is connected with needle-valve (3), the needle-valve (3) and the pipe of alloy-type hydrogen-storage tank (1)
Road is provided with filter (2), and needle-valve (3) the exit parallel connection is provided with pressure gauge (4) and snap joint (5), described quickly to connect
Head (5) outlet be connected afterwards with the hydrogen refining device (9-1) through the Drinking cup lid (7-1) by stainless steel tube, it is described not
The outer wall of rust steel pipe and Drinking cup lid (7-1) formation are sealedly and fixedly connected.
2. portable over-saturation High Purity Hydrogen molecule water preparation apparatus according to claim 1, it is characterised in that：It is described stainless
The outer wall of steel pipe is sealedly connected and fixed with Drinking cup lid (7-1) by argon arc welding.
3. portable over-saturation High Purity Hydrogen molecule water preparation apparatus according to claim 1, it is characterised in that：The cup
Lid (7-1) is coordinated with cup (7) by screw thread and silicagel pad tightens sealing.
4. portable over-saturation High Purity Hydrogen molecule water preparation apparatus according to claim 1, it is characterised in that：The powder
(1-3) is La0.55Ce0.45Ni4Co hydrogen-storage alloy powders.
5. portable over-saturation High Purity Hydrogen molecule water preparation apparatus according to claim 1, it is characterised in that：The foam
Copper coin (1-2) and multi-hole copper tube (1-4) are fixed by soldering connection, and the porosity ranges of foam copper coin (1-2) are 80%~90%.
6. portable over-saturation High Purity Hydrogen molecule water preparation apparatus according to claim 1, it is characterised in that：It is described stainless
The pore-size distribution of steel sintering refinement slices (9-1) is 50~500nm.
7. the application method of movable type over-saturation High Purity Hydrogen molecule water preparation apparatus as claimed in claim 1, it is characterised in that
Comprise the following steps：
(1) hydrogen water preparation process：
Cup (7) is put into semiconductor refrigerating seat (6) by (1-1) first；
(1-2) starts semiconductor refrigerating seat (6), starts refrigeration, drinking water (8) is poured into cup (7)；
Hydrogen refining device (9) is put into the bottom of cup (7) by (1-3), tightens Drinking cup lid (7-1)；
(1-4) opens needle-valve (3) and is filled with hydrogen into cup (7), and hydrogen flowing velocity is adjusted by needle-valve (3)；
(1-5) treats that pressure gauge (4) pointer is stable and points to 1MPa or so, closes needle-valve (3), waits 20~30 minutes；
(1-6) presses the hydrogen in pressure releasing device (7-2) releasing cup (7), closes semiconductor refrigerating seat (6), outwards winding Drinking cup lid (7-
1) over-saturation High Purity Hydrogen molecular water, is obtained, cup (7) is taken out and drinks hydrogen water；
(2) hydrogen of alloy-type hydrogen-storage tank fills step：
(2-1) looks first at pressure gauge (4) pointer, when instruction pressure<0.8MPa, prepares to carry out hydrogen to alloy-type hydrogen-storage tank (1)
Gas is filled；
(2-2) close needle-valve (3), using alloy-type hydrogen-storage tank (1), filter (2), pressure gauge (4), needle-valve (3) as integrally from
Snap joint (5) place is pulled out；
(2-3) then using alloy-type hydrogen-storage tank (1), filter (2), pressure gauge (4), needle-valve (3) as overall fast with hydrogen source
Quick coupling is connected, and wherein hydrogen source is the Steel Cylinder for High-purity Hydrogen that commercially available purity is 99.999%, opens needle-valve (3), and hydrogen is store to alloy-type
Gas is flushed with hydrogen in tank (1), pressure gauge (4) pointer is observed, treats that pressure gauge (4) pointer points to 1.5MPa, closes needle-valve (3)；
(2-4) is using alloy-type hydrogen-storage tank (1), filter (2), pressure gauge (4), ball valve (3) as overall from hydrogen source snap joint
Pull out, then using alloy-type hydrogen-storage tank (1), filter (2), pressure gauge (4), needle-valve (3) as overall from portable over-saturation
Connected at the snap joint of High Purity Hydrogen molecular water Preparation equipment.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710211781.2A CN107032472A (en) | 2017-04-01 | 2017-04-01 | Portable over-saturation High Purity Hydrogen molecule water preparation apparatus and its application method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710211781.2A CN107032472A (en) | 2017-04-01 | 2017-04-01 | Portable over-saturation High Purity Hydrogen molecule water preparation apparatus and its application method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107032472A true CN107032472A (en) | 2017-08-11 |
Family
ID=59534770
Family Applications (1)
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Application publication date: 20170811 |