CN106986590B - A kind of ceramic tile adhesive mortar, its preparation method and ceramic tile adhesion technique - Google Patents
A kind of ceramic tile adhesive mortar, its preparation method and ceramic tile adhesion technique Download PDFInfo
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- CN106986590B CN106986590B CN201710187056.6A CN201710187056A CN106986590B CN 106986590 B CN106986590 B CN 106986590B CN 201710187056 A CN201710187056 A CN 201710187056A CN 106986590 B CN106986590 B CN 106986590B
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/04—Portland cements
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00008—Obtaining or using nanotechnology related materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00637—Uses not provided for elsewhere in C04B2111/00 as glue or binder for uniting building or structural materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
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- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
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- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
The invention discloses a kind of ceramic tile adhesive mortar, its preparation method and ceramic tile adhesion technique.The ceramic tile adhesive mortar, is made up of the raw material of following parts by weight：The 700kg of quartz sand 300, the 600kg of portland cement 300, the 100kg of flyash 50, the 80kg of organobentonite 50, the 15kg of calcium formate 7, the 15kg of redispersable latex powder 6, the 8kg of cellulose ether 2, the 8kg of lignocellulosic 4, nano-TiO22 5kg, the 5kg of thixotropic lubricant 1.5, the 5kg of air entraining agent 3, the 5kg of fire retardant 3, antifreeze 3 5kg, the 1kg of starch ether 0.1 and the 250kg of water 150.The preferred each component of mortar of the present invention optimizes proportioning and obtains the excellent ceramic tile adhesive mortar of bond properties, is provided simultaneously with high water reducing rate, high intensity and ultraviolet radiation resisting, prevents aging etc. from acting on.
Description
Technical field
The present invention relates to building material technical field, is a kind of ceramic tile adhesive mortar, its preparation method and porcelain specifically
Brick adhesion technique.
Background technology
With the fast development of construction industry in recent years, the ceramic tile for pasting the ornament materials such as ceramic tile, face brick, floor tile bonds
Agent is widely used in the facing decoration places of the buildings such as inside and outside metope, ground, bathroom, kitchen.However, existing ceramic tile bonding
Agent, belong to rigid material mostly, cause cement mortar there is no enough adhesive force between ceramic tile after shaping, in external rings
Border, as temperature change, illumination particularly under the influence of long-term rainwater and illumination, ceramic tile adhesive mortar can cause certain change
Property, cause the reduction of its adhesive property.Or produced under the influence of ground or wall sinking, crack, external force effect etc. different
Stress and trickle movement, easily to lose original cohesive force between ceramic tile and binding face, cause hollowing even ceramic tile to take off
The phenomenon fallen produces, and not only have impact on the environmental beauty of building, it could even be possible to the personal safety of people is threatened, there is
Serious hidden danger.Therefore, it is that current building materials field is urgently to be resolved hurrily to develop a kind of tile adhesives with strong cohesive force
A problem.
Publication No. CN104844085A Chinese patent, disclose a kind of building exterior wall heat preserving tile adhesives and its system
Preparation Method and construction technology, its adhesive include cement, coarse whiting, quartz sand, hydroxypropyl methyl cellulose, rubber powder, rubber powder optimization
Element and mortar optimization agent；Its preparation method be according to mixing each component, drying more than 24 hours and naturally cool to room temperature, stir
What the step of machine stirs, heats and be again stirring for was carried out；First have to convert four kilograms of adhesives according to every liter of water during Specific construction
Row mixes, and is stirred into paste binder and mortar is completely spread basal plane with scraper dedicated, then have tooth form with scraper plate
While pulling up out striated in basal plane, last arranged in sequence stickup is simultaneously plain.Disclosure of the invention adhesive simultaneously combines its preparation
Method, and provide its construction technology；But its preparation technology is relatively simple, mortar sophistication is relatively low, causes its cohesive
Can be relatively poor.Publication No. CN105347737A Chinese patent, a kind of waterproof tile paste mortar is disclosed, by quality hundred
Divide more composed of the following components than counting：It is cement 42%, flyash 5%, yellow ground 26.3-37.8%, CHARACTERISTICS OF TAILINGS SAND 13.5-25.0%, outer
Add agent 1.7%；Described additive is modifying agent and thickening agent, and described modifying agent is cellulose ether, air entraining agent, water reducer
One or more mixtures, the present invention be effectively utilized a large amount of CHARACTERISTICS OF TAILINGS SANDs and the residue discharged after ore dressing or smelting and
The flyash that industrial waste is formed not only greatly reduces cost, and realizes the composition proportion of green non-pollution, reduces
The usage amount of natural yellow sand increases boundary mortar by one or more mixtures of cellulose ether, air entraining agent, water reducer simultaneously
Adhesive property and air content.But its bond properties has much room for improvement.
The defects of for China's adhesive mortar performance and its production, construction, the subject matter present in, with significantly
Degree improves adhesive mortar application property, caking property, crack resistance, weatherability, meets tile paste thin layer construction, present inventor has performed
Long-term research.
The content of the invention
In view of this, the purpose of the present invention is in view of the shortcomings of the prior art, there is provided a kind of bond properties is good, uvioresistant
The excellent ceramic tile adhesive mortar of line, anti-freezing property, solve ceramic tile easily come off problem and meanwhile reach it is longer bonding the time effect
Fruit.
To reach above-mentioned purpose, the present invention uses following technical scheme：
A kind of ceramic tile adhesive mortar, is made up of the raw material of following parts by weight：Quartz sand 300-700kg, portland cement
300-600kg, flyash 50-100kg, organobentonite 50-80kg, calcium formate 7-15kg, redispersable latex powder 6-15kg,
Cellulose ether 2-8kg, lignocellulosic 4-8kg, nano-TiO22-5kg, thixotropic lubricant 1.5-5kg, air entraining agent 3-5kg, resistance
Fire agent 3-5kg, antifreeze 3-5kg, starch ether 0.1-1kg and water 150-250kg.
Preferably, the thixotropic lubricant is aluminium-magnesium silicate thixotropic lubricant.
Preferably, the air entraining agent is that composite air entraining agent is mixed by polyether phosphate and α-sodium olefin sulfonate with identical weight ratio
Compounding is closed to form.
Preferably, the fire retardant is Al (OH)3Fire retardant.
Preferably, the antifreeze is compound antifreezer, includes the component of following parts by weight：Polycarboxylic acid series high-performance diminishing
Agent 18-30 parts, triethanolamine 3-11 parts, sodium acetate 3-10 parts, sodium alkyl benzene sulfonate 0.5-1 parts, dimethyl sulfoxide (DMSO) 55-60 parts；
Its preparation method first adds the triethanolamine of half, adds alkyl benzene sulphonate for sodium acetate high temperature is dissolved in dimethyl sulfoxide
Sodium, adds second half triethanolamine and polycarboxylate high performance water-reducing agent, and high-temperature stirring is uniformly.
Compared with traditional water reducer, polycarboxylate high performance water-reducing agent has many features：1. on synthesis technique, poly- carboxylic
The polycondensation synthesis that sour series high-performance dehydragent is used using unsaturated monomer copolymerization rather than conventional water reducing agents, therefore such
The synthesis material of water reducer is many, generally there is polyethylene glycol, (methyl) acrylic acid, allyl alcohol polyethenoxy ether etc..2.
On molecular structure, the molecular structure of polycarboxylate high performance water-reducing agent is Linear comb structure, rather than conventional water reducing agents are single
Linear structure.Polymerization has a variety of different active groups on such water reducer main chain, such as hydroxy-acid group (- COOH), hydroxyl base
Group (- OH), sulfonic group (- SO3Na) etc., can produce electrostatic repulsive force；Its side chain carries hydrophilic nonpolar activity
Group, there is higher space steric effect.Due to its extensive raw material sources, unique molecular structure, so have preceding two
For water reducer it is incomparable the advantages of, without using formaldehyde, belong to green product, therefore plus in building-up process, it has also become
One of emphasis and focus of concrete admixture research field.
Auxiliary material is added in ordinary mortar, it is possible to increase the bond properties of mortar, according to the different additives for requiring to use
Species is a lot, mainly plays waterproof, freeze proof, early strong, cracking resistance and impervious etc., but should before use these additives
Determine that it is good with the compatibility of inorganic coagulation material and the durability of mortar is had no adverse effects by testing.
Present invention also offers a kind of preparation method of ceramic tile adhesive mortar, comprise the following steps：
1) by the quartz sand of the parts by weight, portland cement, flyash, organobentonite and calcium formate, in flour mill
Middle carry out grinding, rotating speed 120-150r/min, grinding 9-10 hours, the powder that particle diameter is 1.2-1.4mm is obtained, powder is put
Enter in high temperature furnace, carry out temperature control firing；Come out of the stove natural cooling, after cooling in flour mill grinding 2-3 hours again, mixed
Thing A particle diameters are 0.8-1mm；
2) by redispersable latex powder, cellulose ether, lignocellulosic, nano-TiO2, thixotropic lubricant, air entraining agent, resistance
Agent is fired, antifreeze, grinding is carried out in flour mill, rotating speed 80-100r/min, grinding 2-3 hours, it is 0.6- to obtain particle diameter
0.8mm powder, is heated to powder, 700 DEG C of heating-up temperature, is incubated 2-3 hours, after cooling in flour mill grinding 2- again
3 hours, the particle diameter for obtaining mixture B was 0.3-0.5mm；
3) obtain mixture A by step 1) and step 2) obtained into mixture B to be fitted into mechanical mixer, mechanical mixture
0.5-1 hours, fall back, add starch ether, mechanical mixture 1-2 hours, obtain ceramic tile adhesive mortar.
Preferably, the method that institute's temperature control is fired is to be fired according to heating at a slow speed, middling speed heating and 3 processes of constant temperature：
200 DEG C are warming up at a slow speed with 2 DEG C/min speed, is warming up to 800 DEG C afterwards with 5 DEG C/min speed middling speed, and then constant temperature is protected
Temperature 2 hours.
When making adhesive mortar, the sand particle diameter as raw material should cover 0-4mm all sizes, so just relatively more suitable
It is fit to do the fine aggregate of mortar；Using wood fibre in ceramic tile cementing mortar, it is intended to improve stretching using its three-dimensional random distribution
Adhesion strength, and can significantly improve shrinkage it is desirable that having contributed workability and rupture strength and with the addition of air entraining agent of the present invention
Can, and with the addition of thickening agent of the present invention and significantly improve adhesion strength.
A kind of ceramic tile adhesion technique, comprises the following steps：
1) basic unit pre-processes：The concrete for protruding metope is picked into flat, metope feather plucking；Rewater moistening；The metope feather plucking
Concrete operations are, to the concrete wall surface dabbing of big punching block construction, and are completely brushed one times with wire brush or first that surface is very smooth
Substrate concrete surface dirt, dirt clean up, and are brushed off the greasy dirt of plate face with 10% caustic soda water, then with water purification by alkali lye
Wash down, dry；
2) pretreatment of mortar：Mortar is heated to 35-45 DEG C before smearing；
3) applying mortar, stickup ceramic tile：To step 1) pre-process basic unit on smearing step 2) pretreatment ceramic tile bond
Mortar, paste ceramic tile；
4) product protection, quality examination：The product protection is on the metope of the good ceramic tile of surface bonding, sprays hydrophobic
Agent, the hydrophober are formulated as：Weight compares hydrophober：Water=1:1, the hydrophober is organosilicon moisture repellent, is then carried out
Quality examination, ensure ceramic tile bonding quality.
Preferably, the smearing method of the ceramic tile adhesive mortar is that each time thickness is 5mm, rubs with the hands and puts down after smearing, waters every other day
Maintenance；When first pass six to seventy percent is dry, you can smear second time, thickness about 8-12mm, strike off immediately, rub hair with the hands, watering every other day is supported
Shield, then the operating method of the 3rd time is smeared with second time, untill bedding mortar is floating.
The beneficial effects of the invention are as follows：
1. the invention provides a kind of ceramic tile adhesive mortar, it is excellent that screening each component optimizes proportioning acquisition bond properties
Ceramic tile adhesive mortar, by researching and developing for many years：Obtain the rational proportion of the mortar major ingredient：M quartz sands：M silicate cements
Mud：Flyash：Organobentonite：Redispersable latex powder：Cellulose ether：Lignocellulosic：Nano-TiO2=300-700：
300-600：50-100：50-80：6-15：2-8：4-8：2-5；With reference to the additive of this formula and only in the range of the proportioning
Special preparation method, ensure that the excellent specific property of this formula mortar.
Using industrial residue waste material, the reasonable utilization of resource is realized：Quartz sand and powder in ceramic tile adhesive mortar of the present invention
Coal ash is to utilize ironworks waste residue, desulfurization ash and slag, industrial tailings and discarded building waste residue, metallurgical slag, ore, fire resisting
The general industrial solid wastes such as material, bauxite clinker, diamond dust and frit make, and can reduce the use to natural sand.
It is further preferred that 1.1) add air entraining agent in slurry component, the air entraining agent by polyether phosphate and
α-sodium olefin sulfonate is formed with identical weight than mixing compounding, can effectively play bleed, the function of defoaming, can be effective
The compactness between bubble, reinforced mortar material present in the materials such as quartz sand, cement is eliminated, so as to improve the viscous of mortar
Close performance；1.2) fire retardant Al (OH) is added3, by improving the thermal capacitance of polymer, it is absorbed before heat decomposition temperature is reached
More heats, so as to improve its fire resistance, and the Al (OH) after heating3The aqueous solution is capable of the viscous of effective reinforced mortar
Degree, further reach the effect of increase mortar bond properties；1.3) antifreeze is added, first, antifreeze enables to mortar to exist
Possesses fire-retardant and freeze proof performance on the basis of conventional binder performance；Meanwhile the antifreeze is compound antifreezer, including such as
The component of lower parts by weight：Polycarboxylate high performance water-reducing agent 18-30 parts, triethanolamine 3-11 parts, sodium acetate 3-10 parts, alkylbenzene
Sodium sulfonate 0.5-1 parts, dimethyl sulfoxide (DMSO) 55-60 parts；Its preparation method first adds for sodium acetate high temperature is dissolved in dimethyl sulfoxide
The triethanolamine of half, adds sodium alkyl benzene sulfonate, adds second half triethanolamine and polycarboxylic acid series high-performance diminishing
Agent, high-temperature stirring uniformly.It is high with highly viscous polycarboxylic-acid using the dimethyl sulfoxide (DMSO) of the high molten boiling point of high viscosity as solvent
Performance water reducer can be in reinforced mortar between each composition caking property, avoid being disintegrated caused by using water as single solvent existing
As.
Mortar of the invention as fire retardant uses redispersable latex powder, cold cut polyvinyl alcohol powder and hydroxypropyl methyl
Cellulose ether so that the mechanical property of mortar is greatly improved, particularly the tensile bond strength of mortar, is common viscous
Tie mortar 5-10 times, also with preferable weatherability, stable performance, good endurance.The addition of micro constitutent strengthens well
The properties of ceramic tile adhesive mortar, the addition of organobentonite and starch ether can significantly improve the impervious, anti-of mortar
Fragility, decrement property, water retention, impervious rank reach 12 grades, and the two coordinative role is than single addition organobentonite or starch ether
Reach more prominent effect；Nano-TiO2Can make to bond between mortar particle it is closer and form parcel and reach it is impervious simultaneously
Contraction can be reduced, especially in the presence of a harsh environment, it is possible to reduce shrink, this is particularly important for effectively control cracking；Antifreeze
Add be able to ensure that cold environment in still keeps the good bond properties of ceramic tile adhesive mortar, even if in the winter time also only
Shorter curing age is needed, ensure that engineering progress speed；Nano-TiO2Addition with thixotropic lubricant interaction can have
The resistance to chemical corrosion of effect enhancing ceramic tile adhesive mortar；It is provided simultaneously with uvioresistant photograph on the basis of high water reducing rate, high intensity
Penetrate, prevent aging etc. from acting on.
2. the invention provides a kind of preparation method of ceramic tile adhesive mortar, with reference to the property of mortar each component, by difference
Component is handled respectively, such as mixture A is prepared into the particle that particle diameter is 0.8-1mm, and mixture B is prepared into granularity size is
0.3-0.5mm, makes more very thin aggregate, and is added in mixture B and have lignocellulosic, it is intended to using its it is three-dimensional disorderly to
Distribution improves tensile bond strength；Effectively in reinforced mortar antigravity exfoliation ability.Its industrialized production obtains the quality of mortar
Guarantee has been arrived, the preparation link of job site has been simplified, substantially improves the working environment of job site, improve building
Quality, save substantial amounts of human resources.
3. present invention also offers a kind of ceramic tile adhesion technique, the method for feather plucking processing, applying mortar from base table, to rear
Between phase, protect, the good bonding effect of ceramic tile ensure that with the operation of system.
Embodiment
Embodiment 1
A kind of ceramic tile adhesive mortar, is made up of the raw material of following parts by weight：Quartz sand 300kg, portland cement 300kg,
Flyash 50kg, organobentonite 50kg, calcium formate 7kg, redispersable latex powder 6kg, cellulose ether 2kg, lignocellulosic
4kg, nano-TiO22kg, aluminium-magnesium silicate thixotropic lubricant 1.5kg, air entraining agent 3kg, fire retardant 3kg, antifreeze 3kg, starch ether
0.1kg and water 150kg；Wherein, the air entraining agent be composite air entraining agent by polyether phosphate with α-sodium olefin sulfonate with identical heavy
Amount forms than mixing compounding；The fire retardant is Al (OH)3Fire retardant；The antifreeze is compound antifreezer, including following weight
Measure the component of part：18 parts of polycarboxylate high performance water-reducing agent, 3 parts of triethanolamine, 3 parts of sodium acetate, 0.5 part of sodium alkyl benzene sulfonate,
55 parts of dimethyl sulfoxide (DMSO)；Its preparation method first adds the triethanolamine of half for sodium acetate high temperature is dissolved in dimethyl sulfoxide, then
Sodium alkyl benzene sulfonate is added, adds second half triethanolamine and polycarboxylate high performance water-reducing agent, high-temperature stirring is uniformly
Into.
Its preparation method, comprise the following steps：
1) by the quartz sand of above-mentioned parts by weight, portland cement, flyash, organobentonite and calcium formate, in flour mill
Middle carry out grinding, rotating speed 120r/min, grinding 9 hours, the powder that particle diameter is 1.2mm is obtained, powder is put into high temperature furnace,
Temperature control firing is carried out according to 3 heating at a slow speed, middling speed heating and constant temperature processes：200 are warming up at a slow speed with 2 DEG C/min speed
DEG C, 800 DEG C are warming up to 5 DEG C/min speed middling speed afterwards, then constant temperature is incubated 2 hours；Come out of the stove natural cooling, after cooling
Grinding 2 hours again in flour mill, it is 0.8mm to obtain mixture A particle diameters；
2) by redispersable latex powder, cellulose ether, lignocellulosic, nano-TiO2, thixotropic lubricant, air entraining agent, resistance
Agent is fired, antifreeze, grinding is carried out in flour mill, rotating speed 80r/min, grinding 2 hours, obtains the powder that particle diameter is 0.6mm,
Powder is heated, 600 DEG C of heating-up temperature, is incubated 2 hours, after cooling in flour mill grinding 2 hours again, obtain mixture
B particle diameter is 0.3mm；
3) obtain mixture A by step 1) and step 2) obtained into mixture B to be fitted into mechanical mixer, mechanical mixture
0.5 hour, fall back, add starch ether, mechanical mixture 1 hour, obtain ceramic tile adhesive mortar.
A kind of ceramic tile adhesion technique, comprises the following steps：
1) basic unit pre-processes：The concrete for protruding metope is picked into flat, metope feather plucking；Rewater moistening；The metope feather plucking
Concrete operations are, to the concrete wall surface dabbing of big punching block construction, and are completely brushed one times with wire brush or first that surface is very smooth
Substrate concrete surface dirt, dirt clean up, and are brushed off the greasy dirt of plate face with 10% caustic soda water, then with water purification by alkali lye
Wash down, dry；
2) pretreatment of mortar：Mortar is heated to 35 DEG C before smearing；
3) applying mortar, stickup ceramic tile：To step 1) pre-process basic unit on smearing step 2) pretreatment ceramic tile bond
Mortar, paste ceramic tile；The smearing method of the ceramic tile adhesive mortar is that each time thickness is 3mm, rubs with the hands and puts down after smearing, and watering every other day is supported
Shield；When first pass six to seventy percent is dry, you can smear second time, thickness about 8mm, strike off immediately, rub hair with the hands, every other day water seasoning, then
It is same second time to smear the operating method of the 3rd time, untill bedding mortar is floating；
4) product protection, quality examination：The product protection is on the metope of the good ceramic tile of surface bonding, sprays hydrophobic
Agent, the hydrophober are formulated as：Weight compares hydrophober：Water=1:1, the hydrophober is organosilicon moisture repellent, is then carried out
Quality examination, ensure ceramic tile bonding quality.
Embodiment 2
A kind of ceramic tile adhesive mortar, is made up of the raw material of following parts by weight：Quartz sand 700kg, portland cement 600kg,
Flyash 100kg, organobentonite 80kg, calcium formate 15kg, redispersable latex powder 15kg, cellulose ether 8kg, wood fibre
Plain 8kg, nano-TiO25kg, aluminium-magnesium silicate thixotropic lubricant 5kg, air entraining agent 5kg, fire retardant 5kg, antifreeze 5kg, starch ether
1kg and water 250kg；The air entraining agent is that composite air entraining agent is mixed by polyether phosphate and α-sodium olefin sulfonate with identical weight ratio
Compounding forms；The fire retardant is Al (OH)3Fire retardant；The antifreeze is compound antifreezer, includes the group of following parts by weight
Point：30 parts of polycarboxylate high performance water-reducing agent, 11 parts of triethanolamine, 10 parts of sodium acetate, 1 part of sodium alkyl benzene sulfonate, dimethyl are sub-
60 parts of sulfone；Its preparation method first adds the triethanolamine of half, adds alkyl for sodium acetate high temperature is dissolved in dimethyl sulfoxide
Benzene sulfonic acid sodium salt, adds second half triethanolamine and polycarboxylate high performance water-reducing agent, and high-temperature stirring is uniformly.
Its preparation method, comprise the following steps：
1) by the quartz sand of above-mentioned parts by weight, portland cement, flyash, organobentonite and calcium formate, in flour mill
Middle carry out grinding, rotating speed 150r/min, grinding 10 hours, the powder that particle diameter is 1.4mm is obtained, powder is put into high temperature furnace
In, carry out temperature control firing according to 3 heating at a slow speed, middling speed heating and constant temperature processes：It is warming up at a slow speed with 3 DEG C/min speed
300 DEG C, 800 DEG C are warming up to 5 DEG C/min speed middling speed afterwards, then constant temperature is incubated 3 hours；Come out of the stove natural cooling, cooling
Grinding 3 hours again in flour mill afterwards, it is 1mm to obtain mixture A particle diameters；
2) by redispersable latex powder, cellulose ether, lignocellulosic, nano-TiO2, thixotropic lubricant, air entraining agent, resistance
Agent is fired, antifreeze, grinding is carried out in flour mill, rotating speed 100r/min, grinding 3 hours, obtains the powder that particle diameter is 0.8mm
End, powder is heated, 700 DEG C of heating-up temperature, is incubated 3 hours, after cooling in flour mill grinding 3 hours again, mixed
Compound B particle diameter is 0.5mm；
3) obtain mixture A by step 1) and step 2) obtained into mixture B to be fitted into mechanical mixer, mechanical mixture 1
Hour, fall back, add starch ether, mechanical mixture 1.5 hours, obtain ceramic tile adhesive mortar.
A kind of ceramic tile adhesion technique, comprises the following steps：
1) basic unit pre-processes：The concrete for protruding metope is picked into flat, metope feather plucking；Rewater moistening；The metope feather plucking
Concrete operations are, to the concrete wall surface dabbing of big punching block construction, and are completely brushed one times with wire brush or first that surface is very smooth
Substrate concrete surface dirt, dirt clean up, and are brushed off the greasy dirt of plate face with 10% caustic soda water, then with water purification by alkali lye
Wash down, dry；
2) pretreatment of mortar：Mortar is heated to 45 DEG C before smearing；
3) applying mortar, stickup ceramic tile：To step 1) pre-process basic unit on smearing step 2) pretreatment ceramic tile bond
Mortar, paste ceramic tile；The smearing method of the ceramic tile adhesive mortar is that each time thickness is 5mm, rubs with the hands and puts down after smearing, and watering every other day is supported
Shield；When first pass six to seventy percent is dry, you can smear second time, thickness about 12mm, strike off immediately, rub hair with the hands, every other day water seasoning, then
It is same second time to smear the operating method of the 3rd time, untill bedding mortar is floating；
4) product protection, quality examination：The product protection is on the metope of the good ceramic tile of surface bonding, sprays hydrophobic
Agent, the hydrophober are formulated as：Weight compares hydrophober：Water=1:1, the hydrophober is organosilicon moisture repellent, is then carried out
Quality examination, ensure ceramic tile bonding quality.
Embodiment 3
A kind of ceramic tile adhesive mortar, is made up of the raw material of following parts by weight：Quartz sand 500kg, portland cement 450kg,
Flyash 75kg, organobentonite 65kg, calcium formate 11kg, redispersable latex powder 10kg, cellulose ether 5kg, wood fibre
Plain 6kg, nano-TiO23.5kg, aluminium-magnesium silicate thixotropic lubricant 3kg, air entraining agent 4kg, fire retardant 4kg, antifreeze 4kg, starch
Ether 0.6kg and water 200kg；The air entraining agent is for composite air entraining agent by polyether phosphate and α-sodium olefin sulfonate with identical weight ratio
Mixing compounding forms；The fire retardant is Al (OH)3Fire retardant；The antifreeze is compound antifreezer, including following parts by weight
Component：24 parts of polycarboxylate high performance water-reducing agent, 7 parts of triethanolamine, 6 parts of sodium acetate, 0.7 part of sodium alkyl benzene sulfonate, diformazan
57 parts of base sulfoxide；Its preparation method first adds the triethanolamine of half, added for sodium acetate high temperature is dissolved in dimethyl sulfoxide
Sodium alkyl benzene sulfonate, adds second half triethanolamine and polycarboxylate high performance water-reducing agent, and high-temperature stirring is uniformly.
Its preparation method, comprise the following steps：
1) by the quartz sand of above-mentioned parts by weight, portland cement, flyash, organobentonite and calcium formate, in flour mill
Middle carry out grinding, rotating speed 135r/min, grinding 9.5 hours, the powder that particle diameter is 1.3mm is obtained, powder is put into high temperature furnace
In, carry out temperature control firing according to 3 heating at a slow speed, middling speed heating and constant temperature processes：It is warming up at a slow speed with 2.5 DEG C/min speed
250 DEG C, 800 DEG C are warming up to 5 DEG C/min speed middling speed afterwards, then constant temperature is incubated 2.5 hours；Come out of the stove natural cooling, it is cold
But after in flour mill grinding 2.5 hours again, it is 0.9mm to obtain mixture A particle diameters；
2) by redispersable latex powder, cellulose ether, lignocellulosic, nano-TiO2, thixotropic lubricant, air entraining agent, resistance
Agent is fired, antifreeze, grinding is carried out in flour mill, rotating speed 90r/min, grinding 2.5 hours, obtains the powder that particle diameter is 0.7mm
End, powder is heated, 700 DEG C of heating-up temperature, is incubated 2.5 hours, after cooling in flour mill grinding 2.5 hours again, obtain
Particle diameter to mixture B is 0.4mm；
3) obtain mixture A by step 1) and step 2) obtained into mixture B to be fitted into mechanical mixer, mechanical mixture
0.75 hour, fall back, add starch ether, mechanical mixture 0.85 hour, obtain ceramic tile adhesive mortar.
A kind of ceramic tile adhesion technique, comprises the following steps：
1) basic unit pre-processes：The concrete for protruding metope is picked into flat, metope feather plucking；Rewater moistening；The metope feather plucking
Concrete operations are, to the concrete wall surface dabbing of big punching block construction, and are completely brushed one times with wire brush or first that surface is very smooth
Substrate concrete surface dirt, dirt clean up, and are brushed off the greasy dirt of plate face with 10% caustic soda water, then with water purification by alkali lye
Wash down, dry；
2) pretreatment of mortar：Mortar is heated to 40 DEG C before smearing；
3) applying mortar, stickup ceramic tile：To step 1) pre-process basic unit on smearing step 2) pretreatment ceramic tile bond
Mortar, paste ceramic tile；The smearing method of the ceramic tile adhesive mortar is that each time thickness is 4mm, rubs with the hands and puts down after smearing, and watering every other day is supported
Shield；When first pass six to seventy percent is dry, you can smear second time, thickness about 10mm, strike off immediately, rub hair with the hands, every other day water seasoning, then
It is same second time to smear the operating method of the 3rd time, untill bedding mortar is floating；
4) product protection, quality examination：The product protection is on the metope of the good ceramic tile of surface bonding, sprays hydrophobic
Agent, the hydrophober are formulated as：Weight compares hydrophober：Water=1:1, the hydrophober is organosilicon moisture repellent, is then carried out
Quality examination, ensure ceramic tile bonding quality.
Embodiment 4
A kind of ceramic tile adhesive mortar, is made up of the raw material of following parts by weight：Quartz sand 350kg, portland cement 350kg,
Flyash 60kg, organobentonite 60kg, calcium formate 8kg, redispersable latex powder 7kg, cellulose ether 3kg, lignocellulosic
5kg, nano-TiO23kg, aluminium-magnesium silicate thixotropic lubricant 2kg, air entraining agent 4kg, fire retardant 4kg, antifreeze 4kg, starch ether
0.3kg and water 170kg；The air entraining agent is that composite air entraining agent is mixed by polyether phosphate and α-sodium olefin sulfonate with identical weight ratio
Compounding is closed to form；The fire retardant is Al (OH)3Fire retardant；The antifreeze is compound antifreezer, including following parts by weight
Component：20 parts of polycarboxylate high performance water-reducing agent, 4 parts of triethanolamine, 4 parts of sodium acetate, 0.6 part of sodium alkyl benzene sulfonate, dimethyl
56 parts of sulfoxide；Its preparation method first adds the triethanolamine of half, adds alkane for sodium acetate high temperature is dissolved in dimethyl sulfoxide
Base benzene sulfonic acid sodium salt, adds second half triethanolamine and polycarboxylate high performance water-reducing agent, and high-temperature stirring is uniformly.
Its preparation method, comprise the following steps：
1) by the quartz sand of above-mentioned parts by weight, portland cement, flyash, organobentonite and calcium formate, in flour mill
Middle carry out grinding, rotating speed 130r/min, grinding 9.5 hours, the powder that particle diameter is 1.3mm is obtained, powder is put into high temperature furnace
In, carry out temperature control firing according to 3 heating at a slow speed, middling speed heating and constant temperature processes：It is warming up at a slow speed with 2.2 DEG C/min speed
230 DEG C, 800 DEG C are warming up to 5 DEG C/min speed middling speed afterwards, then constant temperature is incubated 2.8 hours；Come out of the stove natural cooling, it is cold
But after in flour mill grinding 2.5 hours again, it is 0.9mm to obtain mixture A particle diameters；
2) by redispersable latex powder, cellulose ether, lignocellulosic, nano-TiO2, thixotropic lubricant, air entraining agent, resistance
Agent is fired, antifreeze, grinding is carried out in flour mill, rotating speed 88r/min, grinding 2.2 hours, obtains the powder that particle diameter is 0.6mm
End, powder is heated, 700 DEG C of heating-up temperature, is incubated 2.7 hours, after cooling in flour mill grinding 2.6 hours again, obtain
Particle diameter to mixture B is 0.35mm；
3) obtain mixture A by step 1) and step 2) obtained into mixture B to be fitted into mechanical mixer, mechanical mixture
0.6 hour, fall back, add starch ether, mechanical mixture 1 hour, obtain ceramic tile adhesive mortar.
A kind of ceramic tile adhesion technique, comprises the following steps：
1) basic unit pre-processes：The concrete for protruding metope is picked into flat, metope feather plucking；Rewater moistening；The metope feather plucking
Concrete operations are, to the concrete wall surface dabbing of big punching block construction, and are completely brushed one times with wire brush or first that surface is very smooth
Substrate concrete surface dirt, dirt clean up, and are brushed off the greasy dirt of plate face with 10% caustic soda water, then with water purification by alkali lye
Wash down, dry；
2) pretreatment of mortar：Mortar is heated to 38 DEG C before smearing；
3) applying mortar, stickup ceramic tile：To step 1) pre-process basic unit on smearing step 2) pretreatment ceramic tile bond
Mortar, paste ceramic tile；The smearing method of the ceramic tile adhesive mortar is that each time thickness is 5mm, rubs with the hands and puts down after smearing, and watering every other day is supported
Shield；When first pass six to seventy percent is dry, you can smear second time, thickness about 9mm, strike off immediately, rub hair with the hands, every other day water seasoning, then
It is same second time to smear the operating method of the 3rd time, untill bedding mortar is floating；
4) product protection, quality examination：The product protection is on the metope of the good ceramic tile of surface bonding, sprays hydrophobic
Agent, the hydrophober are formulated as：Weight compares hydrophober：Water=1:1, the hydrophober is organosilicon moisture repellent, is then carried out
Quality examination, ensure ceramic tile bonding quality.
Embodiment 5
A kind of ceramic tile adhesive mortar, is made up of the raw material of following parts by weight：Quartz sand 400kg, portland cement 400kg,
Flyash 70kg, organobentonite 70kg, calcium formate 9kg, redispersable latex powder 7kg, cellulose ether 3kg, lignocellulosic
5kg, nano-TiO23kg, aluminium-magnesium silicate thixotropic lubricant 2.5kg, air entraining agent 4kg, fire retardant 4kg, antifreeze 4kg, starch ether
0.5kg and water 190kg；The air entraining agent is that composite air entraining agent is mixed by polyether phosphate and α-sodium olefin sulfonate with identical weight ratio
Compounding is closed to form；The fire retardant is Al (OH)3Fire retardant；The antifreeze is compound antifreezer, including following parts by weight
Component：22 parts of polycarboxylate high performance water-reducing agent, 5 parts of triethanolamine, 5 parts of sodium acetate, 0.7 part of sodium alkyl benzene sulfonate, dimethyl
57 parts of sulfoxide；Its preparation method first adds the triethanolamine of half, adds alkane for sodium acetate high temperature is dissolved in dimethyl sulfoxide
Base benzene sulfonic acid sodium salt, adds second half triethanolamine and polycarboxylate high performance water-reducing agent, and high-temperature stirring is uniformly.
Its preparation method, see embodiment 3.
Embodiment 6
A kind of ceramic tile adhesive mortar, is made up of the raw material of following parts by weight：Quartz sand 450kg, portland cement 500kg,
Flyash 80kg, organobentonite 80kg, calcium formate 10kg, redispersable latex powder 8kg, cellulose ether 4kg, lignocellulosic
6kg, nano-TiO24kg, aluminium-magnesium silicate thixotropic lubricant 3.5kg, air entraining agent 4.5kg, fire retardant 4.5kg, antifreeze 4.5kg,
Starch ether 0.6kg and water 210kg；The air entraining agent be composite air entraining agent by polyether phosphate with α-sodium olefin sulfonate with identical heavy
Amount forms than mixing compounding；The fire retardant is Al (OH)3Fire retardant；The antifreeze is compound antifreezer, including following weight
Measure the component of part：23 parts of polycarboxylate high performance water-reducing agent, 7 parts of triethanolamine, 6 parts of sodium acetate, 0.8 part of sodium alkyl benzene sulfonate,
58 parts of dimethyl sulfoxide (DMSO)；Its preparation method first adds the triethanolamine of half for sodium acetate high temperature is dissolved in dimethyl sulfoxide, then
Sodium alkyl benzene sulfonate is added, adds second half triethanolamine and polycarboxylate high performance water-reducing agent, high-temperature stirring is uniformly
Into.
Its preparation method, see embodiment 3.
Embodiment 7
A kind of ceramic tile adhesive mortar, is made up of the raw material of following parts by weight：Quartz sand 500kg, portland cement 550kg,
Flyash 85kg, organobentonite 55kg, calcium formate 12kg, redispersable latex powder 9kg, cellulose ether 6kg, lignocellulosic
7kg, nano-TiO24.5kg, aluminium-magnesium silicate thixotropic lubricant 4kg, air entraining agent 5kg, fire retardant 5kg, antifreeze 5kg, starch ether
0.7kg and water 500kg；The air entraining agent is that composite air entraining agent is mixed by polyether phosphate and α-sodium olefin sulfonate with identical weight ratio
Compounding is closed to form；The fire retardant is Al (OH)3Fire retardant；The antifreeze is compound antifreezer, including following parts by weight
Component：25 parts of polycarboxylate high performance water-reducing agent, 8 parts of triethanolamine, 8 parts of sodium acetate, 0.9 part of sodium alkyl benzene sulfonate, dimethyl
59 parts of sulfoxide；Its preparation method first adds the triethanolamine of half, adds alkane for sodium acetate high temperature is dissolved in dimethyl sulfoxide
Base benzene sulfonic acid sodium salt, adds second half triethanolamine and polycarboxylate high performance water-reducing agent, and high-temperature stirring is uniformly.
Its preparation method, see embodiment 3.
Embodiment 8
A kind of ceramic tile adhesive mortar, is made up of the raw material of following parts by weight：Quartz sand 600kg, portland cement 600kg,
Flyash 90kg, organobentonite 65kg, calcium formate 14kg, redispersable latex powder 14kg, cellulose ether 7kg, wood fibre
Plain 8kg, nano-TiO25kg, aluminium-magnesium silicate thixotropic lubricant 4.5kg, air entraining agent 3.5kg, fire retardant 4.5kg, antifreeze 3kg,
Starch ether 0.9kg and water 230kg；The air entraining agent be composite air entraining agent by polyether phosphate with α-sodium olefin sulfonate with identical heavy
Amount forms than mixing compounding；The fire retardant is Al (OH)3Fire retardant；The antifreeze is compound antifreezer, including following weight
Measure the component of part：28 parts of polycarboxylate high performance water-reducing agent, 10 parts of triethanolamine, 9 parts of sodium acetate, 1 part of sodium alkyl benzene sulfonate, two
58 parts of methyl sulfoxide；Its preparation method first adds the triethanolamine of half, then add for sodium acetate high temperature is dissolved in dimethyl sulfoxide
Enter sodium alkyl benzene sulfonate, add second half triethanolamine and polycarboxylate high performance water-reducing agent, high-temperature stirring is uniformly.
Its preparation method, see embodiment 3.
Comparative example 1, comparative example 1 is substantially the same manner as Example 3, and its difference is, by flyash with the quartz of equivalent
Sand substitutes.
Comparative example 2, comparative example 2 is substantially the same manner as Example 3, and its difference is, by cellulase with equivalent
Quartz sand substitutes.
Comparative example 3, comparative example 3 is substantially the same manner as Example 3, and its difference is, removes the nano-TiO2。
Effect detection
The ceramic tile cementing mortar prepared by this formula carries out adhesive property detection, test result with reference to JC/T547-2005
(being shown in Table 3).
The performance of the ceramic tile cementing mortar of table 3
Table 3 shows that ceramic tile cementing mortar prepared by the present invention has good adhesive property；It can be obtained from data above
Go out, the best match ratio of adhesive mortar is m quartz sands：M portland cements：Flyash：Organobentonite：Redispersable latex
Powder：Cellulose ether：Lignocellulosic：Nano-TiO2=500：450：75：65：10：5：6：3.5.
It can also obtain as drawn a conclusion simultaneously：Add after a series of chemical addition agents, the performance quilt of ceramic tile cementing mortar
Effectively enhancing, the basic performance and basis for having broken conventional slurry first match, in the proportioning of conventional slurry, flyash
The half for being cement weight is optimal, and in the formula of the present invention, the weight ratio of flyash and cement is 450：75；This be by
In introducing organobentonite, nano-TiO2, antifreeze, fire retardant and starch ether increase adhesive mortar it is freeze proof, it is fire-retardant, protect
While water-based energy, the fundamental property of mortar is improved, enhances its bond properties.
Finally illustrate, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, this area is common
Other modifications or equivalent substitution that technical staff is made to technical scheme, without departing from technical solution of the present invention
Spirit and scope, all should cover among scope of the presently claimed invention.
Claims (2)
1. a kind of ceramic tile adhesive mortar, it is characterised in that be made up of the raw material of following parts by weight：Quartz sand 300-700kg, silicic acid
Salt cement 300-600kg, flyash 50-100kg, organobentonite 50-80kg, calcium formate 7-15kg, redispersable latex powder
6-15kg, cellulose ether 2-8kg, lignocellulosic 4-8kg, nano-TiO22-5kg, thixotropic lubricant 1.5-5kg, air entraining agent
3-5kg, fire retardant 3-5kg, antifreeze 3-5kg, starch ether 0.1-1kg and water 150-250kg；
The thixotropic lubricant is aluminium-magnesium silicate thixotropic lubricant；
The air entraining agent is that composite air entraining agent is formed by polyether phosphate and α-sodium olefin sulfonate with identical weight ratio mixing compounding；
The fire retardant is Al (OH)3Fire retardant；
The antifreeze is compound antifreezer, includes the component of following parts by weight：Polycarboxylate high performance water-reducing agent 18-30 parts,
Triethanolamine 3-11 parts, sodium acetate 3-10 parts, sodium alkyl benzene sulfonate 0.5-1 parts, dimethyl sulfoxide (DMSO) 55-60 parts；Its preparation method
For sodium acetate high temperature is dissolved in dimethyl sulfoxide, the triethanolamine of half is first added, adds sodium alkyl benzene sulfonate, added another
The triethanolamine and polycarboxylate high performance water-reducing agent of half, with high-temperature stirring uniformly.
2. a kind of ceramic tile adhesion technique, it is characterised in that comprise the following steps：
1) basic unit pre-processes：The concrete for protruding metope is picked into flat, metope feather plucking；Rewater moistening；The metope feather plucking is specific
Operate and be, to the concrete wall surface dabbing of big punching block construction, and completely brushed one times with wire brush；
2) pretreatment of mortar：Mortar is heated to 35-45 DEG C before smearing；The mortar is mortar described in claim 1；
3）Applying mortar, paste ceramic tile：To step 1）Smearing step 2 in the basic unit of pretreatment）The ceramic tile adhesive mortar of pretreatment,
Paste ceramic tile；The smearing method of the ceramic tile adhesive mortar is that first pass thickness is 3-5mm, rubs with the hands and puts down after smearing, every other day water seasoning；
When first pass six to seventy percent is dry, you can smear second time, thickness 8-12mm, strike off immediately, rub hair with the hands, every other day water seasoning, then
Smear the 3rd time, its operating method is with second time, untill bedding mortar is floating；
4）Product protection, quality examination：The product protection is on the metope of the good ceramic tile of surface bonding, sprays hydrophober, institute
State being formulated as hydrophober：Weight compares hydrophober：Water=1:1, the hydrophober is organosilicon moisture repellent, then carries out quality inspection
Look into, ensure ceramic tile bonding quality.
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| CN108585667B (en) * | 2018-02-26 | 2020-09-29 | 上海牛元工贸有限公司 | Adhesive for high-adhesion ceramic tiles and preparation method thereof |
| CN108439853A (en) * | 2018-05-07 | 2018-08-24 | 滁州市炬基节能新型建材有限公司 | A kind of Multifunctional dry-mixed mortar additive and preparation method thereof |
| CN109369082B (en) * | 2018-12-06 | 2021-06-18 | 广西托肯建材有限公司 | Preparation method of mortar for paving floor tiles |
| CN110145087A (en) * | 2019-06-11 | 2019-08-20 | 曹磊 | A kind of construction method of stone material adhesion agent |
| CN110469068A (en) * | 2019-07-29 | 2019-11-19 | 安徽智恒节能材料科技有限公司 | A kind of construction technology of exterior wall decorating tile |
| CN112250368A (en) * | 2020-11-18 | 2021-01-22 | 广东合睿德新型材料有限公司 | High-permeability crystallization anti-drop ceramic tile adhesive |
| CN113860825B (en) * | 2021-11-17 | 2022-06-21 | 科顺民用建材有限公司 | Anti-ultraviolet radiation ceramic tile sizing material composition, anti-ultraviolet radiation ceramic tile sizing material, and preparation method and application thereof |
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| US5456751A (en) * | 1993-09-03 | 1995-10-10 | Trustees Of The University Of Pennsylvania | Particulate rubber included concrete compositions |
| CN101591153A (en) * | 2009-06-23 | 2009-12-02 | 常州市宇乔建材科技有限公司 | Composite air entraining agent and the mortar of making thereof |
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