CN106930112A - A kind of preparation method of environment-friendly polyester nonwoven Moisture absorption cloth - Google Patents

A kind of preparation method of environment-friendly polyester nonwoven Moisture absorption cloth Download PDF

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Publication number
CN106930112A
CN106930112A CN201710077934.9A CN201710077934A CN106930112A CN 106930112 A CN106930112 A CN 106930112A CN 201710077934 A CN201710077934 A CN 201710077934A CN 106930112 A CN106930112 A CN 106930112A
Authority
CN
China
Prior art keywords
moisture absorption
bath
water
preparation
terylene
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710077934.9A
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Chinese (zh)
Inventor
李淑芳
夏冬
刘文静
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Changzhou Vocational Institute of Textile and Garment
Original Assignee
Changzhou Vocational Institute of Textile and Garment
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Changzhou Vocational Institute of Textile and Garment filed Critical Changzhou Vocational Institute of Textile and Garment
Priority to CN201710077934.9A priority Critical patent/CN106930112A/en
Publication of CN106930112A publication Critical patent/CN106930112A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/643Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/507Polyesters
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16Synthetic fibres, other than mineral fibres
    • D06M2101/30Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32Polyesters

Abstract

The invention discloses a kind of preparation method of environment-friendly polyester nonwoven Moisture absorption cloth, including spun lacing terylene non-woven fabric through DP 92 impregnate the treatment of drying, find that bath raio is 1 when concentration is 5% 8% in dipping:The effect of moisture absorption is best when 20~30.The characteristics of for the difference of terylene non-woven fabric hygroscopicity present in prior art, this Moisture absorption cloth is arranged by terylene spunlace non-woven cloth through the hydrophilic finishing agent DP 92 of the feature of environmental protection, fabric after arrangement not only has soft, cost performance high, also with good hygroscopicity, have excellent antistatic properties the features such as.

Description

A kind of preparation method of environment-friendly polyester nonwoven Moisture absorption cloth
Technical field
The invention belongs to field of nonwoven fabric technology, more particularly to a kind of preparation method of environment-friendly polyester nonwoven Moisture absorption cloth.
Background technology
Moisture absorption cloth is a kind of disposable cleaning amenities, because it has cleaning, the basic function of moisturizing skin and just As cleaning supplies essential in people's life the features such as carrying.Moisture absorption cloth typically selects spunlace non-woven cloth, and raw material is normal From cotton, viscose glue and terylene.Although some natural materials such as string can be used, major part is still fine using terylene Dimension.Terylene is a kind of quite varied textile material of application, and the Moisture absorption cloth being made of it has the advantages that soft, cost performance is high; But its molecular structure is closely, crystallinity is higher, the surface low hygroscopicity for causing of energy is poor, antistatic behaviour is poor, it is difficult to meet it defend The need for raw field is applied, it is therefore necessary to it is modified, improves its hygroscopicity, health field is met as far as possible to fabric Demand.
The content of the invention
The purpose of the present invention is to solve the shortcomings of the prior art, there is provided a kind of simple and environmentally-friendly terylene Moisture absorption cloth, it is this The need for Moisture absorption cloth can meet health field application.Technical scheme is after being processed terylene spun laced fabric with hydrophilic finishing agent Obtain, comprise the following steps that:
1) hydrophilic finishing agent DP-92 is prepared:To contain parent in dimethyl terephthalate (DMT), ethylene glycol, polyethylene glycol and molecule The organosilicone copolymer of water base group is obtained for raw material through ester exchange, polycondensation reaction;
2) water-bath is carried out being warming up to 80 DEG C, the solution that will be prepared heats taking-up after 30min in being placed on water-bath;
3) thermostat water bath is down to 50 DEG C;
4) terylene spun laced fabric is put into water-bath and impregnates 30min;
5) terylene spun laced fabric is taken out, extrudes moisture through milling train;Drying box is modulated 105 DEG C, 5min is dried.
Find that bath raio is 1 when concentration is in 5%-8% in dipping:The effect of moisture absorption is best when 20~30.Organosilicon Condensate:Containing elemental silicon and with the linear polysiloxane of reactivity in molecular structure, after this polymer, can fiber Surface covers the film of a strata siloxanes, so as to obtain satisfied hydrophily, and make fabric have certain washability and Flexibility.
Ester exchange:Ester and alcohol/acid/ester (different esters) generated under acid or the catalysis of alkali a new ester and new alcohol/ The reaction of acid/ester.
Polycondensation reaction:It is the monomer with two or more functional groups, react to each other generation macromolecular compound, together When have simple molecules (such as H2O, HX, alcohol etc.) chemical reaction.
Beneficial effect
(1) because the Moisture absorption cloth is arranged by special organosilicone copolymer finishing agent, resulting fabric have compared with Good flexibility;Permeability is good simultaneously.
(2) Moisture absorption cloth has excellent hygroscopicity, and its hygroscopicity substantially exceeds pure cotton fabric, can be reduced in certain limit The usage amount of cotton fiber, effectively reduces cost.
(3) the Moisture absorption cloth feature of environmental protection is good, can meet demand of the health field to fabric.
Specific embodiment
Technical scheme in implementing to the present invention below carries out clearly complete description, it is clear that the embodiment in described is only It is a part of embodiment in the present invention, and technical scheme implements not limited to this.
1st, it is 0.004g/cm to prepare 3 pieces of grammes per square metres2, quality (is referred to as sample 1, sample for 1g terylene spunlace non-woven cloth 2, sample 3).
2nd, hydrophilic finishing agent DP-92 is prepared:With dimethyl terephthalate (DMT), ethylene glycol, polyethylene glycol and special organosilicon Condensate etc. is obtained for raw material through ester exchange, polycondensation reaction.
3rd, solution is prepared:DP-92 of the compound concentration in the range of 5%-8%.
4th, water-bath is carried out being warming up to 80 DEG C, the solution that will be prepared heats taking-up after 30min in being placed on water-bath.
5th, thermostat water bath is down to 50 DEG C.
6th, take solution in the 3 of 0.1g respectively is configured to bath raio 1:Solution in the range of 20~30 is put into beaker 1, beaker 2, in beaker 3, and it is put into heating in 50 DEG C of water-bath.
7th, by the sample 1 in step 1, sample 2, sample 3 is put into beaker 1, and beaker 2 impregnates 30min in beaker 3.
8th, cloth is taken out, extrudes moisture through milling train.
9th, drying box is modulated 105 DEG C, dries 5min, obtain embodiment 1, embodiment 2, embodiment 3.
10th, water imbibition test:Under the pressure condition of 2kPa, the liquid of 100ml is toppled over to the fabric top of embodiment, surveyed Try it and fully absorb the required time (unit is the second), as a result as shown in table 1.
The water suction experimental result of table 1
As can be seen from the above tests, the water absorbing properties of Moisture absorption cloth prepared by the inventive method are much better than unprocessed mistake Terylene spunlace non-woven cloth.
Although the present invention is disclosed as above with preferred embodiment, it is not limited to the present invention, therefore of the invention What protection domain should be defined by claims is defined.

Claims (2)

1. a kind of preparation method of environment-friendly polyester nonwoven Moisture absorption cloth, it is characterised in that:Terylene spun laced fabric is entered with hydrophilic finishing agent Obtained after row treatment, comprised the following steps that:
1) hydrophilic finishing agent DP-92 is prepared:To contain hydrophilic group in dimethyl terephthalate (DMT), ethylene glycol, polyethylene glycol and molecule The organosilicone copolymer of group is obtained for raw material through ester exchange, polycondensation reaction;
2) water-bath is carried out being warming up to 80 DEG C, the solution that will be prepared heats taking-up after 30min in being placed on water-bath;
3) thermostat water bath is down to 50 DEG C;
4) terylene spun laced fabric is put into water-bath and impregnates 30min;
5) terylene spun laced fabric is taken out, extrudes moisture through milling train;Drying box is modulated 105 DEG C,
Dry 5min.
2. preparation method as claimed in claim 1, it is characterised in that:The compound concentration of hydrophilic finishing agent DP-92 is 5%- 8%.
CN201710077934.9A 2017-02-14 2017-02-14 A kind of preparation method of environment-friendly polyester nonwoven Moisture absorption cloth Pending CN106930112A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710077934.9A CN106930112A (en) 2017-02-14 2017-02-14 A kind of preparation method of environment-friendly polyester nonwoven Moisture absorption cloth

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710077934.9A CN106930112A (en) 2017-02-14 2017-02-14 A kind of preparation method of environment-friendly polyester nonwoven Moisture absorption cloth

Publications (1)

Publication Number Publication Date
CN106930112A true CN106930112A (en) 2017-07-07

Family

ID=59424110

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710077934.9A Pending CN106930112A (en) 2017-02-14 2017-02-14 A kind of preparation method of environment-friendly polyester nonwoven Moisture absorption cloth

Country Status (1)

Country Link
CN (1) CN106930112A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109440471A (en) * 2018-10-10 2019-03-08 谢荣国 A kind of moisture control agent and preparation method thereof applied to mop
CN109914121A (en) * 2017-12-12 2019-06-21 中山市卓益服饰有限公司 A kind of production method of the ventilative baby children's underwear of moisture absorption
CN113089179A (en) * 2021-04-07 2021-07-09 苏州优衣宝无纺布有限公司 Preparation process of hydrophilic antibacterial non-woven fabric

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
刘瑞云 等: "有机硅改性聚醋纤维亲水整理剂的合成及其应用", 《印染助剂》 *
杨安明 等: "有机硅改性亲水聚酯整理剂的合成及应用", 《印染助剂》 *
杨安明: "有机硅改性亲水聚酯整理剂的合成及性能研究", 《中国优秀硕士学位论文全文数据库 工程科技I辑》 *
陈金辉 等: "涤纶织物耐久柔软性多功能亲水整理剂DP-9993的制备及应用性能研究", 《第一届广东纺织助剂行业年会论文集》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109914121A (en) * 2017-12-12 2019-06-21 中山市卓益服饰有限公司 A kind of production method of the ventilative baby children's underwear of moisture absorption
CN109440471A (en) * 2018-10-10 2019-03-08 谢荣国 A kind of moisture control agent and preparation method thereof applied to mop
CN113089179A (en) * 2021-04-07 2021-07-09 苏州优衣宝无纺布有限公司 Preparation process of hydrophilic antibacterial non-woven fabric

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Application publication date: 20170707