CN106929132A - A kind of Oil for High Speed Aluminum Drawbench and preparation method thereof - Google Patents

A kind of Oil for High Speed Aluminum Drawbench and preparation method thereof Download PDF

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Publication number
CN106929132A
CN106929132A CN201710267861.XA CN201710267861A CN106929132A CN 106929132 A CN106929132 A CN 106929132A CN 201710267861 A CN201710267861 A CN 201710267861A CN 106929132 A CN106929132 A CN 106929132A
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CN
China
Prior art keywords
parts
oil
additive
high speed
drawbench
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710267861.XA
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Chinese (zh)
Inventor
郑金周
贾书伟
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Zhengzhou Optris Technology Co Ltd
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Zhengzhou Optris Technology Co Ltd
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Priority to CN201710267861.XA priority Critical patent/CN106929132A/en
Publication of CN106929132A publication Critical patent/CN106929132A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04Mixtures of base-materials and additives
    • C10M169/045Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution and non-macromolecular compounds
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2203/00Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/02Well-defined aliphatic compounds
    • C10M2203/022Well-defined aliphatic compounds saturated
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2203/00Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/10Petroleum or coal fractions, e.g. tars, solvents, bitumen
    • C10M2203/1006Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28Esters
    • C10M2207/2805Esters used as base material
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/22Heterocyclic nitrogen compounds
    • C10M2215/223Five-membered rings containing nitrogen and carbon only
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/046Overbasedsulfonic acid salts
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04Phosphate esters
    • C10M2223/041Triaryl phosphates
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04Phosphate esters
    • C10M2223/042Metal salts thereof
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/64Environmental friendly compositions
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/72Extended drain
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00Specified use or application for which the lubricating composition is intended
    • C10N2040/20Metal working
    • C10N2040/24Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

The invention discloses a kind of Oil for High Speed Aluminum Drawbench and preparation method thereof, wherein, Oil for High Speed Aluminum Drawbench includes each component of following mass fraction:80 95 parts of base oil, 10 22 parts of additive.The mass fraction of each component is in base oil:55 63 parts of Nanyang No. 100,5 10 parts of 150BS, 5 10 parts of Esters oil, the mass fraction of each component is in additive:13 parts of tricresyl phosphate, 16 parts of BTA, double 14 parts of the octyl group basic zinc salts of phosphoric acid, 37 parts of low molecular polyisobutylene, 46 parts of oiliness improver, 20ppm anti-foaming agents.Its preparation method is:Base oil is placed in mediation kettle, two hours of constant temperature, are stirred at 60 DEG C to 70 DEG C, and additive is then sequentially added in proportion, stir one or two hour, be well mixed.The aluminum wire drawing oil security performance is high, and greasy property is splendid, and aluminium powder sinking speed is fast, and oil product consumption is few, and the drain period has been elongated significantly, and the aluminium wire shiny appearance for being drawn out is uniform, is produced without the imperial robe, meanwhile, workshop taste is small, improves working environment.

Description

A kind of Oil for High Speed Aluminum Drawbench and preparation method thereof
Technical field
The present invention relates to technical field of lubricating oil, and in particular to be a kind of Oil for High Speed Aluminum Drawbench and preparation method thereof.
Background technology
Aluminum wire drawing oil is a kind of metal working oil, also referred to as aluminium drawing oil, aluminium drawing oil, is the drawing for aluminium and its alloy A kind of auxiliary agent of technique, with the effect such as lubrication, cleaning, cooling, antirust.
At present, it is necessary to add base oil and additive in the production process of aluminum wire drawing oil.During use to be considered The problem of aluminium powder sinking speed, selected base oil viscosity is not very big, and additive typically selects antirust agent, antiwear additive to resist Oxygen agent, anti-foaming agent.But actual production is when using, there are problems that a lot.Such as smolder, catch fire, aluminium powder sinking speed is too slow, draw It is coarse that outward appearance occurs in aluminum steel after pulling out, and color becomes not enough light, there is drawing trace.In addition, aluminum wire drawing oil oxidation is too fast, oil product consumption Also fast, the drain period shortens.And, smell is than larger, not enough environmental protection in use.Therefore, drawn to solve aluminium in the prior art Silk oil production prepare in the presence of problem, the present invention base oil and additive have been done further it is selected with reasonably match somebody with somebody Than, there is provided a kind of Oil for High Speed Aluminum Drawbench and preparation method thereof.
The content of the invention
In the presence of solving the problems, such as that in the prior art prepared by aluminum wire drawing oil production, the invention provides a kind of high speed Aluminum wire drawing oil and preparation method thereof.
To achieve the above object, the technical solution used in the present invention is:A kind of Oil for High Speed Aluminum Drawbench, by base oil and adding Plus agent is constituted, each component content is respectively according to mass fraction:Base oil 80-95 parts, additive 10-22 parts;Described base Plinth oil is the 150BS by Nanyang 100, Esters oil mixing composition;Described additive is by tricresyl phosphate, the nitrogen of benzo three The double octyl group basic zinc salts of azoles, phosphoric acid, low molecular polyisobutylene, oiliness improver, anti-foaming agent and high base number petroleum sulfonate composition.
Further, the mass fraction of each component is in described base oil:No. 100 55-63 parts of Nanyang, 150BS 5-10 Part, Esters oil 5-10 parts.
Further, the mass fraction of each component is in described additive:Tricresyl phosphate 1-3 parts, the nitrogen of benzo three Azoles 1-6 parts, double 1-4 parts of the octyl group basic zinc salts of phosphoric acid, low molecular polyisobutylene 3-7 parts, oiliness improver 4-6 parts, 20ppm anti-foaming agents.
Further, the preparation method of described Oil for High Speed Aluminum Drawbench is as follows:
A. the base oil is placed in mediation kettle, two hours of constant temperature, stir at 60 DEG C to 70 DEG C;
B. the additive is sequentially added in proportion, one or two hour is stirred, and is well mixed.
Beneficial effects of the present invention
The present invention has done further selected to base oil and additive, by rational proportioning, there is provided one kind takes into account economy, Safety, the aluminum wire drawing oil and its production method of environmental protection:
1)Aluminum wire drawing oil poor safety performance in use is solved, the problem caught fire of smoldering;
2)The rapid subsidence of aluminium powder is effectively guaranteed, so as to the harmful effect for avoiding aluminium powder from causing product quality;
3)Oil product consumption is reduced, the drain period has been elongated significantly, improve the economic benefit of enterprise;
4)The aluminium wire shiny appearance for being drawn out is uniform, is produced without the imperial robe, high lubricating effect, and at the same time, workshop taste is small, changes It has been apt to working environment.
Specific embodiment
Technical scheme will be clearly and completely described by specific embodiment below, it is clear that retouched The embodiment stated is only a part of embodiment of the invention, rather than whole embodiments.
In order to improve the quality of existing aluminum wire drawing oil and the economic benefit of enterprise, the invention provides a kind of High-speed Aluminium wire drawing Oil and preparation method thereof.Wherein, Oil for High Speed Aluminum Drawbench is made up of base oil and additive, and each component content is figured according to mass parts Respectively:Base oil 80-95 parts, additive 10-22 parts.Wherein, described base oil is by Nanyang 100,150BS and ester Class oil is mixed;Described additive by tricresyl phosphate, BTA, the double octyl group basic zinc salts of phosphoric acid, low point Sub- polyisobutene, oiliness improver, anti-foaming agent and high base number petroleum sulfonate composition.
As one kind preferred embodiment, the mass fraction of each component is in described base oil:The 55- of Nanyang 100 63 parts, 150BS 5-10 parts, Esters oil 5-10 parts.
Further, the mass fraction of each component is in the additive:Tricresyl phosphate 1-3 parts, BTA 1-6 parts, double 4 parts of the octyl group basic zinc salt 1- of phosphoric acid, low molecular polyisobutylene 3-7 parts, oiliness improver 4-6 parts, 20ppm anti-foaming agents.
Preferably, Oil for High Speed Aluminum Drawbench provided by the present invention is prepared from as follows:
A. the base oil is placed in mediation kettle, two hours of constant temperature, stir at 60 DEG C to 70 DEG C;
B. the additive is sequentially added in proportion, one or two hour is stirred, and is well mixed.
The present invention is reasonably matched on the basis of selected base oil and additive to it, solves aluminium wire drawing Poor safety performance in oily use, smolders and catches fire, and aluminium powder settles too slow problem;Meanwhile, oil product consumption is reduced, elongate significantly Drain period, improve the economic benefit of enterprise;Also, the aluminium wire shiny appearance for being drawn out is uniform, is produced without the imperial robe, lubrication Excellent;Workshop taste is small, improves working environment.
Although the present invention is disclosed as above with preferred embodiment, they be not for limiting the present invention, it is any to be familiar with This those skilled in the art, the various change made without departing from the spirit and scope of the invention or retouching, all should still belong to the present invention Patent covering scope within.

Claims (4)

1. a kind of Oil for High Speed Aluminum Drawbench, is made up of base oil and additive, it is characterised in that each component content is according to mass fraction It is respectively:Base oil 80-95 parts, additive 10-22 parts;Described base oil is that, by Nanyang 100,150BS, Esters oil is mixed It is combined into;Described additive is different by tricresyl phosphate, BTA, the double octyl group basic zinc salts of phosphoric acid, low molecular weight polycaprolactone Butylene, oiliness improver, anti-foaming agent and high base number petroleum sulfonate composition.
2. a kind of Oil for High Speed Aluminum Drawbench according to claim 1, it is characterised in that the matter of each component in described base oil Measuring number is:No. 100 55-63 parts, 150BS 5-10 parts, Esters oil 5-10 parts of Nanyang.
3. a kind of Oil for High Speed Aluminum Drawbench according to claim 1, it is characterised in that the matter of each component in described additive Measuring number is:Tricresyl phosphate 1-3 parts, BTA 1-6 parts, double 1-4 parts of the octyl group basic zinc salts of phosphoric acid, low molecular weight polycaprolactone is different Butylene 3-7 parts, oiliness improver 4-6 parts, 20ppm anti-foaming agents.
4. a kind of preparation method of Oil for High Speed Aluminum Drawbench, it is characterised in that be prepared from by step in detail below:
A. the base oil is placed in mediation kettle, two hours of constant temperature, stir at 60 DEG C to 70 DEG C;
B. the additive is sequentially added in proportion, one or two hour is stirred, and is well mixed.
CN201710267861.XA 2017-04-22 2017-04-22 A kind of Oil for High Speed Aluminum Drawbench and preparation method thereof Pending CN106929132A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710267861.XA CN106929132A (en) 2017-04-22 2017-04-22 A kind of Oil for High Speed Aluminum Drawbench and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710267861.XA CN106929132A (en) 2017-04-22 2017-04-22 A kind of Oil for High Speed Aluminum Drawbench and preparation method thereof

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CN106929132A true CN106929132A (en) 2017-07-07

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111575095A (en) * 2020-05-27 2020-08-25 中国石油化工股份有限公司 Aluminum wire drawing oil composition, preparation method and application
CN114426903A (en) * 2021-10-14 2022-05-03 劲诺(厦门)润滑科技有限公司 Efficient environment-friendly wire drawing liquid and preparation method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103695128A (en) * 2013-12-18 2014-04-02 广西大学 Lubricant of small aluminum-drawing bucket box

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103695128A (en) * 2013-12-18 2014-04-02 广西大学 Lubricant of small aluminum-drawing bucket box

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111575095A (en) * 2020-05-27 2020-08-25 中国石油化工股份有限公司 Aluminum wire drawing oil composition, preparation method and application
CN114426903A (en) * 2021-10-14 2022-05-03 劲诺(厦门)润滑科技有限公司 Efficient environment-friendly wire drawing liquid and preparation method thereof

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RJ01 Rejection of invention patent application after publication

Application publication date: 20170707

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