CN106957968B - A kind of reductive jar for smelting magnesium metal - Google Patents

A kind of reductive jar for smelting magnesium metal Download PDF

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Publication number
CN106957968B
CN106957968B CN201710387211.9A CN201710387211A CN106957968B CN 106957968 B CN106957968 B CN 106957968B CN 201710387211 A CN201710387211 A CN 201710387211A CN 106957968 B CN106957968 B CN 106957968B
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China
Prior art keywords
reduction
gallbladder
reductive jar
tank
magnesium metal
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CN201710387211.9A
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CN106957968A (en
Inventor
杨沛胥
张少军
车玉思
张伟东
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Zhengzhou University
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Zhengzhou University
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/20Obtaining alkaline earth metals or magnesium
    • C22B26/22Obtaining magnesium
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B14/00Crucible or pot furnaces
    • F27B14/04Crucible or pot furnaces adapted for treating the charge in vacuum or special atmosphere
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B14/00Crucible or pot furnaces
    • F27B14/08Details peculiar to crucible or pot furnaces
    • F27B14/0806Charging or discharging devices

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

The present invention relates to a kind of metal smelting device, specifically a kind of reductive jar for smelting magnesium metal, including reduction tank body, the reduction tank body are hollow tubular structure, the reduction tank base is in frustum-like shape, and restores tank base and be provided with slag notch;Heat-conducting plate is fixedly installed in the reduction inner tank wall, the reduction tank interior central part is movably set with the reduction gallbladder of tubular, the diameter of the reduction gallbladder is greater than the diameter of reduction tank base slag notch, the reductive jar of smelting magnesium metal of the invention, unique structure, enormously simplify charging, the operation slagged tap, the high temperature open time of reductive jar is shortened simultaneously, it avoids high-temperature oxydation and shortens the working life, the time of reduction reaction is also substantially reduced simultaneously, improve production efficiency, the heat-conducting plate of longitudinal measure in reductive jar body, increase the intensity for restoring tank body, service life is obviously prolonged.

Description

A kind of reductive jar for smelting magnesium metal
Technical field
The present invention relates to a kind of metal smelting device, specifically a kind of reductive jar for smelting magnesium metal.
Background technique
Reductive jar is the capital equipment of magnesium Metal Production, and mean level is mounted in reduction furnace, referred to as horizontal tank.Horizontal tank exists Charge is few, feed the deficiencies of inconvenient, service life is short of slagging tap.In order to overcome horizontal tank disadvantages mentioned above, charge is big, can be automatic Charging is slagged tap, the longer Vertical type reduction tank of service life is come into being, i.e., reductive jar is vertically installed in reduction furnace, referred to as perpendicular Tank.A kind of entitled metal smelting Vertical type reduction tank of such as Patent No. 200510074923.2 and assembly of reduction furnace, For another example the entitled a kind of reductive jar of metal smelting of Patent No. 200910254122.2 of the present inventor's invention, with horizontal tank It compares, all has the characteristics that charging charge is big, service life is longer.But so far, existing magnesium metal smelt erects tank still In the presence of charging, tapping operation is complicated, the recovery time is longer and production cost is higher the deficiencies of, to Smelting magnesium enterprise bring it is many not Just.
Summary of the invention
Goal of the invention of the invention is to overcome defect present in background technique, thus realize it is a kind of charging, the side of slagging tap Just quick, the reaction time is obviously shortened, and tank intensity is big, the reductive jar with long service life for smelting magnesium metal.
For achieving the above object, the technical scheme is that it is a kind of smelt magnesium metal reductive jar, including reduction Tank body, the reduction tank body are hollow tubular structure, and the reduction tank base is in frustum-like shape, and restores tank base and be provided with Slag notch;Heat-conducting plate is fixedly installed in the reduction inner tank wall, the reduction tank interior central part is movably set with cylinder The diameter of the reduction gallbladder of shape, the reduction gallbladder is greater than the diameter of reduction tank base slag notch.
As the preferred technical solution of the present invention, vertical and circumference uniform distribution is solid on side wall in reductive jar body for the heat-conducting plate Fixed setting, can be such that raw material is uniformly heated unanimously.
As the preferred technical solution of the present invention, the quantity of the heat-conducting plate is 4 ~ 50, and the height of heat-conducting plate is 10mm~200mm。
As the preferred technical solution of the present invention, the cross-sectional shape of the reduction gallbladder is circle, and restores the internal diameter of gallbladder For 50mm ~ 400mm.
As the preferred technical solution of the present invention, restores and be provided with the recirculation hole that magnesium vapor passes through on the side wall of gallbladder, facilitate height The magnesium vapor that temperature generates can be separated more smoothly from raw material, and recirculation hole circumference uniform distribution on reduction gallbladder side wall is staggeredly set It sets, and recirculation hole is circular hole or strip-shaped hole.
The working principle of the reductive jar of smelting magnesium metal of the invention:
After restoring charging feedstock outside gallbladder in reductive jar body, with externally heated to reductive jar to 1200 DEG C left sides of reduction furnace The right side, magnesium quilt when being evacuated to absolute pressure 100Pa or less from top to reduction tank body with vacuum pump, in reductive jar body in raw material It restores, and the recirculation hole on reduction gallbladder is passed through with the state of steam and enters reduction gallbladder inner cylinder, eventually arrive at the top of reductive jar Low-temperature space crystallize into solid-state magnesium;It after reduction reaction, uncaps and disposably mentions operation reduction gallbladder on the whole, will can quickly go back Former slag is discharged from slag notch.
The reductive jar of smelting magnesium metal of the invention the utility model has the advantages that
1. the reductive jar of smelting magnesium metal of the invention, unique structure restore and are fixedly installed heat-conducting plate in inner tank wall, Reduction gallbladder is the global facility that in tank and can move up and down, and overcomes the device being made of in the past multiple charging baskets, The operation for enormously simplifying charging, slagging tap, while the high temperature open time for shortening reductive jar, avoid high-temperature oxydation and shortening makes Use the service life.
2. the reductive jar of smelting magnesium metal of the invention, charge out magnesium, tank bottom of tank deck is slagged tap, and is arranged in reductive jar body Heat-conducting plate is accelerated the endothermic process of the intracorporal material of reductive jar, is shortened also along the radial equipartition of the reduction inner tank wall Original reaction time, improve production efficiency, at the same in reductive jar body longitudinal measure heat-conducting plate, make restore tank body intensity add Greatly, service life is obviously prolonged.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the reductive jar of smelting magnesium metal of the invention;
Fig. 2 is the A-A schematic cross-sectional view of Fig. 1.
In figure: 1- restores tank body, 2- slag notch, 3- heat-conducting plate, 4- reduction gallbladder, 5- recirculation hole, 6- raw material.
Specific embodiment
The reductive jar of smelting magnesium metal of the invention is done more in detail with reference to the accompanying drawing and by specific embodiment Thin description.
Embodiment 1:
The reductive jar of smelting magnesium metal of the invention, including reduction tank body 1, the reduction tank body 1 are hollow tubular structure, 1 bottom of reduction tank body is in frustum-like shape, and restores 1 bottom of tank body and be provided with slag notch 2;It is erected on 1 inner wall of reduction tank body Straight and circumference uniform distribution is fixedly installed heat-conducting plate 3, and the reduction 1 inside center portion of tank body is movably set with the reduction gallbladder 4 of tubular, The diameter of the reduction gallbladder 4 is greater than the diameter of reduction 1 bottom slag notch 2 of tank body.
The quantity of the heat-conducting plate 3 is 10, and the height of heat-conducting plate 3 is 50mm.
The cross-sectional shape of the reduction gallbladder 4 is circle, and the internal diameter for restoring gallbladder 4 is 200mm.
It is provided with the recirculation hole 5 that magnesium vapor passes through on the side wall of the reduction gallbladder 4, the magnesium vapor for facilitating high temperature to generate can be more It is smoothly separated from raw material, the recirculation hole 5 circumference uniform distribution on reduction 4 side wall of gallbladder is staggered, and recirculation hole 5 is circle Hole.
Embodiment 2:
Same as Example 1 repeats no more, the difference is that:
The recirculation hole 5 is strip-shaped hole.
The foregoing is merely the schematical specific embodiment of the present invention, the range being not intended to limit the invention is any The equivalent changes and modifications that those skilled in the art is made under the premise of not departing from present inventive concept and principle should all belong to In the scope of protection of the invention.

Claims (4)

1. a kind of reductive jar for smelting magnesium metal, including reduction tank body, the reduction tank body are hollow tubular structure, feature exists In: the reduction tank base is in frustum-like shape, and restores tank base and be provided with slag notch;It is fixed in the reduction inner tank wall It is provided with heat-conducting plate, vertical and circumference uniform distribution is fixedly installed the heat-conducting plate on side wall in reductive jar body, the reduction tank body Inside center portion is movably set with the reduction gallbladder of tubular, and the reduction gallbladder is the entirety portion that can be moved up and down in tank Part, the diameter of the reduction gallbladder are greater than the diameter of reduction tank base slag notch, are provided with magnesium vapor on the side wall of the reduction gallbladder By recirculation hole;
It after reduction reaction, uncaps and disposably mentions the operation reduction gallbladder on the whole, reducing slag is discharged from slag notch.
2. the reductive jar according to claim 1 for smelting magnesium metal, it is characterised in that: the quantity of the heat-conducting plate is 4 ~ 50 Item, and the height of heat-conducting plate is 10mm ~ 200mm.
3. the reductive jar according to claim 1 for smelting magnesium metal, it is characterised in that: the cross-sectional shape of the reduction gallbladder Internal diameter for circle, and reduction gallbladder is 50mm ~ 400mm.
4. the reductive jar according to claim 1 for smelting magnesium metal, it is characterised in that: the recirculation hole is in reduction gallbladder side wall Upper circumference uniform distribution is staggered, and recirculation hole is circular hole or strip-shaped hole.
CN201710387211.9A 2017-05-27 2017-05-27 A kind of reductive jar for smelting magnesium metal Active CN106957968B (en)

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Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114774716B (en) * 2022-06-06 2024-05-03 陕西秦龙电力股份有限公司 Pidgeon method magnesium metal reduction device

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101520276A (en) * 2009-03-20 2009-09-02 候冰洋 Vacuum smelting and reducing device capable of collecting metal magnesium
CN101706206A (en) * 2009-12-01 2010-05-12 开泰镁业有限公司 Metal smelting reduction pot
CN204421605U (en) * 2014-12-29 2015-06-24 徐东明 Magnesium metal erects heat storage formula reduction furnace inside and outside tank
CN104164563B (en) * 2014-06-27 2016-08-24 宁夏太阳镁业有限公司 A kind of metal reducing jar
CN206736328U (en) * 2017-05-27 2017-12-12 郑州大学 A kind of reductive jar for smelting magnesium metal

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101210282A (en) * 2006-12-28 2008-07-02 刘伟杰 Multifunctional reduction tank reinforcing equipment
CN101706204B (en) * 2009-09-11 2012-07-25 中南大学 External heat vertical retort magnesium smelting device
CN103740949B (en) * 2013-12-31 2015-02-04 深圳市华星光电技术有限公司 Device and method for pre-treating magnesium metal

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101520276A (en) * 2009-03-20 2009-09-02 候冰洋 Vacuum smelting and reducing device capable of collecting metal magnesium
CN101706206A (en) * 2009-12-01 2010-05-12 开泰镁业有限公司 Metal smelting reduction pot
CN104164563B (en) * 2014-06-27 2016-08-24 宁夏太阳镁业有限公司 A kind of metal reducing jar
CN204421605U (en) * 2014-12-29 2015-06-24 徐东明 Magnesium metal erects heat storage formula reduction furnace inside and outside tank
CN206736328U (en) * 2017-05-27 2017-12-12 郑州大学 A kind of reductive jar for smelting magnesium metal

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