CN106833039A - A kind of molten moisture film and preparation method thereof - Google Patents
A kind of molten moisture film and preparation method thereof Download PDFInfo
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- CN106833039A CN106833039A CN201710006495.2A CN201710006495A CN106833039A CN 106833039 A CN106833039 A CN 106833039A CN 201710006495 A CN201710006495 A CN 201710006495A CN 106833039 A CN106833039 A CN 106833039A
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- moisture film
- preparation
- molten moisture
- deionized water
- mixed liquor
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
Abstract
The invention discloses a kind of molten moisture film and preparation method thereof.The NaOH that mass fraction is 8% 14% is put into deionized water, then the potassium permanganate that mass fraction is 0.4% 0.6% is put into deionized water again, react 5 10 minutes, last the potassium hydroxide that mass fraction is 0.8% 1.2% is put into deionized water again, reaction is obtained electrostatic liquid after 5 10 minutes；Mixed liquor is obtained after electrostatic liquid is mixed with petroleum ether, electrostatic liquid is 8 with the mass ratio of petroleum ether:1‑12:1；Mixed liquor is smeared, baking is obtained molten moisture film after 20 40 minutes at a temperature of 35 DEG C 45 DEG C.The raw material proportioning provided by the present invention and molten moisture film obtained in preparation method, it has good adhesion and adhesive force, soluble in water, will not remain in contact medium surface.
Description
Technical field
The present invention relates to a kind of molten moisture film and preparation method thereof.
Background technology
In existing glass production line, what glass was usually linearly transmitted, therefore edging chamfer mechanism can only be right
Two relative sides of glass are processed.Glass is turned to, it is necessary to pass through steering mechanism after completion of processing, to process glass
The two other side of glass.And glass is captured by steering mechanism and is turned to, impression easily is left in glass surface, to glass product
Quality and subsequent detection processing impact, it is therefore desirable to smear a kind of with good attached on the manipulator of steering mechanism
Put forth effort and medium soluble in water.
The content of the invention
It is an object of the invention to provide a kind of with good adhesive force and molten moisture film soluble in water and preparation method thereof.
First purpose of the invention is to provide a kind of preparation method of molten moisture film.
To reach above-mentioned purpose, the technical solution adopted by the present invention is：
A kind of preparation method of molten moisture film, comprises the following steps：
（1）By mass fraction it is again then 0.4%-0.6% by mass fraction for the NaOH of 8%-14% is put into deionized water
Potassium permanganate be put into the deionized water, react 5-10 minute, finally again by mass fraction be 0.8%-1.2% hydroxide
Potassium is put into the deionized water, and reaction is obtained electrostatic liquid after 5-10 minutes；
（2）Mixed liquor is obtained after the electrostatic liquid is mixed with petroleum ether, the electrostatic liquid is with the mass ratio of the petroleum ether
8:1-12:1；
（3）The mixed liquor is smeared, the prepared molten moisture film after baking 20-40 minute at a temperature of 35 DEG C -45 DEG C.
Preferably, in the step（3）In continue to smear the mixed liquor on the obtained molten moisture film, then 35 DEG C-
Toasted 20-40 minutes at a temperature of 45 DEG C, repeat the step 2-3 times.
Preferably, the mass fraction of the NaOH is 10%-12%.
Preferably, the mass fraction of the potassium permanganate is 0.5%.
Preferably, the mass fraction of the potassium hydroxide is 1%.
Preferably, the electrostatic liquid and the mass ratio of the petroleum ether are 10:1.
Preferably, in the step（3）In, the temperature for toasting the mixed liquor is 40 DEG C, toast the mixed liquor when
Between be 30 minutes.
Preferably, the resistivity of the deionized water is 1*10-18Ω·m。
Second object of the present invention is to provide a kind of using molten moisture film obtained in above-mentioned preparation method.
Due to the utilization of above-mentioned technical proposal, the present invention has following advantages compared with prior art：It is of the invention a kind of molten
Moisture film and preparation method thereof, the raw material proportioning provided by the present invention and molten moisture film obtained in preparation method, it has good
It is adhesion and adhesive force, soluble in water, contact medium surface will not be remained in.
Specific embodiment
Below by specific embodiment, the present invention is described in detail, but these exemplary embodiments are not to this
The real protection scope of invention constitutes any type of any restriction.
Embodiment 1：A kind of preparation method of molten moisture film, comprises the following steps：
（1）The NaOH that mass fraction is 10% is put into resistivity for 1*10-18In the deionized water of Ω m, then again will
Mass fraction is that 0.45% potassium permanganate is put into deionized water, reacts 5 minutes, finally again by hydrogen that mass fraction is 0.9%
Potassium oxide is put into deionized water, and reaction is obtained electrostatic liquid after 8 minutes；
（2）Mixed liquor is obtained after electrostatic liquid is mixed with petroleum ether, wherein electrostatic liquid and the mass ratio of petroleum ether is 9:1；
（3）The mixed liquor is smeared, baking is obtained molten moisture film after 28 minutes at a temperature of 39 DEG C；
（4）In step（3）In continue on obtained molten moisture film to smear mixed liquor, then toasted 28 minutes at a temperature of 39 DEG C, weight
Multiple step 2 time.Make the adhesive force of obtained molten moisture film more preferable.
The proportion of molten moisture film obtained in the preparation method be 1.01,20 DEG C at pH value between 7-8, sheet resistance is 1*
107Ω。
Embodiment 2：A kind of preparation method of molten moisture film, comprises the following steps：
（1）The NaOH that mass fraction is 11% is put into resistivity for 1*10-18In the deionized water of Ω m, then again will
Mass fraction is that 0.5% potassium permanganate is put into deionized water, reacts 6 minutes, finally again by hydroxide that mass fraction is 1%
Potassium is put into deionized water, and reaction is obtained electrostatic liquid after 6 minutes；
（2）Mixed liquor is obtained after electrostatic liquid is mixed with petroleum ether, wherein electrostatic liquid and the mass ratio of petroleum ether is 10:1；
（3）The mixed liquor is smeared, baking is obtained molten moisture film after 30 minutes at a temperature of 40 DEG C；
（4）In step（3）In continue on obtained molten moisture film to smear mixed liquor, then toasted 30 minutes at a temperature of 40 DEG C, weight
Multiple step 3 time.Make the adhesive force of obtained molten moisture film more preferable.
The above embodiments merely illustrate the technical concept and features of the present invention, its object is to allow person skilled in the art
Scholar will appreciate that present disclosure and be carried out that it is not intended to limit the scope of the present invention, all according to the present invention
The equivalent change or modification that Spirit Essence is made, should all cover within the scope of the present invention.
Claims (9)
1. a kind of preparation method of molten moisture film, it is characterised in that：Comprise the following steps：
（1）By mass fraction it is again then 0.4%-0.6% by mass fraction for the NaOH of 8%-14% is put into deionized water
Potassium permanganate be put into the deionized water, react 5-10 minute, finally again by mass fraction be 0.8%-1.2% hydroxide
Potassium is put into the deionized water, and reaction is obtained electrostatic liquid after 5-10 minutes；
（2）Mixed liquor is obtained after the electrostatic liquid is mixed with petroleum ether, the electrostatic liquid is with the mass ratio of the petroleum ether
8:1-12:1；
（3）The mixed liquor is smeared, the prepared molten moisture film after baking 20-40 minute at a temperature of 35 DEG C -45 DEG C.
2. the preparation method of a kind of molten moisture film according to claim 1, it is characterised in that：In the step（3）In be obtained
Described molten moisture film on continue to smear the mixed liquor, then toasted 20-40 minute at a temperature of 35 DEG C -45 DEG C, repeatedly the step
It is rapid 2-3 times.
3. the preparation method of a kind of molten moisture film according to claim 1, it is characterised in that：The quality of the NaOH point
Number is 10%-12%.
4. the preparation method of a kind of molten moisture film according to claim 1, it is characterised in that：The quality of the potassium permanganate point
Number is 0.5%.
5. the preparation method of a kind of molten moisture film according to claim 1, it is characterised in that：The quality of the potassium hydroxide point
Number is 1%.
6. the preparation method of a kind of molten moisture film according to claim 1, it is characterised in that：The electrostatic liquid and the oil
The mass ratio of ether is 10:1.
7. the preparation method of a kind of molten moisture film according to claim 1, it is characterised in that：In the step（3）In, baking
The temperature of the mixed liquor is 40 DEG C, and the time for toasting the mixed liquor is 30 minutes.
8. the preparation method of a kind of molten moisture film according to claim 1, it is characterised in that：The resistivity of the deionized water
It is 1*10-18Ω·m。
9. molten moisture film obtained in the preparation method according to any one of claim 1-8.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710006495.2A CN106833039B (en) | 2017-01-05 | 2017-01-05 | A kind of molten moisture film and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710006495.2A CN106833039B (en) | 2017-01-05 | 2017-01-05 | A kind of molten moisture film and preparation method thereof |
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| Publication Number | Publication Date |
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| CN106833039A true CN106833039A (en) | 2017-06-13 |
| CN106833039B CN106833039B (en) | 2019-04-16 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1609146A (en) * | 2003-06-30 | 2005-04-27 | 有限会社和幸 | Inorganic paint composition |
| CN103058528A (en) * | 2012-12-24 | 2013-04-24 | 广州市平驰国际贸易有限公司 | Waterproof and oilproof glass water-drawing agent, preparation method thereof and application method thereof |
| CN104073369A (en) * | 2014-06-30 | 2014-10-01 | 黄惠娟 | Traceless detergent for automobile glass |
| CN105238355A (en) * | 2015-10-26 | 2016-01-13 | 陈麒雅 | Long-acting glass antifog membrane and preparation method thereof |
| US20160177116A1 (en) * | 2014-12-22 | 2016-06-23 | Koji Katsuragi | Image forming set, image forming apparatus, and image forming method |
-
2017
- 2017-01-05 CN CN201710006495.2A patent/CN106833039B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1609146A (en) * | 2003-06-30 | 2005-04-27 | 有限会社和幸 | Inorganic paint composition |
| CN103058528A (en) * | 2012-12-24 | 2013-04-24 | 广州市平驰国际贸易有限公司 | Waterproof and oilproof glass water-drawing agent, preparation method thereof and application method thereof |
| CN104073369A (en) * | 2014-06-30 | 2014-10-01 | 黄惠娟 | Traceless detergent for automobile glass |
| US20160177116A1 (en) * | 2014-12-22 | 2016-06-23 | Koji Katsuragi | Image forming set, image forming apparatus, and image forming method |
| CN105238355A (en) * | 2015-10-26 | 2016-01-13 | 陈麒雅 | Long-acting glass antifog membrane and preparation method thereof |
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|---|---|
| CN106833039B (en) | 2019-04-16 |
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