CN107022231A - Corrosion-resistant and high-temperature resistant instrument draws ink with electronics wheat - Google Patents
Corrosion-resistant and high-temperature resistant instrument draws ink with electronics wheat Download PDFInfo
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- CN107022231A CN107022231A CN201710069940.XA CN201710069940A CN107022231A CN 107022231 A CN107022231 A CN 107022231A CN 201710069940 A CN201710069940 A CN 201710069940A CN 107022231 A CN107022231 A CN 107022231A
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- parts
- ink
- polyester resin
- resin
- corrosion
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
- C09D11/104—Polyesters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
- C09D11/103—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds of aldehydes, e.g. phenol-formaldehyde resins
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
Ink is drawn with electronics wheat the invention discloses a kind of corrosion-resistant and high-temperature resistant instrument, it includes resin Composition and curing agent, and wherein resin Composition is formulated by the raw material of following parts by weight：2~10 parts of PBT resin, 11~19 parts of silicone modified polyester resin, 2~9 parts of 290 polyester resin, 5~15 parts of amino resins, 6~15 parts of cyclohexanone spin in Japan, 11~19 parts of dibasic ester, 11~19 parts of isophorone, 6~15 parts of propylene glycol methyl ether acetate, 2~8 parts of 120 carbon blacks of Cabot M, 2~8 parts of copper-chrome black, 2~8 parts of filler.This ink at 190 DEG C in ink in 5 minutes without sticking out phenomenon, ink will not be by boiling hotization in the case of ink pellet surface hardness rapidly lifting, and printing adaptability is good；Do not corroded at 180 DEG C at 1 minute by 3M glue, its ethanol-tolerant, case hardness is high, good with base material adhesive force, the various print requests of electronics wheat drawing can be met.
Description
Technical field
The invention belongs to technical field of ink, and in particular to a kind of corrosion-resistant and high-temperature resistant instrument with electronics wheat draw ink and its
Preparation method.
Background technology
Mylar film, is generally referred to by cross cutting（DIECUT）By drawing or specified stamp is into sheet material.Wheat, which is drawn, metal
With nonmetallic two kinds, metal mylar film it is conventional have the drawing of copper foil wheat, aluminium foil wheat is drawn, and main function is conductive；And nonmetallic wheat is drawn
It is insulating effect mostly, common materials have PC, PET, for the surface protection of thin film switch or electronic and electrical equipment, or part is absolutely
Edge.The color of mylar film has a variety of, conventional to have transparent, white, black, and other colors can require to print according to specified.Mylar film
With high insulation resistance, proof voltage is high, moisture resistant, gas, the invasion and attack of hyperpyrexia and chemical substance, low-shrinkage, be difficult it is brittle resistance to
The characteristics such as abrasion.
In a kind of existing electronics mylar film preparation technology, it is necessary to using 3-layer PET material 170 DEG C or so 5 minutes
Inside do laminating process, and used ink can not meet its requirement, and also need to paste 3M glue after laminating process, and existing oil
Ink it is difficult to ensure that can not be corroded for 1 minute at 160 DEG C or so by 3M glue, it is also difficult to which it is good with base material adhesive force to ensure, it is therefore desirable to set
Count out and draw ink with higher resistant to elevated temperatures electronics wheat.
The content of the invention
The purpose of the present invention is to draw oil there is provided a kind of corrosion-resistant and high-temperature resistant instrument electronics wheat on the basis of existing technology
Ink.
It is a further object of the present invention to provide the preparation side that a kind of above-mentioned corrosion-resistant and high-temperature resistant instrument draws ink with electronics wheat
Method
The purpose of the present invention can be reached by following measures：
A kind of corrosion-resistant and high-temperature resistant instrument with electronics wheat draw ink, it include resin Composition and curing agent, wherein resin Composition by
The raw material of following parts by weight is formulated：2~10 parts of PBT resin, 11~19 parts of silicone modified polyester resin, Japan spins 290
2~9 parts of polyester resin, 5~15 parts of amino resins, 6~15 parts of cyclohexanone, 11~19 parts of dibasic ester, isophorone 11~19
Part, 6~15 parts of propylene glycol methyl ether acetate, 2~8 parts of Cabot M-120 carbon blacks, 2~8 parts of copper-chrome black, 2~8 parts of filler.
In a kind of preferred scheme, resin Composition is formulated by the raw material of following parts by weight：2~8 parts of PBT resin, has
2~8 parts of 290 polyester resin, 6~14 parts of amino resins, cyclohexanone 6~14 spin in 12~17 parts of machine silicon-modified polyester resin, Japan
Part, 12~18 parts of dibasic ester, 12~18 parts of isophorone, 6~15 parts of propylene glycol methyl ether acetate, Cabot M-120 carbon blacks 3
~7 parts, 3~7 parts of copper-chrome black, 3~7 parts of filler.
In another preferred scheme, resin Composition is formulated by the raw material of following parts by weight：3~6 parts of PBT resin,
13~16 parts of silicone modified polyester resin, Japan's 3~6 parts of 290 polyester resin of spinning, 8~12 parts of amino resins, cyclohexanone 8~
12 parts, 13~17 parts of dibasic ester, 13~17 parts of isophorone, 8~12 parts of propylene glycol methyl ether acetate, Cabot M-120 carbon
Black 4~6 parts, 4~6 parts of copper-chrome black, 4~6 parts of filler.
In a kind of preferred scheme, resin Composition is formulated by the raw material of following parts by weight：4.5 parts of PBT resin,
5 parts of 290 polyester resin, 10 parts of amino resins, 10 parts of cyclohexanone, dibasic ester spin in 15 parts of silicone modified polyester resin, Japan
15 parts, 15 parts of isophorone, 10 parts of propylene glycol methyl ether acetate, 5 parts of Cabot M-120 carbon blacks, 5 parts of copper-chrome black, 5 parts of filler.
The curing agent of the present invention is selected from diethylenetriamine or aminoethyl piperazine, and the consumption of curing agent spins 290 for described Japan
The 0.5/10~2/10 of polyester resin weight.Used after resin Composition is prepared in proportion with curing agent when using ink.
The silicone modified polyester resin of the present invention is selected from Shanghai towards the happy JY7200 of space SKP001, GR-2005 or pretty:15
Silicone modified polyester resin.
Amino resins in the present invention can use Lauxite (UF) or melamine resin (MF).
The filler of the present invention is selected from kaolin, bentonite, talcum powder, barium sulfate, flatting silica, titanium dioxide, calcite in powder, silicon
Lime stone, dolomite dust, transparent powder or calcium carbonate.
A kind of above-mentioned corrosion-resistant and high-temperature resistant instrument draws the preparation side of the preparation method, wherein resin Composition of ink with electronics wheat
Method is：First by PBT, silicone modified polyester resin, Japan spin 290 polyester resin and amino resins and cyclohexanone, dibasic ester,
Isophorone and the propylene glycol methyl ether acetate high-speed stirred at 30 DEG C~80 DEG C are uniform, add Cabot M-120 carbon blacks, copper
Chrome black and filler are ground to fineness≤5 μm after being stirred, and produce.Resin Composition is matched somebody with somebody in proportion with curing agent when using ink
Used after system.
The electronics wheat of the present invention draws ink to can apply to the printing aspect that instrument electronics wheat draws material, can also enter one
Step is applied in terms of the printing of other field product material.
In the solution of the present invention, 290 polyester resin and amino are spun using PBT resin, silicone modified polyester resin, Japan
Four kinds of resins of resin, by their synergies under special ratios, and under the cooperation of other components, greatly improved oil
High temperature resistant, adhesive force, printing adaptability and the performance such as anticorrosive of ink.The corrosion-resistant and high-temperature resistant instrument of the present invention is drawn with electronics wheat
Ink PET adhesive force is excellent on PC materials, a variety of colors can meet resistant to elevated temperatures requirement.It is at 190 DEG C in 5 minutes
Interior ink is without phenomenon is sticked out, and ink will not be by boiling hotization in the case of ink pellet surface hardness rapidly lifting, and printing adaptability is good；
Do not corroded at 180 DEG C at 1 minute by 3M glue, its ethanol-tolerant, case hardness is high, good with base material adhesive force, can meet electronics wheat
The various print requests drawn.
Embodiment
Present disclosure is described further with reference to embodiments.But protection scope of the present invention is not limited to following
Each embodiment.
Embodiment 1
Resin Composition is formulated by the raw material of following parts by weight：4.5 parts of PBT resin, silicone modified polyester resin
（SKP001）15 parts, Japan's 5 parts of 290 polyester resin of spinning, 10 parts of amino resins (UF), 10 parts of cyclohexanone, 15 parts of dibasic ester,
15 parts of isophorone, 10 parts of propylene glycol methyl ether acetate, 5 parts of Cabot M-120 carbon blacks, 5 parts of copper-chrome black, 5 parts of barium sulfate.
The preparation method of resin Composition is：290 polyester resin and ammonia are first spun into PBT, silicone modified polyester resin, Japan
The high-speed stirred at 30 DEG C~80 DEG C is uniform with cyclohexanone, dibasic ester, isophorone and propylene glycol methyl ether acetate for base resin,
Add after Cabot M-120 carbon blacks, copper-chrome black and filler are stirred and be ground to fineness≤5 μm, produce.
Curing agent is diethylenetriamine, and the consumption of curing agent spins the 1/10 of 290 polyester resin weight for Japan.Using oil
Used after resin Composition is prepared in proportion with curing agent when black.
Embodiment 2
Resin Composition is formulated by the raw material of following parts by weight：4.5 parts of PBT resin, silicone modified polyester resin
（SKP001）17 parts, Japan's 4 parts of 290 polyester resin of spinning, 12 parts of amino resins (UF), 12 parts of cyclohexanone, 14 parts of dibasic ester,
16 parts of isophorone, 9 parts of propylene glycol methyl ether acetate, 4 parts of Cabot M-120 carbon blacks, 6 parts of copper-chrome black, 5 parts of flatting silica.
The preparation of resin Composition and curing agent are same as Example 1.
Embodiment 3
Resin Composition is formulated by the raw material of following parts by weight：5 parts of PBT resin, silicone modified polyester resin（JY7200:
15）14 parts, 7 parts of 290 polyester resin, 8 parts of amino resins (UF), 8 parts of cyclohexanone, 16 parts of dibasic ester, isophorone spin in Japan
16 parts, 11 parts of propylene glycol methyl ether acetate, 6 parts of Cabot M-120 carbon blacks, 4 parts of copper-chrome black, 5 parts of titanium dioxide.
The preparation of resin Composition and curing agent are same as Example 1.
Embodiment 4
Resin Composition is formulated by the raw material of following parts by weight：4.5 parts of PBT resin, silicone modified polyester resin
（JY7200:15）16 parts, 6 parts of 290 polyester resin, 8 parts of amino resins (UF), 10 parts of cyclohexanone, dibasic ester 15 spin in Japan
Part, 15 parts of isophorone, 10 parts of propylene glycol methyl ether acetate, 5 parts of Cabot M-120 carbon blacks, 5 parts of copper-chrome black, calcite in powder 5
Part.
The preparation of resin Composition and curing agent are same as Example 1.
Comparative example 1
The PBT resin in the resin Composition of embodiment 1 is removed, the consumption of silicone modified polyester resin is changed to 19.5 parts, other
Condition is same as Example 1.
Comparative example 2
The silicone modified polyester resin resin in the resin Composition of embodiment 1 is removed, the consumption of PBT resin is changed to 19.5 parts,
Other conditions are same as Example 1.
Comparative example 3
290 polyester resin spin in the Japan removed in the resin Composition of embodiment 1, and the consumption of amino resins is changed into 15 parts, other
Part is same as Example 1.
Comparative example 4
The amino resins in the resin Composition of embodiment 1 is removed, the consumption that Japan is spun into 290 polyester resin is changed to 15 parts, other
Part is same as Example 1.
Embodiment 5：Ink performance is tested
First resin Composition is prepared in proportion with curing agent, adds after 10~20% isophorone diluents stir and is printed on
PET base material surface, is put into 80 DEG C of baking box and bakes 30 minutes, obtain electronics wheat and draw semi-finished product, to the semi-finished product after being completed for printing
Film is tested.
The high temperature resistant of film is not sticked out using film at 190 DEG C in ink in 5 minutes, and its middle grade 0 is good, grade
1 is to stick out phenomenon.
The glue of resistance to 3M of film is used not to be corroded at 180 DEG C after patch 3M glue on film at 1 minute by 3M glue, its middle grade
0 is good, and grade 1 is to have burn into obscission.
Film PET adhesive force on PC materials with reference to standard GB/T/T9286-1998《Paint and varnish paint film
Draw lattice experiment》[test of ten stroke lattice tape pull methods is carried out, test result is expressed as 0-5 grades, wherein 0 grade best, 5 grades most
Difference.
The hardness of film is with reference to standard GB/T/T6739-1996《Hardness of film pencil determination method》It is measured, is divided into
Totally 13 grades of 6H to 6B, wherein 6H is most hard, and 6B is most soft.
The ethanol-tolerant test of film：99.5% alcohol is soaked, on the coated film sample after doing solid work using cloth, with 20mm or so
Stroke, come and go apply 50 times.Its middle grade 0 is font content intact and can clearly recognized that grade 1 is font content intact and clear
It can recognize but font has slight abrasion and faded, grade 2 is that font has and significantly weares and teares and fade.
The ink film that each example is obtained by more than carries out performance test, as a result such as following table.
| Performance | Hardness H | Adhesive force | Ethanol-tolerant | High temperature resistant | The glue of resistance to 3M |
| Embodiment 1 | 5 | 1 | 0 | 0 | 0 |
| Embodiment 2 | 4 | 1 | 0 | 0 | 0 |
| Embodiment 3 | 4 | 1 | 0 | 0 | 0 |
| Embodiment 4 | 4 | 1 | 0 | 0 | 0 |
| Comparative example 1 | 3 | 3 | 1 | 1 | 1 |
| Comparative example 2 | 3 | 3 | 1 | 1 | 1 |
| Comparative example 3 | 3 | 2 | 1 | 1 | 1 |
| Comparative example 4 | 3 | 2 | 2 | 1 | 1 |
Claims (9)
1. a kind of corrosion-resistant and high-temperature resistant instrument draws ink with electronics wheat, it is characterised in that it includes resin Composition and curing agent, its
Middle resin Composition is formulated by the raw material of following parts by weight：2~10 parts of PBT resin, silicone modified polyester resin 11~19
Part, 2~9 parts of 290 polyester resin spins in Japan, and 5~15 parts of amino resins, 6~15 parts of cyclohexanone, 11~19 parts of dibasic ester is different
11~19 parts of phorone, 6~15 parts of propylene glycol methyl ether acetate, 2~8 parts of Cabot M-120 carbon blacks, 2~8 parts of copper-chrome black is filled out
2~8 parts of material.
2. corrosion-resistant and high-temperature resistant instrument according to claim 1 with electronics wheat draw ink, it is characterised in that resin Composition by
The raw material of following parts by weight is formulated：2~8 parts of PBT resin, 12~17 parts of silicone modified polyester resin, Japan spins 290
2~8 parts of polyester resin, 6~14 parts of amino resins, 6~14 parts of cyclohexanone, 12~18 parts of dibasic ester, isophorone 12~18
Part, 6~15 parts of propylene glycol methyl ether acetate, 3~7 parts of Cabot M-120 carbon blacks, 3~7 parts of copper-chrome black, 3~7 parts of filler.
3. corrosion-resistant and high-temperature resistant instrument according to claim 2 with electronics wheat draw ink, it is characterised in that resin Composition by
The raw material of following parts by weight is formulated：3~6 parts of PBT resin, 13~16 parts of silicone modified polyester resin, Japan spins 290
3~6 parts of polyester resin, 8~12 parts of amino resins, 8~12 parts of cyclohexanone, 13~17 parts of dibasic ester, isophorone 13~17
Part, 8~12 parts of propylene glycol methyl ether acetate, 4~6 parts of Cabot M-120 carbon blacks, 4~6 parts of copper-chrome black, 4~6 parts of filler.
4. corrosion-resistant and high-temperature resistant instrument according to claim 3 with electronics wheat draw ink, it is characterised in that resin Composition by
The raw material of following parts by weight is formulated：290 polyester trees are spun by 4.5 parts of PBT resin, 15 parts of silicone modified polyester resin, Japan
5 parts of fat, 10 parts of amino resins, 10 parts of cyclohexanone, 15 parts of dibasic ester, 15 parts of isophorone, 10 parts of propylene glycol methyl ether acetate,
5 parts of Cabot M-120 carbon blacks, 5 parts of copper-chrome black, 5 parts of filler.
5. the corrosion-resistant and high-temperature resistant instrument according to any one in Claims 1 to 4 draws ink with electronics wheat, its feature exists
Diethylenetriamine or aminoethyl piperazine are selected from the curing agent, the consumption of curing agent spins 290 polyester resin weights for described Japan
The 0.5/10~2/10 of amount.
6. the corrosion-resistant and high-temperature resistant instrument according to any one in Claims 1 to 4 draws ink with electronics wheat, its feature exists
Shanghai is selected from towards the happy JY7200 of space SKP001, GR-2005 or pretty in the silicone modified polyester resin:15 is organic-silicon-modified
Polyester resin.
7. the corrosion-resistant and high-temperature resistant instrument according to any one in Claims 1 to 4 draws ink with electronics wheat, its feature exists
Kaolin, bentonite, talcum powder, barium sulfate, flatting silica, titanium dioxide, calcite in powder, wollastonite, white clouds are selected from the filler
Stone flour, transparent powder or calcium carbonate.
8. the corrosion-resistant and high-temperature resistant instrument in a kind of Claims 1 to 4 described in any one draws the preparation side of ink with electronics wheat
Method, it is characterised in that the preparation method of the resin Composition is：PBT, silicone modified polyester resin, Japan first are spun into 290 to gather
Ester resin and the amino resins height at 30 DEG C~80 DEG C with cyclohexanone, dibasic ester, isophorone and propylene glycol methyl ether acetate
Speed stirs, and adds after Cabot M-120 carbon blacks, copper-chrome black and filler are stirred and is ground to fineness≤5 μm, produces.
9. the corrosion-resistant and high-temperature resistant instrument in a kind of Claims 1 to 4 described in any one draws the preparation side of ink with electronics wheat
Method, it is characterised in that it is described resin Composition is prepared in proportion with curing agent when using ink after use.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710069940.XA CN107022231A (en) | 2017-02-08 | 2017-02-08 | Corrosion-resistant and high-temperature resistant instrument draws ink with electronics wheat |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710069940.XA CN107022231A (en) | 2017-02-08 | 2017-02-08 | Corrosion-resistant and high-temperature resistant instrument draws ink with electronics wheat |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107022231A true CN107022231A (en) | 2017-08-08 |
Family
ID=59525587
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710069940.XA Withdrawn CN107022231A (en) | 2017-02-08 | 2017-02-08 | Corrosion-resistant and high-temperature resistant instrument draws ink with electronics wheat |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107022231A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110845908A (en) * | 2019-10-16 | 2020-02-28 | 苏州市贝特利高分子材料股份有限公司 | Black printing ink for mobile phone explosion-proof membrane back plate |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105199479A (en) * | 2015-09-02 | 2015-12-30 | 王景泉 | Black ink for mylar prepared on basis of PET (polyester) materials and preparation method of black ink |
-
2017
- 2017-02-08 CN CN201710069940.XA patent/CN107022231A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105199479A (en) * | 2015-09-02 | 2015-12-30 | 王景泉 | Black ink for mylar prepared on basis of PET (polyester) materials and preparation method of black ink |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110845908A (en) * | 2019-10-16 | 2020-02-28 | 苏州市贝特利高分子材料股份有限公司 | Black printing ink for mobile phone explosion-proof membrane back plate |
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Application publication date: 20170808 |
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