CN107019002A - Culture of Chinese mitten crab pool-cleaning agent and preparation method thereof - Google Patents
Culture of Chinese mitten crab pool-cleaning agent and preparation method thereof Download PDFInfo
- Publication number
- CN107019002A CN107019002A CN201710408315.3A CN201710408315A CN107019002A CN 107019002 A CN107019002 A CN 107019002A CN 201710408315 A CN201710408315 A CN 201710408315A CN 107019002 A CN107019002 A CN 107019002A
- Authority
- CN
- China
- Prior art keywords
- cleaning agent
- culture
- parts
- mitten crab
- chinese mitten
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
Abstract
The invention belongs to pharmaceutic preparation for livestock field, more particularly to a kind of culture of Chinese mitten crab pool-cleaning agent and preparation method thereof, the culture of Chinese mitten crab pool-cleaning agent of the present invention is using tea seed cake, nano zine oxide, perilla leaf as active component, sterilization antibacterial efficacy with wide spectrum, there is extremely strong killing action to aquatic livestocks such as various wild fisheses, loach, shrimp, crabs, also there is good killing action to various bacteriums, virus, fungi and parasite, worm's ovum simultaneously, be effectively reduced the generation of various diseases；In addition, the pool-cleaning agent of the present invention is also equipped with good, cheap, the easy to use advantage of component safety and environmental protection, continuation；The preparation method of the culture of Chinese mitten crab pool-cleaning agent of the present invention is simple, workable, it is adaptable to industrial production.
Description
Technical field
The invention belongs to pharmaceutic preparation for livestock field, more particularly to a kind of culture of Chinese mitten crab pool-cleaning agent and preparation method thereof.
Background technology
Some wild fisheses, loach, shrimp, crab etc. are commonly present during the aqueous systems of culture of Chinese mitten crab, while there is also more bacterium, disease
Poison, fungi, parasite combine worm's ovum etc., influence the upgrowth situation and survival rate of river crab, therefore need to be cleaned up the pond, and kill wild fishes
Deng aquatic livestock and bacterium etc..
The conventional chemistry of existing market medicine of cleaning up the pond has chrysanthemum esters, metrifonate, bleaching powder, quick lime, ribes dregs of rice etc.；Chrysanthemum ester
Class medicine be a class efficiently, wide spectrum, low toxicity and biodegradable synthetic pesticide, but the shell-fish such as cray, river crab, freshwater shrimp moves
Thing is more sensitive to chrysanthemum esters medicine, can directly kill the shellfish such as cray, river crab in pond, and such medicine has residual
It can influence cultivate next year；Metrifonate has good elimination effect for swamp eel and loach, but improper use can influence the kind in the coming year
Grass, and then have a negative impact to culture of Chinese mitten crab；The principle that quick lime is cleaned up the pond is to meet that chemistry occurs after water by quick lime (CaO)
Reaction, and substantial amounts of heat is released, highly basic is generated, so as to be rapidly reached sterilizing and kill the purpose of harmful organisms, simultaneously
The calcium carbonate of generation can make the soft of mud change, but its sterilizing and kill harmful organisms effect be not notable；In leached tea oil slag
Tea Saponin has haemocylolysis and ichthyotoxin effect, can kill trash fish, tadpole, spiral shell, freshwater mussel, leech and the part aquatic insect in the pool,
It is substantially invalid to bacterium etc.；Single chemistry medicine of cleaning up the pond possesses certain limitation, can be solved the above problems by compound.
The content of the invention
It is unstable that chemical medicine of cleaning up the pond present in present invention solution prior art possesses certain limitation, medicine of cleaning up the pond
Technical problem.
To solve the above problems, technical scheme is as follows：
A kind of culture of Chinese mitten crab pool-cleaning agent, includes the raw material of following parts by weight：
Tea seed cake：40-64 parts；
Nano zine oxide：10-14 parts；
Perilla leaf：8-16 parts；
Chitosan quaternary ammonium salt：4-8 parts；
Sodium alginate：4-8 parts.
Wherein tea seed cake, nano zine oxide, perilla leaf are active component, and the Tea Saponin in tea seed cake has haemocylolysis and ichthyotoxin
Effect, can kill trash fish, tadpole, spiral shell, freshwater mussel, leech and the part aquatic insect in the pool, but substantially invalid to bacterium etc.；Nano oxygen
Changing zinc has the sterilization antibacterial efficacy of wide spectrum, it with water and air under conditions of, in the sun especially in the photograph of ultraviolet
Penetrate down, can voluntarily decomposite the hole of the electronegative electronics moved freely and positively charged, concurrent biochemical reaction, generation
Elemental oxygen and OH, they have stronger chemism, particularly elemental oxygen to be reacted with gas chromatography, while energy and bacterium
Interior organic matter reaction, so that bacterium can be killed in a short time；Perilla leaf is the natural component with bactericidal action, further
Increase sterilization species；Chitosan quaternary ammonium salt and sodium alginate are coated on outside active component, strengthen pool-cleaning agent stability.
Preferably, the culture of Chinese mitten crab pool-cleaning agent includes the raw material of following parts by weight：
Tea seed cake：56 parts；
Nano zine oxide：12 parts；
Perilla leaf：10 parts；
Chitosan quaternary ammonium salt：5 parts；
Sodium alginate：5 parts.
Preferably, a diameter of 10-50nm of the nano zine oxide, diameter is smaller, and specific surface area is bigger, nano zine oxide
Bactericidal effect more preferably.
A kind of preparation method of culture of Chinese mitten crab pool-cleaning agent, comprises the following steps：
A. the tea seed cake is ground into 500-700 mesh powder with pulverizer, adds during quality is its 3-8 times water, mix
The nano zine oxide is added after uniform, is stirred；
B. perilla leaf is dried, is fabricated to 500-700 mesh powder, add the step A resulting solutions, added after being well mixed
Enter homogeneous 2-4 times in high pressure homogenizer；
C. the chitosan quaternary ammonium salt is dissolved in the water, the step B obtained solutions added under being stirred vigorously continue to stir
For a period of time；
D. the sodium alginate is dissolved in water, the step C obtained solutions added under being stirred vigorously, when continuing to stir one section
Between after, add homogeneous 3-4 times in high pressure homogenizer；
E. step D resulting solutions are evaporated to obtain culture of Chinese mitten crab pool-cleaning agent.
Preferably, high pressure homogenizer pressure described in step B is 300-400bar, and nanoparticle is made under high pressure.
Preferably, more than step C mixing speeds 6000rpm, more than the mixing time 1min, to increase the uniform journey of system
Degree.
Preferably, more than step D mixing speeds 6000rpm, more than the mixing time 1min, to increase the uniform journey of system
Degree.
Preferably, high pressure homogenizer pressure described in step D is 300-400bar, and chitosan quaternary ammonium salt and sea is made under high pressure
The nanoparticle of mosanom cladding.
Relative to prior art, advantages of the present invention is as follows,
The culture of Chinese mitten crab pool-cleaning agent of the present invention is using tea seed cake, nano zine oxide, perilla leaf as active component, killing with wide spectrum
Bacterium antibacterial efficacy, has extremely strong killing action to aquatic livestocks such as various wild fisheses, loach, shrimp, crabs, while to various thin
Bacterium, virus, fungi and parasite, worm's ovum also have good killing action, are effectively reduced the generation of various diseases；In addition, this
The pool-cleaning agent of invention is also equipped with that component safety and environmental protection, killing rate are fast, continuation is good, dispersed strong, cheap, easy to use
Advantage；
The preparation method of the culture of Chinese mitten crab pool-cleaning agent of the present invention is simple, workable, it is adaptable to industrial production.
Embodiment
Embodiment 1：
A kind of culture of Chinese mitten crab pool-cleaning agent, includes the raw material of following parts by weight：
Tea seed cake：40 parts；
Nano zine oxide：10 parts；
Perilla leaf：8 parts；
Chitosan quaternary ammonium salt：4 parts；
Sodium alginate：4 parts.
Embodiment 2：
A kind of culture of Chinese mitten crab pool-cleaning agent, includes the raw material of following parts by weight：
Tea seed cake：64 parts；
Nano zine oxide：14 parts；
Perilla leaf：16 parts；
Chitosan quaternary ammonium salt：8 parts；
Sodium alginate：8 parts.
Embodiment 3：
A kind of culture of Chinese mitten crab pool-cleaning agent, includes the raw material of following parts by weight：
Tea seed cake：56 parts；
Nano zine oxide：12 parts；
Perilla leaf：10 parts；
Chitosan quaternary ammonium salt：5 parts；
Sodium alginate：5 parts.
Embodiment 4：
Culture of Chinese mitten crab pool-cleaning agent is prepared using embodiment 1-3 raw material proportioning, preparation method comprises the following steps：
A. the tea seed cake is ground into 500-700 mesh powder with pulverizer, adds during quality is its 3-8 times water, mix
The nano zine oxide is added after uniform, is stirred；
B. perilla leaf is dried, is fabricated to 500-700 mesh powder, add the step A resulting solutions, added after being well mixed
Enter homogeneous 3 times in high pressure homogenizer, high pressure homogenizer pressure is 350bar；
C. the chitosan quaternary ammonium salt is dissolved in the water, the step B obtained solutions added under being stirred vigorously, mixing speed
6000rpm, continues to stir 1min；
D. the sodium alginate is dissolved in water, the step C obtained solutions added under being stirred vigorously, when continuing to stir one section
Between after, add homogeneous 4 times in high pressure homogenizer, high pressure homogenizer pressure is 400bar；
E. step D resulting solutions are evaporated to obtain culture of Chinese mitten crab pool-cleaning agent.
Embodiment 5：
Bacterium insect killing effect is tested
The water in culture of Chinese mitten crab experimental plot is gathered, is dispensed in equal volume into 4 same containers, at the beginning of test vibrios and Aeromonas
Beginning concentration C0, the quality such as culture of Chinese mitten crab pool-cleaning agent and the tea seed cake that will be prepared using embodiment 1-3 raw material proportioning add 4 it is identical
In container, respectively at the concentration C that vibrios and Aeromonas are tested after 12 hours, 24 hours, 48 hours, sterilization rate=(C is calculated0-
C)/C0, as a result such as table one：
The sterilization rate of the pool-cleaning agent of table one
Embodiment 6：
Bacterium insect killing effect is tested
The water in culture of Chinese mitten crab experimental plot is gathered, dispenses in equal volume into 4 same containers, lobster is delivered into each container
5, loach 10, crucian 10, the culture of Chinese mitten crab pool-cleaning agent that will be prepared using embodiment 1-3 raw material proportioning and the matter such as tea seed cake
Amount add 4 same containers in, respectively at after 5 hours, 10 hours, 20 hours observe aquatic livestock general mortality rate, as a result such as
Table two：
The pool-cleaning agent of table two is used for the death rate of aquatic livestock
It should be noted that above-described embodiment is only presently preferred embodiments of the present invention, not for limiting the present invention's
Protection domain, the equivalent substitution or replacement made on the basis of the above belongs to protection scope of the present invention.
Claims (8)
1. a kind of culture of Chinese mitten crab pool-cleaning agent, it is characterised in that include the raw material of following parts by weight：
Tea seed cake：40-64 parts；
Nano zine oxide：10-14 parts；
Perilla leaf：8-16 parts；
Chitosan quaternary ammonium salt：4-8 parts；
Sodium alginate：4-8 parts.
2. culture of Chinese mitten crab pool-cleaning agent as claimed in claim 1, it is characterised in that include the raw material of following parts by weight：
Tea seed cake：56 parts；
Nano zine oxide：12 parts；
Perilla leaf：10 parts；
Chitosan quaternary ammonium salt：5 parts；
Sodium alginate：5 parts.
3. culture of Chinese mitten crab pool-cleaning agent as claimed in claim 1 or 2, it is characterised in that a diameter of 10- of the nano zine oxide
50nm。
4. a kind of preparation method of culture of Chinese mitten crab pool-cleaning agent as described in claim any one of 1-3, it is characterised in that including with
Lower step：
A. the tea seed cake is ground into 500-700 mesh powder with pulverizer, added during quality is its 3-8 times water, it is well mixed
After add the nano zine oxide, stir；
B. perilla leaf is dried, is fabricated to 500-700 mesh powder, add the step A resulting solutions, added after being well mixed high
Press homogeneous 2-4 times in homogenizer；
C. the chitosan quaternary ammonium salt is dissolved in the water, the step B obtained solutions added under being stirred vigorously continue to stir one section
Time；
D. the sodium alginate is dissolved in water, the step C obtained solutions added under being stirred vigorously continue to stir a period of time
Afterwards, homogeneous 3-4 times in high pressure homogenizer is added；
E. step D resulting solutions are evaporated to obtain culture of Chinese mitten crab pool-cleaning agent.
5. the preparation method of culture of Chinese mitten crab pool-cleaning agent as claimed in claim 4, it is characterised in that high-pressure homogeneous described in step B
Machine pressure is 300-400bar.
6. the preparation method of culture of Chinese mitten crab pool-cleaning agent as claimed in claim 4, it is characterised in that the step C mixing speeds
More than 6000rpm, more than mixing time 1min.
7. the preparation method of culture of Chinese mitten crab pool-cleaning agent as claimed in claim 4, it is characterised in that the step D mixing speeds
More than 6000rpm, more than mixing time 1min.
8. the preparation method of culture of Chinese mitten crab pool-cleaning agent as claimed in claim 4, it is characterised in that high-pressure homogeneous described in step D
Machine pressure is 300-400bar.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710408315.3A CN107019002A (en) | 2017-06-02 | 2017-06-02 | Culture of Chinese mitten crab pool-cleaning agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710408315.3A CN107019002A (en) | 2017-06-02 | 2017-06-02 | Culture of Chinese mitten crab pool-cleaning agent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107019002A true CN107019002A (en) | 2017-08-08 |
Family
ID=59530046
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710408315.3A Pending CN107019002A (en) | 2017-06-02 | 2017-06-02 | Culture of Chinese mitten crab pool-cleaning agent and preparation method thereof |
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| Country | Link |
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| CN (1) | CN107019002A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108432809A (en) * | 2018-03-30 | 2018-08-24 | 湖南淳湘农林科技有限公司 | A kind of cleaner for the cultivation of shrimp crab |
| CN110214731A (en) * | 2019-07-18 | 2019-09-10 | 安徽众渔生物科技有限公司 | One seed shrimp crab culture pond trash fish scavenger |
| CN111937915A (en) * | 2020-07-07 | 2020-11-17 | 临沂垂闲商贸有限公司 | Aquatic organism inducer and preparation method thereof |
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| CN1977618A (en) * | 2006-12-06 | 2007-06-13 | 福州大学 | Method for preparing tea saporin pool-cleaning agent using tea dreg as raw material |
| CN102342283A (en) * | 2011-07-28 | 2012-02-08 | 浙江省淡水水产研究所 | Combined preparation for killing wild fishes in shrimp and crab pond |
| CN106727923A (en) * | 2017-01-17 | 2017-05-31 | 普宁康特生物科技有限公司 | A kind of anti-bacteriostatic solution of Quaternary Ammonium Salt of Chitosan silver particles and preparation method thereof |
-
2017
- 2017-06-02 CN CN201710408315.3A patent/CN107019002A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1977618A (en) * | 2006-12-06 | 2007-06-13 | 福州大学 | Method for preparing tea saporin pool-cleaning agent using tea dreg as raw material |
| CN102342283A (en) * | 2011-07-28 | 2012-02-08 | 浙江省淡水水产研究所 | Combined preparation for killing wild fishes in shrimp and crab pond |
| CN106727923A (en) * | 2017-01-17 | 2017-05-31 | 普宁康特生物科技有限公司 | A kind of anti-bacteriostatic solution of Quaternary Ammonium Salt of Chitosan silver particles and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108432809A (en) * | 2018-03-30 | 2018-08-24 | 湖南淳湘农林科技有限公司 | A kind of cleaner for the cultivation of shrimp crab |
| CN110214731A (en) * | 2019-07-18 | 2019-09-10 | 安徽众渔生物科技有限公司 | One seed shrimp crab culture pond trash fish scavenger |
| CN111937915A (en) * | 2020-07-07 | 2020-11-17 | 临沂垂闲商贸有限公司 | Aquatic organism inducer and preparation method thereof |
| CN111937915B (en) * | 2020-07-07 | 2022-05-20 | 临沂垂闲商贸有限公司 | Aquatic organism inducer and preparation method thereof |
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Application publication date: 20170808 |
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