CN107010599A - A kind of sodium hypochlorite continuous production device - Google Patents
A kind of sodium hypochlorite continuous production device Download PDFInfo
- Publication number
- CN107010599A CN107010599A CN201710201106.1A CN201710201106A CN107010599A CN 107010599 A CN107010599 A CN 107010599A CN 201710201106 A CN201710201106 A CN 201710201106A CN 107010599 A CN107010599 A CN 107010599A
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- chlorine
- absorption tower
- inlet
- leading portion
- storage tank
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B11/00—Oxides or oxyacids of halogens; Salts thereof
- C01B11/04—Hypochlorous acid
- C01B11/06—Hypochlorites
- C01B11/062—Hypochlorites of alkali metals
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Abstract
The invention discloses a kind of sodium hypochlorite continuous production device, including：N number of leading portion absorption tower and N number of leading portion absorption tower one-to-one N number of storage container, tail gas absorber and light alkali storage tank, and N≤1；Efferent duct is mounted in storage container and on light alkali storage tank, efferent duct is provided with suction pump and cooler.The sodium hypochlorite continuous production device that the present invention is provided, chlorine flow direction is with light alkali flow direction on the contrary, chlorine is inversely contacted with light alkali.So, purity highest chlorine reacts with the minimum mixed solution of alkali lye content, the mixed gas that then chlorine content is gradually reduced is contacted with the mixing liquid that alkali lye content gradually rises, finally in absorption tower, and the extremely low unreacted chlorine of content is directly mixed with light alkali in gas.So, it is ensured that the absorption to chlorine, that is, cost has been saved, the pollution problem of exhaust emissions is solved again.
Description
Technical field
Filled the present invention relates to chemical products process units technical field, more particularly to a kind of sodium hypochlorite continuous production
Put.
Background technology
Sodium hypochlorite is a kind of high-efficient oxidant and chlorine-containing disinfectant, as bleaching agent, oxidant and water scavengine agent, is used for
Papermaking, weaving, light industry etc., chlorinating agent oxidative synthesis hydrazine hydrate, azodicarbonamide are used as in Organic chemical products production
And chlorated fulminuric acid.It is one of chlor-alkali industry in one of product produced as chlorine industry, sodium hypochlorite produce reality
Branch, general to be produced using caustic soda chloridising, i.e., with chlorine and caustic soda, (less than 15 DEG C) reactions are made under cryogenic
, its production method has two kinds of batch process and continuity method.In the market is more at present to be produced using batch process, i.e., using with cooler pan
The reactor of pipe, is passed directly into reaction in sodium hydroxide solution by chlorine and obtains liquor natrii hypochloritis.
The process units of this type is open system, and having that functional reliability is poor, cooling coil heat exchange efficiency is low can not
Removing heat of reaction in time causes that liquor natrii hypochloritis's quality is unstable, effective chlorine density is difficult to control to, chlorine absorption is incomplete
Etc. defect.In addition, in production, chlorine and sodium hydroxide solution are mixed by compressed air bubbling, reaction end is relied on
Manual sampling is analyzed, and effect is poor, and reactor gas phase can not be reclaimed effectively, and environmental pollution is more serious, to operator's health
Damage.
Therefore, from the actual conditions of production technology, exploitation can realize continuous production, and tail gas recycle can be realized again
Device, with great safe and environment-friendly and economic benefit, also provide reference for the production of chemical industry other products.
The content of the invention
The technical problem existed based on background technology, the present invention proposes a kind of sodium hypochlorite continuous production device.
A kind of sodium hypochlorite continuous production device proposed by the present invention, including：N number of leading portion absorption tower and N number of leading portion are inhaled
Receive tower one-to-one N number of storage container, tail gas absorber and light alkali storage tank, and N≤1；
Efferent duct is mounted in storage container and on light alkali storage tank, efferent duct is provided with suction pump and cooler；
Tail gas absorber be provided with inlet exhaust gas, exhaust port, light alkali import and first product floss hole, first product floss hole,
Inlet exhaust gas, light alkali import and the arrangement of exhaust port sequence from low to uper part；Each leading portion absorption tower is provided with chlorine inlet, chlorine
Outlet, inlet and liquid outlet, wherein, liquid outlet, chlorine inlet, inlet and the arrangement of chlorine gas outlet sequence from low to uper part；
N number of leading portion absorption tower is arranged in order, and the chlorine inlet on first leading portion absorption tower is connected with chlorine feedway, its
Chlorine gas outlet of the chlorine inlet on remaining leading portion absorption tower with previous leading portion absorption tower is connected, last leading portion absorption tower
Chlorine gas outlet connect tail gas absorber inlet exhaust gas；The lye import of tail gas absorber and the efferent duct of light alkali storage tank connect
It is logical；The first product floss hole of tail gas absorber is connected with last storage container, the liquid outlet on each leading portion absorption tower with
Corresponding storage container connection, the efferent duct of m-th storage container is connected with the inlet on the M-1 leading portion absorption tower, 2≤M
≤ N, and inlet of the efferent duct also with n-th leading portion absorption tower of n-th storage container connect, first leading portion absorption tower
Efferent duct is connected to hypo acid pan tank；
It is equipped with offgas outlet at the top of storage container and is connected with the inlet exhaust gas of tail gas absorber.
Preferably, drain valve is provided with the liquid outlet on last leading portion absorption tower.
Preferably, packing layer is equipped with each leading portion absorption tower, chlorine inlet and inlet are located under packing layer respectively
Side and top.
Preferably, packing layer is provided with tail gas absorber, inlet exhaust gas and light alkali import are located at the lower section of packing layer respectively
And top.
Preferably, it is located in tail gas absorber above packing layer provided with correspondence at least one tower tray, and tail gas absorber
Each tower tray is provided with light alkali import, and also is provided with light alkali import on tail gas absorber between packing layer and tower tray.
Preferably, the waste gas outlet connected with the inlet exhaust gas of tail gas absorber also is provided with hypo acid pan tank.
Preferably, exhaust pump is installed at exhaust port.
Preferably, cooler uses panel cooler, and cooler input port connection cooling water input unit, and cooler is defeated
Outlet connection cooling-water drain device.
Preferably, in addition to blender, the input port of blender is used to input clear water and alkali lye, and its delivery outlet connects light alkali
Storage tank.
Preferably, including two leading portion absorption towers, one section of absorption tower and two sections of absorption towers, one section of absorption of correspondence are referred to as
The storage container on tower and two sections of absorption towers is referred to as finished product storage tank and semi-finished product storage tank；The chlorine inlet connection on one section of absorption tower
Chlorine feedway, the chlorine gas outlet on one section of absorption tower connects the chlorine inlet on two sections of absorption towers, and the chlorine on two sections of absorption towers goes out
Mouth connection inlet exhaust gas；The efferent duct of light alkali storage tank connects the light alkali import of tail gas absorber, the first product discharge of tail gas absorber
Mouth connects semi-finished product storage tank with the liquid outlet on two sections of absorption towers；The efferent duct of semi-finished product storage tank is respectively communicated with one section of absorption tower
Inlet and the inlet on two sections of absorption towers；The liquid outlet connection semi-finished product storage tank on two sections of absorption towers, one section of absorption tower goes out liquid
Mouth connection finished product storage tank；The efferent duct connection hypo acid pan tank of finished product storage tank；
Waste gas outlet, and the tail gas with tail gas absorber are equipped with the top of the top of semi-finished product storage tank and finished product storage tank
Inlet communication.
The sodium hypochlorite continuous production device that the present invention is provided, chlorine flow direction is with light alkali flow direction on the contrary, chlorine and light alkali
Reverse contact.In this way, purity highest chlorine reacts with the minimum mixed solution of alkali lye content, then chlorine content is gradually reduced
Mixed gas contacted with the mixing liquid that alkali lye content gradually rises, finally in absorption tower, content is extremely low not in gas
The chlorine of reaction is directly mixed with light alkali.So, it is ensured that the absorption to chlorine, that is, cost has been saved, tail gas row is solved again
The pollution problem put.
In the present invention, by the cooler on light alkali storage tank efferent duct, for by the mixed light alkali of 32% alkali lye and water
Cooled down, it is ensured that the low-temp reaction of light alkali and chlorine；Then, the cooler on each storage container efferent duct is to entering leading portion
Mixed solution before the reaction of absorption tower is cooled down, it is ensured that the low temperature of reaction environment in each leading portion absorption tower, it is ensured that
The stabilization of sodium hypochlorite.
Brief description of the drawings
Fig. 1 is a kind of sodium hypochlorite continuous production device schematic diagram proposed by the present invention.
Embodiment
A kind of sodium hypochlorite continuous production device proposed by the present invention, including：N number of leading portion absorption tower and N number of leading portion are inhaled
Receive tower one-to-one N number of storage container, tail gas absorber T-03, light alkali storage tank V-03 and blender MX0, N≤1.
Efferent duct is mounted in storage container and on light alkali storage tank V-03, efferent duct is provided with suction pump P0 and cooler
E0.After suction pump P0 work, the liquid in corresponding storage container or light alkali storage tank can be suctioned out, cooler E0 is to process
Liquid is cooled down.In present embodiment, cooler E0 uses panel cooler, when it is implemented, can also use other forms
Cooler.And cooler E0 input ports connection cooling water input unit, cooler E0 delivery outlets connection cooling-water drain device.
In this way, carrying out cold compensation by the flowing of cooling water, the liquid in efferent duct can be cooled by way of heat exchange,
Ensure the low temperature output of storage container or the liquid in light alkali storage tank.
Tail gas absorber T-03 is provided with inlet exhaust gas, exhaust port, light alkali import and first product floss hole, first product discharge
Mouth, inlet exhaust gas, light alkali import and the arrangement of exhaust port sequence from low to uper part.Each leading portion absorption tower provided with chlorine inlet,
Chlorine gas outlet, inlet and liquid outlet, wherein, liquid outlet, chlorine inlet, inlet and chlorine gas outlet sequence from low to uper part row
Row.N number of leading portion absorption tower is arranged in order, and the chlorine inlet on first leading portion absorption tower is connected with chlorine feedway, remaining
Chlorine gas outlet of the chlorine inlet on leading portion absorption tower with previous leading portion absorption tower is connected, the chlorine on last leading portion absorption tower
Gas outlet connection tail gas absorber T-03 inlet exhaust gas.
Blender MX0 input port is used to input clear water and alkali lye, and its delivery outlet connects light alkali storage tank V-03.In this way, alkali
Liquid and water are mixed to form light alkali and are stored in light alkali storage tank.Tail gas absorber T-03 lye import is with light alkali storage tank V-03's
Efferent duct is connected.Light alkali solution in light alkali storage tank V-03 is under corresponding suction pump P0 effects by the cooling of corresponding cooler
Tail gas absorber T-03 and the chlorine reaction acquisition sodium hypochlorite in tower are entered by efferent duct afterwards, unreacted gas passes through tail
Aspiration tower T-03 exhaust port high altitude discharge.Exhaust pump C0 is installed in present embodiment, at exhaust port.
Tail gas absorber T-03 first product floss hole connects with last storage container, and each leading portion absorption tower goes out
Liquid mouth is connected with corresponding storage container, and the inlet on the efferent duct of m-th storage container and the M-1 leading portion absorption tower connects
It is logical, 2≤M≤N, and inlet of the efferent duct also with n-th leading portion absorption tower of n-th storage container connect, first leading portion
The efferent duct on absorption tower is connected to hypo acid pan tank V-04.
In present embodiment, drain valve is provided with the liquid outlet on last leading portion absorption tower.In this way, tail gas absorber T-
In 03 the mixed solution of included part sodium hypochlorite into last be n-th storage container, then by n-th storage
The n-th leading portion absorption tower that the efferent duct of container enters under discharge valve closed mode, treats the solution emptying in n-th storage container
Afterwards, then the drain valve on n-th leading portion absorption tower is opened, time chlorine will have been improved with chlorine reaction in n-th leading portion absorption tower
The mixed solution of sour sodium content is discharged into n-th storage container；Then efferent duct of the mixed solution Jing Guo n-th storage container
Continue to improve the content of sodium hypochlorite in mixed solution with chlorine reaction into the N-1 leading portion absorption tower.Similarly, mixed solution
Sequentially pass through m-th storage container, the M-1 second, leading portion absorption tower ... leading portion absorption tower, second storage container,
Enter first storage container behind one leading portion absorption tower, then by the efferent duct of first storage container in corresponding cooling
Enter the storage of hypo acid pan tank after device cooling.
In present embodiment, packing layer R0 is equipped with each leading portion absorption tower, chlorine inlet and inlet are located at respectively to be filled out
Bed of material R0 above and below.In this way, may be such that gas-liquid is sufficiently mixed by packing layer R0, best assimilation effect is reached, is carried
High chlorine utilization.Similarly, packing layer R0 is provided with tail gas absorber T-03, inlet exhaust gas and light alkali import are located at filler respectively
Layer R0 above and below.It is equipped with offgas outlet at the top of storage container and is connected with tail gas absorber T-03 inlet exhaust gas.
The waste gas outlet connected with tail gas absorber T-03 inlet exhaust gas also is provided with hypo acid pan tank V-04.
In present embodiment, unreacted gas enters tail gas absorber T-03, each storage in each leading portion absorption tower
Gas in container and hypo acid pan tank also enters tail gas absorber.It is located in tail gas absorber T-03 above packing layer R0 and sets
There is at least one tower tray Y0, and each tower tray Y0 of correspondence is provided with light alkali import, and tail gas absorber T-03 on tail gas absorber T-03
On light alkali import also is provided between packing layer R0 and tower tray Y0.In this way, the chlorine in tail gas absorber in mixed gas is basic
Can be fully absorbed in packing layer R0 by light alkali, even if least a portion of chlorine through packing layer R0 can also tower tray effect under with
Light alkali, which is sufficiently mixed, to be predominantly absorbed.Tower tray Y0 setting, which is avoided, contains unreacted chlorine in tail gas.
When it is implemented, being respectively provided with the liquid outlet on each leading portion absorption tower and at the first product floss hole of tail gas absorber
On-line Product analysis meter, effectively to control each section of absorption tower to go out time acid content in liquid, it is ensured that hypo acid quality of finished.
The sodium hypochlorite continuous production device that the present invention is provided, chlorine flow direction is with light alkali flow direction on the contrary, chlorine and light alkali
Reverse contact.In this way, in first leading portion absorption tower, purity highest chlorine reacts with the minimum mixed solution of alkali lye content,
The mixed gas that then chlorine content is gradually reduced is contacted with the mixing liquid that alkali lye content gradually rises, finally in tail gas absorption
In tower, the extremely low unreacted chlorine of content is directly mixed with light alkali in gas.So, it is ensured that the absorption to chlorine, that is, save
About cost, solves the pollution problem of exhaust emissions again.
Embodiment 1
Reference picture 1, the sodium hypochlorite continuous production device that the embodiment is provided, including two leading portion absorption towers, respectively
Referred to as one section absorption tower T-01 and two sections of absorption tower T-02, one section of absorption tower T-01 of correspondence and two sections of absorption tower T-02 storage are held
Device is referred to as finished product storage tank V-01 and semi-finished product storage tank V-02.
One section of absorption tower T-01 chlorine inlet connection chlorine feedway, one section of absorption tower T-01 chlorine gas outlet connection
Two sections of absorption tower T-02 chlorine inlet, two sections of absorption tower T-02 chlorine gas outlet connection inlet exhaust gas.Light alkali storage tank V-03's
Efferent duct connection tail gas absorber T-03 light alkali import, tail gas absorber T-03 first product floss hole and two sections of absorption tower T-02
Liquid outlet connect semi-finished product storage tank V-02.Semi-finished product storage tank V-02 efferent duct is respectively communicated with entering for one section of absorption tower T-01
The inlet of liquid mouthful and two sections of absorption tower T-02.Two sections of absorption tower T-02 liquid outlet connection semi-finished product storage tank V-02, one section of suction
Receive tower T-01 liquid outlet connection finished product storage tank V-01.Finished product storage tank V-01 efferent duct connection hypo acid pan tank V-04.
It is equipped with waste gas outlet at the top of semi-finished product storage tank V-02 top and finished product storage tank V-01, and and tail gas absorption
Tower T-03 inlet exhaust gas connection.In the present embodiment, alkali lye and the blended device MX0 of water form light alkali and enter light alkali storage tank, light
Light alkali in alkali storage tank enters tail gas absorber by efferent duct under suction pumping action after cooler；In tail gas absorber
Light alkali generates sodium hypochlorite and tail gas with chlorine reaction, and unreacted gas phase draws high-order emptying, sodium hypochlorite and residue through blower fan
Light alkali mixed solution enter semi-finished product storage tank；Mixed solution in semi-finished product storage tank passes through the corresponding suction pump of semi-finished product storage tank
Enter one section of absorption tower and two sections of absorption towers with cooler；Alkaline reaction life in chlorine and mixed solution in two sections of absorption towers
Into sodium hypochlorite, then the mixed solution in two sections of absorption towers returns to semi-finished product storage tank；By the circulation on two sections of absorption towers, half into
Hypochlorous acid alkali content increase in product storage tank, alkali lye is reduced；In one section of absorption tower, chlorine and remaining alkali lye in mixed solution are anti-
Sodium hypochlorite content's mixed solution up to standard should be obtained and finished product storage tank is delivered to；Liquor natrii hypochloritis's process pair in finished product storage tank
The suction pump answered and cooler output storage.
The residue that residual gas in one section of absorption tower enters in tail gas absorber, two sections of absorption towers by two sections of absorption towers
Gas enters the gas in tail gas absorber, tail gas absorber after the light Alkali absorption processing on tower tray in exhaust pump C0 effects
Lower high-order emptying.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (10)
1. a kind of sodium hypochlorite continuous production device, it is characterised in that including：N number of leading portion absorption tower and N number of leading portion absorb
Tower one-to-one N number of storage container, tail gas absorber (T-03) and light alkali storage tank (V-03), and N≤1；
Efferent duct is mounted in storage container and on light alkali storage tank (V-03), efferent duct is provided with suction pump (P0) and cooler
(E0)；
Tail gas absorber (T-03) is provided with inlet exhaust gas, exhaust port, light alkali import and first product floss hole, first product discharge
Mouth, inlet exhaust gas, light alkali import and the arrangement of exhaust port sequence from low to uper part；Each leading portion absorption tower provided with chlorine inlet,
Chlorine gas outlet, inlet and liquid outlet, wherein, liquid outlet, chlorine inlet, inlet and chlorine gas outlet sequence from low to uper part row
Row；
N number of leading portion absorption tower is arranged in order, and the chlorine inlet on first leading portion absorption tower is connected with chlorine feedway, remaining
Chlorine gas outlet of the chlorine inlet on leading portion absorption tower with previous leading portion absorption tower is connected, the chlorine on last leading portion absorption tower
The inlet exhaust gas of gas outlet connection tail gas absorber (T-03)；The lye import of tail gas absorber (T-03) and light alkali storage tank (V-
03) efferent duct connection；The first product floss hole of tail gas absorber (T-03) is connected with last storage container, each leading portion
The liquid outlet on absorption tower is connected with corresponding storage container, the efferent duct of m-th storage container and the M-1 leading portion absorption tower
Inlet connection, 2≤M≤N, and inlet of the efferent duct also with n-th leading portion absorption tower of n-th storage container connect,
The efferent duct on first leading portion absorption tower is connected to hypo acid pan tank (V-04)；
It is equipped with offgas outlet at the top of storage container and is connected with the inlet exhaust gas of tail gas absorber (T-03).
2. sodium hypochlorite continuous production device as claimed in claim 1, it is characterised in that last leading portion absorption tower
Drain valve is provided with liquid outlet.
3. sodium hypochlorite continuous production device as claimed in claim 1, it is characterised in that be equipped with each leading portion absorption tower
Packing layer (R0), chlorine inlet and inlet are located at the above and below of packing layer (R0) respectively.
4. sodium hypochlorite continuous production device as claimed in claim 1, it is characterised in that set in tail gas absorber (T-03)
There is packing layer (R0), inlet exhaust gas and light alkali import are located at the above and below of packing layer (R0) respectively.
5. sodium hypochlorite continuous production device as claimed in claim 4, it is characterised in that tail gas absorber (T-03) interior position
Provided with each tower tray (Y0) of correspondence at least one tower tray (Y0), and tail gas absorber (T-03) provided with light above packing layer (R0)
Light alkali import also is provided with alkali import, and tail gas absorber (T-03) between packing layer (R0) and tower tray (Y0).
6. sodium hypochlorite continuous production device as claimed in claim 1, it is characterised in that on hypo acid pan tank (V-04)
The waste gas outlet connected provided with the inlet exhaust gas with tail gas absorber (T-03).
7. sodium hypochlorite continuous production device as claimed in claim 1, it is characterised in that the row of being provided with exhaust port
Air pump (C0).
8. sodium hypochlorite continuous production device as claimed in claim 1, it is characterised in that cooler (E0) is using board-like cold
But device, and cooler (E0) input port connection cooling water input unit, cooler (E0) delivery outlet connection cooling-water drain device.
9. sodium hypochlorite continuous production device as claimed in claim 1, it is characterised in that also including blender (MX0), is mixed
The input port of clutch (MX0) is used to input clear water and alkali lye, and its delivery outlet connects light alkali storage tank (V-03).
10. the sodium hypochlorite continuous production device as described in any one of claim 1 to 9, it is characterised in that before two
Section absorption tower, is referred to as one section of absorption tower (T-01) and two sections of absorption towers (T-02), correspondence one section of absorption tower (T-01) and two
The corresponding storage container in section absorption tower (T-02) is referred to as finished product storage tank (V-01) and semi-finished product storage tank (V-02)；One section of absorption
The chlorine inlet connection chlorine feedway of tower (T-01), the chlorine gas outlet of one section of absorption tower (T-01) connects two sections of absorption towers
(T-02) chlorine inlet, the chlorine gas outlet connection inlet exhaust gas of two sections of absorption towers (T-02)；The output of light alkali storage tank (V-03)
The light alkali import of pipe connection tail gas absorber (T-03), the first product floss hole of tail gas absorber (T-03) and two sections of absorption tower (T-
02) liquid outlet connects semi-finished product storage tank (V-02)；The efferent duct of semi-finished product storage tank (V-02) is respectively communicated with one section of absorption tower
(T-01) inlet and the inlet of two sections of absorption towers (T-02)；The liquid outlet connection semi-finished product storage of two sections of absorption towers (T-02)
Groove (V-02), the liquid outlet connection finished product storage tank (V-01) of one section of absorption tower (T-01)；The efferent duct of finished product storage tank (V-01) connects
Logical hypo acid pan tank；
It is equipped with waste gas outlet at the top of the top of semi-finished product storage tank (V-02) and finished product storage tank (V-01), and and tail gas absorption
The inlet exhaust gas connection of tower (T-03).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710201106.1A CN107010599B (en) | 2017-03-30 | 2017-03-30 | Sodium hypochlorite continuous production device |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710201106.1A CN107010599B (en) | 2017-03-30 | 2017-03-30 | Sodium hypochlorite continuous production device |
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| CN107010599B CN107010599B (en) | 2023-07-07 |
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| CN107673311A (en) * | 2017-11-30 | 2018-02-09 | 山东尚舜化工有限公司 | A kind of continuous device and method for preparing the high-concentrated sodium hypochlorite aqueous solution |
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| Publication number | Publication date |
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| CN107010599B (en) | 2023-07-07 |
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