CN106908377A - A kind of pre-etching experiment sample mount - Google Patents

A kind of pre-etching experiment sample mount Download PDF

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Publication number
CN106908377A
CN106908377A CN201710253543.8A CN201710253543A CN106908377A CN 106908377 A CN106908377 A CN 106908377A CN 201710253543 A CN201710253543 A CN 201710253543A CN 106908377 A CN106908377 A CN 106908377A
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China
Prior art keywords
support frame
sample
sheet coupon
base
bar
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CN201710253543.8A
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Chinese (zh)
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CN106908377B (en
Inventor
周松
马少华
回丽
王磊
许良
刘思奇
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Shenyang Aerospace University
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Shenyang Aerospace University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N17/00Investigating resistance of materials to the weather, to corrosion, or to light
    • G01N17/04Corrosion probes
    • G01N17/043Coupons
    • G01N17/046Means for supporting or introducing coupons

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  • Life Sciences & Earth Sciences (AREA)
  • Biodiversity & Conservation Biology (AREA)
  • Ecology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Environmental Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

A kind of pre-etching experiment sample mount, including base plate, base carrier, sheet coupon support frame and bar sample support frame;Base plate is provided with positioning roll adjustment jack, and base carrier bottom is provided with positioning roll adjustment inserted block, and the two inserting coordinates;Base carrier, sheet coupon support frame and bar sample support top of the trellis are equipped with sample support frame positioning jack, and sheet coupon support frame and bar sample support frame bottom are equipped with sample support frame positioning inserted block, and the two inserting coordinates;Sheet coupon support frame is provided with some sheet coupon draw-in grooves;Bar sample support frame is provided with some bar sample draw-in grooves;Two base carriers be arrangeding in parallel are inserted on base plate by respective positioning roll adjustment inserted block, and the spacing of two base carriers is adapted with specimen length;Sheet coupon support frame and bar sample support frame quantity are some, and some sheet coupon support frames and bar sample support frame are inserted into base carrier with single kind or mixed species multiple-level stack form.

Description

A kind of pre-etching experiment sample mount
Technical field
The invention belongs to pre-etching experimental technique field, more particularly to a kind of pre-etching experiment sample mount.
Background technology
Metal erosion refers to that metal surface and surrounding medium occur chemistry or electrochemical action and make what metal was damaged Phenomenon, metal erosion phenomenon endangers extremely serious throughout the every field of national economy.
In the actual military service of metal material, corrosion advance damage is relatively conventional, and structural metallic material is subject fatigue While Cyclic Load, also mutually produce and act on the corrosive medium in environment, most commonly seen is exactly metal material Corrosion advance damage after fatigue behaviour, and it is this corrosion advance damage after fatigue behaviour can not only consume substantial amounts of metal material Material, also significantly have impact on the service life during material military service while wasting metals resources, cause equipment premature failure, seriously When even trigger catastrophic accident and jeopardize personal safety.
During the military service of metal material, etching problem into one of influence fatigue of materials performance it is important because Element, therefore, assessment material corrosion advance damage after fatigue behaviour become Metal Material Fatigue performance test important content it One, and rationally the corrosion advance damage of simulation metal material then becomes particularly significant.Under normal conditions, material corrosion advance damage Fatigue property test is all that the sample that will be processed in advance first carries out accelerating pre-etching experiment, then carries out fatigue property test.And The corrosion advance damage degree of metal material depends not only on material in itself, additionally depend on the characteristic of corrosive medium, environmental condition and The relative property of its change, and accelerate the usual way of pre-etching experiment, it is that sample is sufficiently submerged in the corruption configured to laboratory In the corrosive medium at erosion solution or the scene of taking from, then the corrosiveness for carrying out certain hour.
In pre-etching experiment is accelerated, sample needs to be fully contacted with corrosive medium, and sample generally needs heap to stack Put, and traditional stacking modes of emplacement can cause sample interval too small, not simply fail to ensure that specimen surface is uniform with corrosive medium Contact, the test section for also resulting in sample contacts with each other, so as to trigger unnecessary physical damnification.In order to solve to accelerate pre-etching Sample arranging problem in experiment, technical staff also devises some for the support of sample arranging, but these current branch therewith Frame more or less still suffers from weak point.
1., the Chinese patent of Publication No. CN2672645, discloses a kind of test sheet shelf, and it is mainly used in salt fog examination Tryoff, test sheet shelf is connected and composed by support, rotatable test piece placing body and keeper, but the test sheet shelf can be placed Sample quantities very little, it is impossible to pre-etching experiment is carried out to a large amount of samples.
2., the Chinese patent of Publication No. CN202159008U, discloses a kind of test piece support for corrosion test, its It is mainly used in the corrosion test of petrochemical plant emphasis corrosion location, the test piece support is by pitman between two ends installing plate, plate And the shading ring composition on pitman, although can put a fairly large number of sample on test piece support, specimen shape is limited System, and it is not used to putting for fatigue testing specimen.
3., the Chinese patent of Publication No. CN102954929A, discloses a kind of test-piece support for corrosion test, the test piece Support is made up of annulus, pole, lacing film bar and nut, and is adopted come the sample of suitable for multiple sizes, but sample by suspended structure Can cause the fixation of sample very unstable with hang, collision easily be produced between sample, so as to cause sample introduction serious Physical damnification interference.
Therefore, design one kind can simultaneously meet sample and place that quantity is big, specimen shape is unrestricted and sample places steady Qualitative good sample mount is very necessary in metallic material corrosion advance damage and fatigue property test.
The content of the invention
For the problem that prior art is present, the present invention provides a kind of pre-etching experiment sample mount, can expire simultaneously Sufficient sample placement quantity is big, the requirement that specimen shape is unrestricted and sample shelf-stability is good, and for metallic material corrosion is pre- Damage and fatigue property test provides stable pre-etching lesion assessment.
To achieve these goals, the present invention is adopted the following technical scheme that:A kind of pre-etching experiment sample mount, including Base plate, base carrier, sheet coupon support frame and bar sample support frame;A row is offered on the base plate equidistant Positioning roll adjustment jack, positioning roll adjustment inserted block is provided with the base carrier bottom, and the positioning roll adjustment in base carrier is inserted Block coordinates with the positioning roll adjustment jack inserting on base plate;At the top of the base support top of the trellis, sheet coupon support frame and Bar sample support top of the trellis offers sample support frame positioning jack;In the sheet coupon support frame and bar sample branch Support bottom is provided with sample support frame positioning inserted block, and the sample support frame positioning jack positions inserted block with sample support frame Inserting coordinates.
Some sheet coupon draw-in grooves are equidistantly provided with the sheet coupon support frame.
The spacing of the adjacent sheet coupon draw-in groove is not less than 5mm.
Some bar sample draw-in grooves are equidistantly provided with the bar sample support frame.
The spacing of the adjacent bar sample draw-in groove is not less than 10mm.
The base carrier quantity is two, and two base carriers be arranged in parallel, and two base carriers pass through Respective positioning roll adjustment inserted block is inserted on base plate, and the spacing of two base carriers is adapted with specimen length.
The sheet coupon support frame and bar sample support frame quantity are some, and some sheet coupon support frames and bar are tried Sample support frame is inserted into base carrier in the form of single kind multiple-level stack, or some sheet coupon support frames and bar Sample support frame is inserted into base carrier in the form of mixed species multiple-level stack.
Beneficial effects of the present invention:
The present invention compared with prior art, can simultaneously meet sample and place that quantity is big, specimen shape is unrestricted and examination The good requirement of sample shelf-stability, and for the pre-etching that metallic material corrosion advance damage and fatigue property test provide stabilization is damaged Assessment.
Brief description of the drawings
Fig. 1 is a kind of pre-etching experiment sample mount (stacking two-layer sheet coupon altogether) structural representation of the invention;
Fig. 2 is a kind of pre-etching experiment sample mount (stacking two-layer bar sample altogether) structural representation of the invention;
Fig. 3 is a kind of pre-etching experiment sample mount (stacking two-layer composite sample altogether) structural representation of the invention;
Fig. 4 is base arrangement schematic diagram of the invention;
Fig. 5 is base carrier structural representation of the invention;
Fig. 6 is sheet coupon support frame structure schematic diagram of the invention;
Fig. 7 is bar sample support frame structural representation of the invention;
In figure, 1-base plate, 2-base carrier, 3-sheet coupon support frame, 4-bar sample support frame, 5-fixed Position roll adjustment jack, 6-positioning roll adjustment inserted block, 7-sample support frame positioning jack, 8-sample support frame positioning inserted block, 9-plate Material sample draw-in groove, 10-bar sample draw-in groove, 11-sheet coupon, 12-bar sample.
Specific embodiment
The present invention is described in further detail with specific embodiment below in conjunction with the accompanying drawings.
As shown in Fig. 1~7, a kind of pre-etching experiment sample mount, including base plate 1, base carrier 2, sheet coupon Support frame 3 and bar sample support frame 4;A row is offered on the base plate 1 and positions roll adjustment jack 5 at equal intervals, described The bottom of base carrier 2 is provided with positioning roll adjustment inserted block 6, determining on the positioning roll adjustment inserted block 6 in base carrier 2 and base plate 1 Position roll adjustment jack 5 is inserted and coordinated;In the top of the base carrier 2, the top of sheet coupon support frame 3 and bar sample support The top of frame 4 offers sample support frame positioning jack 7;In the sheet coupon support frame 3 and the bottom of bar sample support frame 4 Sample support frame positioning inserted block 8 is provided with, the sample support frame positioning jack 7 is inserted with sample support frame positioning inserted block 8 Coordinate.
Some sheet coupon draw-in grooves 9 are equidistantly provided with the sheet coupon support frame 3.
The spacing of the adjacent sheet coupon draw-in groove 9 is not less than 5mm.When sheet coupon 11 is installed to sheet coupon support frame After 3, can make that there is larger gap between sheet coupon 11, and then ensure that all of sheet coupon 11 can be with corrosive medium It is fully contacted, while can avoid being collided each other between sheet coupon 11 again, so as to prevent because of the physics that collision triggers Damage.
Some bar sample draw-in grooves 10 are equidistantly provided with the bar sample support frame 4.
The spacing of the adjacent bar sample draw-in groove 10 is not less than 10mm.When bar sample 12 is installed to bar sample support After frame 4, can make that there is larger gap between bar sample 12, and then ensure that all of bar sample 12 can be situated between with corrosion Matter is fully contacted, while can avoid being collided each other between bar sample 12 again, so as to prevent because of the thing that collision triggers Reason is damaged.
The quantity of the base carrier 2 is two, and two base carriers 2 be arranged in parallel, and two base carriers 2 are led to Cross respective positioning roll adjustment inserted block 6 to be inserted on base plate 1, the spacing of two base carriers 2 is adapted with specimen length.Work as examination When the length dimension of sample changes, only two spacing of base carrier 2 need to be adjusted, so that it may meet the sample under corresponding size Install.
The sheet coupon support frame 3 and bar sample support 4 quantity of frame are some, some sheet coupon support frames 3 and rod Material sample support frame 4 is inserted into base carrier 2 in the form of single kind multiple-level stack, or some sheet coupon support frames 3 and bar sample support frame 4 be inserted into base carrier 2 in the form of mixed species multiple-level stack.When using multiple-level stack When, the sample support frame on upper strata can also play the effect of stabilization by compaction to lower sample, while by multiple-level stack, once may be used To complete the installation of more samples, so as to improve the efficiency of pre-etching experiment.
In the present embodiment, base plate 1, base carrier 2, sheet coupon support frame 3 and bar for constituting sample mount Sample support frame 4 can select the making of the corrosion-resistant materials such as polyethylene, politef or polypropylene.
In the present embodiment, positioning roll adjustment jack 5 uses rectangle jack, matched positioning roll adjustment inserted block 6 then to use square Shape inserted block;Sample support frame positioning jack 7 uses circular socket holes, and matched sample support frame positioning inserted block 8 is then using circle Cylindricality inserted block.
In the present embodiment, the quantity of sheet coupon draw-in groove 9 on sheet coupon support frame 3 is 19, i.e. each pair sheet coupon 19 sheet coupons 11 can be installed simultaneously on support frame 3;The quantity of bar sample draw-in groove 10 on bar sample support frame 4 is 9, 9 bar samples 12 can be simultaneously installed on each pair bar sample support frame 4.
As shown in figure 1, sheet coupon 11 this type of sample is only installed in sample mount, and sheet coupon is supported Frame 3 carries out two-layer stacking altogether.
As shown in Fig. 2 bar sample 12 this type of sample is only installed in sample mount, and bar sample support The bar sample support frame 4 that frame 4 carries out three level stack, particularly third layer altogether is only used for being compacted and stablizing the bar sample on upper strata 12, bar sample 12 is not placed thereon.
As shown in figure 3, sheet coupon 11 and the two kinds of sample of bar sample 12 are installed simultaneously in sample mount, and Sheet coupon support frame 3 and bar sample support frame 4 stack altogether three layers, and bar sample 12 is located at the lower floor of sheet coupon 11, special It is not that the bar sample support frame 4 of third layer is only used for being compacted and stablizing the sheet coupon 11 on upper strata, bar is not placed thereon Sample 12.
Scheme in embodiment and being not used to limits scope of patent protection of the invention, it is all without departing from carried out by the present invention etc. Effect is implemented or is changed, and is both contained in the scope of the claims of this case.

Claims (7)

1. a kind of pre-etching experiment sample mount, it is characterised in that:Including base plate, base carrier, sheet coupon support frame And bar sample support frame;A row is offered on the base plate and positions roll adjustment jack at equal intervals, in the base carrier Bottom is provided with positioning roll adjustment inserted block, and the positioning roll adjustment inserted block in base carrier is matched somebody with somebody with the positioning roll adjustment jack inserting on base plate Close;At the top of the base support top of the trellis, sheet coupon support frame and bar sample support top of the trellis offers sample Support frame positioning jack;Sample support frame positioning is provided with the sheet coupon support frame and bar sample support frame bottom Inserted block, the sample support frame positioning jack coordinates with the positioning inserted block inserting of sample support frame.
2. a kind of pre-etching experiment sample mount according to claim 1, it is characterised in that:In the sheet coupon branch Some sheet coupon draw-in grooves are equidistantly provided with support.
3. a kind of pre-etching experiment sample mount according to claim 2, it is characterised in that:The adjacent sheet coupon The spacing of draw-in groove is not less than 5mm.
4. a kind of pre-etching experiment sample mount according to claim 1, it is characterised in that:In the bar sample branch Some bar sample draw-in grooves are equidistantly provided with support.
5. a kind of pre-etching experiment sample mount according to claim 1, it is characterised in that:The adjacent bar sample The spacing of draw-in groove is not less than 10mm.
6. a kind of pre-etching experiment sample mount according to claim 1, it is characterised in that:The base carrier number It is two to measure, and two base carriers be arranged in parallel, and two base carriers are inserted into by respective positioning roll adjustment inserted block On base plate, the spacing of two base carriers is adapted with specimen length.
7. a kind of pre-etching experiment sample mount according to claim 1, it is characterised in that:The sheet coupon support Frame and bar sample support frame quantity are some, and some sheet coupon support frames and bar sample support frame are with single kind multilayer heap Folded form is inserted into base carrier, or some sheet coupon support frames and bar sample support frame are with mixed species multilayer The form of stacking is inserted into base carrier.
CN201710253543.8A 2017-04-18 2017-04-18 Sample support for pre-corrosion test Active CN106908377B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109540778A (en) * 2019-01-15 2019-03-29 华北水利水电大学 A kind of the quantitative assessment device and test method of 7N01 aluminium alloy exfoliation Corrosion
CN115629029A (en) * 2022-07-25 2023-01-20 中国长江三峡集团有限公司 Steel strand dry-wet cycle corrosion test device and test method

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109540778A (en) * 2019-01-15 2019-03-29 华北水利水电大学 A kind of the quantitative assessment device and test method of 7N01 aluminium alloy exfoliation Corrosion
CN115629029A (en) * 2022-07-25 2023-01-20 中国长江三峡集团有限公司 Steel strand dry-wet cycle corrosion test device and test method

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