CN106978235A - A kind of concrete synergy releasing agent - Google Patents

A kind of concrete synergy releasing agent Download PDF

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Publication number
CN106978235A
CN106978235A CN201710224710.6A CN201710224710A CN106978235A CN 106978235 A CN106978235 A CN 106978235A CN 201710224710 A CN201710224710 A CN 201710224710A CN 106978235 A CN106978235 A CN 106978235A
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CN
China
Prior art keywords
parts
fluosilicate
releasing agent
silicate
sodium
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Pending
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CN201710224710.6A
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Chinese (zh)
Inventor
冯月娥
李娟�
曹自俊
张会平
杨玉君
杨敏琦
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GANSU ZHITONG SCIENCE & TECHNOLOGY ENGINEERING DETECTION CONSULTATION Co Ltd
Original Assignee
GANSU ZHITONG SCIENCE & TECHNOLOGY ENGINEERING DETECTION CONSULTATION Co Ltd
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Priority to CN201710224710.6A priority Critical patent/CN106978235A/en
Publication of CN106978235A publication Critical patent/CN106978235A/en
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B28—WORKING CEMENT, CLAY, OR STONE
    • B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B7/00—Moulds; Cores; Mandrels
    • B28B7/38—Treating surfaces of moulds, cores, or mandrels to prevent sticking
    • B28B7/384—Treating agents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B28—WORKING CEMENT, CLAY, OR STONE
    • B28B—SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS; SHAPING SLAG; SHAPING MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
    • B28B7/00—Moulds; Cores; Mandrels
    • B28B7/38—Treating surfaces of moulds, cores, or mandrels to prevent sticking
    • B28B7/388—Treating surfaces of moulds, cores, or mandrels to prevent sticking with liquid material, e.g. lubricating
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    • C10M2207/10—Carboxylix acids; Neutral salts thereof
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    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
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    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/105—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing three carbon atoms only
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    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
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    • C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2217/02—Macromolecular compounds obtained from nitrogen containing monomers by reactions only involving carbon-to-carbon unsaturated bonds
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    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
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    • C10M2227/04—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions having a silicon-to-carbon bond, e.g. organo-silanes
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Abstract

The present invention relates to a kind of concrete synergy releasing agent, the releasing agent is made up of agitated uniform, the abundant dissolving of raw material of following weight parts：4.5 ~ 10 parts of soap powder, 71 ~ 80 parts of water, 3 ~ 5 parts of fluosilicate, 10 ~ 15 parts of silicate, 0 ~ 2 part of emulsifying agent, defoamer 0.5 ~ 1.5,0 ~ 0.5 part of preservative.Inventive formulation is reasonable, production cost is low, favorable working performance, is mainly used in, to appearance requirement harshness, the releasing agent of all kinds of specifications and models cement concrete construction members being made using plastic mould.

Description

A kind of concrete synergy releasing agent
Technical field
The present invention relates to technical field of concrete, more particularly to a kind of concrete synergy releasing agent.
Background technology
In recent decades, with the continuous improvement of science and technology and people's living standard, requirement of the people to each side is also more next It is higher.Especially to some external things, such as image, sense organ, appearance etc..Concrete construction is no exception, and concrete takes off The application of mould agent technology plays a leading role to presentation quality, the important investigation class also developed as concrete construction technology Topic.
The content of the invention
The technical problems to be solved by the invention be to provide a kind of formula rationally, raw material are easy to get and with low cost, work Performance is good, with lifting product aesthetic property, belong to environmentally friendly concrete synergy releasing agent.
To solve the above problems, a kind of concrete synergy releasing agent of the present invention, it is characterised in that：The releasing agent by The raw materials of following weight parts it is agitated it is uniform, fully dissolving and be made：4.5 ~ 10 parts of soap powder, 71 ~ 80 parts of water, fluosilicate 3 ~ 5 parts, 10 ~ 15 parts of silicate, 0 ~ 2 part of emulsifying agent, defoamer 0.5 ~ 1.5,0 ~ 0.5 part of preservative.
The soap powder refers to soap being crushed to 300 ~ 400 mesh after the moisture content obtained by 60 ~ 70 DEG C of dry 4 ~ 6h Less than 0.5% powder.
The fluosilicate be prodan, aluminum fluosilicate, ammonium fluosilicate, lithium fluorosilicate, calcium fluosilicate, potassium fluosilicate, Two or more in magnesium fluosilicate.
The silicate is two in sodium metasilicate, magnesium silicate, alumina silicate, potassium silicate, lithium metasilicate, ammonium silicate, aluminium-magnesium silicate Plant or several.
The defoamer is Ninol, lauroyl isopropanolamine, gelatin, glycerin polyether, dimethyl siloxane, poly dimethyl One or more in silicone oil, tributyl phosphate, octanol, diamylamine, polyvinyl lactam, polypropylene glycol.
The emulsifying agent is sulfated castor oil, three phenethyl phenol oxirane, turkey red oil, petroleum sodium sulfonate, secondary The sour soap of alcohol radical sodium sulphate, loose ester, phenethyl phenol polyethenoxy ether phosphorus, neopelex, two polyglycereol, fatty acid ester, One or more in diglycerol polypropylene glycol ether, glycerin polyoxyethylene ether polyoxypropylene ether fatty acid ester.
The preservative is natrium nitrosum, sorbic acid, dehydroactic acid sodium, benzoic acid, calcium propionate, sodium lactate, diacetic acid One or both of sodium, potassium sorbate.
The present invention has advantages below compared with prior art：
1st, the present invention in be added with emulsifying agent, preservative, store for a long time it is not stratified, do not precipitate, never degenerate.
2nd, fluosilicate, silicate, defoamer are added with the present invention, therefore, with modification concrete component outward appearance, is made Solid object surface forms the overcoat of fine and close quasi-vitreous, not only increases durability, is easy to the demoulding, irrelevant arrisdefect, improves Presentation quality also improves perception aesthetic beauty.
3rd, raw material of the present invention are easy to get, are formulated reasonable and easy to process, and not only environmental protection and energy saving are pollution-free, and cost is low It is honest and clean.
4th, present invention is mainly used for harsh to appearance requirement, all kinds of specifications and models cement concretes are made using plastic mould The releasing agent of component.
Embodiment
A kind of concrete synergy releasing agent of embodiment 1, the releasing agent is by following weight parts（kg）Raw material it is agitated it is uniform, Fully dissolve and be made：4.5 parts of soap powder, 73 parts of water, 3 parts of fluosilicate, 15 parts of silicate, 1.5 parts of emulsifying agent, defoamer 1.0th, 0 part of preservative.
Wherein：
Fluosilicate refers to prodan, aluminum fluosilicate by 1：1 weight ratio is mixed.
Silicate refers to sodium metasilicate, magnesium silicate by 1：2 weight ratio is mixed.
Emulsifying agent refers to phenethyl phenol polyethenoxy ether phosphorus.
Defoamer refers to gelatin, glycerin polyether by 1：1 weight ratio is mixed.
A kind of concrete synergy releasing agent of embodiment 2, the releasing agent is by following weight parts（kg）Raw material it is agitated it is uniform, Fully dissolve and be made：6.5 parts of soap powder, 75 parts of water, 4 parts of fluosilicate, 12 parts of silicate, 1.0 parts of emulsifying agent, defoamer 1.2nd, 0.3 part of preservative.
Wherein：
Fluosilicate refers to ammonium fluosilicate, lithium fluorosilicate, magnesium fluosilicate by 1:1:1 weight ratio is mixed.
Silicate refers to lithium metasilicate, ammonium silicate, aluminium-magnesium silicate by 1:1:1 weight ratio is mixed.
Emulsifying agent refers to sulfated castor oil, three phenethyl phenol oxirane, turkey red oil by 1:1:1 weight is than mixed Conjunction is formed.
Defoamer refers to lauroyl isopropanolamine, polydimethyl siloxane fluid, tributyl phosphate by 1:1:1 weight is than mixing Into.
Preservative refers to benzoic acid, calcium propionate by 1:1 weight ratio is mixed.
A kind of concrete synergy releasing agent of embodiment 3, the releasing agent is by following weight parts（kg）Raw material it is agitated it is uniform, Fully dissolve and be made：7.8 parts of soap powder, 73 parts of water, 4 parts of fluosilicate, 13 parts of silicate, 1.5 parts of emulsifying agent, defoamer 0.5th, 0.2 part of preservative.
Wherein：
Fluosilicate refers to prodan, aluminum fluosilicate, ammonium fluosilicate by 1:1:1 weight ratio is mixed.
Silicate refers to sodium metasilicate, magnesium silicate, alumina silicate by 1:1:1 weight ratio is mixed.
Emulsifying agent refers to fatty acid ester, diglycerol polypropylene glycol ether, glycerin polyoxyethylene ether polyoxypropylene ether fatty acid ester By 1:1:1 weight ratio is mixed.
Defoamer refers to tributyl phosphate, octanol, polyvinyl lactam by 1:1:1 weight ratio is mixed.
Preservative refers to benzoic acid, calcium propionate by 1:1 weight ratio is mixed.
A kind of concrete synergy releasing agent of embodiment 4, the releasing agent is by following weight parts（kg）Raw material it is agitated it is uniform, Fully dissolve and be made：9.5 parts of soap powder, 75 parts of water, 3 parts of fluosilicate, 11 parts of silicate, 2 parts of emulsifying agent, defoamer 1.0th, 0.3 part of preservative.
Wherein：
Fluosilicate refers to calcium fluosilicate, potassium fluosilicate by 1:1 weight ratio is mixed.
Silicate refers to lithium metasilicate, ammonium silicate by 1:1 weight ratio is mixed.
Emulsifying agent refers to turkey red oil, petroleum sodium sulfonate by 1:1 weight ratio is mixed.
Defoamer refers to polydimethyl siloxane fluid, tributyl phosphate by 1:1 weight ratio is mixed.
Preservative refers to sorbic acid, dehydroactic acid sodium by 1:1 weight ratio is mixed.
A kind of concrete synergy releasing agent of embodiment 5, the releasing agent is by following weight parts（kg）Raw material it is agitated it is uniform, Fully dissolve and be made：9.0 parts of soap powder, 71 parts of water, 5 parts of fluosilicate, 12 parts of silicate, 1.2 parts of emulsifying agent, defoamer 1.5th, 0.3 part of preservative.
Wherein：
Fluosilicate refers to prodan, potassium fluosilicate, magnesium fluosilicate by 1:1:1 weight ratio is mixed.
Silicate refers to sodium metasilicate potassium silicate, lithium metasilicate, aluminium-magnesium silicate by 1:1:1 weight ratio is mixed.
Emulsifying agent refers to the sour soap of loose ester, phenethyl phenol polyethenoxy ether phosphorus by 1:1 weight ratio is mixed.
Defoamer refers to Ninol, octanol by 1:1:1 weight ratio is mixed.
Preservative refers to sodium Diacetate.
A kind of concrete synergy releasing agent of embodiment 6, the releasing agent is by following weight parts（kg）Raw material it is agitated it is uniform, Fully dissolve and be made：7.0 parts of soap powder, 74 parts of water, 4 parts of fluosilicate, 13 parts of silicate, 1.0 parts of emulsifying agent, defoamer 0.5th, 0.2 part of preservative.
Wherein：
Fluosilicate refers to prodan, magnesium fluosilicate by 1:1 weight ratio is mixed.
Silicate refers to sodium metasilicate, lithium metasilicate by 1:1 weight ratio is mixed.
Emulsifying agent refers to secondary alcohol groups sodium sulphate, the sour soap of loose ester, phenethyl phenol polyethenoxy ether phosphorus by 1:1:1 weight is than mixed Conjunction is formed.
Defoamer refers to tributyl phosphate polyvinyl lactam by 1:1 weight ratio is mixed.
Preservative refers to sodium lactate.
A kind of concrete synergy releasing agent of embodiment 7, the releasing agent is by following weight parts（kg）Raw material it is agitated it is uniform, Fully dissolve and be made：8.5 parts of soap powder, 77 parts of water, 3 parts of fluosilicate, 10 parts of silicate, 0.8 part of emulsifying agent, defoamer 0.5th, 0.2 part of preservative.
Wherein：
Fluosilicate refers to prodan, calcium fluosilicate, potassium fluosilicate by 1:1:1 weight ratio is mixed.
Silicate refers to sodium metasilicate, lithium metasilicate, aluminium-magnesium silicate by 1:1:1 weight ratio is mixed.
Emulsifying agent refers to neopelex, two polyglycereol, diglycerol polypropylene glycol ether by 1:1:1 weight is than mixed Conjunction is formed.
Defoamer refers to lauroyl isopropanolamine, polydimethyl siloxane fluid, tributyl phosphate, octanol, diamylamine, polypropylene glycol By 1:1:1 weight ratio is mixed.
Preservative refers to benzoic acid, calcium propionate by 1:1 weight ratio is mixed.
A kind of concrete synergy releasing agent of embodiment 8, the releasing agent is by following weight parts（kg）Raw material it is agitated it is uniform, Fully dissolve and be made：5.5 parts of soap powder, 80 parts of water, 3 parts of fluosilicate, 10 parts of silicate, 0.5 part of emulsifying agent, defoamer 0.8th, 0.2 part of preservative.
Wherein：
Fluosilicate refers to prodan, calcium fluosilicate, potassium fluosilicate, magnesium fluosilicate by 1:1:1:1 weight ratio is mixed.
Silicate refers to sodium metasilicate, lithium metasilicate, ammonium silicate by 1:1:1 weight ratio is mixed.
Emulsifying agent is two polyglycereol, diglycerol polypropylene glycol ether by 1:1 weight ratio is mixed.
Defoamer refers to polyvinyl lactam, polypropylene glycol by 1:1 weight ratio is mixed.
Preservative refers to sorbic acid, benzoic acid by 1:1 weight ratio is mixed.
A kind of concrete synergy releasing agent of embodiment 9, the releasing agent is by following weight parts（kg）Raw material it is agitated it is uniform, Fully dissolve and be made：10 parts of soap powder, 74 parts of water, 3 parts of fluosilicate, 11 parts of silicate, 1.0 parts of emulsifying agent, defoamer 0.5th, 0.5 part of preservative.
Wherein：
Fluosilicate refers to prodan lithium fluorosilicate, potassium fluosilicate, magnesium fluosilicate by 1:1:1 weight ratio is mixed.
Silicate refers to sodium metasilicate, alumina silicate, potassium silicate by 1:1:1 weight ratio is mixed.
Emulsifying agent refers to secondary alcohol groups sodium sulphate, diglycerol polypropylene glycol ether, glycerin polyoxyethylene ether polyethenoxy ether fat Acid esters presses 1:1:1 weight ratio is mixed.
Defoamer refers to dimethyl siloxane, octanol, polypropylene glycol by 1:1:1 weight ratio is mixed.
Preservative refers to sodium lactate, potassium sorbate by 1:1 weight ratio is mixed.
In above-described embodiment 1 ~ 9, soap powder refers to soap being crushed to 300 ~ 400 mesh after obtained by 60 ~ 70 DEG C of dry 4 ~ 6h Moisture content be less than 0.5% powder.
Fluosilicate is prodan, aluminum fluosilicate, ammonium fluosilicate, lithium fluorosilicate, calcium fluosilicate, potassium fluosilicate, fluorine silicon Two or more in sour magnesium.
Silicate be sodium metasilicate, magnesium silicate, alumina silicate, potassium silicate, lithium metasilicate, ammonium silicate, aluminium-magnesium silicate in two kinds or It is several.
Defoamer is Ninol, lauroyl isopropanolamine, gelatin, glycerin polyether, dimethyl siloxane, poly dimethyl silicon One or more in oil, tributyl phosphate, octanol, diamylamine, polyvinyl lactam, polypropylene glycol.
Emulsifying agent is sulfated castor oil, three phenethyl phenol oxirane, turkey red oil, petroleum sodium sulfonate, secondary alcohol groups It is the sour soap of sodium sulphate, loose ester, phenethyl phenol polyethenoxy ether phosphorus, neopelex, two polyglycereol, fatty acid ester, double sweet One or more in oily polypropylene glycol ether, glycerin polyoxyethylene ether polyoxypropylene ether fatty acid ester.
Preservative is natrium nitrosum, sorbic acid, dehydroactic acid sodium, benzoic acid, calcium propionate, sodium lactate, sodium Diacetate, mountain One or both of potassium sorbate.

Claims (7)

1. a kind of concrete synergy releasing agent, it is characterised in that：The releasing agent by following weight parts raw material it is agitated it is uniform, fill Divide dissolving and be made：4.5 ~ 10 parts of soap powder, 71 ~ 80 parts of water, 3 ~ 5 parts of fluosilicate, 10 ~ 15 parts of silicate, emulsifying agent 0 ~ 2 Part, defoamer 0.5 ~ 1.5,0 ~ 0.5 part of preservative.
2. a kind of concrete synergy releasing agent as claimed in claim 1, it is characterised in that：The soap powder refers to soap It is crushed to 300 ~ 400 mesh and is less than 0.5% powder after the moisture content obtained by 60 ~ 70 DEG C of dry 4 ~ 6h.
3. a kind of concrete synergy releasing agent as claimed in claim 1, it is characterised in that：The fluosilicate is fluosilicic acid Two or more in sodium, aluminum fluosilicate, ammonium fluosilicate, lithium fluorosilicate, calcium fluosilicate, potassium fluosilicate, magnesium fluosilicate.
4. a kind of concrete synergy releasing agent as claimed in claim 1, it is characterised in that：The silicate is sodium metasilicate, silicon Two or more in sour magnesium, alumina silicate, potassium silicate, lithium metasilicate, ammonium silicate, aluminium-magnesium silicate.
5. a kind of concrete synergy releasing agent as claimed in claim 1, it is characterised in that：The defoamer is Ninol, the moon Osmanthus acyl isopropanolamine, gelatin, glycerin polyether, dimethyl siloxane, polydimethyl siloxane fluid, tributyl phosphate, octanol, diamylamine, One or more in polyvinyl lactam, polypropylene glycol.
6. a kind of concrete synergy releasing agent as claimed in claim 1, it is characterised in that：The emulsifying agent is sulphation castor-oil plant Oil, three phenethyl phenol oxirane, turkey red oil, petroleum sodium sulfonate, secondary alcohol groups sodium sulphate, the sour soap of loose ester, phenethyl phenol are gathered Oxygen vinethene phosphorus, neopelex, two polyglycereol, fatty acid ester, diglycerol polypropylene glycol ether, glycerin polyoxyethylene ether One or more in polyoxypropylene ether fatty acid ester.
7. a kind of concrete synergy releasing agent as claimed in claim 1, it is characterised in that：The preservative be natrium nitrosum, One or both of sorbic acid, dehydroactic acid sodium, benzoic acid, calcium propionate, sodium lactate, sodium Diacetate, potassium sorbate.
CN201710224710.6A 2017-04-07 2017-04-07 A kind of concrete synergy releasing agent Pending CN106978235A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110157536A (en) * 2019-05-30 2019-08-23 杭州中荷智慧城市科技有限公司 A kind of environment-friendly type concrete release agent
CN112608785A (en) * 2020-12-17 2021-04-06 甘肃五环公路工程有限公司 Release agent for improving concrete surface compactness
CN115247097A (en) * 2022-07-27 2022-10-28 四川天宇油脂化学有限公司 Concrete release agent based on glycerol extract and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1502336A1 (en) * 1987-08-11 1989-08-23 А.И.Мин йло, В.И.Вараксин, В.К.Живых, О.Ф.Двор дкина и В.Т.Соломойченко Lubricant for metal moulds
CN102634406A (en) * 2011-02-09 2012-08-15 白玉清 Concrete mold release agent
CN105385494A (en) * 2015-12-03 2016-03-09 新疆现代石油化工股份有限公司 Mold release agent for cement product and preparation method thereof
CN105713713A (en) * 2016-01-20 2016-06-29 江苏苏博特新材料股份有限公司 Surface reinforced concrete release agent

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1502336A1 (en) * 1987-08-11 1989-08-23 А.И.Мин йло, В.И.Вараксин, В.К.Живых, О.Ф.Двор дкина и В.Т.Соломойченко Lubricant for metal moulds
CN102634406A (en) * 2011-02-09 2012-08-15 白玉清 Concrete mold release agent
CN105385494A (en) * 2015-12-03 2016-03-09 新疆现代石油化工股份有限公司 Mold release agent for cement product and preparation method thereof
CN105713713A (en) * 2016-01-20 2016-06-29 江苏苏博特新材料股份有限公司 Surface reinforced concrete release agent

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110157536A (en) * 2019-05-30 2019-08-23 杭州中荷智慧城市科技有限公司 A kind of environment-friendly type concrete release agent
CN112608785A (en) * 2020-12-17 2021-04-06 甘肃五环公路工程有限公司 Release agent for improving concrete surface compactness
CN115247097A (en) * 2022-07-27 2022-10-28 四川天宇油脂化学有限公司 Concrete release agent based on glycerol extract and preparation method thereof

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Application publication date: 20170725