CN106974853A

CN106974853A - A kind of plastotype hair jelly of dumb light texture and preparation method thereof

Info

Publication number: CN106974853A
Application number: CN201610933845.5A
Authority: CN
Inventors: 田鹏新
Original assignee: Individual
Current assignee: Individual
Priority date: 2016-11-01
Filing date: 2016-11-01
Publication date: 2017-07-25

Abstract

The present invention relates to one kind sizing Hair Stying Products, more particularly, to a kind of plastotype hair jelly of dumb light texture, it is calculated by weight, includes following material：13 parts of emulsifying agent, 0.2 1 parts of stabilizer, 3 12 parts of film forming agent, 15 20 parts of conditioner, 5 15 parts of NMF.By the way that addition is mixed with the xanthans of metal ion in right amount in hair jelly, instead of the waxy substance in pomade, its water solubility causes possess easy to clean in cleaning process, and and hair jelly in film forming material there is good combination effect, by adding mentioned emulsifier, under relatively low mixing speed i.e. can reach good emulsifying effectiveness, with the longer holding time, and material has good homogeneity in hair jelly, and its viscosity can reach 6000 8000cp, with gratifying fixed effect.

Description

A kind of plastotype hair jelly of dumb light texture and preparation method thereof

Technical field

The present invention relates to one kind sizing Hair Stying Products, plastotype hair jelly and its making side more particularly, to a kind of dumb light texture Method.

Background technology

Current pomade, hair jelly as sizing Hair Stying Products, are approved, current hair by numerous hair style hairstylists and consumer Glue product is main based on dumb light gloss, and pomade is due to wherein containing waxy substance, with certain brightness texture, for needing Show for the moulding of nature, be a kind of more excellent selection using hair jelly relative to pomade.

And because mainly using wax for raw material in pomade, for user, excessive use pomade is easily because of wax When being contacted with scalp and produce sticky sense, and needing to remove moulding, the wax mixed with shipwreck is in scale removal process, to user For itself, cleaning is more inconvenient.

At present by with good meeting MJPZ, with certain sticky polymer as hair style plastotype agent, instead of Original waxy product, is welcome by consumer, and in shape-designing, with good counterbalance effect, but for it is long when Between sizing and the higher medium-length hair moulding of torsion resistance, under slight mechanical load easily produce lose hair style fixed, but Exaggeration for bob moulding or in the short time is moulding still to make us more satisfied.

Such composition includes the copolymerization of copolymer, methyl vinyl ether and the maleic anhydride of vinylacetate and crotonic acid Copolymer, polyurethane, NVP, silicon based polymers of thing, acrylic or methacrylic acid and other monomers etc.. This analog copolymer is more to possess certain adherence, and meets adhesion of the MJPZ for skin of head, finger with good Property there is good improvement, but be slightly soluble in the property of water and make such product still relative difficulty, cleaning in scale removal process During have certain difficulty.

The content of the invention

Applicant is in the hair styling gel product that studies for a long period of time, based in hair styling gel, and product meets MJPZ, sticky Property, the consideration of the time soundness of water solubility and moulding, resistance to mechanical load, it is intended to develop one kind and wax be reduced or avoided Use, another appropriate addition is with the good copolymer for meeting MJPZ, and using the solution for the water-soluble composition for possessing high viscosity Certainly scheme, to develop such easy to clean, to meet MJPZ good and possess the hair jelly product of satisfactorily moulding effect, and passes through The component of changing section hair jelly, helps to lift the glossiness after hair jelly product plastotype.

In most of commercial Applications, such as food industry, chemical engineering industry, xanthans as rheology modifier, by with When copolymer segment is combined, the effect of tool lifting viscosity can be produced, its viscosity is about 600-1400cp, and with making us Satisfied water soluble characteristic, applicant undressed xanthans is made an addition to such as vinylacetate and crotonic acid copolymer, Copolymer, sour copolymer, polyurethane, the N- with other monomers of acrylic or methacrylic of methyl vinyl ether and maleic anhydride When in the copolymers such as vinyl pyrrolidone, silicon based polymers, the fixed effect of the composition of formation be not enough to it is satisfactory, only It is suitable for the sizing of bob moulding, it has certain resistance to mechanical loading but sizing is not lasting enough, by adding a small amount of wax Composition can extend its fixed effect, but prolonged place easily is layered each component of product, for product sale more not Profit.

Applicant, it was unexpectedly observed that being held using ironware under conditions of more high temperature, is added with R＆D process The semi-finished product of xanthans and natural plant gum, component separation time has extended relatively, but its chance MJPZ is still to be improved.

On this basis, applicant from the method using heat treatment, metal-modified xanthans, addition natural plant gum by being entered Row is developed, and develops the gratifying product of several fixed effects in the process, and on this basis, is removed and contained in hair jelly Some lubricant components, make reduction product turbidity to 20NTU or so, have the more natural vision print of low and deep and effect after plastotype As.

The component of the composition of the hair styling gel of the present invention is as follows：

A kind of plastotype hair jelly of dumb light texture, it is characterised in that calculate by weight, include following material：Emulsifying agent 1-3 Part, 0.2-1 parts of stabilizer, 3-12 parts of film forming agent, 15-20 parts of conditioner, 5-15 parts of NMF；

Described emulsifying agent includes stearic acid ether -2, stearic acid ether -21, glycerin monostearate, methyl glucose ether distearyl Mixture more than one or both of acid esters or lauryl sodium sulfate；

Described stabilizer is carbomer；

Described film forming agent includes acrylic acid esters co-polymer and polyvinylpyrrolidone/acetate ethylene copolymer or vinylpyridine Pyrrolidone/acetate ethylene copolymer；

Described conditioner is the xanthans, dimethyl silicone polymer, OK a karaoke club that are mixed with metal ion for accounting for conditioner 5%-30% Glue, cationic cellulose；

Or account for the conditioner 3%-25% xanthans for being mixed with metal ion, and dimethyl silicone polymer, fenugreek gum, locust bean Glue；

Described NMF includes mixture more than hexylene glycol, polyethylene glycol, one or both of glycerine or sorbierite.

In order to lift the plastotype power of this product, and hair style is in dumb light after plastotype, and more natural state, can be using pressing below The material of parts by weight, is matched：1-3 parts of emulsifying agent, 0.2-1 parts of stabilizer, 5-15 parts of film forming agent, 15-20 parts of conditioner, 5-15 parts of NMF；

Described stabilizer is Acritamer 940 or Carbopol 941；

Described film forming agent includes acrylic acid esters co-polymer or polyvinylpyrrolidone or vinyl pyrrolidone/vinyl acetate Copolymer or vinylacetate/butenoic acid/vinyl neodecanoic acid ester terpolymer or diethylene glycol (DEG)/cyclohexanedimethanol/isophthalic Two acid esters/sulphur isophthalate copolymer；

Described conditioner be account for conditioner 5%-30% be mixed with ferric ion and selected from least one of magnesium, calcium divalence Xanthans, dimethyl silicone polymer, carragheen, the cationic cellulose of ion；

Or account for the bivalent ions xanthans of at least one of conditioner 3%-25% magnesium, calcium, and dimethyl silicone polymer, perfume (or spice) Bean gum, locust bean gum；

Preferably, described film forming agent is acrylate/octylacrylamido or acrylate or polyethylene Pyrrolidones or vinyl pyrrolidone/acetate ethylene copolymer or vinylacetate/butenoic acid/vinyl neodecanoic acid ester ternary Copolymer or diethylene glycol (DEG)/cyclohexanedimethanol/isophthalate/sulphur isophthalate copolymer.

Preferably, described conditioner be account for 15-20 parts of % of conditioner be mixed with ferric ion and selected from magnesium, calcium At least one of bivalent ions xanthans, 10%-20% carragheens, 5%-15% cationic celluloses and it is remaining be poly- diformazan Radical siloxane is constituted；

Or account for the bivalent ions xanthans of at least one of conditioner 3%-25% magnesium, calcium, 10%-20% fenugreek gums, 8%-16% Locust bean gum, and it is remaining for dimethyl silicone polymer composition；

As a further improvement, also comprising plant additive, camomile extract, accumulated snow may be selected in described plant additive Any one in careless extract, black bearberry glucoside extract.

As a further improvement, also comprising odorant, it is fragrant that bouquet type composition, Fruity type may be selected in described odorant The composition of any one or more in essence, Costus essence.

This product for being not added with plant extracts, odorant, its manufacture can be made using following methods：

（1）By weight by raw material preparation, the material in addition to stabilizer is mixed with 100 ~ 150 parts of deionized waters, heated To 50 ~ 75 DEG C, 20-45min is kept, hair jelly semi-finished product are obtained；

（2）The hair jelly semi-finished product after finishing will be heated in agitated kettle, in being stirred at 50-60 DEG C with 300-500r/min speed 3-5min；

（3）Be cooled to 40-45 DEG C it is follow-up it is continuous be kept stirring for, add after stabilizer and continue to stir until hair jelly cooling, obtains described Hair styling gel.

For this product of addition plant extracts, odorant, its manufacture can be made using following methods：

（3）Be cooled to 40-45 DEG C it is follow-up it is continuous be kept stirring for, add after stabilizer and continue to stir until hair jelly is cooled to 35-40 DEG C；

（4）Add remaining material and continue to be kept stirring for, after making each component uniform, obtain described plastotype hair jelly.

The present invention at least has following usefulness：

（1）By the way that addition is mixed with the xanthans of metal ion in right amount in hair jelly, instead of the waxy substance in pomade, it is water-soluble So that possess easy to clean in cleaning process, and and hair jelly in film forming material there is good combination effect, pass through addition Mentioned emulsifier, good emulsifying effectiveness is can reach under relatively low mixing speed, with the longer holding time, and hair jelly Middle material has good homogeneity；

（2）Good for most of MJPZs of meeting, with certain sticky polymer as hair style plastotype agent, its viscosity is about For 4000-5000cp, it is difficult to meet under sizing and the higher medium-length hair moulding of torsion resistance, and slight mechanical load for a long time Easily produce and lose hair style fixed, its viscosity effect can be lifted for the xanthans for adding appropriate, but comparatively do not possess Preferable homogeneity, needs uniform mixing before use；But the xanthans of metal ion is being mixed with by addition, and is being carried out necessarily After heat treatment, its viscosity can reach 6500-7000cp, and the hair style for most of medium-length hairs is moulded with good plastotype effect Really, and resistance to mechanical load has good application effect, the duration is satisfactory；Especially to add at least one in magnesium, calcium Plant after bivalent ions xanthans, its viscosity can further improve 8000-8500cp, for the hair style of medium-length hair or even long hair Mould with the hair style stable retention time at least over 6 hours, and the resistance to mechanical deformability under low blast has order The effect of people's satisfaction.

（3）By using with the relatively low natural plant gum of permeability, it is to avoid the use of grease, control the turbidity of reduction this product In 20NTU with left and right, moulding is in have low and deep and natural moulding after sizing, and avoids the addition of many greases of sauce from making scalp because of oil Fat and produce tacky sense of discomfort.

Embodiment

In order that the objects, technical solutions and advantages of the present invention are more easily understood, with reference to embodiments, to the present invention It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to Limit the present invention.

Embodiment 1

A kind of plastotype hair jelly of dumb light texture, calculates, includes following material by weight：

- 24 parts of stearic acid ether, -21 4 parts of stearic acid ether, 3.5 parts of glycerin monostearate；

2.5 parts of Acritamer 940；

20 parts of 40 parts of acrylic acid esters co-polymer and polyvinylpyrrolidone；

It is mixed with 45 parts of 95.5 parts of 14.5 parts of xanthans, dimethyl silicone polymer, carragheen, the cationic cellulose of metal ion 35 parts；

Described NMF is 40 parts of hexylene glycol, 10 parts of glycerine.

The processing of hair jelly is carried out using following step：

（1）By above-mentioned raw materials by weight by raw material preparation, the material in addition to stabilizer is mixed with 1200 parts of deionized waters Close, be heated to 50 ~ 65 DEG C, keep 20-30min, obtain hair jelly semi-finished product；

This product is advantageous in that, with certain glossiness, finished product turbidity is 18-20NTU, is suitable for brightness relatively low Color development such as black, the use of brown hair quality；Sticky sense for skin of head stimulates small, is easy to moulding for moulding, and cleaning side Just, it is adaptable to which the moulding of bob or even medium-length hair is moulded.

Embodiment 2

- 21 4 parts of stearic acid ether, 3.5 parts of glycerin monostearate, 4 parts of methyl glucose ether distearate, dodecyl sulphur Sour 5 parts of sodium

910 1 parts of carbomer, 2 parts of Acritamer 940；

20 parts of acrylic acid esters co-polymer, 20 parts of vinyl pyrrolidone/acetate ethylene copolymer, vinylacetate/butenoic acid/ 25 parts of vinyl neodecanoic acid ester terpolymer；

It is mixed with 45 parts of 95.5 parts of 14.5 parts of xanthans, dimethyl silicone polymer, carragheen, the cationic fiber of divalence magnesium ion 35 parts of element；

Described NMF is 40 parts of hexylene glycol, 15 parts of polyethylene glycol.

The processing of hair jelly is carried out using following step：

（1）By above-mentioned raw materials by weight by raw material preparation, the material in addition to stabilizer is mixed with 1300 parts of deionized waters Close, be heated to 50 ~ 60 DEG C, keep 20-25min, obtain hair jelly semi-finished product；

（2）The hair jelly semi-finished product after finishing will be heated in agitated kettle, in being stirred at 50-60 DEG C with 400-500r/min speed 3-5min；

（3）Be cooled to 40-43 DEG C it is follow-up it is continuous be kept stirring for, add after stabilizer and continue to stir until hair jelly cooling, obtains described Hair styling gel.

This product is advantageous in that dumb light moulding and with low reflective texture, and finished product turbidity is 20-23NTU, is sent out after sizing The more natural eye impressions of matter, are suitable for the use of multiple color hair quality, and the sticky sense of skin of head stimulates smaller, is easy to Moulding for moulding, it is easy to clean, it is adaptable to which that the moulding of bob or even medium-length hair is moulded.

Embodiment 3

6.5 parts of jojoba oil, 4.5 parts of caprylic/capric triglyceride, 3 parts of isopropyl myristate, hydroxy stearic acid octyl group 12 5 parts of Arrcostab；

- 28 parts of stearic acid ether, 5 parts of glycerin monostearate, 4 parts of methyl glucose ether distearate, lauryl sodium sulfate 1 part；

1.5- parts of carbomer 910,2 parts of Acritamer 940；

40 parts of acrylic acid esters co-polymer, polyvinylpyrrolidone or 18 parts of vinyl pyrrolidone/acetate ethylene copolymer, two Glycol/cyclohexanedimethanol/isophthalate/38 parts of sulphur isophthalate copolymer；

It is mixed with 38 parts of the xanthans of divalence magnesium ion, 115 parts of dimethyl silicone polymer, 42 parts of fenugreek gum, 8 parts of locust bean gum；

20 parts of hexylene glycol, 15 parts of polyethylene glycol, 15 parts of sorbierite；

10 parts of camomile extract, 5 parts of Costus essence.

（1）By weight by raw material preparation, the material in addition to stabilizer is mixed with 1350 parts of deionized waters, heated To 50 ~ 75 DEG C, 30-45min is kept, hair jelly semi-finished product are obtained；

（3）Be cooled to 40-45 DEG C it is follow-up it is continuous be kept stirring for, add after carbomer 910, Acritamer 940 and continue to stir until hair jelly It is cooled to 35-40 DEG C；

（4）Add camomile extract, Costus essence and continue to be kept stirring for, after making each component uniform, obtain described modeling Type hair jelly.

Relative to the product of embodiment 2, this product is advantageous in that with certain quiet and beautiful fragrance, and being relatively adapted to man makes With there is low and deep natural style and reflectance is relatively low, hair quality does not have sticky eye impressions, finished product turbidity on plastotype after-vision For 21-23.5NTU, it is suitable for the use of the high-luminance colour hair quality such as gold, red, and more naturally, being glued to skin of head Soapy feeling stimulates smaller, is easy to moulding for moulding, easy to clean, it is adaptable to which that the moulding of bob or even medium-length hair is moulded.

Embodiment 4

6 parts of isopropyl myristate, 10 parts of hydroxy stearic acid octyldodecyl, 11 parts of isopropyl palmitate；

7-9 parts of stearic acid ether -2,1.5-4 parts of glycerin monostearate, 1-3 parts of methyl glucose ether distearate, dodecane 2-6 parts of base sodium sulphate

1.5-2.5 parts of carbomer 910,1-2 parts of Acritamer 940；

35 parts of acrylate/octylacrylamido, polyvinylpyrrolidone or vinyl pyrrolidone/vinyl acetate are common 22 parts of polymers, diethylene glycol (DEG)/cyclohexanedimethanol/isophthalate/55 parts of sulphur isophthalate copolymer；

Be mixed with 32 parts of the xanthans of ferric ion and divalent calcium ions, 117 parts of dimethyl silicone polymer, 43 parts of fenugreek gum, 15 parts of locust bean gum；

8.5 parts of black bearberry glucoside extract, 4 parts of Gotu Kola P.E, 4.5 parts of bouquet type composition, 5 parts of Fruity type essence.

（4）Add black bearberry glucoside extract extract, Gotu Kola P.E, bouquet type composition, Fruity type essence and continue holding and stir Mix, after making each component uniform, obtain described plastotype hair jelly.

Relative to the product of embodiment 2, this product is advantageous in that with certain flowers and fruits fragrance, and being relatively adapted to Ms makes With there is low and deep natural style and reflectance is relatively low, hair quality does not have sticky eye impressions, finished product turbidity on plastotype after-vision For 20-21.5NTU, it is suitable for multiple color, the use of brightness hair quality, and more naturally, the sticky sense to skin of head is stimulated Smaller and fixed effect is good, this product resistance to mechanical load force is high, and sizing intensity is suitable for the breakthrough moulding of medium-length hair or even long hair Customization.

Because various changes, meaning can be carried out in the case where not departing from the scope of the invention and essence to above-mentioned theme Figure be include in foregoing description or appended claims defined in all themes be construed to the description of this invention and say It is bright.Many modifications and variations can be carried out to the present invention according to above-mentioned teaching.

Claims

1. a kind of plastotype hair jelly of dumb light texture, it is characterised in that calculate by weight, include following material：Emulsifying agent 1-3 Part, 0.2-1 parts of stabilizer, 3-12 parts of film forming agent, 15-20 parts of conditioner, 5-15 parts of NMF；

Described emulsifying agent includes methyl glucoside polyethenoxy ether distearate, potassium cetyl phosphate, diethanol amine ten One kind in six alkyl phosphates, glycerin monostearate, sorbitan laurate esters or lauryl sodium sulfate or two Plant the mixture of the above；

Described stabilizer is carbomer；

2. a kind of plastotype hair jelly of dumb light texture as claimed in claim 1, it is characterised in that calculate by weight, comprising Following material：1-3 parts of emulsifying agent, 0.2-1 parts of stabilizer, 5-15 parts of film forming agent, 15-20 parts of conditioner, 5-15 parts of NMF；

Described stabilizer is Acritamer 940 or Carbopol 941；

3. a kind of plastotype hair jelly of dumb light texture as claimed in claim 2, it is characterised in that described film forming agent is acrylic acid Ester/octylacrylamido or acrylate or polyvinylpyrrolidone or vinyl pyrrolidone/vinyl acetate copolymerization Thing or vinylacetate/butenoic acid/vinyl neodecanoic acid ester terpolymer or diethylene glycol (DEG)/cyclohexanedimethanol/isophthalic acid Ester/sulphur isophthalate copolymer.

4. a kind of plastotype hair jelly of dumb light texture as claimed in claim 2, it is characterised in that described conditioner is to account for conditioning 15-20 parts of %'s of agent is mixed with ferric ion and selected from the bivalent ions xanthans of at least one of magnesium, calcium, 10%-20% cards It is dimethyl silicone polymer composition to draw glue, 5%-15% cationic celluloses and remainder；

Or account for the bivalent ions xanthans of at least one of conditioner 3%-25% magnesium, calcium, 10%-20% fenugreek gums, 8%-16% Locust bean gum, and it is remaining for dimethyl silicone polymer composition.

5. a kind of plastotype hair jelly of dumb light texture as claimed in claim 1 or 2, it is characterised in that also comprising plant additive, Any one in camomile extract, Gotu Kola P.E, black bearberry glucoside extract may be selected in described plant additive.

6. a kind of plastotype hair jelly of dumb light texture as claimed in claim 3, it is characterised in that described also comprising odorant The composition of any one or more in bouquet type composition, Fruity type essence, Costus essence may be selected in odorant.

7. a kind of preparation method of the plastotype hair jelly of dumb light texture as described in claim 1-4 any one, its feature exists In：

By weight by raw material preparation, the material in addition to stabilizer is mixed with 100 ~ 150 parts of deionized waters, 50 are heated to ~ 75 DEG C, 20-45min is kept, hair jelly semi-finished product are obtained；

The hair jelly semi-finished product after finishing will be heated in agitated kettle, in stirring 3- at 50-60 DEG C with 300-500r/min speed 5min；

Be cooled to 40-45 DEG C it is follow-up it is continuous be kept stirring for, add after stabilizer and continue to stir until hair jelly cooling, obtain described determining Type hair jelly.

8. a kind of preparation method of the plastotype hair jelly of dumb light texture as described in claim 5 or 6, it is characterised in that：