CN106975423A - Raw material for alkylation molecular proportion control system - Google Patents

Raw material for alkylation molecular proportion control system Download PDF

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Publication number
CN106975423A
CN106975423A CN201710308764.0A CN201710308764A CN106975423A CN 106975423 A CN106975423 A CN 106975423A CN 201710308764 A CN201710308764 A CN 201710308764A CN 106975423 A CN106975423 A CN 106975423A
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CN
China
Prior art keywords
pipeline
feedstock
raw material
valve
tank
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710308764.0A
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Chinese (zh)
Inventor
曲本华
王飞
李睿
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Ningxia Pan Thai Energy Technology Co Ltd
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Ningxia Pan Thai Energy Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Ningxia Pan Thai Energy Technology Co Ltd filed Critical Ningxia Pan Thai Energy Technology Co Ltd
Priority to CN201710308764.0A priority Critical patent/CN106975423A/en
Publication of CN106975423A publication Critical patent/CN106975423A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/02Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest

Abstract

Raw material for alkylation molecular proportion control system, the present invention relates to chemical producing system technical field;It includes high olefin feedstock tank, isobutane feedstock tank, a pump, No. two pumps, a valve group, No. two valve groups, a flowmeter and No. two flowmeters;High olefin feedstock tank is connected by pipeline with No. two pumps, and No. two pumps are connected by pipeline with No. two valve groups, and No. two valve groups are connected by pipeline with No. two flowmeters;Described isobutane feedstock tank is connected by pipeline with a pump, and a pump is connected by pipeline with a valve group, and a valve group is connected by pipeline with a flowmeter;The outlet of a described flowmeter and No. two flowmeters is connected by pipeline with merging after pipeline is connected with feedstock device.The ratio of iso-butane and butylene in its strict control raw material for alkylation, it is ensured that alkylated reaction is smoothed out, it is to avoid because molecular proportion controls the bad fluctuation caused, it is ensured that product quality, it is ensured that the length of device, peace, steady operation, practicality are stronger.

Description

Raw material for alkylation molecular proportion control system
Technical field
The present invention relates to chemical producing system technical field, and in particular to raw material for alkylation molecular proportion control system.
Background technology
Alkyl plant is the alkylation process for the purpose of producing motor petrol, aviation gasoline, uses two class raw materials, One class raw material is isoparaffin, because alkylated reaction follows carbonium ion mechanism, it is desirable to which alkane has tertiary carbon atom, so only It can be found in >=C4 alkane;Another kind of raw material is small-numerator olefin, including propylene, butylene and amylene.Butylene is best Raw material for alkylation, preferably, acid consumption is also minimum for product quality, and the acid consumption of propylene and amylene is almost several times of butylene.In recent years by Developed faster in producing high-octane rating blending component by propylene dimerization, therefore selection propylene raw material for alkylation is done Method is fewer and fewer, as amylene itself can as automotive fuel component, almost no one it as raw material for alkylation, therefore The raw material of alkylation olefin is most importantly butylene, and it includes 4 kinds of isomers:Isobutene, 1- butylene, cis-2-butene and trans- 2- Butylene.Raw material for alkylation molecular proportion is the important Con trolling index of alkyl plant, and molecular proportion is too high, then iso-butane is superfluous, superfluous Iso-butane can increase the load of alkyl plant, influence the production capacity of device, reduce the yield of isooctane, increase steam consumption Amount;Molecular proportion is too low, and system iso-butane can be caused few, influences reaction effect, alkylation is paid reaction increase, reduction isooctane Quality, causes alkyl plant to be not normally functioning.So raw material for alkylation molecular proportion must be controlled strictly.
The content of the invention
It is reasonable in design, make in view of the defects and deficiencies of the prior art, the present invention intends to provide one kind is simple in construction With convenient raw material for alkylation molecular proportion control system, it strictly controls the ratio of iso-butane and butylene in raw material for alkylation, really Protect alkylated reaction to be smoothed out, it is to avoid because molecular proportion controls the bad fluctuation caused, it is ensured that product quality, it is ensured that dress The length put, peace, steady operation, practicality are stronger.
To achieve the above object, the technical solution adopted by the present invention is:It includes high olefin feedstock tank, isobutane feedstock Tank, a pump, No. two pumps, a valve group, No. two valve groups, a flowmeter and No. two flowmeters;High olefin feedstock tank passes through pipe Road is connected with No. two pumps, and No. two pumps are connected by pipeline with No. two valve groups, and No. two valve groups are connected by pipeline with No. two flowmeters; Described isobutane feedstock tank is connected by pipeline with a pump, and a pump is connected by pipeline with a valve group, a valve group It is connected by pipeline with a flowmeter;The outlet of a described flowmeter and No. two flowmeters is by pipeline with merging pipeline It is connected after connection with feedstock device.
Further, described merging pipeline is provided with blender.
Further, a described valve group and No. two valve groups are constituted by three stop valves and a straight-through adjusting valve, Two of which stop valve is in parallel with another stop valve after being connected with straight-through adjusting valve.
Further, described high olefin feedstock tank is high olefin feedstock spherical tank.
Further, described isobutane feedstock tank is isobutane feedstock spherical tank.
Further, a described flowmeter and No. two flowmeters are mass flowmenter.
The technological process of the present invention is as follows:
First, high isobutane feedstock and high olefin feedstock are separately stored in high olefin feedstock tank and isobutane feedstock tank first;
2nd, two pumps are used again(I.e. No. one pump and No. two pumps)Feeding is carried out, and is respectively mounted in the exit of two pumps two valves Group(I.e. No. one valve group and No. two valve groups), while installing two mass flows(I.e. No. one flowmeter and No. two flowmeters), according to The difference of raw material controls high olefin feedstock and isobutane feedstock by a flowmeter by adjusting a valve group and No. two valve groups With the accurate metering of No. two flowmeters;
3rd, high olefin feedstock and isobutane feedstock are that feedstock device connects after a flowmeter and No. two flowmeters After being sufficiently mixed in the pipeline of the merging connect, into process units, it is ensured that raw molecule ratio is 1~1.5:Between 1.
After said structure, the present invention has the beneficial effect that:
1st, the strict ratio for controlling iso-butane and butylene in raw material for alkylation is 1~1.5:1, it is ensured that alkylated reaction smoothly enters OK, it is ensured that the normal production of device;
2nd, after raw material for alkylation molecular proportion control system comes into operation, raw molecule ratio is controlled well, and being needed according to device can be steady Surely raw molecule ratio is controlled, it is to avoid because molecular proportion controls the bad fluctuation caused, it is ensured that product quality, it is ensured that The length of device, peace, steady operation.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing There is the accompanying drawing used required in technology description to be briefly described, it should be apparent that, drawings in the following description are only this Some embodiments of invention, for those of ordinary skill in the art, without having to pay creative labor, may be used also To obtain other accompanying drawings according to these accompanying drawings.
Fig. 1 is the process chart of the present invention.
Description of reference numerals:
High olefin feedstock tank 1, isobutane feedstock tank 2, pump 3, No. two pumps 4, valve group 5, No. two valve groups 6, a flows Meter 7, No. two flowmeters 8, blender 9, merging pipelines 10.
Embodiment
The present invention is further illustrated below in conjunction with the accompanying drawings.
Referring to as shown in figure 1, the technical scheme that present embodiment is used is:It includes high olefin feedstock tank 1, isobutyl Alkane head tank 2, a pump 3, No. two pumps 4, a valve group 5, No. two valve groups 6, a flowmeter 7 and No. two flowmeters 8;High alkene Head tank 1 is connected by pipeline with No. two pumps 4, and No. two pumps 4 are connected by pipeline with No. two valve groups 6, and No. two valve groups 6 pass through pipeline It is connected with No. two flowmeters 8;Described isobutane feedstock tank 2 is connected by pipeline with a pump 3, a pump 3 by pipeline with A number valve group 5 is connected, and a valve group 5 is connected by pipeline with a flowmeter 7;A described flowmeter 7 and No. two flows The outlet of meter 8 is merged after pipeline 10 is connected by pipeline to be connected with feedstock device.
Further, described merging pipeline 10 is provided with blender 9.
Further, a described valve group 5 and No. two valve groups 6 are by three stop valves and a straight-through adjusting valve structure Into two of which stop valve is in parallel with another stop valve after being connected with straight-through adjusting valve.
Further, described high olefin feedstock tank 1 is high olefin feedstock spherical tank.
Further, described isobutane feedstock tank 2 is isobutane feedstock spherical tank.
Further, a described flowmeter 7 and No. two flowmeters 8 are mass flowmenter.
The technological process of present embodiment is as follows:
First, high isobutane feedstock and high olefin feedstock are separately stored in high olefin feedstock tank 1 and isobutane feedstock tank 2 first In;
2nd, two pumps are used again(I.e. No. one pump 3 and No. two pumps 4)Feeding is carried out, and two are respectively mounted in the exit of two pumps Valve group(I.e. No. one valve group 5 and No. two valve groups 6), while installing two mass flows(I.e. No. one flowmeter 7 and No. two flowmeters 8), according to the different by adjusting a valve group 5 and No. two valve groups 6 of raw material, control high olefin feedstock and isobutane feedstock to pass through The accurate metering of a number flowmeter 7 and No. two flowmeters 8;
3rd, high olefin feedstock and isobutane feedstock are feedstock device after a flowmeter 7 and No. two flowmeters 8 After being sufficiently mixed in the pipeline of the merging of connection, into process units, it is ensured that raw molecule ratio is 1~1.5:Between 1.
After said structure, present embodiment has the beneficial effect that:Present embodiment provides a kind of structure letter Single, reasonable in design, easy to use raw material for alkylation molecular proportion control system, its strictly control in raw material for alkylation iso-butane and The ratio of butylene, it is ensured that alkylated reaction is smoothed out, it is to avoid because molecular proportion controls the bad fluctuation caused, it is ensured that production Quality, it is ensured that the length of device, peace, steady operation, practicality are stronger.
It is described above, it is merely illustrative of the technical solution of the present invention and unrestricted, those of ordinary skill in the art are to this hair Other modifications or equivalent substitution that bright technical scheme is made, without departing from the spirit and scope of technical solution of the present invention, It all should cover among scope of the presently claimed invention.

Claims (7)

1. raw material for alkylation molecular proportion control system, it is characterised in that:It includes high olefin feedstock tank, isobutane feedstock tank, one Number pump, No. two pumps, a valve group, No. two valve groups, a flowmeter and No. two flowmeters;High olefin feedstock tank passes through pipeline and two Number pump connection, No. two pumps are connected by pipeline with No. two valve groups, and No. two valve groups are connected by pipeline with No. two flowmeters;Described Isobutane feedstock tank is connected by pipeline with a pump, and a pump is connected by pipeline with a valve group, and a valve group passes through pipe Road is connected with a flowmeter;After the outlet of a described flowmeter and No. two flowmeters is connected by pipeline with merging pipeline It is connected with feedstock device.
2. raw material for alkylation molecular proportion control system according to claim 1, it is characterised in that:On described merging pipeline Provided with blender.
3. raw material for alkylation molecular proportion control system according to claim 1, it is characterised in that:A described valve group and No. two valve groups are constituted by three stop valves and straight-through adjusting valve, after two of which stop valve is connected with straight-through adjusting valve and Another stop valve is in parallel.
4. raw material for alkylation molecular proportion control system according to claim 1, it is characterised in that:Described high olefin feedstock Tank is high olefin feedstock spherical tank.
5. raw material for alkylation molecular proportion control system according to claim 1, it is characterised in that:Described isobutane feedstock Tank is isobutane feedstock spherical tank.
6. raw material for alkylation molecular proportion control system according to claim 1, it is characterised in that:A described flowmeter It is mass flowmenter with No. two flowmeters.
7. raw material for alkylation molecular proportion control system according to claim 1, it is characterised in that:Its technological process is such as Under:
(1) high isobutane feedstock and high olefin feedstock, are separately stored in high olefin feedstock tank and isobutane feedstock tank first In;
(2) feeding, is carried out with two pumps again, and two valve groups are respectively mounted in the exit of two pumps, while installing two matter Flow is measured, according to the different by adjusting a valve group and No. two valve groups of raw material, high olefin feedstock and isobutane feedstock warp is controlled Cross the accurate metering of a flowmeter and No. two flowmeters;
(3), high olefin feedstock and isobutane feedstock are feedstock device after a flowmeter and No. two flowmeters After being sufficiently mixed in the pipeline of the merging of connection, into process units, it is ensured that raw molecule ratio is 1~1.5:Between 1.
CN201710308764.0A 2017-05-04 2017-05-04 Raw material for alkylation molecular proportion control system Pending CN106975423A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710308764.0A CN106975423A (en) 2017-05-04 2017-05-04 Raw material for alkylation molecular proportion control system

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710308764.0A CN106975423A (en) 2017-05-04 2017-05-04 Raw material for alkylation molecular proportion control system

Publications (1)

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CN106975423A true CN106975423A (en) 2017-07-25

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1116562A (en) * 1993-12-30 1996-02-14 菲利浦石油公司 Alkylation reactor with internal acid cooling zones
CN1639101A (en) * 2002-03-06 2005-07-13 三菱丽阳株式会社 Method of managing easily polymerizable substance and easily polymerizable substance managing apparatus
CN203710992U (en) * 2013-12-31 2014-07-16 东莞市广华化工有限公司 Quantitative proportioning device for reaction kettle
CN104722246A (en) * 2015-03-24 2015-06-24 江苏创新石化有限公司 Automatic flow proportioning device for tubular reactor
CN205517463U (en) * 2016-04-28 2016-08-31 天津滨海新区大港泰丰化工有限公司 Automatic batching mediation device
CN205797134U (en) * 2016-07-01 2016-12-14 南通天泽化工有限公司 A kind of thiamine waste water leads to ammonia automix device continuously
CN206103921U (en) * 2016-09-28 2017-04-19 上海中孚特种油品有限公司 Device of production fin oil

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1116562A (en) * 1993-12-30 1996-02-14 菲利浦石油公司 Alkylation reactor with internal acid cooling zones
CN1639101A (en) * 2002-03-06 2005-07-13 三菱丽阳株式会社 Method of managing easily polymerizable substance and easily polymerizable substance managing apparatus
CN203710992U (en) * 2013-12-31 2014-07-16 东莞市广华化工有限公司 Quantitative proportioning device for reaction kettle
CN104722246A (en) * 2015-03-24 2015-06-24 江苏创新石化有限公司 Automatic flow proportioning device for tubular reactor
CN205517463U (en) * 2016-04-28 2016-08-31 天津滨海新区大港泰丰化工有限公司 Automatic batching mediation device
CN205797134U (en) * 2016-07-01 2016-12-14 南通天泽化工有限公司 A kind of thiamine waste water leads to ammonia automix device continuously
CN206103921U (en) * 2016-09-28 2017-04-19 上海中孚特种油品有限公司 Device of production fin oil

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
刘初春 等: "硫酸烷基化机理与运行优化", 《中外能源》 *

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Application publication date: 20170725