CN106833148A - A kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying and preparation method thereof - Google Patents
A kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying and preparation method thereof Download PDFInfo
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- CN106833148A CN106833148A CN201710104959.3A CN201710104959A CN106833148A CN 106833148 A CN106833148 A CN 106833148A CN 201710104959 A CN201710104959 A CN 201710104959A CN 106833148 A CN106833148 A CN 106833148A
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- 238000005507 spraying Methods 0.000 title claims abstract description 62
- 239000003292 glue Substances 0.000 title claims abstract description 61
- 230000001954 sterilising effect Effects 0.000 title claims abstract description 36
- 238000000746 purification Methods 0.000 title claims abstract description 23
- 230000001877 deodorizing effect Effects 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 239000001993 wax Substances 0.000 claims abstract description 36
- 239000007788 liquid Substances 0.000 claims abstract description 35
- 238000004378 air conditioning Methods 0.000 claims abstract description 28
- 239000003921 oil Substances 0.000 claims abstract description 24
- 239000004264 Petrolatum Substances 0.000 claims abstract description 20
- 229940066842 petrolatum Drugs 0.000 claims abstract description 20
- 235000019271 petrolatum Nutrition 0.000 claims abstract description 20
- 239000000341 volatile oil Substances 0.000 claims abstract description 20
- 239000011701 zinc Substances 0.000 claims abstract description 20
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 20
- 229920002367 Polyisobutene Polymers 0.000 claims abstract description 17
- 238000006243 chemical reaction Methods 0.000 claims abstract description 17
- 238000001914 filtration Methods 0.000 claims abstract description 16
- 239000002994 raw material Substances 0.000 claims abstract description 14
- 239000004200 microcrystalline wax Substances 0.000 claims abstract description 13
- 238000001816 cooling Methods 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 230000035484 reaction time Effects 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims abstract description 7
- 238000010257 thawing Methods 0.000 claims abstract description 7
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000005977 Ethylene Substances 0.000 claims abstract description 4
- 235000007164 Oryza sativa Nutrition 0.000 claims description 6
- 235000009566 rice Nutrition 0.000 claims description 6
- 240000007594 Oryza sativa Species 0.000 claims 1
- 238000010422 painting Methods 0.000 abstract description 6
- 238000012360 testing method Methods 0.000 description 20
- 238000002474 experimental method Methods 0.000 description 13
- 230000000694 effects Effects 0.000 description 12
- 238000004659 sterilization and disinfection Methods 0.000 description 12
- 230000037396 body weight Effects 0.000 description 9
- 241000700605 Viruses Species 0.000 description 8
- 241000699666 Mus <mouse, genus> Species 0.000 description 7
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 6
- 239000004576 sand Substances 0.000 description 6
- 241000209094 Oryza Species 0.000 description 5
- 241000894006 Bacteria Species 0.000 description 4
- 239000000919 ceramic Substances 0.000 description 4
- 230000007423 decrease Effects 0.000 description 4
- 239000000428 dust Substances 0.000 description 4
- 230000002147 killing effect Effects 0.000 description 4
- 241001494479 Pecora Species 0.000 description 3
- 238000011109 contamination Methods 0.000 description 3
- 238000007598 dipping method Methods 0.000 description 3
- 238000003304 gavage Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- 241001466460 Alveolata Species 0.000 description 2
- 231100000460 acute oral toxicity Toxicity 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 235000013339 cereals Nutrition 0.000 description 2
- 239000012153 distilled water Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 231100000614 poison Toxicity 0.000 description 2
- 230000007096 poisonous effect Effects 0.000 description 2
- 230000006641 stabilisation Effects 0.000 description 2
- 238000011105 stabilization Methods 0.000 description 2
- 208000024891 symptom Diseases 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 230000002588 toxic effect Effects 0.000 description 2
- 231100000820 toxicity test Toxicity 0.000 description 2
- 231100000027 toxicology Toxicity 0.000 description 2
- 229920001817 Agar Polymers 0.000 description 1
- 241000256113 Culicidae Species 0.000 description 1
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 241000255925 Diptera Species 0.000 description 1
- 206010060891 General symptom Diseases 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241000699670 Mus sp. Species 0.000 description 1
- 241000700157 Rattus norvegicus Species 0.000 description 1
- -1 Tissuemat E Substances 0.000 description 1
- 230000001154 acute effect Effects 0.000 description 1
- 239000008272 agar Substances 0.000 description 1
- 238000004887 air purification Methods 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 230000000249 desinfective effect Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 206010016256 fatigue Diseases 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 230000002496 gastric effect Effects 0.000 description 1
- 230000037308 hair color Effects 0.000 description 1
- 238000001802 infusion Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000013642 negative control Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 238000003305 oral gavage Methods 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 230000001575 pathological effect Effects 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 239000008279 sol Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 231100000456 subacute toxicity Toxicity 0.000 description 1
- 238000009602 toxicology test Methods 0.000 description 1
- 241000712461 unidentified influenza virus Species 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D123/00—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers
- C09D123/02—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
- C09D123/04—Homopolymers or copolymers of ethene
- C09D123/06—Polyethene
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D123/00—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers
- C09D123/02—Coating compositions based on homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
- C09D123/18—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms
- C09D123/20—Homopolymers or copolymers of hydrocarbons having four or more carbon atoms having four to nine carbon atoms
- C09D123/22—Copolymers of isobutene; Butyl rubber ; Homo- or copolymers of other iso-olefines
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
- C09D191/06—Waxes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
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- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
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- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Plant Pathology (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The present invention is that a kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying and preparation method thereof.It is made up of by weight following raw materials according：5 35 grams of polyisobutene, 8 45 grams of Tissuemat E, 6 25 grams of petrolatum, 4 21 grams of slack wax, 5 18 grams of white oil, 6 16 grams of slack wax, 3 15 grams of microwax, 0.01 1 grams of Nano-Zinc, 5 25 grams of essential oil.Preparation method, step 1 is melted：Above-mentioned raw materials carry out water-bath or oil bath heating respectively, treat to melt completely to liquid；Step 2 hybrid reaction：The liquid of the polyisobutene of above-mentioned thawing to liquid, ethylene waxes, petrolatum, slack wax, white oil, slack wax, microwax, Nano-Zinc, essential oil is added into reactor under normal temperature, normal pressure, stir, reaction temperature is controlled at 123 142 DEG C, pressure is 47 kilograms, and the reaction time is 20 50 minutes；Step 3 is cooled down：By above-mentioned reacted liquid cooling to 75 DEG C, reacted liquid is flowed into bottle fills, being cooled to normal temperature and obtaining cold-resistant heat-resisting application has the nanometer painting glue spraying that various screen packs, air purifier filtration core, air-conditioning filter net, window are husky, door and window is husky.
Description
Technical field
The invention belongs to air purification field.Especially a kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying and its system
Preparation Method.
Background technology
At present, HEPA high efficiency particulate airs, Alveolate activated carbon screen pack, ceramic element for using both at home and abroad etc. are used as a kind of
The material of purification filtering, is widely used in various air-conditionings, and used as screen pack etc., these screen packs only have filtering hair to air purifier
Send out the effect of meal dirt, it is impossible to filter the bacterial virus in air, cannot more decompose toxic and harmful and stink, such as
PM2.5,0.1-2.0 μm of airborne dust particle diameter, 0.5-1.5 μm of bacterium, 0.08-0.1 μm of mould, acarid 0.5-1 mm, influenza virus
0.09-1.0 μm, it is seen that existing screen pack is accomplished to eliminate stink and sterilization without method.Filter screen accumulates dust due to long-term simultaneously,
Moisture, itself also breed bacteria, virus, goes mouldy, and blocks the problem of ventilation filter.Even to this day, do not make also both at home and abroad
With time real effectively fast deodorization taste, sterilization, the screen pack for killing the virus, ceramic element and filter (filter core) long, nanometer painting
Glue spraying can eliminate nanoscale PM2.5, and energy sterilization is killed the virus, and screen pack, ceramic filtering are sprayed and painted on to there is presently no painting glue spraying
The nanometer of core and filter (filter core) applies glue spraying invention, in order to eliminate the healthy of PM2.5 and the common people.Invention one kind is used
Time is long, it is real effectively eliminate the sterilized nanometer of stink apply glue spraying by screen pack, air purifier filtration core, air-conditioning filter net,
It is very necessary that window is husky, door and window sand is supported the use, and glue spraying is applied also to current screen pack both domestic and external, window sand, door and window sand nanometer
It is world's blank.
The content of the invention
It is an object of the invention to provide one kind there is high efficiency to eliminate nanoscale PM2.5, elimination toxic and harmful smelly
Taste and the nanometer painting glue spraying that sterilized can be killed the virus, nanometer apply glue spraying and are sprayed and painted on various screen packs, air purifier filtration core, sky
The nanometer of the matching used screen pack deodorizing sterilizing purification such as screen pack, window sand, door and window sand is adjusted to apply glue spraying.
The nanometer for providing the purification of screen pack deodorizing sterilizing of another object of the present invention applies the preparation method of glue spraying.
A kind of nanometer of screen pack deodorizing sterilizing purification of the present invention applies glue spraying, it is characterised in that by following raw materials according by weight
Composition：
It is 5-35 grams of polyisobutene, 8-45 grams of Tissuemat E, 6-25 grams of petrolatum, 4-21 grams of slack wax, 5-18 grams of white oil, loose
6-16 grams of wax, 3-15 grams of microwax, 0.01-1 grams of Nano-Zinc, 5-25 grams of essential oil.
A kind of nanometer of screen pack deodorizing sterilizing purification of the present invention applies the preparation method of glue spraying, it is characterised in that step is such as
Under：
Step 1 is melted：By 5-35 grams of raw material polyisobutene, 8-45 grams of Tissuemat E, 6-25 grams of petrolatum, slack wax 4-21
Gram, 5-18 grams of white oil, 6-16 grams of slack wax, 3-15 grams of microwax, 0.01-1 grams of Nano-Zinc, 5-25 grams of essential oil.Carry out respectively
Water-bath or oil bath heating, treat to melt completely to liquid；
Step 2 hybrid reaction：By the polyisobutene of above-mentioned thawing to liquid, ethylene waxes, petrolatum, frivolous under normal temperature, normal pressure
Slack wax, white oil, slack wax, microwax, Nano-Zinc, the liquid of essential oil add reactor, stir, and reaction temperature control exists
123-142 DEG C, pressure is 4-7 kilograms, and the reaction time is 20-50 minutes；
Step 3 is cooled down：By above-mentioned reacted liquid cooling to 75 DEG C, reacted liquid is flowed into bottle and fills interior, be cooled to often
Temperature obtains cold-resistant heat-resisting application that various screen packs, air purifier filtration core, air-conditioning filter net, window are husky, door and window is husky receives
Rice applies glue spraying.
First, nanometer of the invention applies the experiment of glue spraying Safety and toxicology.
Test specimen nanometer applies glue spraying：Test specimen adds deionized water configuration to obtain final product.
（One）Acute oral toxicity test:
Take fasting 16h before the experiment of mouse 80 to be randomly divided into 4 groups every group 40 male and female half and half by body weight gavage gives respectively, this hair
Bright nanometer spray coating sol solution and distilled water, administration group and blank control group are given by 0.4ml/10g body weight gavages, are seen after administration
Record reaction of animals symptom, Continuous Observation 14d are examined, and records body weight or possible death condition.
After result administration, there are the symptoms such as loose stools, perpendicular hair, lassitude in mouse.When administration 7d weighs, administration group male is small
Mouse relatively has highly significant difference (p=0.01), mouse, general symptom after administration 14d with blank control group male mice weight ratio
Change without exception, body weight increase is normal, compares without significant difference with control group.
Conclusion：It is 2g/kg that nanometer of the present invention applies glue spraying gavage and gives mouse maximum dosage, and clinical day is used equivalent to people
Without 1 dead mouse in 3 times of dosage, 14d observation periods, mouse outward appearance change without exception after administration, feed, drinking-water, body weight increase
Long and activity is normal.
（Two）Nanometer applies the experiment of glue spraying Safety and toxicology
1st, acute oral toxicity test:
SPF grades of Wistar rat 60 for choosing body weight 180-200 g is only divided into experimental group and control group male and female half and half.Acute warp
Mouthful toxicity test press 1.00ml/100g body weight, by nanometer used apply gastric infusion Continuous Observation 14d of glue spraying record body weight,
1.00ml/100g body weight is pressed in diet, the experiment of death condition Subacute toxicity, daily oral gavage contamination, negative control group
Give sterile distilled water.Continuous contamination 28d, 24h broken ends take blood after last contamination, detect every routine blood indexes and to main
Organ carries out pathologic finding.
Conclusion：The indices indices of each dosage group and control group ratio in this detection unit range of normal value
Compared with difference is not statistically significant.Concentration nanometer applies glue spraying in nontoxic.
（Three）Nanometer spray coating glue skin toxicology test:
The made nanometer of the present invention applies 500 grams of glue spraying, dilutes 300 times, and dipping is carried out to 33 sheep, and after dipping 7 days, sheep is without any
Reaction, and hair color light is pure white, without mosquitos and flies interference, Follow-up observation shows after dipping, and sheep occurs without vermin after bath.
（Four）Nanometer applies glue spraying and is painted into the experiment of air-conditioning filter net sterilizing rate
Nanometer prepared by the present invention applies glue spraying and is painted into 2 pieces of air-conditioning filter net, is put into air-conditioning air inlet, and air-conditioning start is flat 15
The side 30 minutes sterilizing rate 81-99% in interior, contact 15 minutes sterilizing rates 99.9% of sterilization.
（Five）Nanometer applies glue spraying and is painted into the experiment of air-conditioning filter net sterilizing rate
Made nanometer applies glue spraying and is painted into 2 pieces of air-conditioning filter net, is put into special bus air-conditioning circulate in the wind mouthful result of the test as follows：
Killing effect table 5,
| Nanometer applies glue spraying | Air disinfection（30th, 60 minutes） |
| It is painted into 2 pieces of air-conditioning filter net | 96% |
| It is painted into 2 pieces of air-conditioning filter net | 99% |
（Six）Nanometer applies glue spraying sterilization experiment
Nanometer applies glue spraying according to national hospital antiseptic hygiene standard (GBl5982-1995), and nanometer applies glue spraying and is sprayed on HEPA filterings
Net, HEPA screen packs is put into air purifier, and air purifier is booted up in 31 square metres of relatively closed room
Carry out tertiary air Disinfection Effect experiment.Wherein, room temperature is 25 DEG C, relative humidity 80%；Layouted using east, south, west, north
Method, height of sampling is 1.2 meters, is layouted 0.8 meter from wall；Exposed in sampled point with the General nutrition agar plate of 9 cm diameters
After 10 minutes, 37 DEG C of cultures calculate clump count in 48 hours.It is below the experiment effect of experiment.
（1）Experiment condition：There is 5 people activity interior in test process, does not wear masks.There are 10 people to pass in and out room in experimentation
Between.
（2）Test result：It is shown in Table 6.
The killing effect of bacterium in the room air of table 6
| Stage | Average killing rate % | |
| Reset condition | 3739 | 0% |
| Sterilization 30 minutes | 31 | 99.5% |
| Sterilization 60 minutes | 21 | 99.995 |
| Sterilization is shut down after 60 minutes and is tested 50 minutes | 25 | 90.905 |
（Seven）Nanometer applies glue spraying air conditioner filter element and is contrasted with Nissan air conditioner filter element actual filtration effectiveness results（In-car PM2.5 numbers
Value）
Test condition：
Outdoor PM2.5 numerical value on the day of test is 40 or so, and the PM2.5 numerical value of same time in-car is 38 or so, and temperature is taken the photograph for 34
Family name's degree, it is calm.Test carriage is Nissan, and two filter core for using is that Nissan air conditioner filter element and nanometer apply the filter of glue spraying air-conditioning
Core, PM2.5 numerical value is gathered once at intervals of two minutes, and inside and outside each test of circulation is once.
Tester：
The tester for using is portable, and two groups of data can be individually read in real time, is respectively small particle（Fine dust,
The fine particles such as bacterium, smog）Quantity in every 0.01 cubic feet；Bulky grain thing（Bulky grain dust, pollen, spore etc. are thick
Particulate matter）Quantity in every 0.01 cubic feet.These are all have the east having a strong impact on to human respiratory tract's system on the whole
West.The data for showing screen display are the average value of every 6 seconds.
Test result：
The change of data on tester can be intuitive to see very much during test, be surveyed using common air-conditioning filter core
During examination, the speed that PM2.5 values decline is very average, and after installing nanometer painting glue spraying air conditioner filter element, under in-car PM2.5 values are quick
Drop.
Interior circulation state
In the state of common air-conditioning filter core is installed, the speed that in-car PM2.5 values decline is slow, and final stabilization exists after 10 minutes
20 or so；And it is about i.e. stable in 0 or so, gap after 5 minutes PM2.5 values under nanometer applies glue spraying air conditioner filter element state are installed
Or it is no small.
Data under interior circulation state are more accurate, because eliminating influences of the PM2.5 for test in the outer air of car.
Under the test condition of interior circulation, the about decline per minute of common air-conditioning filter core finally stablizes left 16 after 1 or so, 10 minutes
The right side, has filtered out in-car 55% or so PM2.5；And install nanometer apply glue spraying air conditioner filter element in the state of, open air-conditioning less than 1
Minute P2.5 values are just fallen below within 3.33, many soon when PM2.5 decrease speeds ratio is using common filter core, and final stabilization exists
0 value.
Test effect table 7
Nanometer painting glue spraying air conditioner filter element is better than common air-conditioning filter core as can be seen from the table.
(8) test effect table 8
Nanometer applies glue spraying and is sprayed on HEPA screen packs, and HEPA screen packs are put into air-conditioning air inlet and activated carbon air conditioner filter element pair
Than air-conditioning is booted up carries out effect experiment in 25 square metres of relatively closed room.
Test result is shown in Table 8.
Test effect table 8
（Nine）Nanometer applies glue spraying and is sprayed on the contrast of HEPA screen packs, HEPA high efficiency particulate airs, Alveolate activated carbon screen pack, ceramics
Filter core effect experiment is shown in Table 9:
Test effect table 9：
Advantages and positive effects of the present invention are as follows：
（1）Key solve nanometer apply glue spraying spray to various screen packs, air purifier filtration core, air-conditioning filter net, window it is husky,
In door and window sand etc., PM2 is eliminated with efficient fast decoupled poisonous and harmful stink, high efficiency, 5, strong disinfecting kills the virus, quickly disappears
The creativeness for eliminating the unusual smell.
（2）Breach domestic and international existing screen pack, air purifier filtration core, air-conditioning filter net except PM2.5 is low, can not
Sterilization is killed the virus, can not eliminate the unusual smell, the problem of use time short effect difference.
（3）Realizing can both eliminate PM2.5, and energy sterilization is killed the virus, various poisonous and harmful stinks removed, with practicality
Property, with having a extensive future.
Specific embodiment
Technology contents of the invention are described further with reference to embodiment；Following embodiments be it is illustrative, no
It is limited, it is impossible to limit protection scope of the present invention with following embodiments.
Embodiment 1
The present embodiment is that a kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying and preparation method thereof.
A kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying, it is characterised in that：It is made up of by weight following raw materials according：
It is 5-35 grams of polyisobutene, 8-45 grams of Tissuemat E, 6-25 grams of petrolatum, 4-21 grams of slack wax, 5-18 grams of white oil, loose
6-16 grams of wax, 3-15 grams of microwax, 0.01-1 grams of Nano-Zinc, 5-25 grams of essential oil.
A kind of nanometer of screen pack deodorizing sterilizing purification of the present invention applies the preparation method of glue spraying, it is characterised in that step is such as
Under：
Step 1 is melted：By 5-35 grams of raw material polyisobutene, 85-45 grams of Tissuemat E, 6-25 grams of petrolatum, slack wax 4-21
Gram, 5-18 grams of white oil, 6-16 grams of slack wax, 3-15 grams of microwax, 0.01-1 grams of Nano-Zinc, 5-25 grams of essential oil.Carry out respectively
Oil bath heating, treats to melt completely to liquid；
Step 2 hybrid reaction：By the polyisobutene of above-mentioned thawing to liquid, ethylene waxes, petrolatum, frivolous under normal temperature, normal pressure
Slack wax, white oil, slack wax, microwax, Nano-Zinc, the liquid of essential oil add reactor, stir, and reaction temperature control exists
142 DEG C, pressure is 7 kilograms, and the reaction time is 20-50 minutes；
Step 3 is cooled down：By above-mentioned reacted liquid cooling to 75 DEG C, reacted liquid is flowed into bottle and fills interior, be cooled to often
Temperature obtains cold-resistant heat-resisting application that various screen packs, air purifier filtration core, air-conditioning filter net, window are husky, door and window is husky receives
Rice applies glue spraying.
Embodiment 2
The present embodiment is that a kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying and preparation method thereof.
A kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying, it is characterised in that：It is made up of by weight following raw materials according：
It is 15 grams of polyisobutene, 20 grams of Tissuemat E, 10 grams of petrolatum, 10 grams of slack wax, 10 grams of white oil, 10 grams of slack wax, micro-
10 grams of brilliant wax, 0.01 gram of Nano-Zinc, 14.99 grams of essential oil.
A kind of nanometer of screen pack deodorizing sterilizing purification applies the preparation method of glue spraying, it is characterised in that step is as follows：
Step 1 is melted：By 15 grams of raw material polyisobutene, 20 grams of Tissuemat E, 10 grams of petrolatum, 10 grams of slack wax, white oil 10
Gram, 10 grams of slack wax, 10 grams of microwax, 0.01 gram of Nano-Zinc, 14.99 grams of essential oil carry out oil bath heating, treat to melt completely to
Liquid；
Step 2 hybrid reaction：By the polyisobutene of above-mentioned thawing to liquid, Tissuemat E, petrolatum, slack wax, white oil, dredge
Loose wax, microwax, Nano-Zinc, essential oil.Liquid add reactor, stir, reaction temperature control in 123 DEG C, pressure
It it is 4 kilograms, the reaction time is 50 minutes；
Step 3 is cooled down：By above-mentioned reacted liquid cooling to 75 DEG C, reacted liquid is flowed into bottle and fills interior, be cooled to often
Temperature obtains cold-resistant heat-resisting application that various screen packs, air purifier filtration core, air-conditioning filter net, window are husky, door and window is husky receives
Rice applies glue spraying.
Embodiment 3
The present embodiment is that a kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying and preparation method thereof.
A kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying, it is characterised in that：It is made up of by weight following raw materials according：
23 grams of polyisobutene, 19 grams of petrolatum, 12 grams of slack wax, 1 gram of Nano-Zinc, 16 grams of essential oil.
A kind of nanometer of screen pack deodorizing sterilizing purification applies the preparation method of glue spraying, it is characterised in that step is as follows：
Step 1 is melted：23 grams of raw material polyisobutene, 19 grams of petrolatum, 12 grams of slack wax, 1 gram of Nano-Zinc, 16 grams of essential oil are entered
Row oil bath heating, treats to melt completely to liquid；
Step 2 hybrid reaction：By the polyisobutene of above-mentioned thawing to liquid, petrolatum, slack wax, Nano-Zinc, essential oil liquid
Body adds reactor, stirs, and at 136 DEG C, pressure is 5 kilograms for reaction temperature control, and the reaction time is 50 minutes；
Step 3 is cooled down：By above-mentioned reacted liquid cooling to 75 DEG C, reacted liquid is flowed into bottle and fills interior, be cooled to often
Temperature obtains cold-resistant heat-resisting application that various screen packs, air purifier filtration core, air-conditioning filter net, window are husky, door and window is husky receives
Rice applies glue spraying.
Embodiment 4
The present embodiment is that a kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying and preparation method thereof.
A kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying, it is characterised in that：It is made up of by weight following raw materials according：
25 grams of petrolatum, 8 grams of white oil, 0.01 gram of Nano-Zinc, 11 grams of essential oil.
A kind of nanometer of screen pack deodorizing sterilizing purification applies the preparation method of glue spraying, it is characterised in that step is as follows：
Step 1 is melted：25 grams of raw material petrolatum, 8 grams of white oil, 0.01 gram of Nano-Zinc, 11 grams of essential oil are carried out into oil bath heating, is treated
Melt completely to liquid；
Step 2 hybrid reaction：The liquid of the petrolatum of above-mentioned thawing to liquid, white oil, Nano-Zinc, essential oil is added into reaction
Kettle, stirs, and at 132 DEG C, pressure is 4 kilograms for reaction temperature control, and the reaction time is 30 minutes；
Step 3 is cooled down：By above-mentioned reacted liquid cooling to 75 DEG C, reacted liquid is flowed into bottle and fills interior, be cooled to often
Temperature obtains cold-resistant heat-resisting application that various screen packs, air purifier filtration core, air-conditioning filter net, window are husky, door and window is husky receives
Rice applies glue spraying.
Claims (2)
1. a kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying, it is characterised in that be made up of by weight following raw materials according：
It is 5-35 grams of polyisobutene, 8-45 grams of Tissuemat E, 6-25 grams of petrolatum, 4-21 grams of slack wax, 5-18 grams of white oil, loose
6-16 grams of wax, 3-15 grams of microwax, 0.01-1 grams of Nano-Zinc, 5-25 grams of essential oil.
2. a kind of nanometer of screen pack deodorizing sterilizing purification according to claim 1 applies the preparation method of glue spraying, its feature
It is step as follows：
Step 1 is melted：By 5-35 grams of raw material polyisobutene, 8-45 grams of Tissuemat E, 6-25 grams of petrolatum, slack wax 4-21
Gram, 5-18 grams of white oil, 6-16 grams of slack wax, 3-15 grams of microwax, 0.01-1 grams of Nano-Zinc, 5-25 grams of essential oil；Carry out respectively
Water-bath or oil bath heating, treat to melt completely to liquid；
Step 2 hybrid reaction：By the polyisobutene of above-mentioned thawing to liquid, ethylene waxes, petrolatum, frivolous under normal temperature, normal pressure
Slack wax, white oil, slack wax, microwax, Nano-Zinc, the liquid of essential oil add reactor, stir, and reaction temperature control exists
123-142 DEG C, pressure is 4-7 kilograms, and the reaction time is 20-50 minutes；
Step 3 is cooled down：By above-mentioned reacted liquid cooling to 75 DEG C, reacted liquid is flowed into bottle and fills interior, be cooled to often
Temperature obtains cold-resistant heat-resisting application that various screen packs, air purifier filtration core, air-conditioning filter net, window are husky, door and window is husky receives
Rice applies glue spraying.
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| CN201710104959.3A CN106833148A (en) | 2017-02-25 | 2017-02-25 | A kind of nanometer of screen pack deodorizing sterilizing purification applies glue spraying and preparation method thereof |
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Cited By (1)
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Application publication date: 20170613 |