CN107029595A - A kind of automatic recipe maker and distribution - Google Patents

A kind of automatic recipe maker and distribution Download PDF

Info

Publication number
CN107029595A
CN107029595A CN201710348448.6A CN201710348448A CN107029595A CN 107029595 A CN107029595 A CN 107029595A CN 201710348448 A CN201710348448 A CN 201710348448A CN 107029595 A CN107029595 A CN 107029595A
Authority
CN
China
Prior art keywords
mixing
reagent
stirring tank
pot
stirring
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710348448.6A
Other languages
Chinese (zh)
Inventor
李源
任红波
刘冠华
刘江华
景正兰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qinghai Xingaoke Materials Research Institute Co Ltd
Original Assignee
Qinghai Xingaoke Materials Research Institute Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qinghai Xingaoke Materials Research Institute Co Ltd filed Critical Qinghai Xingaoke Materials Research Institute Co Ltd
Priority to CN201710348448.6A priority Critical patent/CN107029595A/en
Publication of CN107029595A publication Critical patent/CN107029595A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/20Measuring; Control or regulation
    • B01F35/21Measuring
    • B01F35/211Measuring of the operational parameters
    • B01F35/2112Level of material in a container or the position or shape of the upper surface of the material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • B01F35/717Feed mechanisms characterised by the means for feeding the components to the mixer
    • B01F35/71805Feed mechanisms characterised by the means for feeding the components to the mixer using valves, gates, orifices or openings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/49Mixing drilled material or ingredients for well-drilling, earth-drilling or deep-drilling compositions with liquids to obtain slurries

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)

Abstract

The invention discloses a kind of automatic recipe maker and distribution, described device includes mixing and stirring tank (1), the mixing and stirring tank (1) is connected by material pipe (2) with material pot (3), the mixing and stirring tank (1) is connected with n reagent pot (5) respectively by n reagent pipeline (4), and the mixing and stirring tank (1) is connected by waterpipe (6) with pure water source;Liquid level gauge is set on the mixing and stirring tank (1), and bottom sets discharge nozzle (7);Agitator (11) in motor (10), motor (10) driving mixing and stirring tank (1) is set at the top of the mixing and stirring tank (1);Flowmeter, feed pump and pipeline valve are respectively provided with the material pipe (2), n reagent pipeline (4).The present invention reduces the dependence in high-purity superfine active aluminium powder sand grinding process to people and work intensity, and improve efficiency, the purity for reducing cost, keeping product.

Description

A kind of automatic recipe maker and distribution
Technical field
The invention belongs to aluminum oxide preparing technical field, in particular it relates to a kind of automatic recipe maker and dispensing Method.
Background technology
Nowadays generation of electricity by new energy and electric vehicle industrialization are developed rapidly, have promoted the flourishing again of alumina industry Development.The production that relevant policies support nano alumina powder is carried out by country.And prepare ultra micro nano alumina powder and be accomplished by it It is modified, conventional method of modifying is exactly chemical modification at present, changes the surface characteristic of powder by adding auxiliary agent, at present All it is that, by human metering auxiliary agent, human metering auxiliary agent can measure inaccurate, cause product unstable in industry, it is extremely difficult to ensure production Product quality, is largely dependent upon the sense of responsibility of operative employee.
The content of the invention
It is an object of the present invention to provide a kind of automatic recipe maker, the device reduces in high-purity superfine active aluminium powder Dependence to people and work intensity in sand grinding process, and improve efficiency, the purity for reducing cost, keeping product.
To reach above-mentioned purpose, present invention employs following technical scheme:
A kind of automatic recipe maker, described device includes mixing and stirring tank 1, and the mixing and stirring tank 1 passes through material pipe 2 Connected with material pot 3, the mixing and stirring tank 1 is connected with n reagent pot 5 respectively by n reagent pipeline 4, the mixing is stirred Tank 1 is mixed to connect with pure water source by waterpipe 6;Liquid level gauge is set in the mixing and stirring tank 1, and bottom sets discharge nozzle 7;It is described The top of mixing and stirring tank 1 sets the agitator 11 in motor 10, the driving mixing and stirring tank 1 of motor 10;
Flowmeter, feed pump and pipeline valve are respectively provided with the material pipe 2, n reagent pipeline 4;The materail tube Road 2, n reagent pipeline 4 connect with flushing pipe 8, and set valve on the flushing pipe before tie point;
Flowmeter is set on the waterpipe 6;
The bottom of the material pot 3 and n reagent pot 5 sets and is respectively provided with waste pipe 9;The material pot 3 and n reagent pot Liquid level gauge is respectively provided with 5.
In the present invention, the positive integer that the n in the n reagent pipeline and n reagent pot is >=1.Preferably, the n= 4。
In the present invention, n reagent pot can hold reagent of the viscosity in 0-10000m.Pa.s various required additions.
Present invention also offers the automatic blending method based on a kind of above-mentioned automatic recipe maker, methods described includes as follows Step:
1) according to the sequencing of addition reagent, the reagent in reagent pot is transported to mixing and stirring tank respectively in sequence In, the feed time of reagent pot is set as 0-5min, and flow is controlled in 0-10L/min;
2) 0-600L high purity deionized waters are added by the flowmeter on waterpipe and is used as decentralized medium, reagent is divided Dissipate dilution stirring 0-10min;
3) material in material pot is transported in mixing and stirring tank by feed pump, feed time 0-20min, flow 0- 50L/min, makes material and various reagents be thoroughly mixed uniformly, mixing time 0-10min;Material after stirring passes through The discharge nozzle for mixing pot bottom releases slurry, is transported to lower procedure.
Liquid level gauge is fitted with each reagent pot can monitor the surplus of reagent in real time, and reagent is mended in time Fill;Each reagent pot and material pot are equipped with the flushing pipe of pre-washing function, prevent the cross pollution of reagent;According to different technique Condition, control is adjusted to addition amount of reagent.
Advantages of the present invention:
The device of the present invention is primarily to avoid inaccurate, the reduction of the chemical feeding quantity caused by artificial destabilizing factor Artificial multiplicating, inaccurately operate the loss of material brought, the inhomogeneity of nano alumina powder jointed different batches granularity And the pollution of sample purity.The device of the present invention can greatly save manpower, reduce labor intensity, it is ensured that per batch The stability of the Wuli-Shili-Renli system approach of material.Need to add the higher dispersant of viscosity in alumina powder sand grinding process, it is right This present invention improves feed way, and from screw pump, conventional pump is not beaten into thick slurry, mixing and stirring tank is sent into.Agitator tank Bottom is mounted with electronic scale, is controlled using programmable controller, sets the addition of each medicament, medicament is accurately added Enter mixing and stirring tank.The nano-powder purity produced by the present apparatus is high, and batch granularity, uniform properties are consistent, and production thing is not wasted Material, reduces the labor intensity of people, reduces production cost.
The present invention is full-automatic control system;Manpower can be saved;It can add one or more kinds of different types of simultaneously Auxiliary agent.Auxiliary agent can accurately be added by flowmeter, it is ensured that product stability.Instrument Automatic Control dosing, quick, essence It is accurate, do not pollute;Control system can control multiple chemicals dosing plants, medicament is sequentially added into storage tank;Pass through liquid level gauge, pressure gauge Real-time online observes production process;Production process is neatly orderly;Manpower is reduced, it is cost-effective.
Brief description of the drawings
Fig. 1 is the structural representation of automatic dispensation apparatus of the present invention.
Reference:1st, mixing and stirring tank;2nd, material pipe;3rd, material pot;4th, reagent pipeline;5th, reagent pot;6th, water pipe Road;7th, discharge nozzle;8th, flushing pipe;9th, waste pipe;10th, motor;11st, agitator 11.
Embodiment
With the drawings and specific embodiments, the present invention is further detailed explanation below.
Embodiment 1
As shown in figure 1, a kind of automatic recipe maker, described device includes mixing and stirring tank 1, the mixing and stirring tank 1 is led to Cross material pipe 2 to connect with material pot 3, the mixing and stirring tank 1 is connected with n reagent pot 5 respectively by n reagent pipeline 4, The mixing and stirring tank 1 is connected by waterpipe 6 with pure water source;Liquid level gauge is set in the mixing and stirring tank 1, bottom is set out Expects pipe 7;The top of mixing and stirring tank 1 sets the agitator 11 in motor 10, the driving mixing and stirring tank 1 of motor 10;
Flowmeter, feed pump and pipeline valve are respectively provided with the material pipe 2, n reagent pipeline 4;The materail tube Road 2, n reagent pipeline 4 connect with flushing pipe 8, and set valve on the flushing pipe before tie point;
Flowmeter is set on the waterpipe 6;
The bottom of the material pot 3 and n reagent pot 5 sets and is respectively provided with waste pipe 9;The material pot 3 and n reagent pot Liquid level gauge is respectively provided with 5.
In the present invention, the n=4 in the n reagent pipeline and n reagent pot.
Embodiment 2
When the auxiliary agent of the addition of production nano aluminium oxide is a kind of, by the reagent in a reagent pot, (viscosity exists 500mPa.s) it is transported in mixing and stirring tank, the feed time of reagent pot is set as 2min, and flow is controlled in 1L/min.Pass through The flowmeter of waterpipe adds 200L high purity deionized waters as decentralized medium, and scattered dilution stirring 4min is carried out to reagent;Again The material in material pot is transported in mixing and stirring tank by feed pump, feed time 5min, flow 20L/min make material It is thoroughly mixed uniformly with reagent, mixing time 10min;Material after stirring is by mixing the discharging of pot bottom Pipe releases slurry, is transported to lower procedure.
Liquid level gauge is fitted with each reagent pot can monitor the surplus of reagent in real time, and reagent is mended in time Fill;Each reagent pot and material pot are equipped with the pipeline of pre-washing function, prevent the cross pollution of reagent;According to different technique bars Part, control is adjusted to addition amount of reagent.
Embodiment 3
When the auxiliary agent for producing the addition of nano aluminium oxide is two kinds, by 2 reagent pots reagent (viscosity is respectively 100, 900mPa.s) it is transported in mixing and stirring tank, the feed time of a reagent pot is set as 1min, and flow is controlled in 2L/min, The feed time of another reagent pot is set as 3min, and flow is controlled in 1L/min.Added by the flowmeter on waterpipe 300L high purity deionized waters carry out scattered dilution stirring 5min to reagent as decentralized medium;Again by feed pump by material pot In material be transported in mixing and stirring tank, feed time 10min, flow 20L/min are sufficiently stirred for material and various reagents It is well mixed, mixing time 10min;Material after stirring releases slurry by mixing the discharge nozzle of pot bottom, It is transported to lower procedure.
Liquid level gauge is fitted with each reagent pot can monitor the surplus of reagent in real time, and reagent is mended in time Fill;Each reagent pot and material pot are equipped with the pipeline of pre-washing function, prevent the cross pollution of reagent;According to different technique bars Part, control is adjusted to addition amount of reagent.
Embodiment 4
When the auxiliary agent for producing the addition of nano aluminium oxide is three kinds, by the examination in 3 reagent pots (be set as 1,2,3# tanks) Agent (viscosity is respectively 100,500,900mPa.s) is transported in mixing and stirring tank, and the feed time of 3# reagent pots is set as 1min, flow control is set as 2min in 2L/min, the feed time of 2# reagent pots, and flow is controlled in 1L/min, 1# reagent pots Feed time be set as 2min, flow is controlled in 0.5L/min.500L high purity deionized waters are added by waterpipe flowmeter As decentralized medium, scattered dilution stirring 5min is carried out to reagent;The material in material pot is transported to by feed pump again mixed Close in agitator tank, feed time 15min, flow 20L/min make material and various reagents be thoroughly mixed uniformly, during stirring Between 10min;Material after stirring releases slurry by mixing the discharge nozzle of pot bottom, is transported to lower procedure.
Liquid level gauge is fitted with each reagent pot can monitor the surplus of reagent in real time, and reagent is mended in time Fill;Each reagent pot and material pot are equipped with the pipeline of pre-washing function, prevent the cross pollution of reagent;According to different technique bars Part, control is adjusted to addition amount of reagent.
It should be noted last that, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted.Although ginseng The present invention is described in detail according to embodiment, it will be apparent to an ordinarily skilled person in the art that to the technical side of the present invention Case is modified or equivalent substitution, and without departure from the spirit and scope of technical solution of the present invention, it all should cover in the present invention Right among.

Claims (4)

1. a kind of automatic recipe maker, it is characterised in that described device includes mixing and stirring tank (1), the mixing and stirring tank (1) Connected by material pipe (2) with material pot (3), the mixing and stirring tank (1) is tried with n respectively by n reagent pipeline (4) Agent tank (5) is connected, and the mixing and stirring tank (1) is connected by waterpipe (6) with pure water source;Set on the mixing and stirring tank (1) Liquid level gauge is put, bottom sets discharge nozzle (7);Motor (10), motor (10) driving are set at the top of the mixing and stirring tank (1) Agitator (11) in mixing and stirring tank (1);
Flowmeter, feed pump and pipeline valve are respectively provided with the material pipe (2), n reagent pipeline (4);The materail tube Road (2), n reagent pipeline (4) connect with flushing pipe (8), and set valve on the flushing pipe before tie point;
Flowmeter is set on the waterpipe (6);
The bottom of the material pot (3) and n reagent pot (5) sets and is respectively provided with waste pipe (9);The material pot (3) and n examination Agent tank is respectively provided with liquid level gauge on (5).
2. a kind of automatic recipe maker according to claim 1, it is characterised in that the n reagent pipeline and n reagent The positive integer that n in tank is >=1.
3. a kind of automatic recipe maker according to claim 2, it is characterised in that the n=4.
4. based on a kind of automatic blending method of any one of claim 1-3 automatic recipe makers, methods described is included such as Lower step:
1) according to the sequencing of addition reagent, the reagent in reagent pot is transported in mixing and stirring tank respectively in sequence, The feed time of reagent pot is set as 0-5min, and flow is controlled in 0-10L/min;
2) 0-600L high purity deionized waters are added by the flowmeter on waterpipe and is used as decentralized medium, reagent carried out scattered dilute Release stirring 0-10min;
3) material in material pot is transported in mixing and stirring tank by feed pump, feed time 0-20min, flow 0-50L/ Min, makes material and various reagents be thoroughly mixed uniformly, mixing time 0-10min;Material after stirring passes through mixing The discharge nozzle of stirring pot bottom releases slurry, is transported to lower procedure.
CN201710348448.6A 2017-05-17 2017-05-17 A kind of automatic recipe maker and distribution Pending CN107029595A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710348448.6A CN107029595A (en) 2017-05-17 2017-05-17 A kind of automatic recipe maker and distribution

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710348448.6A CN107029595A (en) 2017-05-17 2017-05-17 A kind of automatic recipe maker and distribution

Publications (1)

Publication Number Publication Date
CN107029595A true CN107029595A (en) 2017-08-11

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CN201710348448.6A Pending CN107029595A (en) 2017-05-17 2017-05-17 A kind of automatic recipe maker and distribution

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Country Link
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109078515A (en) * 2018-09-28 2018-12-25 广东浪淘砂新型材料有限公司 A kind of intelligence liquid compounding system and its application method
CN111644116A (en) * 2020-04-30 2020-09-11 兰州兰石中科纳米科技有限公司 Batching device
CN115427138A (en) * 2020-04-30 2022-12-02 兰州兰石中科纳米科技有限公司 Multiphase interface reactor

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001340736A (en) * 2000-05-31 2001-12-11 Tokico Ltd Mixing device
CN205850773U (en) * 2016-08-16 2017-01-04 杭州凡腾科技股份有限公司 A kind of dispenser automatically
CN205907497U (en) * 2016-08-16 2017-01-25 杭州凡腾科技股份有限公司 Auxiliary agent dispenser
CN207042323U (en) * 2017-05-17 2018-02-27 青海新高科材料研究院有限公司 A kind of automatic recipe maker

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001340736A (en) * 2000-05-31 2001-12-11 Tokico Ltd Mixing device
CN205850773U (en) * 2016-08-16 2017-01-04 杭州凡腾科技股份有限公司 A kind of dispenser automatically
CN205907497U (en) * 2016-08-16 2017-01-25 杭州凡腾科技股份有限公司 Auxiliary agent dispenser
CN207042323U (en) * 2017-05-17 2018-02-27 青海新高科材料研究院有限公司 A kind of automatic recipe maker

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109078515A (en) * 2018-09-28 2018-12-25 广东浪淘砂新型材料有限公司 A kind of intelligence liquid compounding system and its application method
CN111644116A (en) * 2020-04-30 2020-09-11 兰州兰石中科纳米科技有限公司 Batching device
CN115427138A (en) * 2020-04-30 2022-12-02 兰州兰石中科纳米科技有限公司 Multiphase interface reactor
JP7539486B2 (en) 2020-04-30 2024-08-23 蘭州蘭石中科納米科技有限公司 Multiphase Interface Reactor

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Application publication date: 20170811

RJ01 Rejection of invention patent application after publication