CN106988020A - A kind of composite fiber web, ricinus silk composite and preparation method thereof - Google Patents
A kind of composite fiber web, ricinus silk composite and preparation method thereof Download PDFInfo
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- CN106988020A CN106988020A CN201710200883.4A CN201710200883A CN106988020A CN 106988020 A CN106988020 A CN 106988020A CN 201710200883 A CN201710200883 A CN 201710200883A CN 106988020 A CN106988020 A CN 106988020A
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- composite fiber
- composite
- terylene
- fiber web
- ricinus silk
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/015—Natural yarns or filaments
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/005—Synthetic yarns or filaments
- D04H3/009—Condensation or reaction polymers
- D04H3/011—Polyesters
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H3/00—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
- D04H3/08—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating
- D04H3/14—Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between thermoplastic yarns or filaments produced by welding
- D04H3/153—Mixed yarns or filaments
Abstract
It is a kind of composite of use ricinus silk processing, specially a kind of composite fiber web, ricinus silk composite and preparation method thereof the present invention relates to textile material field.Composite fiber web, is mainly formed by following components by weight percentage by mixed weaving：Ricinus silk 50%~55%, terylene 30%~35% and Tencelsun fibers 15%~18%.A kind of ricinus silk composite, is formed by composite fiber web braiding.A kind of preparation method of ricinus silk composite, multiple composite fiber webs are superimposed in a layered fashion, the part or all of terylene in institute's composite fiber web is in molten condition and is kept preset time, are cooled down.The present invention raises the added value of product of ricinus silk.Present invention also offers a kind of ricinus silk composite manufacturing technique, the effect with anti-electromagnetism, ultra-violet radiation resisting and antibacterial thermal insulating.
Description
Technical field
The present invention relates to textile material field, it is a kind of composite of use ricinus silk processing, is specially a kind of multiple
Condensating fiber net, ricinus silk composite and preparation method thereof.
Background technology
Castor silkworm is the wild silkworm of field grown, eats castor leaf, also eats cassava leaves, crane wood leaf, tree-of-heaven leaf, horse pine needle and Shan Wu
CedarLeaves, are a kind of adaptability very strong polyphagy silkworms.Castor silkworm has polyvoltinism, under optimum conditions without duration of diapause, can be annual
It is continuous to raise, it can be bred for continuous 7 times within 1 year in China, therefore its raw material sources extremely enriches, economic benefit is considerable.Castor-oil plant
Aperture is left in silk cocoon one end, and the husks of castor silkworm was not only thick but also many, and husks accounts for 3.6%, and with cocoon layer without obvious boundary, castor silkworm
The cocoon layer of cocoon is thin, and cocoon layer accounts for 10%, and cocoon layer is soft, lacks elasticity, and thickness is elastic to differ greatly.Due to these characteristics, castor-oil plant
Silkworm cocoon reelability filament length is very short, and typically only 15~25m, its size deviation is larger, between 0.83~1.65dtex, it is impossible to reel silk from cocoons
Silk, the at present application both at home and abroad for ricinus silk is concentrated mainly on silk spinning, either processes silk comforter batt or by regenerating silkworm
The mode of silk-fibroin carries out the research and development of composite, but its technological process is longer, significantly limit its application and promotes,
Function is single, and value-added content of product is extremely low.
The content of the invention
It is an object of the invention to provide a kind of composite fiber web, have with anti-electromagnetism and anti-ultraviolet radiation and also and resist
The function such as bacterium, warming.
What the present invention was realized in：
A kind of composite fiber web, is mainly formed by following components by weight percentage by mixed weaving：Castor silkworm
Silk 50%~55%, terylene 30%~35% and Tencelsun fibers 15%~18%.
Invention further provides a kind of ricinus silk composite, formed by the braiding of above-mentioned composite fiber web.
Present invention also offers a kind of ricinus silk composite manufacturing technique, by the way that multilayer composite fiber net is folded
Plus, the ricinus silk composite of an entirety is formd, with constitutionally stable advantage, composite fiber web is also retains and is had
The function such as the anti-electromagnetism that has, anti-ultraviolet radiation, antibacterial, warming.
A kind of ricinus silk composite manufacturing technique, is superimposed, made in a layered fashion by multiple above-mentioned composite fiber webs
The terylene in composite fiber web is in molten condition and keeps preset time, cools down.
The beneficial effect of such scheme：
The invention provides a kind of composite fiber web, using ricinus silk as base material, also by added with terylene and
Tencelsun fibers, make composite fiber web have the performance of good anti-electromagnetism, ultra-violet radiation resisting and antibacterial thermal insulating.This hair
The composite fiber web of bright offer also makes ricinus silk serve not only as silk spinning or processing silk comforter batt use, can be also used for shape
Into multifunctional material, the operation strategies of ricinus silk are enhanced, and raise the added value of product of ricinus silk.
Present invention also offers the preparation method of a kind of ricinus silk composite and ricinus silk composite, pass through
Multilayer composite fiber net is overlapped to form sandwich construction, then makes to form bonding between multilayer composite fiber net by heating,
Ultimately form constitutionally stable ricinus silk composite.Because being combined using multilayer composite fiber net, ricinus silk is multiple
Condensation material equally has the technique effect of above-mentioned composite fiber web.But compared with above-mentioned composite fibre, because ricinus silk is multiple
Condensation material forms for multiple layer combination, and Stability Analysis of Structures, and its anti-electromagnetism, ultra-violet radiation resisting and antibacterial thermal insulating performance will be better than
Composite fiber web.
Brief description of the drawings
In order to illustrate the technical solution of the embodiments of the present invention more clearly, below will be attached to what is used required in embodiment
Figure is briefly described, it will be appreciated that the following drawings illustrate only certain embodiments of the present invention, therefore is not construed as pair
The restriction of scope, for those of ordinary skill in the art, on the premise of not paying creative work, can also be according to this
A little accompanying drawings obtain other related accompanying drawings.
Fig. 1 is a kind of structural representation of the orifice plate used in the embodiment of the present invention；
Fig. 2 shows a kind of structural representation of the shaped device used in the embodiment of the present invention.
Icon：100- shaped devices；110- bottom plates；120- orifice plates；130- frames；140- cell bodies；The infrared heat driers of 150-；
160- supersonic oscillations devices；170- fixed mounts；121- mesh.
Embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and is not construed as limiting the scope of the present invention.It is unreceipted specific in embodiment
Condition person, the condition advised according to normal condition or manufacturer is carried out.Agents useful for same or the unreceipted production firm person of instrument, be
The conventional products that can be obtained by commercially available purchase.The component of embodiments of the present invention, which are generally described and illustrated herein in the accompanying drawings
It can arrange and design with a variety of configurations.Therefore, below to the detailed of the embodiments of the invention that provide in the accompanying drawings
Thin description is not intended to limit the scope of claimed invention, but is merely representative of the selected embodiment of the present invention.It is based on
Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of creative work is not made
Embodiment, belongs to the scope of protection of the invention.
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention
In accompanying drawing, the technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is
A part of embodiment of the present invention, rather than whole embodiments.The present invention implementation being generally described and illustrated herein in the accompanying drawings
The component of example can be arranged and designed with a variety of configurations.Therefore, reality of the invention below to providing in the accompanying drawings
The detailed description for applying example is not intended to limit the scope of claimed invention, but is merely representative of the selected implementation of the present invention
Example.Based on the embodiment in the present invention, what those of ordinary skill in the art were obtained under the premise of creative work is not made
Every other embodiment, belongs to the scope of protection of the invention.
It should be noted that：Similar label and letter represents similar terms in following accompanying drawing, therefore, once a certain Xiang Yi
It is defined in individual accompanying drawing, then it further need not be defined and explained in subsequent accompanying drawing.
In the description of the invention, it is necessary to explanation, the orientation or position of the instruction such as term " on ", " under ", " interior ", " outer "
It is or the orientation or position that the invention product is usually put when using based on orientation shown in the drawings or position relationship to put relation
Relation is put, the description present invention is for only for ease of and simplifies description, rather than indicate or imply that the device or element of meaning are necessary
With specific orientation, with specific azimuth configuration and operation, therefore it is not considered as limiting the invention.
In the description of the invention, in addition it is also necessary to explanation, unless otherwise clearly defined and limited, term " setting ",
" installation ", " connected ", " connection " should be interpreted broadly, for example, it may be fixedly connected or be detachably connected, or one
Connect body；Can be mechanical connection or electrical connection；Can be joined directly together, can also be indirect by intermediary
It is connected, can is the connection of two element internals.For the ordinary skill in the art, on being understood with concrete condition
State the concrete meaning of term in the present invention.
A kind of composite fiber web, it is mainly formed by following components by weight percentage by mixed weaving：Castor-oil plant
Silk 50%~55%, terylene 30%~35% and Tencelsun fibers 15%~18%.
Further, composite fiber web is mainly formed by following components in percentage by weight by mixed weaving：
Ricinus silk 51%~52%, terylene 31%~32% and Tencelsun fibers 16%~18%.
Castor silkworm fibre length 40-45mm, fiber number：1.5-2.0dtex.
Further, terylene includes the terylene of weight identical first and the second terylene.
Wherein, the first terylene is the low melt point polyester fiber that fusing point is 110 DEG C~120 DEG C, low melt point polyester fiber fibre length 40-
45mm, line density：2.5-3.0dtex, fusing point：110℃.Second terylene is the silver-plated terylene that surface is coated with silver, and silver-plated terylene is fine
Tie up length 40-45mm, line density：2.5-3.0dtex.
Tencelsun fibre length 40-45mm, line density：2.42.5-3.0dtex.Tencelsun fibers be called and do " my god
Silk ", is wood pulp, water and the mixing of solvent oxidation amine based on coniferous tree, is heated to being completely dissolved, will not be produced in course of dissolution
Raw any derivative and chemical action, the direct fabrics through removal of impurities, its molecular structure is simple carbohydrate.
Tencelsun fibers can be decomposed completely in soil, environmentally safe；In addition, the amine oxide solvent pair used in production
Human body is completely harmless, is almost entirely capable of reclaiming, can Reusability, the cellulosic molecule in production contained by material pulp do not play chemistry
It is environmental protection or green fiber outside change, no coupling product, no discarded object discharge factory.
In the present embodiment, composite fiber web be by ricinus silk, low melt point polyester fiber fiber, silver-plated polyester fiber and
Tencelsun fibers are completed by blowing-carding-drawing unit by mixing, shredding, removal of impurities, braiding.
Blowing-carding-drawing unit is existing commercial equipment, and the present invention is not construed as limiting to its concrete structure.
A kind of composite fiber web that the present embodiment is provided, using ricinus silk as base-material, by by low melt point polyester fiber, silver-plated wash
Synthetic fibre and Tencelsun fibers carry out mixed weaving and obtained.Make composite fiber web have good anti-electromagnetism, ultra-violet radiation resisting and
The performance of antibacterial thermal insulating.
The present embodiment additionally provides a kind of ricinus silk composite based on above-mentioned composite fiber web and preparation method thereof,
Ricinus silk composite is formed by the braiding of above-mentioned composite fiber web.The preparation method of ricinus silk composite, including：It is multiple
Above-mentioned composite fiber web is superimposed in a layered fashion makes the terylene in composite fiber web be in molten condition and keep preset time,
Cooling.
S101, multiple composite fiber webs superposition：
In the present embodiment, multiple area identical composite fiber webs are tiled according to horizontal and vertical alternate order,
The number of plies of tiling is determined according to final use, for example, when needing thicker multilayer composite fiber net, can make the web of tiling
Quantity is more；When needing relatively thin multilayer composite fiber net, the web negligible amounts of tiling can be made, but the number of plies of tiling begins
It is more than or equal to two eventually.
The environment of tiling should be more smooth plane, and in the present embodiment, multiple composite fiber webs are enterprising in orifice plate 120
Row tiling.
Orifice plate 120 can be separately provided also combines the progress assembly of other structures body as needed.For example, in the present invention
What embodiment additionally provided another multilayer composite fiber net produces mode, and multiple composite fiber webs are placed on into shaped device
It is that multiple composite fiber webs are placed in orifice plate 120 further in 100.
On the surface of orifice plate 120, multiple composite fiber webs are placed with.Shaped device 100 see figure in the present embodiment
2, shaped device 100 includes the frame 130 for being used to place the orifice plate 120 of composite fiber web and be flexibly connected with the two ends of orifice plate 120,
Frame 130 is also connected with bottom plate 110.Frame 130 constitutes one section of cell body 140 with opening with bottom plate 110.Orifice plate
120 be that and orifice plate 120 offers the mesh 121 through the two ends of orifice plate 120 with certain thickness sheet material.In the present embodiment,
Mesh number >=500 of orifice plate 120.The quantity of orifice plate 120 can be single, or multiple.In the present embodiment, in order to increase
Multilayer composite fiber net in unit interval is produced, and the quantity of orifice plate 120 is more than 1, is two, one sets away from bottom plate 110
Put, one is set close to bottom plate 110.In the present embodiment, close between the nearest orifice plate 120 of bottom plate 110 and bottom plate 110 away from
From for 100mm, in other embodiments or 1/3rd or 2/3rds；The distance between two orifice plates 120 are 70mm,
Can also be more than 70mm and less than 70mm in other embodiments.In the present embodiment, the connection position of frame 130 and orifice plate 120
The place of putting is provided with fixed mount 170, and orifice plate 120 is realized on fixed mount 170 and is flexibly connected with frame 130 by riding upon, but
In other embodiment, however not excluded that using such as clamping, spin movable connection method.
S102, melting composite fiber web：
, as needed can be to composite fibre before being melted to composite fiber web after the superposition of multiple composite fiber webs
Net is pre-processed.For example, making lay between multiple composite fiber webs by pretreatment to be more uniformly distributed, further, melting is answered
, can also be to composite fiber web oscillation treatment after condensating fiber net.It is main to be noted that to being directly overlapped by orifice plate 120
Obtain multilayer composite fiber net, or the multilayer composite fiber net by pretreatment can be melted and answered with obtaining ricinus silk
Condensation material.
The step of oscillation treatment for example including：Multilayer composite fiber net is placed in water-bath, and high frequency is carried out to it
Mechanical oscillation.The method that multilayer composite fiber net is placed in water-bath include directly by the multilayer composite fiber net being superimposed from
Carry out high-frequency mechanical vibration is removed on orifice plate 120, in addition to shaped device 100 is placed on the progress higher-order of oscillation in water-bath and is shaken
It is dynamic, it is additionally included in shaped device 100 to inject water and be provided with high frequency machinery oscillation device in shaped device 100 and is vibrated
Operation.In the present embodiment, refering to Fig. 2, in order to ensure that multilayer composite fiber net will not make each composite fiber web because of mobile
Between mutually produce displacement, set high frequency machinery to vibrate dress using the water filling in shaped device 100 and in the shaped device 100
Put.
High-frequency mechanical vibration may include various ways, in the present embodiment, using supersonic oscillations to multilayer composite fiber
Net carries out high-frequency mechanical vibration.Refering to Fig. 2, in order to realize the supersonic oscillations to multilayer composite fiber net, in shaped device 100
Inner bottom plating 110 is provided with supersonic oscillations device 160 at position.It is that activity connects between supersonic oscillations device 160 and bottom plate 110
Connect, supersonic oscillations device 160 can set operating power according to the quantity of multilayer composite fiber net.In the present embodiment, when
When the quantity of multilayer composite fiber net is two, the frequency of supersonic oscillations device 160 is 28~48KHz, and power is 1.5~2Kw,
Duration of oscillation is 10~20min.Supersonic oscillations device 160 is existing commercial equipment, and the present invention is not limited its concrete structure
It is fixed.
In the present embodiment, the size of water consumption is determined according to the quantity of multi-layered web in water-bath.But minimum water
The upper surface 50mm that amount should be the multilayer composite fiber net that can exceed the remote setting of bottom plate 110 is defined.
High-frequency mechanical vibration is carried out to the multilayer composite fiber net of tiling by supersonic oscillations, in composite fibre net surface
Producing " cavitation " effect makes fiber carry out micro-shifting, can reach evenly laid out purpose.
In the present embodiment, realize that multilayer composite fiber net is evenly laid out by the sonic oscillation in water-bath.With traditional people
The mode that work cleaning is overlapped again is compared, it is necessary to carry out manpower operation, and the evenly laid out effect being finally reached will height
In manual work.Also, the effect of cleaning multilayer composite fiber net can also be realized indirectly by being cleaned by water-bath, with traditional mode
Compare, it is not necessary to addition auxiliary cleaning solvent, so as to get multi-layer fiber composite web in no chemical residues.
And a continuous conductive network of closing is formed during sonic oscillation in multilayer composite fiber net, can be right
Extraneous electromagnetic wave produces reflection and drainage, and the outer layer for being blocked in film cannot be introduced into material internal space, therefore, composite wood
The anti-electromagnetic radiation function admirable of material.
In the present embodiment, the mode of heating is by many of water bath sonicator ripple vibration by infrared 150 pairs of heat drier
Layer composite fiber web is heated.Infrared heat drier 150 can be single device, can also be connected with shaped device 100.At this
It is red in order to reduce the probability for making that displacement is produced between composite fiber web because of transfer multilayer composite fiber net in embodiment
Outer heat drier 150 is connected with shaped device 100.
In the present embodiment, multiple infrared heat driers 150 are uniformly arranged in frame 130 respectively.Wherein, in order to realize
The damage to infrared heat drier 150 is not resulted in water-bath oscillatory work, frame 130 can be set with the one side that cell body 140 is contacted
Put water-tight device.Water-tight device is included in the one side contacted with cell body 140 the waterproof membrane that is sticked, in addition to can carry out flexible up and down
The Telescopic Fixed block body in fixed, left and right.In the present embodiment, being sticked in the one side that frame 130 is contacted with cell body 140 has waterproof
Film.
The step of heating：Water in shaped device 100 is subjected to discharge operation, discharge opens infrared drying after terminating
Device 150 carries out drying to web.
In the present embodiment, in the present embodiment, the frame 130 of shaped device 100 is provided with the drainpipe being in communication with the outside,
And valve is provided with drainpipe, unlatching and closure for controlling drainpipe.
The drying temperature of infrared heat drier 150 is 110 DEG C~120 DEG C, and criteria thus the drying time is 5~10 minutes.
In the present embodiment, drying is carried out to multilayer composite fiber net by infrared drying device, can be made in composite fiber web
Low-melting fiber melt, so as to produce inter-adhesive between promoting the composite fiber web being in contact, make multiple compound fibres
Dimension net forms an organic whole, so as to finally give membranaceous ricinus silk composite.
The ricinus silk composite that the ricinus silk composite manufacturing technique provided by the present embodiment is made, passes through
Sonic oscillation and infrared drying, with good anti-electromagnetism, uvioresistant, antibacterial effect, also with good warmth retention property.
Specifically by sonic oscillation, make ricinus silk composite that there is stable architectural characteristic, can keep for a long time
More still air, so that the fiber solid thermal conductivity factor in whole ricinus silk composite is low, with good
Thermal property.Due to using low melt point polyester fiber fiber as one kind in mixing material and by infrared drying to low melting point
Polyester fiber is heated so that the place only in each composite fiber web contact point during watery fusion occurs than larger
Melt binding, the laminated structure of large area is not produced, from without influenceing the overall air permeability energy of ricinus silk composite.Cause
Make arrangement between multilayer composite fiber net uniform for sonic oscillation, gas permeability is better than traditional woven fabric.So, finally
Obtained ricinus silk composite has good hot wet migration energy.
Embodiment one
Composite fiber web, is formed by ricinus silk 130g, terylene 78g and Tencelsun fiber 39g by mixed weaving.
Terylene includes the first terylene 39g, the second terylene 39g.The composite fiber web being woven into is square structure, and each length of side is 1m.Its
In single ricinus silk fibre length be 45mm, fiber number is 1.5dtex；The fibre length of single first terylene is 40mm, line
Density is 2.5dtex, and fusing point is 110 DEG C；The fibre length of single second terylene is 40mm, and line density is 2.5dtex；It is single
The length of Tencelsun fibers is 40mm, and line density is 2.42dtex.
The preparation method of ricinus silk composite, which includes first being overlapped 5 composite fiber webs, obtains MULTILAYER COMPOSITE fibre
Net is tieed up, then is heated after being vibrated to multilayer composite fiber net.
The superposition of multilayer composite fiber net：5 composite fiber webs are carried out successively according to horizontal and vertical alternate order
Superposition.
The vibration of multi-layered web：The multilayer composite fiber net for being superimposed shaping is placed on orifice plate 120, and filled to shaping
Put and open the progress supersonic oscillations of supersonic oscillations device 160 10min in 100 after injection water.Supersonic oscillations device 160 it is super
Frequency of sound wave is 28KHz, and power is 1.5Kw, obtains the uniform multilayer composite fiber net that tiles.
The heating of multi-layered web：By drainpipe by outside the water discharge device in shaped device 100, infrared drying is opened
Device 150 carries out the drying of 5 minutes to multi-layered web, and drying temperature is 110 DEG C, finally gives membranaceous ricinus silk composite wood
Material.
Embodiment two
Composite fiber web, is formed by ricinus silk 130g, terylene 80g and Tencelsun fiber 40g by mixed weaving.
Terylene includes the first terylene 40g, the second terylene 40g.The composite fiber web being woven into is square structure, and each length of side is 1m.Its
In single ricinus silk fibre length be 43mm, fiber number is 1.7dtex；The fibre length of single first terylene is 43mm, line
Density is 2.7dtex, and fusing point is 110 DEG C；The fibre length of single second terylene is 43mm, and line density is 2.7dtex；It is single
The length of Tencelsun fibers is 43mm, and line density is 2.7dtex.
The preparation method of ricinus silk composite, which includes first being overlapped 5 composite fiber webs, obtains MULTILAYER COMPOSITE fibre
Net is tieed up, then is heated after being vibrated to multilayer composite fiber net.
The superposition of multilayer composite fiber net：5 composite fiber webs are carried out successively according to horizontal and vertical alternate order
Superposition.
The vibration of multi-layered web：The multilayer composite fiber net for being superimposed shaping is placed on orifice plate 120, and filled to shaping
Put and open the progress supersonic oscillations of supersonic oscillations device 160 15min in 100 after injection water.Supersonic oscillations device 160 it is super
Frequency of sound wave is 38KHz, and power is 1.7Kw, obtains the uniform multilayer composite fiber net that tiles.
The heating of multi-layered web：By drainpipe by outside the water discharge device in shaped device 100, infrared drying is opened
Device 150 carries out the drying of 7 minutes to multi-layered web, and drying temperature is 110 DEG C, finally gives membranaceous ricinus silk composite wood
Material.
Embodiment three
Composite fiber web, is formed by ricinus silk 130g, terylene 82g and Tencelsun fiber 42g by mixed weaving.
Terylene includes the first terylene 41g, the second terylene 41g.The composite fiber web being woven into is square structure, and each length of side is 1m.Its
In single ricinus silk fibre length be 45mm, fiber number is 2.0dtex；The fibre length of single first terylene is 45mm, line
Density is 3.0dtex, and fusing point is 110 DEG C；The fibre length of single second terylene is 45mm, and line density is 3.0dtex；It is single
The length of Tencelsun fibers is 45mm, and line density is 3.0dtex.
The preparation method of ricinus silk composite, which includes first being overlapped 5 composite fiber webs, obtains MULTILAYER COMPOSITE fibre
Net is tieed up, then is heated after being vibrated to multilayer composite fiber net.
The superposition of multilayer composite fiber net：5 composite fiber webs are carried out successively according to horizontal and vertical alternate order
Superposition.
The vibration of multi-layered web：The multilayer composite fiber net for being superimposed shaping is placed on orifice plate 120, and filled to shaping
Put and open the progress supersonic oscillations of supersonic oscillations device 160 20min in 100 after injection water.Supersonic oscillations device 160 it is super
Frequency of sound wave is 48KHz, and power is 2.0Kw, obtains the uniform multilayer composite fiber net that tiles.
The heating of multi-layered web：By drainpipe by outside the water discharge device in shaped device 100, infrared drying is opened
Device 150 carries out the drying of 10 minutes to multi-layered web, and drying temperature is 110 DEG C, finally gives membranaceous ricinus silk and is combined
Material.
Example IV
Composite fiber web, is formed by ricinus silk 130g, terylene 79g and Tencelsun fiber 40g by mixed weaving.
Terylene includes the first terylene 39.5g and the second terylene 39.5g.The composite fiber web being woven into is square structure, and each length of side is
1m.The fibre length of wherein single ricinus silk is 45mm, and fiber number is 1.5dtex；The fibre length of single first terylene is
40mm, line density is 2.5dtex, and fusing point is 110 DEG C；The fibre length of single second terylene is 40mm, and line density is
2.5dtex；The length of single Tencelsun fibers is 40mm, and line density is 2.42dtex.
The preparation method of ricinus silk composite, which includes first being overlapped 5 composite fiber webs, obtains MULTILAYER COMPOSITE fibre
Net is tieed up, then is heated after being vibrated to multilayer composite fiber net.
The superposition of multilayer composite fiber net：5 composite fiber webs are carried out successively according to horizontal and vertical alternate order
Superposition.
The vibration of multi-layered web：The multilayer composite fiber net for being superimposed shaping is placed on orifice plate 120, and filled to shaping
Put and open the progress supersonic oscillations of supersonic oscillations device 160 10min in 100 after injection water.Supersonic oscillations device 160 it is super
Frequency of sound wave is 28KHz, and power is 1.5Kw, obtains the uniform multilayer composite fiber net that tiles.
The heating of multi-layered web：By drainpipe by outside the water discharge device in shaped device 100, infrared drying is opened
Device 150 carries out the drying of 5 minutes to multi-layered web, and drying temperature is 110 DEG C, finally gives membranaceous ricinus silk composite wood
Material.
Embodiment five
Composite fiber web, is formed by ricinus silk 130g, terylene 80g and Tencelsun fiber 43g by mixed weaving.
Terylene includes the first terylene 40g and the second terylene 40g.The composite fiber web being woven into is square structure, and each length of side is 1m.Its
In single ricinus silk fibre length be 43mm, fiber number is 1.7dtex；The fibre length of single first terylene is 43mm, line
Density is 2.7dtex, and fusing point is 110 DEG C；The fibre length of single second terylene is 43mm, and line density is 2.7dtex；It is single
The length of Tencelsun fibers is 43mm, and line density is 2.7dtex.
The preparation method of ricinus silk composite, which includes first being overlapped 5 composite fiber webs, obtains MULTILAYER COMPOSITE fibre
Net is tieed up, then is heated after being vibrated to multilayer composite fiber net.
The superposition of multilayer composite fiber net：5 composite fiber webs are carried out successively according to horizontal and vertical alternate order
Superposition.
The vibration of multi-layered web：The multilayer composite fiber net for being superimposed shaping is placed on orifice plate 120, and filled to shaping
Put and open the progress supersonic oscillations of supersonic oscillations device 160 15min in 100 after injection water.Supersonic oscillations device 160 it is super
Frequency of sound wave is 38KHz, and power is 1.7Kw, obtains the uniform multilayer composite fiber net that tiles.
The heating of multi-layered web：By drainpipe by outside the water discharge device in shaped device 100, infrared drying is opened
Device 150 carries out the drying of 7 minutes to multi-layered web, and drying temperature is 110 DEG C, finally gives membranaceous ricinus silk composite wood
Material.
Embodiment six
Composite fiber web, is formed by ricinus silk 130g, terylene 80g and Tencelsun fiber 45g by mixed weaving.
Terylene includes the first terylene 40g and the second terylene 40g.The composite fiber web being woven into is square structure, and each length of side is 1m.Its
In single ricinus silk fibre length be 45mm, fiber number is 2.0dtex；The fibre length of single first terylene is 45mm, line
Density is 3.0dtex, and fusing point is 110 DEG C；The fibre length of single second terylene is 45mm, and line density is 3.0dtex；It is single
The length of Tencelsun fibers is 45mm, and line density is 3.0dtex.
The preparation method of ricinus silk composite, which includes first being overlapped 5 composite fiber webs, obtains MULTILAYER COMPOSITE fibre
Net is tieed up, then is heated after being vibrated to multilayer composite fiber net.
The superposition of multilayer composite fiber net：5 composite fiber webs are carried out successively according to horizontal and vertical alternate order
Superposition.
The vibration of multi-layered web：The multilayer composite fiber net for being superimposed shaping is placed on orifice plate 120, and filled to shaping
Put and open the progress supersonic oscillations of supersonic oscillations device 160 20min in 100 after injection water.Supersonic oscillations device 160 it is super
Frequency of sound wave is 48KHz, and power is 2.0Kw, obtains the uniform multilayer composite fiber net that tiles.
The heating of multi-layered web：By drainpipe by outside the water discharge device in shaped device 100, infrared drying is opened
Device 150 carries out the drying of 10 minutes to multi-layered web, and drying temperature is 110 DEG C, finally gives membranaceous ricinus silk and is combined
Material.
Comparative example one
Length from the single Rotating fields woven completely by ricinus silk is remembered for 1m ricinus silk woven fabric
It is CS-01, and CS-01 weight is identical with the weight of embodiment one and be closer to the weight of embodiment 2~6.By CS-01
Carried out respectively with embodiment one, embodiment two, embodiment three, example IV, embodiment five, embodiment six antiultraviolet test,
Permeability test and antibacterial test.Embodiment one, embodiment two, embodiment three, example IV, embodiment five, embodiment six
The length on each side is all 1m.
Table 1
UPF and transmittance in table 1 are used for the ultraviolet resistance for characterizing material, above example and
Ultraviolet resistance test is that preventing coating protection tester is tested by antiultraviolet transmission in comparative example one, is tested
Journey is according to GB18830-2009《The evaluation of ultraviolet resistance of fabric》Carry out.Using fabric air-permeability instrument to above-described embodiment
Tested with the permeability of comparative example one.Anti-microbial property survey is carried out to above-described embodiment and comparative example one using succusion
Examination, the strain of test is mainly Escherichia coli and staphylococcus glucose coccus.
With reference to GB18830-2009《The evaluation of ultraviolet resistance of fabric》Regulation, as the UPF ＞ 40 of sample, and T
(UVA) during ＜ 5%, it can be described as " antiultraviolet product ", binding test result, the composite meets wanting for antiultraviolet product
Ask.
As can be seen from Table 1, on ultraviolet resistance, permeability, thermal property and anti-microbial property, embodiment one~reality
The data in comparative example one will be better than by applying each item data of example six.Illustrate the ricinus silk that one~embodiment of embodiment six is provided
Composite will be better than the woven face of common castor silkworm on ultraviolet resistance, permeability, thermal property and anti-microbial property
Material, so that demonstrating ricinus silk composite has good hot wet migration energy and anti-microbial property.
The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, for the skill of this area
For art personnel, the present invention can have various modifications and variations.Within the spirit and principles of the invention, that is made any repaiies
Change, equivalent substitution, improvement etc., should be included in the scope of the protection.
Claims (10)
1. a kind of composite fiber web, it is characterised in that the composite fiber web is main by following components by weight percentage
Formed by mixed weaving：Ricinus silk 50%~55%, terylene 30%~35% and Tencelsun fibers 15%~18%.
2. composite fiber web according to claim 1, it is characterised in that the composite fiber web is main by according to weight percent
Following components than meter is formed by mixed weaving：Ricinus silk 51%~52%, the terylene 31%~32% and described
Tencelsun fibers 16%~18%.
3. composite fiber web according to claim 1, it is characterised in that the terylene includes the terylene of weight identical first
With the second terylene；The fusing point of first terylene is 110 DEG C~120 DEG C；There is silver coating on the second terylene surface.
4. a kind of ricinus silk composite, it is characterised in that by composite fiber web according to any one of claims 1 to 3
Braiding is formed.
5. a kind of preparation method of ricinus silk composite as claimed in claim 4, it is characterised in that including：It is multiple described
Composite fiber web is superimposed in a layered fashion, the part or all of terylene in the composite fiber web is in molten condition simultaneously
Keep preset time, cooling.
6. the preparation method of ricinus silk composite according to claim 5, it is characterised in that be superimposed in a layered fashion
The method of multiple composite fiber webs includes：
Multiple composite fiber webs are successively superimposed according to horizontal and vertical alternate mode.
7. the preparation method of ricinus silk composite according to claim 5, it is characterised in that be superimposed in a layered fashion
After multiple composite fiber webs, the terylene in composite fiber web described in adjacent two layers is set to be in before molten condition,
Also include：
The multiple composite fiber webs being superimposed in a layered fashion are soaked in water, and carry out supersonic oscillations.
8. the preparation method of ricinus silk composite according to claim 7, it is characterised in that described in sonic oscillation
In the step of composite fiber web, the ultrasonic frequency of sonic oscillation is 28~48KHz, and power is 1.5~2Kw, and duration of oscillation is
10~20min.
9. the preparation method of the ricinus silk composite according to claim 7 or 8, it is characterised in that in a layered fashion
Multiple composite fiber webs of superposition are affixed to be provided with the orifice plate in equally distributed multiple holes.
10. the preparation method of ricinus silk composite according to claim 5, it is characterised in that make the compound fibre
The method that the part or all of terylene in dimension net is in molten condition includes：
Using composite fiber web described in infrared heating, heating-up temperature is 110 DEG C~120 DEG C, and the heat time is 5~10min.
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| CN105463930A (en) * | 2015-11-25 | 2016-04-06 | 赖清甜 | Biodegradable fiber paper and preparation method thereof |
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| JPH10325059A (en) * | 1997-05-27 | 1998-12-08 | Japan Vilene Co Ltd | Nonwoven fabric and its production |
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| CA2738486A1 (en) * | 2008-10-06 | 2010-04-15 | Baylor University | Non-woven fabric composites from lignin-rich, large diameter natural fibers |
| CN102561023A (en) * | 2010-11-01 | 2012-07-11 | 西安纵横纺织科技有限公司 | Production process of nano titanium castor-oil plant silk fiber electromagnetic-shielding textile yarn |
| CN103194824B (en) * | 2013-04-08 | 2014-09-10 | 盛宇家纺集团股份有限公司 | Blending process for manufacturing silk fiber on basis of cotton spinning device |
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| CN101962873A (en) * | 2010-08-31 | 2011-02-02 | 东莞市挚爱内衣有限公司 | Production process of sponge-structured high-elasticity non-woven three-dimensional cotton |
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