CN106966704A - One kind synthesis ruby preparation method of dove blood - Google Patents

One kind synthesis ruby preparation method of dove blood Download PDF

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Publication number
CN106966704A
CN106966704A CN201710112045.1A CN201710112045A CN106966704A CN 106966704 A CN106966704 A CN 106966704A CN 201710112045 A CN201710112045 A CN 201710112045A CN 106966704 A CN106966704 A CN 106966704A
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China
Prior art keywords
dove
blood
ruby
synthesis
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710112045.1A
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Chinese (zh)
Inventor
董志东
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Wuzhou Donglin Gem Machinery Co Ltd
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Wuzhou Donglin Gem Machinery Co Ltd
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Publication date
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Priority to CN201710112045.1A priority Critical patent/CN106966704A/en
Publication of CN106966704A publication Critical patent/CN106966704A/en
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64—Burning or sintering processes
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231—Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3241—Chromium oxides, chromates, or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3284—Zinc oxides, zincates, cadmium oxides, cadmiates, mercury oxides, mercurates or oxide forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/658—Atmosphere during thermal treatment
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/66—Specific sintering techniques, e.g. centrifugal sintering
    • C04B2235/666—Applying a current during sintering, e.g. plasma sintering [SPS], electrical resistance heating or pulse electric current sintering [PECS]
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
    • C04B2235/9646—Optical properties
    • C04B2235/9661—Colour

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Materials For Medical Uses (AREA)
  • Adornments (AREA)

Abstract

It is specially with 0.4 by chromium oxide, cadmium oxide, alundum (Al2O3) the invention belongs to artificial gem field, more particularly to a kind of synthesis ruby preparation method of dove blood：0.02:99.58 part by weight is mixed, and is put into after pressed compact in arc discharge device, is synthesized under the protection of inert gas with 85 ± 2A electric current, obtains the blood red jewel of dove, and the blood red color of gemstones of synthesis dove that it is obtained is scarlet, uniform color.

Description

One kind synthesis ruby preparation method of dove blood
Technical field
The invention belongs to artificial gem field, more particularly to a kind of synthesis ruby preparation method of dove blood.
Background technology
Burma produces transparent ruby for cerise, rose, bright-coloured, soft and bright.Jewel is transparent but unlimpid, With 10 times of amplification sem observations, it is seen that some white tiffany shape inclusion enclaves and reflective fissure-plane, Main Basiss color and parcel Body is recognized：Color：It is in cerise (dove blood red), rose, color is rich and gaudy bright but uneven more.If by ruby Put into the white porcelain dish equipped with clear water, it is seen that uneven red patch or band.With fluorescence, the color under strong light More become clear bright-coloured.
Existing artificial synthesized ruby is synthesized using alundum (Al2O3) and chromium oxide, is also unable to reach above-mentioned effect Really.
The content of the invention
Prepare it is an object of the invention to provide a kind of brand-new color is scarlet, synthesis dove blood of uniform color is ruby Method.
In order to realize above-mentioned technique effect, the technical scheme that the present invention is provided is such：One kind synthesis blood red jewel of dove Preparation method, by chromium oxide, cadmium oxide, alundum (Al2O3) with 0.4：0.02:99.58 part by weight is mixed, pressed compact After be put into arc discharge device, synthesized under the protection of inert gas with 85 ± 2A electric current, obtain the blood red treasured of dove Stone.
In the above-mentioned ruby preparation method of synthesis dove blood, the time of described electric discharge is 1.5-2min.
In the above-mentioned ruby preparation method of synthesis dove blood, grain diameter size is 12-13m after pressed compact.
The present invention has the advantage that compared with conventional method：
There is uniform sanguine color by the obtained ruby of method synthesis of the present invention, surface bubble-free and split Trace.
Specific embodiment
Claims of the present invention is described further with reference to embodiment, but not constituted to the present invention Any limitation, it is any with the technical scheme is that made by basis limited number of time modification still fall within the present invention to be protected The content of shield.
Embodiment 1
One kind synthesis ruby preparation method of dove blood, by chromium oxide, cadmium oxide, alundum (Al2O3) with 0.4：0.02: 95.8 part by weight is mixed, and is put into after pressed compact in arc discharge device, with 85 ± 2A under the protection of inert gas Electric current carry out electric discharge synthesis, the particle after pressed compact is placed between positive and negative electrode, and discharge time is 1.5min, pressed compact particle diameter About 12mm, obtains the blood red jewel of dove.
In the above-mentioned ruby preparation method of synthesis dove blood, the time of described electric discharge is 1.5-2min.
In the above-mentioned ruby preparation method of synthesis dove blood, grain diameter size is 12-13mm after pressed compact.
Embodiment 2
One kind synthesis ruby preparation method of dove blood, by chromium oxide, cadmium oxide, alundum (Al2O3) with 0.4：0.02: 99.58 part by weight is mixed, and is put into after pressed compact in arc discharge device, with 85 ± 2A under the protection of inert gas Electric current carry out electric discharge synthesis, the particle after pressed compact is placed between positive and negative electrode, and discharge time is 2min, and pressed compact particle diameter is about For 13mm, the blood red jewel of dove is obtained.
Embodiment 3
One kind synthesis ruby preparation method of dove blood, by chromium oxide, cadmium oxide, alundum (Al2O3) with 0.4：0.02: 99.58 part by weight is mixed, and is put into after pressed compact in arc discharge device, with 85 ± 2A under the protection of inert gas Electric current carry out electric discharge synthesis, the particle after pressed compact is placed between positive and negative electrode, and discharge time is 1.8min, pressed compact particle diameter About 12.5mm, obtains the blood red jewel of dove.
Above-described is only presently preferred embodiments of the present invention, all timess made in the range of the spirit and principles in the present invention What modifications, equivalent substitutions and improvements etc., should be included in the scope of the protection.

Claims (3)

1. one kind synthesis the ruby preparation method of dove blood, it is characterised in that by chromium oxide, cadmium oxide, alundum (Al2O3) with 0.4：0.02:99.58 part by weight is mixed, and is put into after pressed compact in arc discharge device, in the protection of inert gas Under synthesized with 85 ± 2A electric current, obtain the blood red jewel of dove.
2. the synthesis ruby preparation method of dove blood according to claim 1, it is characterised in that the time of described electric discharge For 1.5-2min.
3. the synthesis ruby preparation method of dove blood according to claim 1, it is characterised in that grain diameter is big after pressed compact Small is 12-13mm.
CN201710112045.1A 2017-02-28 2017-02-28 One kind synthesis ruby preparation method of dove blood Pending CN106966704A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710112045.1A CN106966704A (en) 2017-02-28 2017-02-28 One kind synthesis ruby preparation method of dove blood

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710112045.1A CN106966704A (en) 2017-02-28 2017-02-28 One kind synthesis ruby preparation method of dove blood

Publications (1)

Publication Number Publication Date
CN106966704A true CN106966704A (en) 2017-07-21

Family

ID=59329125

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710112045.1A Pending CN106966704A (en) 2017-02-28 2017-02-28 One kind synthesis ruby preparation method of dove blood

Country Status (1)

Country Link
CN (1) CN106966704A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06313186A (en) * 1993-04-30 1994-11-08 Yamakita Sangyo Kk Solid lubricant and sliding apparatus
CN1890408A (en) * 2003-12-01 2007-01-03 大日本印刷株式会社 Artificial corundum crystal
CN101306942A (en) * 2008-06-27 2008-11-19 王昕� Fine-crystal high transparency ruby ceramic materials and low-temperature preparation thereof
CN105239161A (en) * 2015-10-19 2016-01-13 中国科学院青海盐湖研究所 Preparing method for ruby crystals

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06313186A (en) * 1993-04-30 1994-11-08 Yamakita Sangyo Kk Solid lubricant and sliding apparatus
CN1890408A (en) * 2003-12-01 2007-01-03 大日本印刷株式会社 Artificial corundum crystal
CN101306942A (en) * 2008-06-27 2008-11-19 王昕� Fine-crystal high transparency ruby ceramic materials and low-temperature preparation thereof
CN105239161A (en) * 2015-10-19 2016-01-13 中国科学院青海盐湖研究所 Preparing method for ruby crystals

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Application publication date: 20170721