CN106884324A - A kind of preparation method of the bafta of antibiosis anti-acarien - Google Patents

A kind of preparation method of the bafta of antibiosis anti-acarien Download PDF

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Publication number
CN106884324A
CN106884324A CN201710180426.3A CN201710180426A CN106884324A CN 106884324 A CN106884324 A CN 106884324A CN 201710180426 A CN201710180426 A CN 201710180426A CN 106884324 A CN106884324 A CN 106884324A
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China
Prior art keywords
bafta
acarien
preparation
antibiosis anti
drying
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Pending
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CN201710180426.3A
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Chinese (zh)
Inventor
储呈平
刘发富
孙道权
孙宁苓
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XINYUAN COCOON SILK GROUP CO Ltd
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XINYUAN COCOON SILK GROUP CO Ltd
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Priority to CN201710180426.3A priority Critical patent/CN106884324A/en
Publication of CN106884324A publication Critical patent/CN106884324A/en
Pending legal-status Critical Current

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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03Polysaccharides or derivatives thereof
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M16/00Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/04Vegetal fibres
    • D06M2101/06Vegetal fibres cellulosic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/25Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50Modified hand or grip properties; Softening compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Biochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention discloses a kind of preparation method of the bafta of antibiosis anti-acarien, the method is that first bafta is put into water, adds chitosan solution stirring immersion;Then bafta will be put into extract solution immersion liquid again, ultrasonic wave immersion is finally putting into drying and setting machine drying and shaping.The antibiosis anti-acarien bafta that the present invention is provided; not only make product bacteriostasis property good; protection skin; also there is the functional characteristics of ventilative, moisture-inhibiting and uvioresistant; product shows by proliferation inhibiting effect experiment; proliferation inhibition rate more than 99%, anti-mite excellent effect, also with good washability and soft feel.The manufacturing process that the present invention is provided is carried out using natural material, and Environmental Safety, low cost, fabric class is high, and product comfort level is good, and added value is high.

Description

A kind of preparation method of the bafta of antibiosis anti-acarien
Technical field
The invention belongs to after-finishing of textile products field, and in particular to a kind of preparation side of the bafta of antibiosis anti-acarien Method.
Technical background
With the raising of living standards of the people and health perception, requirement of the people to dress ornament is from original endurable solid to U.S. Sight, comfortable and diversified development, while pursuing personalized class product high.And traditional dress fabric unitary function, class is not Height, comfort level is poor, and added value is not high, it is impossible to meet demand of the people to clothes.And antibacterial dress ornament is increasingly by the joyous of people Meet, its application can prevent the bacterial cross-infection between person to person, people and thing, thing and thing, it is by the pattern of health care It is changed into prevention in advance from treatment afterwards.Also known as cotton, it with cotton yarn is the woven fabric of raw material to be to bafta.Bafta with Excellent wearability turns into one of the most frequently used fabric, is widely used in garment material, drapery and TECHNICAL FABRIC.Cotton is Most popular clothes and home-textile.Multi-functional, soft, ventilative, moisture absorption, the comfortableness of annual dress, function admirable and resistance to Wear some in numerous qualities that only cotton enjoys great popularity.With the deep development that textile printing and dyeing is processed, bafta kind Become increasingly abundant, outward appearance and performance and class are also improved constantly.Cotton fabric is cheap, widely applicable, and water imbibition is strong, wear-resisting resistance to Wash, soft comfortable, it is good that winter wears warmth retention property, summer dress is ventilative nice and cool.And bafta is through with people, so Need, with anti-microbial property, also to have with other performance;Because bafta is in wearing process, the sweat of skin surface discharge Liquid, sebum, grease metabolic wastes and the food vestiges from outside will attach on bafta, as microorganisms such as acarids Nutrient source, while cotton is a kind of natural fiber.Contained cellulose and protein in the natural fiber, the life of the bacterium that is also beneficial to use up Long and breeding.And dust mite is one of major reason as allergic reaction illness, human health is seriously threatened;Therefore, antibacterial Anti-mite increasingly receives much concern, the another focus as hygienic finishing processing.The present invention attempts suitable rear whole by selection Reason mode further lifts the antibiosis anti-acarien performance of fabric.
The content of the invention
Present invention aim at a kind of preparation method of the bafta of antibiosis anti-acarien of offer.The preparation method providing cotton fabric Antibiosis anti-acarien function, effect is good, and non-toxic.
The purpose of the present invention is achieved through the following technical solutions:
A kind of preparation method of the bafta of antibiosis anti-acarien, the method comprises the following steps:
1) bafta is put into 45-55 DEG C of water, adds chitosan solution 1-2g/L, bath raio 1:30-35, stirring immersion 20-30 minutes, 75-85 DEG C, insulation boiling-off 45-55 minutes are then warming up to 5-10 DEG C/minute of speed;Then again with 2-5 DEG C/ The speed divided is cooled to 55-65 DEG C, takes out, and is rinsed with normal-temperature water;
2) bafta that will be rinsed well is by bath raio 1:20-25 is put into extract solution immersion liquid, ultrasonic wave immersion, and frequency is 30kHz, temperature is 50-55 DEG C, is incubated 5-10 minutes, with 1-2 DEG C/min of intensification, to 70-80 DEG C, is incubated 20-30 minutes;Institute It is to clean chaulmoogra, the fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta respectively to state extract solution immersion liquid, and 80% is used after smashing mixing Ethanol water bath refluxing extraction and obtain;
3) liquid carrying rate control is put into drying and setting machine in the bafta of 30-50%, drying and shaping temperature is 60-250 DEG C, Speed is 5-50m/min.
Described chitosan solution preparation method is that shitosan is dissolved in 5% acetum, and concentration is 2%, ultrasound To being completely dissolved, bubble-free.
The step 2) in, drying temperature is 100-120 DEG C, and speed is 15-25m/min.
The chaulmoogra, the fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta are by weight 6-10:3-7:5-8:1-3:10-15: The ratio mixing of 8-10, in terms of fresh material.
The chaulmoogra, the fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta are by weight 8:5:6:2:13:9 ratio mixing, In terms of fresh material.
The device have the advantages that:The antibiosis anti-acarien bafta that the present invention is provided, not only makes product bacteriostasis property good, Protection skin, the functional characteristics also with ventilative, moisture-inhibiting and uvioresistant, product shows by proliferation inhibiting effect experiment, breeds Inhibiting rate more than 99%, anti-mite excellent effect, also with good washability and soft feel.The manufacturing process that the present invention is provided Carried out using natural material, Environmental Safety, low cost, fabric class is high, product comfort level is good, and added value is high.
Specific embodiment
Embodiment 1
A kind of preparation method of the bafta of antibiosis anti-acarien, the method comprises the following steps:
1) bafta is put into 45 DEG C of water, adds chitosan solution 1g/L, bath raio 1:30, stirring immersion 20 minutes, Then 75 DEG C, insulation boiling-off 45 minutes are warming up to 5 DEG C/minute of speed;Then 55 DEG C are cooled to 2 DEG C/minute of speed again, are taken Go out, rinsed with normal-temperature water;Chitosan solution preparation method is that shitosan is dissolved in 5% acetum, and concentration is 2%, is surpassed Sound to being completely dissolved, bubble-free.
2) bafta that will be rinsed well is by bath raio 1:20 are put into extract solution immersion liquid, ultrasonic wave immersion, and frequency is 30kHz, temperature is 50 DEG C, is incubated 5 minutes, with 1 DEG C/min of intensification, to 70 DEG C, is incubated 20 minutes;The extract solution immersion liquid is Chaulmoogra, the fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta are cleaned respectively, is carried using the backflow of 80% ethanol water bath after smashing mixing Take and obtain;Chaulmoogra, the fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta are by weight 6:3:5:1:10:8 ratio mixing, with fresh Material meter.
3) liquid carrying rate control is put into drying and setting machine in 30% bafta, drying and shaping temperature is 60 DEG C, and speed is 5m/min。
Embodiment 2
A kind of preparation method of the bafta of antibiosis anti-acarien, the method comprises the following steps:
1) bafta is put into 55 DEG C of water, adds chitosan solution 2g/L, bath raio 1:35, stirring immersion 30 minutes, Then 85 DEG C, insulation boiling-off 45-55 minutes are warming up to 10 DEG C/minute of speed;Then 65 are cooled to 5 DEG C/minute of speed again DEG C, take out, rinsed with normal-temperature water;Chitosan solution preparation method is that shitosan is dissolved in 5% acetum, and concentration is 2%, ultrasound to being completely dissolved, bubble-free.
2) bafta that will be rinsed well is by bath raio 1:25 are put into extract solution immersion liquid, ultrasonic wave immersion, and frequency is 30kHz, temperature is 55 DEG C, is incubated 10 minutes, with 2 DEG C/min of intensifications, to 80 DEG C, is incubated 30 minutes;The extract solution immersion liquid is Chaulmoogra, the fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta are cleaned respectively, is carried using the backflow of 80% ethanol water bath after smashing mixing Take and obtain;Chaulmoogra, the fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta are by weight 10:7:8:3:15:10 ratio mixing, with Fresh material meter.
3) liquid carrying rate control is put into drying and setting machine in the bafta of 30-50%, drying and shaping temperature is 60-250 DEG C, Speed is 5-50m/min.
Embodiment 3
A kind of preparation method of the bafta of antibiosis anti-acarien, the method comprises the following steps:
1) bafta is put into 50 DEG C of water, adds chitosan solution 1.5g/L, bath raio 1:33,26 points of stirring immersion Clock, is then warming up to 80 DEG C, insulation boiling-off 50 minutes with 7 DEG C/minute of speed;Then 60 are cooled to 4 DEG C/minute of speed again DEG C, take out, rinsed with normal-temperature water;Chitosan solution preparation method is that shitosan is dissolved in 5% acetum, and concentration is 2%, ultrasound to being completely dissolved, bubble-free.
2) bafta that will be rinsed well is by bath raio 1:23 are put into extract solution immersion liquid, ultrasonic wave immersion, and frequency is 30kHz, temperature is 53 DEG C, is incubated 8 minutes, with 1.5 DEG C/min of intensifications, to 75 DEG C, is incubated 25 minutes;The extract solution immersion liquid It is to clean chaulmoogra, the fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta respectively, is flowed back using 80% ethanol water bath after smashing mixing Extract and obtain;Chaulmoogra, the fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta are by weight 8:5:6:2:13:9 ratio mixing, with Fresh material meter.
3) liquid carrying rate control is put into drying and setting machine in 40% bafta, drying temperature is 110 DEG C, and speed is 20m/ min。
Embodiment 4
Embodiment 1-3 is obtained into bafta to be tested as follows:
1. physical property:Form, whiteness, intensity, feel etc. are without significant change.
2. antimicrobial spectrum is determined:Planting harmful bacteria to gonococcus, staphylococcus aureus, Escherichia coli etc. more than 20 has efficiently Rejection ability, bacteriostasis rate > 99%.
3. antibacterial effect:
(1) antibiotic rate > 99% (antibiotic property test method rocks flask method using FZ/T01021-92)
(2) mite effect is pressed down:To dust mite, gamasid, trombiculid scattering ratio > 99%.
4. antibiotic fabric washing fastness:
Fastness to washing:6 months later old products are tested new product and produced respectively, and old product washed once for every 5 days, By 18 washings, the bacteriostasis property of textile, GB/T3920-1997 marks are determined with reference to improvement AATCC-100 method of testings Standard determines crock fastness.After washing 36 times, the bacteriostasis rate of old product has declined, and the scattering ratio to dust mite, gamasid, trombiculid is more than 95%, the death rate is up to more than 90%.The bacteriostasis rates such as gonococcus, staphylococcus aureus, Escherichia coli are up to more than 90%.Illustrate warp The antibacterial anti-mite effect of antibiosis anti-acarien bafta of the embodiment of the present invention is good, and fungistatic effect is remained in that after wash for a long time More than 90%.

Claims (5)

1. a kind of preparation method of the bafta of antibiosis anti-acarien, it is characterised in that the method comprises the following steps:
Bafta is put into 45-55 DEG C of water, chitosan solution 1-2g/L, bath raio 1 is added:30-35, stirring immersion 20-30 Minute, 75-85 DEG C, insulation boiling-off 45-55 minutes are then warming up to 5-10 DEG C/minute of speed;Then again with 2-5 DEG C/minute Speed is cooled to 55-65 DEG C, takes out, and is rinsed with normal-temperature water;
The bafta that will be rinsed well is by bath raio 1:20-25 is put into extract solution immersion liquid, ultrasonic wave immersion, and frequency is 30kHz, temperature It is 50-55 DEG C to spend, and is incubated 5-10 minutes, with 1-2 DEG C/min of intensification, to 70-80 DEG C, is incubated 20-30 minutes;The extract solution Immersion liquid is to clean chaulmoogra, the fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta respectively, and 80% ethanol water bath is used after smashing mixing Refluxing extraction and obtain;
Liquid carrying rate control is put into drying and setting machine in the bafta of 30-50%, drying and shaping temperature is 60-250 DEG C, speed It is 5-50m/min.
2. a kind of preparation method of the bafta of antibiosis anti-acarien according to claim 1, it is characterised in that:Described shitosan Solution manufacturing method is that shitosan is dissolved in 5% acetum, and concentration is 2%, ultrasound to being completely dissolved, bubble-free.
3. a kind of preparation method of the bafta of antibiosis anti-acarien according to claim 1, it is characterised in that:The step 2) In, drying temperature is 100-120 DEG C, and speed is 15-25m/min.
4. a kind of preparation method of the bafta of antibiosis anti-acarien according to claim 1, it is characterised in that:The chaulmoogra, The fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta are by weight 6-10:3-7:5-8:1-3:10-15:The ratio mixing of 8-10, with fresh Material meter.
5. a kind of preparation method of the bafta of antibiosis anti-acarien according to claim 1, it is characterised in that:The chaulmoogra, The fruit of summer cypress, cloves, kuh-seng, sweet wormwood and schizonepeta are by weight 8:5:6:2:13:9 ratio mixing, in terms of fresh material.
CN201710180426.3A 2017-03-23 2017-03-23 A kind of preparation method of the bafta of antibiosis anti-acarien Pending CN106884324A (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107354738A (en) * 2017-09-04 2017-11-17 西南大学 Chitosan/cotton antibacterial composite fabric is prepared with NMMO
CN107524000A (en) * 2017-08-01 2017-12-29 江苏新瑞贝科技股份有限公司 A kind of preparation method of natural antibacterial mite-assistant fabricses coating
CN107700203A (en) * 2017-09-25 2018-02-16 安徽华祺汽车装饰有限公司 A kind of processing method of modified soybean fiber
CN108360255A (en) * 2018-01-25 2018-08-03 南通唐盛纺织有限公司 Based on natural plants mite-proofing and antimicrobial material extraction, finishing agent preparation method and application
CN110565380A (en) * 2019-07-30 2019-12-13 互太(番禺)纺织印染有限公司 Production process of antibacterial fabric
CN111021053A (en) * 2019-11-26 2020-04-17 杭州优标科技有限公司 Fiber containing artemisia annua composite extract and preparation method thereof
CN111809392A (en) * 2020-07-24 2020-10-23 上海封林贸易有限公司 Antibacterial underwear and preparation method thereof

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107524000A (en) * 2017-08-01 2017-12-29 江苏新瑞贝科技股份有限公司 A kind of preparation method of natural antibacterial mite-assistant fabricses coating
CN107354738A (en) * 2017-09-04 2017-11-17 西南大学 Chitosan/cotton antibacterial composite fabric is prepared with NMMO
CN107700203A (en) * 2017-09-25 2018-02-16 安徽华祺汽车装饰有限公司 A kind of processing method of modified soybean fiber
CN108360255A (en) * 2018-01-25 2018-08-03 南通唐盛纺织有限公司 Based on natural plants mite-proofing and antimicrobial material extraction, finishing agent preparation method and application
CN110565380A (en) * 2019-07-30 2019-12-13 互太(番禺)纺织印染有限公司 Production process of antibacterial fabric
CN111021053A (en) * 2019-11-26 2020-04-17 杭州优标科技有限公司 Fiber containing artemisia annua composite extract and preparation method thereof
CN111809392A (en) * 2020-07-24 2020-10-23 上海封林贸易有限公司 Antibacterial underwear and preparation method thereof

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Application publication date: 20170623