CN106829071A - A kind of carbon tetrachloride standard specimen automatic packaging system and its method of work - Google Patents
A kind of carbon tetrachloride standard specimen automatic packaging system and its method of work Download PDFInfo
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- CN106829071A CN106829071A CN201611176120.2A CN201611176120A CN106829071A CN 106829071 A CN106829071 A CN 106829071A CN 201611176120 A CN201611176120 A CN 201611176120A CN 106829071 A CN106829071 A CN 106829071A
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- packaging machine
- roller
- standard specimen
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- dimethyl
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B51/00—Devices for, or methods of, sealing or securing package folds or closures; Devices for gathering or twisting wrappers, or necks of bags
- B65B51/04—Applying separate sealing or securing members, e.g. clips
- B65B51/06—Applying adhesive tape
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65H—HANDLING THIN OR FILAMENTARY MATERIAL, e.g. SHEETS, WEBS, CABLES
- B65H35/00—Delivering articles from cutting or line-perforating machines; Article or web delivery apparatus incorporating cutting or line-perforating devices, e.g. adhesive tape dispensers
- B65H35/0006—Article or web delivery apparatus incorporating cutting or line-perforating devices
- B65H35/002—Hand-held or table apparatus
- B65H35/0026—Hand-held or table apparatus for delivering pressure-sensitive adhesive tape
- B65H35/0033—Hand-held or table apparatus for delivering pressure-sensitive adhesive tape and affixing it to a surface
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65H—HANDLING THIN OR FILAMENTARY MATERIAL, e.g. SHEETS, WEBS, CABLES
- B65H35/00—Delivering articles from cutting or line-perforating machines; Article or web delivery apparatus incorporating cutting or line-perforating devices, e.g. adhesive tape dispensers
- B65H35/0006—Article or web delivery apparatus incorporating cutting or line-perforating devices
- B65H35/0073—Details
- B65H35/008—Arrangements or adaptations of cutting devices
Abstract
The invention discloses a kind of carbon tetrachloride standard specimen automatic packaging system and its method of work, by main body rack, master roller, control centre, preceding auxiliary roller-way, clamping device, universal wheel, afterwards auxiliary electric machines for roller, auxiliary roller-way, packaging mechanism are constituted afterwards；The main body rack is provided with master roller and clamping device；Auxiliary roller-way aids in roller-way with rear before the main body rack is respectively arranged at two ends with, wherein auxiliary roller-way side aids in electric machines for roller after being disposed with afterwards, aids in electric machines for roller to aid in roller-way drive connection with rear afterwards；The clamping device top is equipped with packaging mechanism；The universal wheel is located at main body rack corner, and universal wheel is welded and fixed with main body rack；The control centre is located at preceding auxiliary roller-way bottom；A kind of carbon tetrachloride standard specimen automatic packaging system of the present invention, the plant automation degree is high, and stable, high working efficiency greatly reduces labour intensity；The device uses moveable mode, and floor space is small, and Operation and Maintenance is simple, strong adaptability.
Description
Technical field
The invention belongs to sealed in unit field, and in particular to a kind of carbon tetrachloride standard specimen automatic packaging system and its work side
Method.
Background technology
At present when enterprise carries out pattern detection, it is necessary to the standard specimen that is fabricated to producing, and packing envelope is carried out to standard specimen
Dress, and traditional packing packaged type is carried out by manpower mostly, the mode packed by manpower not only it is time-consuming compared with
Long, packing efficiency is low, and has a strong impact on the measure of standard specimen after packing；With the development of technology, manual packaging machine meet the tendency of and
Raw, manual packaging machine main composition part is base, and connecting rod is provided with base, and pressure roller, pressure roller two ends are connected in connecting rod
Blade is provided with, in encapsulation process, manual packaging machine can be packaged to standard specimen, covers adhesive tape, cut off adhesive tape, it has knot
Structure is simple, the characteristics of easy to operate, but is monitored on line on a large scale in enterprise, the encapsulation operation time of this manual packaging machine
More long, automaticity is not high, increased the work operation and labour intensity of operator, can not meet enterprise's production
Need.
The content of the invention
In order to solve the above-mentioned technical problem, the present invention provides a kind of carbon tetrachloride standard specimen automatic packaging system, including：Main body
Support 1, master roller 2, control centre 3, preceding auxiliary roller-way 4, clamping device 5, universal wheel 6 aids in electric machines for roller 7, aids in afterwards afterwards
Roller-way 8, packaging mechanism 9；The main body rack 1 is provided with master roller 2 and clamping device 5, and master roller 2 is rolled with main body rack 1
Connection, clamping device 5 is fixedly connected with main body rack 1；The main body rack 1 is respectively arranged at two ends with preceding auxiliary roller-way 4 and rear auxiliary
Roller-way 8 is helped, wherein auxiliary roller-way 8 side aids in electric machines for roller 7 after being disposed with afterwards, electric machines for roller 7 is aided in afterwards with rear auxiliary roller-way 8
Drive connection；The top of the clamping device 5 is equipped with packaging mechanism 9, and packaging mechanism 9 is fixedly connected with main body rack 1；It is described universal
Wheel 6 is located at 1 four jiaos of main body rack, and the quantity of universal wheel 6 is 4, and universal wheel 6 is welded and fixed with main body rack 1；The control centre
3 are located at preceding auxiliary roller-way 4 bottom, and control centre 3 controls to be connected by wire with rear auxiliary electric machines for roller 7.
Further, the clamping device 5 includes：Grip block 5-1, belt motor 5-2, belt 5-3, power transmission shaft 5-4, folder
Hold limiter 5-5, standard specimen detector 5-6, clamping board motor 5-7；The grip block 5-1 quantity is 2, wherein grip block 5-1
It is provided with belt 5-3；The grip block 5-1 bottom ends are provided with power transmission shaft 5-4, and power transmission shaft 5-4 is rolled with main body rack 1 and connected
Connect, the grip block 5-1 bottoms other end is provided with belt motor 5-2, belt motor 5-2 and belt 5-3 drive connections；The grip block
Motor 5-7 is located at power transmission shaft 5-4 one end, and clamping board motor 5-7 is fixedly connected with main body rack 1；One of grip block
5-1 one end is provided with clamping limiter 5-5 and standard specimen detector 5-6；
The belt motor 5-2, clamping limiter 5-5, standard specimen detector 5-6 and clamping board motor 5-7 are by wire and control
The control of center processed 3 is connected.
Further, the packaging mechanism 9 includes：Upper packaging machine 9-1, upper packaging machine motor 9-2, upper packaging machine are consolidated
Determine frame 9-3, displacement traveller 9-4, lower packaging machine 9-5, shield 9-6, manual spacing left regulation wheel 9-7, upper packaging machine limiter 9-8；
Pressure sensor is provided with inside the displacement traveller 9-4, displacement traveller 9-4 bottom centers are provided with lower packaging machine 9-5, top one end
Packaging machine motor 9-2 is provided with, the top other end is provided with packaging machine limiter 9-8, wherein lower packaging machine 9-5 and displacement
Traveller 9-4 is fixedly connected, and decrease speed sensor is provided with inside lower packaging machine 9-5, and upper packaging machine motor 9-2 is slided with displacement
Post 9-4 drive connections；The lower packaging machine 9-5 tops are disposed with packaging machine fixed mount 9-3, on upper packaging machine fixed mount 9-3
Packaging machine 9-1 is provided with, rate of climb sensor is provided with inside upper packaging machine 9-1, wherein upper packaging machine fixed mount 9-3 and displacement
Traveller 9-4 is slidably connected, and upper packaging machine 9-1 is fixedly connected with upper packaging machine fixed mount 9-3；The upper packaging machine fixed mount 9-3
Front side center is provided with shield 9-6, and shield 9-6 both sides are equipped with manual spacing left regulation wheel 9-7, wherein manually spacing left regulation wheel 9-7 with
Upper packaging machine fixed mount 9-3 is slidably connected, and shield 9-6 is welded and fixed with upper packaging machine fixed mount 9-3；
The pressure sensor, decrease speed sensor, rate of climb sensor, upper packaging machine motor 9-2 and upper encapsulation
Machine limiter 9-8 controls to be connected by wire with control centre 3.
Further, the lower packaging machine 9-5 includes：Framework 9-5-1, adhesive tape fast pulley 9-5-2, adjust spring 9-5-3,
Tensioning wheel 9-5-4, cutter head 9-5-5, stopper slot 9-5-6, directional wheel 9-5-7；The framework 9-5-1 tops are provided with adhesive tape fast pulley
9-5-2, framework 9-5-1 bottoms two ends are provided with tensioning wheel 9-5-4 and directional wheel 9-5-7, wherein tensioning wheel 9-5-4 and framework 9-5-
1 chain connection；Described regulation spring 9-5-3 one end is located on tensioning wheel 9-5-4, and the other end is located on framework 9-5-1；Regulation bullet
Tensioned sensor is provided with inside spring (9-5-3)；The framework 9-5-1 bottom centre is provided with cutter head 9-5-5 and stopper slot 9-
5-6, cutter head 9-5-5 and stopper slot 9-5-6 are fixedly connected with framework 9-5-1.
Further, the adhesive tape fast pulley 9-5-2 is molded by macromolecular material pressing mold, the group of adhesive tape fast pulley 9-5-2
It is as follows into composition and manufacturing process：
First, adhesive tape fast pulley 9-5-2 constituents：
Count by weight, 4- [(5- cyano group -1,6- dihydros -2- hydroxyl-Isosorbide-5-Nitrae-dimethyl -6- oxo -3- pyridine radicals) azo]
72~155 parts of benzoic acid -2- phenoxyethyl acrylates, 128~215 parts of peroxide dioctyl phthalate -4- (1,1- dimethylethyl) hexamethylene diester,
1- carbamic acids 3- (2- methoxycarbonyl phenoxies) -86~165 parts of 1,2-PD ester, 2,2'- (3,3'- bis- chloro- 1,1'- biphenyl -4,
4'- bisazos) 213~288 parts of double [N- (2- methoxyphenyls) -3- oxo-butyramides], 6,6'(2,2'- dimethoxy-4 's,
4'- biphenylenes bisazo) 278~350 parts of two-(naphthalene disulfonate of 5- hydroxyl -4- amino 1,3), cyano group-(3- phenoxy group benzene
Base) methyl -3- (2,2- dichloroethylene) -66~81 parts of 2,2- dimethyl cyclopropane carboxylic acids ester, concentration is 67ppm~85ppm
N- (4- hydroxy phenyls methylene) 179~241 parts of-P-nethoxyaniline, 3,5- double (1,1- dimethyl ethyl) -4- hydroxy benzenes
Formic acid -2, double 254~367 parts of (1, the 1- dimethyl propyl) phenyl esters of 4-, 3,3'- [[3,3'- dimethyl (1,1'- biphenyl) -4,4'-
Diyl] double (azos)] double (4- amino -1-naphthalene sulfonic aicd) 269~398 parts of disodium salts, 70~154 parts of crosslinking agent, 4- hydroxyl -3- first
79~152 parts of epoxide benzyl carbinol, 230~281 parts of carbon peroxy acid-O, O- (1,1- dimethyl propyl)-O- (2- ethylhexyls) ester,
211~285 parts of 2,2- dimethyl -3- (2- methyl-1-propylenes base)-cyclopropane-carboxylic acid cyano group (3- Phenoxyphenyls) methyl esters；
The crosslinking agent is 5- benzyloxy -3- indolecarboxaldehydes, 3- methoxyl groups dopamine hydrochloride, 4- benzyloxy -3- indole acetonitriles
In any one；
2nd, the manufacturing process of adhesive tape fast pulley 9-5-2, comprises the steps of：
1st step：1350~2460 parts of ultra-pure water for adding electrical conductivity to be 6.56 μ S/cm~8.46 μ S/cm in a kettle., starts
Agitator in reactor, rotating speed is 98rpm~126rpm, starts heat pump, reactor temperature is risen to 89 DEG C~142
℃；Sequentially add 4- [(5- cyano group -1,6- dihydro -2- hydroxyl -1,4- dimethyl -6- oxo -3- pyridine radicals) azo] benzoic acid -
2- phenoxyethyl acrylates, peroxide dioctyl phthalate -4- (1,1- dimethylethyls) hexamethylene diester, 1- carbamic acids 3- (2- methoxycarbonyl phenoxies) -
1,2-PD ester, to being completely dissolved, regulation pH value is 8.8~10.6 for stirring, by agitator speed be adjusted to 152rpm~
213rpm, temperature is 124 DEG C~176 DEG C, esterification 8~18 hours；
2nd step：Take 2,2'- (the chloro- 1,1'- biphenyl -4,4'- bisazos of 3,3'- bis-) it is double [N- (2- methoxyphenyls) -3- oxos -
Butyramide], 6,6'(2,2'- dimethoxy-4 's, 4'- biphenylenes bisazo) the two-(naphthalenedisulfonic acid of 5- hydroxyl -4- amino 1,3
Sodium) to be crushed, powder diameter is 1000~1300 mesh；Add cyano group-(3- Phenoxyphenyls) methyl -3- (chloroethenes of 2,2- bis-
Alkenyl) -2,2- dimethyl cyclopropane carboxylic acids ester be well mixed, be laid in pallet, tiling thickness be 25mm~45mm, using agent
Measure for 10.3kGy~15.6kGy, energy for the alpha ray of 7.6MeV~13.5MeV is irradiated 200~300 minutes, and equal agent
The β x ray irradiation xs of amount 100~200 minutes；
3rd step：The mixed-powder processed through the 2nd step is dissolved in N- (4- hydroxy phenyls methylene)-P-nethoxyaniline, is added anti-
Kettle is answered, agitator speed is 263rpm~356rpm, and temperature is 168 DEG C~263 DEG C, and starting vavuum pump makes the vacuum of reactor
- 0.51MPa~2.65MPa is reached, this state response is kept 11~25 hours；Pressure release is simultaneously passed through radon gas, makes reacting kettle inner pressure
It is 1.37MPa~2.64MPa, insulation stands 15~24 hours；Agitator speed is promoted to 364rpm~420rpm, simultaneous reactions
Kettle pressure release is to 0MPa；Sequentially add 3,5- double (the 1,1- dimethyl propylenes of double (1,1- dimethyl ethyls) -4-HBA -2,4-
Base) phenyl ester, 3,3'- [[3,3'- dimethyl (1,1'- biphenyl) -4,4'- diyls] double (azos)] double (4- amino -1-naphthalene sulfonic aicd)
After disodium salt is completely dissolved, crosslinking agent stirring mixing is added so that the hydrophilic lipophilic balance of reactor solution is 6.2~8.4,
Insulation stands 13~22 hours；
4th step：When agitator speed is 284rpm~365rpm, 4- hydroxy 3-methoxybenzenes ethanol, carbon peroxide are sequentially added
Acid-O, O- (1,1- dimethyl propyls)-O- (2- ethylhexyls) esters and 2,2- dimethyl -3- (2- methyl-1-propylenes base)-ring third
Alkane carboxylic acid cyano group (3- Phenoxyphenyls) methyl esters, lifts reactor pressure, reaches 1.63MPa~2.75MPa, and temperature is
215 DEG C~286 DEG C, polymerisation 26~34 hours；Reacting kettle inner pressure is down to 0MPa after the completion of reaction, be cooled to 30 DEG C~
38 DEG C, discharging enters molding press and can be prepared by adhesive tape fast pulley 9-5-2.
Further, the invention also discloses a kind of method of work of carbon tetrachloride standard specimen automatic packaging system, the method
Including following steps：
1st step：Power-on, now standard specimen detector 5-6 real-time detections whether there is standard specimen to pass through, when standard specimen detector 5-6 inspection
When measuring standard specimen and passing through, standard specimen detector 5-6 produces electric signal transmission to control centre 3, control centre 3 control belt motor 5-
2 start with rear auxiliary electric machines for roller 7, and belt motor 5-2 drives standard specimen movement by belt 5-3；Now go up packaging machine 9-1 and under
Packaging machine 9-5 aids in roller-way 8 to be delivered to next work as standard specimen movement is by tape-stripping to standard specimen specified location, and after passing through
Position；
2nd step：When standard specimen lateral dimension changes, now staff is controlled inside clamping device 5 by control centre 3
Clamping board motor 5-7 start, clamping board motor 5-7 by power transmission shaft 5-4 drive two grip block 5-1 away from or be close to,
Realize the change of clamp distance；In grip block 5-1 displacement process, two grip block 5-1's of clamping limiter 5-5 real-time monitorings
Spacing, and produce electric signal to be sent to control centre 3, when grip block 5-1 is moved to extreme position, clamping limiter 5-5 is produced
Raw alarm signal is transmitted to control centre 3, and the control clamping board motor 5-7 of control centre 3 shuts down；
3rd step：When standard specimen longitudinal size changes, now staff is controlled inside packaging mechanism 9 by control centre 3
Upper packaging machine motor 9-2 start, upper packaging machine motor 9-2 fixed by packaging machine in displacement traveller 9-4 drives
Frame 9-3 is moved up and down, the change of packaging machine 9-1 and lower packaging machine 9-5 distances in realization；In upper packaging machine fixed mount 9-3 displacements
During, the position of packaging machine fixed mount 9-3 in upper packaging machine limiter 9-8 real-time monitorings, when upper packaging machine fixed mount 9-3
When moving to extreme position, upper packaging machine limiter 9-8 produces alarm signal to transmit to control centre 3, is sealed in the control of control centre 3
Installation motor 9-2 shuts down.
A kind of carbon tetrachloride standard specimen automatic packaging system disclosed by the invention, the advantage is that：
(1) the plant automation degree is high, and floor space is small, conveniently moving, strong adaptability；
(2) the device Operation and Maintenance is simple, low cost of manufacture；
(3) plant running stabilization, high working efficiency reduces the work operation and labour intensity of operator.
A kind of carbon tetrachloride standard specimen automatic packaging system of the present invention, the plant automation degree is high, stable,
High working efficiency, greatly reduces labour intensity；The device uses moveable mode, and floor space is small, and Operation and Maintenance is simple,
Strong adaptability.
Brief description of the drawings
Fig. 1 is a kind of heretofore described carbon tetrachloride standard specimen automatic packaging system structural representation.
Fig. 2 is heretofore described clamping device structural representation.
Fig. 3 is heretofore described packaging mechanism structural representation.
Fig. 4 is heretofore described lower packaging machine structure schematic diagram.
Fig. 5 is that heretofore described adhesive tape fast pulley fatigue performance changes over time figure.
In figure 1 above~Fig. 4, main body rack 1, master roller 2, control centre 3, preceding auxiliary roller-way 4, clamping device 5, clamping
Plate 5-1, belt motor 5-2, belt 5-3, power transmission shaft 5-4, clamp limiter 5-5, standard specimen detector 5-6, clamping board motor 5-
7, universal wheel 6 aids in electric machines for roller 7 afterwards, and roller-way 8, packaging mechanism 9, upper packaging machine 9-1, upper packaging machine motor are aided in afterwards
9-2, upper packaging machine fixed mount 9-3, displacement traveller 9-4, lower packaging machine 9-5, framework 9-5-1, adhesive tape fast pulley 9-5-2, regulation
Spring 9-5-3, tensioning wheel 9-5-4, cutter head 9-5-5, stopper slot 9-5-6, directional wheel 9-5-7, shield 9-6, manual spacing regulation
Wheel 9-7, upper packaging machine limiter 9-8.
Specific embodiment
A kind of carbon tetrachloride standard specimen automatic packaging system for providing the present invention with reference to the accompanying drawings and examples enters to advance
One step explanation.
As shown in figure 1, being a kind of heretofore described carbon tetrachloride standard specimen automatic packaging system structural representation.From figure
Find out in 1, including：Main body rack 1, master roller 2, control centre 3, preceding auxiliary roller-way 4, clamping device 5, universal wheel 6 is aided in afterwards
Electric machines for roller 7, aid in roller-way 8, packaging mechanism 9 afterwards；The main body rack 1 is provided with master roller 2 and clamping device 5, master roller 2
Rolled with main body rack 1 and be connected, clamping device 5 is fixedly connected with main body rack 1；Before the main body rack 1 is respectively arranged at two ends with
Auxiliary roller-way 4 and rear auxiliary roller-way 8, wherein auxiliary roller-way 8 side aids in electric machines for roller 7 after being disposed with afterwards, aid in roller-way electricity afterwards
Machine 7 and the rear auxiliary drive connection of roller-way 8；The top of the clamping device 5 is equipped with packaging mechanism 9, packaging mechanism 9 and main body rack 1
It is fixedly connected；The universal wheel 6 is located at 1 four jiaos of main body rack, and the quantity of universal wheel 6 is 4, and universal wheel 6 is welded with main body rack 1
It is fixed；The control centre 3 is located at preceding auxiliary roller-way 4 bottom, and control centre 3 is controlled by wire with rear auxiliary electric machines for roller 7
It is connected.
As shown in Fig. 2 being heretofore described clamping device structural representation.Find out from Fig. 2 or Fig. 1, clamping machine
Structure 5 includes：Grip block 5-1, belt motor 5-2, belt 5-3, power transmission shaft 5-4, clamp limiter 5-5, standard specimen detector 5-6,
Clamping board motor 5-7；The grip block 5-1 quantity is 2, and wherein grip block 5-1 is provided with belt 5-3；The grip block 5-1
Bottom end is provided with power transmission shaft 5-4, and power transmission shaft 5-4 is rolled with main body rack 1 and is connected, and the grip block 5-1 bottoms other end is provided with skin
Translator 5-2, belt motor 5-2 and belt 5-3 drive connections；The clamping board motor 5-7 is located at power transmission shaft 5-4 one end, folder
Board motor 5-7 is held to be fixedly connected with main body rack 1；Described one of grip block 5-1 one end is provided with clamping limiter 5-5 and mark
Sample detector 5-6；
The belt motor 5-2, clamping limiter 5-5, standard specimen detector 5-6 and clamping board motor 5-7 are by wire and control
The control of center processed 3 is connected.
As shown in figure 3, being heretofore described packaging mechanism structural representation.Find out from Fig. 3 or Fig. 1, packaging machine
Structure 9 includes：Upper packaging machine 9-1, upper packaging machine motor 9-2, upper packaging machine fixed mount 9-3, displacement traveller 9-4, lower encapsulation
Machine 9-5, shield 9-6, manual spacing left regulation wheel 9-7, upper packaging machine limiter (9-8)；Pressure is provided with inside the displacement traveller 9-4
Force snesor, displacement traveller 9-4 bottom centers are provided with lower packaging machine 9-5, and top one end is provided with packaging machine motor 9-2,
The top other end is provided with packaging machine limiter 9-8, wherein lower packaging machine 9-5 is fixedly connected with displacement traveller 9-4, lower packaging machine
Decrease speed sensor, upper packaging machine motor 9-2 and displacement traveller 9-4 drive connections are provided with inside 9-5；The lower encapsulation
Machine 9-5 tops are disposed with packaging machine fixed mount 9-3, upper packaging machine fixed mount 9-3 and are provided with packaging machine 9-1, upper packaging machine
Rate of climb sensor is provided with inside 9-1, wherein upper packaging machine fixed mount 9-3 and displacement traveller 9-4 is slidably connected, upper packaging machine
9-1 is fixedly connected with upper packaging machine fixed mount 9-3；The upper packaging machine fixed mount 9-3 front sides center is provided with shield 9-6, shield
9-6 both sides are equipped with manual spacing left regulation wheel 9-7, wherein spacing left regulation wheel 9-7 and upper packaging machine fixed mount 9-3 slides company manually
Connect, shield 9-6 is welded and fixed with upper packaging machine fixed mount 9-3；
The pressure sensor, decrease speed sensor, rate of climb sensor, upper packaging machine motor 9-2 and upper encapsulation
Machine limiter 9-8 controls to be connected by wire with control centre 3.
As shown in figure 4, being heretofore described lower packaging machine structure schematic diagram.As seen from Figure 4, lower packaging machine 9-5
Including：Framework 9-5-1, adhesive tape fast pulley 9-5-2, adjust spring 9-5-3, tensioning wheel 9-5-4, cutter head 9-5-5, stopper slot 9-5-
6, directional wheel 9-5-7；The framework 9-5-1 tops are provided with adhesive tape fast pulley 9-5-2, and framework 9-5-1 bottoms two ends are provided with tensioning
Wheel 9-5-4 and directional wheel 9-5-7, wherein tensioning wheel 9-5-4 and framework 9-5-1 chain connections；Described regulation spring 9-5-3 one end
On tensioning wheel 9-5-4, the other end is located on framework 9-5-1；Tensioned sensing is provided with inside regulation spring (9-5-3)
Device；The framework 9-5-1 bottom centre is provided with cutter head 9-5-5 and stopper slot 9-5-6, cutter head 9-5-5 and stopper slot 9-5-6 with
Framework 9-5-1 is fixedly connected.
A kind of course of work of carbon tetrachloride standard specimen automatic packaging system of the present invention is：
1st step：Power-on, now standard specimen detector 5-6 real-time detections whether there is standard specimen to pass through, when standard specimen detector 5-6 inspection
When measuring standard specimen and passing through, standard specimen detector 5-6 produces electric signal transmission to control centre 3, control centre 3 control belt motor 5-
2 start with rear auxiliary electric machines for roller 7, and belt motor 5-2 drives standard specimen movement by belt 5-3；Now go up packaging machine 9-1 and under
Packaging machine 9-5 aids in roller-way 8 to be delivered to next work as standard specimen movement is by tape-stripping to standard specimen specified location, and after passing through
Position；
2nd step：When standard specimen lateral dimension changes, now staff is controlled inside clamping device 5 by control centre 3
Clamping board motor 5-7 start, clamping board motor 5-7 by power transmission shaft 5-4 drive two grip block 5-1 away from or be close to,
Realize the change of clamp distance；In grip block 5-1 displacement process, two grip block 5-1's of clamping limiter 5-5 real-time monitorings
Spacing, and produce electric signal to be sent to control centre 3, when grip block 5-1 is moved to extreme position, clamping limiter 5-5 is produced
Raw alarm signal is transmitted to control centre 3, and the control clamping board motor 5-7 of control centre 3 shuts down；
3rd step：When standard specimen longitudinal size changes, now staff is controlled inside packaging mechanism 9 by control centre 3
Upper packaging machine motor 9-2 start, upper packaging machine motor 9-2 fixed by packaging machine in displacement traveller 9-4 drives
Frame 9-3 is moved up and down, the change of packaging machine 9-1 and lower packaging machine 9-5 distances in realization；In upper packaging machine fixed mount 9-3 displacements
During, the position of packaging machine fixed mount 9-3 in upper packaging machine limiter 9-8 real-time monitorings, when upper packaging machine fixed mount 9-3
When moving to extreme position, upper packaging machine limiter 9-8 produces alarm signal to transmit to control centre 3, is sealed in the control of control centre 3
Installation motor 9-2 shuts down.
A kind of carbon tetrachloride standard specimen automatic packaging system of the present invention, the plant automation degree is high, stable,
High working efficiency, greatly reduces labour intensity；The device uses moveable mode, and floor space is small, and Operation and Maintenance is simple,
Strong adaptability.
The following is the embodiment of the manufacturing process of adhesive tape fast pulley 9-5-2 of the present invention, embodiment is in order to further
Present disclosure is illustrated, but be should not be construed as limiting the invention.Without departing from the spirit and substance of the case in the present invention,
The modification and replacement made to the inventive method, step or condition, belong to the scope of the present invention.
If not specializing, the conventional meanses that technological means used is well known to those skilled in the art in embodiment.
Embodiment 1
Adhesive tape fast pulley 9-5-2 of the present invention is manufactured according to following steps, and is counted by weight：
1st step：1350 parts of the ultra-pure water that electrical conductivity is 6.56 μ S/cm is added in a kettle., starts agitator in reactor, turn
Speed is 98rpm, starts heat pump, reactor temperature is risen to 89 DEG C；Sequentially add 4- [(5- cyano group -1,6- dihydros -2-
Hydroxyl -1,4- dimethyl -6- oxo -3- pyridine radicals) azo] 72 parts of benzoic acid -2- phenoxyethyl acrylates, peroxide dioctyl phthalate -4-
128 parts of (1,1- dimethylethyl) hexamethylene diester, 1- carbamic acids 3- (2- methoxycarbonyl phenoxies) -86 parts of 1,2-PD ester, stirring is extremely
It is completely dissolved, regulation pH value is 8.8, agitator speed is adjusted to 152rpm, temperature is 124 DEG C, esterification 8 hours；
2nd step：Take 2,2'- (the chloro- 1,1'- biphenyl -4,4'- bisazos of 3,3'- bis-) it is double [N- (2- methoxyphenyls) -3- oxos -
Butyramide] 213 parts, 6,6'(2,2'- dimethoxy-4 's, 4'- biphenylenes bisazo) the two-(naphthalene two of 5- hydroxyl -4- amino 1,3
Sodium sulfonate) 278 parts crushed, powder diameter is 1000 mesh；Add cyano group-(3- Phenoxyphenyls) methyl -3- (2,2- dichloros
Vinyl) 66 parts of -2,2- dimethyl cyclopropane carboxylic acids ester is well mixed, is laid in pallet, and tiling thickness is 25mm, using agent
Measure for 10.3kGy, energy for the alpha ray of 7.6MeV is irradiated 200 minutes, and Isodose β x ray irradiation xs 100 minutes；
3rd step：The mixed-powder processed through the 2nd step is dissolved in the N- (4- hydroxy phenyls methylene)-to methoxyl group that concentration is 67ppm
In 179 parts of aniline, reactor is added, agitator speed is 263rpm, and temperature is 168 DEG C, and starting vavuum pump makes the true of reactor
Reciprocal of duty cycle reaches -0.51MPa, keeps this state response 11 hours；Pressure release is simultaneously passed through radon gas, makes reacting kettle inner pressure for 1.37MPa,
Insulation stands 15 hours；Agitator speed is promoted to 364rpm, simultaneous reactions kettle pressure release to 0MPa；Sequentially add 3,5- it is double (1,
1- dimethyl ethyls) -4-HBA -2,4- double 254 parts of (1,1- dimethyl propyls) phenyl ester, 3,3'- [[3,3'- dimethyl
(1,1'- biphenyl) -4,4'- diyls] double (azos)] after double (4- amino -1-naphthalene sulfonic aicd) 269 parts of disodium salts are completely dissolved, add
70 parts of stirring mixing of crosslinking agent so that the hydrophilic lipophilic balance of reactor solution is 6.2, and insulation stands 13 hours；
4th step：When agitator speed is 284rpm~365rpm, 79 parts of 4- hydroxy 3-methoxybenzenes ethanol, carbon are sequentially added
230 parts of peroxy acid-O, O- (1,1- dimethyl propyls)-O- (2- ethylhexyls) ester and 2,2- dimethyl -3- (2- methyl isophthalic acids-the third
Alkenyl) 211 parts of-cyclopropane-carboxylic acid cyano group (3- Phenoxyphenyls) methyl esters, reactor pressure is lifted, 1.63MPa is reached, temperature
It is 215 DEG C to spend, polymerisation 26 hours；Reacting kettle inner pressure is down to 0MPa after the completion of reaction, 30 DEG C are cooled to, discharging enters
Molding press can be prepared by adhesive tape fast pulley 9-5-2.
The crosslinking agent is 5- benzyloxy -3- indolecarboxaldehydes.
Embodiment 2
Adhesive tape fast pulley 9-5-2 of the present invention is manufactured according to following steps, and is counted by weight：
1st step：2460 parts of the ultra-pure water that electrical conductivity is 8.46 μ S/cm is added in a kettle., starts agitator in reactor, turn
Speed is 126rpm, starts heat pump, reactor temperature is risen to 142 DEG C；Sequentially add 4- [(5- cyano group -1,6- dihydros -
2- hydroxyl -1,4- dimethyl -6- oxo -3- pyridine radicals) azo] 155 parts of benzoic acid -2- phenoxyethyl acrylates, peroxide dioctyl phthalate -
215 parts of 4- (1,1- dimethylethyl) hexamethylene diester, 1- carbamic acids 3- (2- methoxycarbonyl phenoxies) -165 parts of 1,2-PD ester, stirring
To being completely dissolved, regulation pH value is 10.6, and agitator speed is adjusted into 213rpm, and temperature is 176 DEG C, esterification 18 hours；
2nd step：Take 2,2'- (the chloro- 1,1'- biphenyl -4,4'- bisazos of 3,3'- bis-) it is double [N- (2- methoxyphenyls) -3- oxos -
Butyramide] 288 parts, 6,6'(2,2'- dimethoxy-4 's, 4'- biphenylenes bisazo) the two-(naphthalene two of 5- hydroxyl -4- amino 1,3
Sodium sulfonate) 350 parts crushed, powder diameter is 1300 mesh；Add cyano group-(3- Phenoxyphenyls) methyl -3- (2,2- dichloros
Vinyl) 81 parts of -2,2- dimethyl cyclopropane carboxylic acids ester is well mixed, is laid in pallet, and tiling thickness is 45mm, using agent
Measure for 15.6kGy, energy for the alpha ray of 13.5MeV is irradiated 300 minutes, and Isodose β x ray irradiation xs 200 minutes；
3rd step：The mixed-powder processed through the 2nd step is dissolved in the N- (4- hydroxy phenyls methylene)-to methoxyl group that concentration is 85ppm
In 241 parts of aniline, reactor is added, agitator speed is 356rpm, and temperature is 263 DEG C, and starting vavuum pump makes the true of reactor
Reciprocal of duty cycle reaches 2.65MPa, keeps this state response 25 hours；Pressure release is simultaneously passed through radon gas, makes reacting kettle inner pressure for 2.64MPa,
Insulation stands 24 hours；Agitator speed is promoted to 420rpm, simultaneous reactions kettle pressure release to 0MPa；Sequentially add 3,5- it is double (1,
1- dimethyl ethyls) -4-HBA -2,4- double 367 parts of (1,1- dimethyl propyls) phenyl ester, 3,3'- [[3,3'- dimethyl
(1,1'- biphenyl) -4,4'- diyls] double (azos)] after double (4- amino -1-naphthalene sulfonic aicd) 398 parts of disodium salts are completely dissolved, add
154 parts of stirring mixing of crosslinking agent so that the hydrophilic lipophilic balance of reactor solution is 8.4, and insulation stands 22 hours；
4th step：Agitator speed be 365rpm when, sequentially add 152 parts of 4- hydroxy 3-methoxybenzenes ethanol, carbon peroxy acid-
281 parts of O, O- (1,1- dimethyl propyls)-O- (2- ethylhexyls) ester and 2,2- dimethyl -3- (2- methyl-1-propylenes base)-ring
285 parts of propanecarboxylic acid's cyano group (3- Phenoxyphenyls) methyl esters, lifts reactor pressure, reaches 2.75MPa, and temperature is 286
DEG C, polymerisation 34 hours；Reacting kettle inner pressure is down to 0MPa after the completion of reaction, 38 DEG C are cooled to, discharging enters molding press i.e.
Adhesive tape fast pulley 9-5-2 can be obtained.
The crosslinking agent is 4- benzyloxy -3- indole acetonitriles.
Embodiment 3
Adhesive tape fast pulley 9-5-2 of the present invention is manufactured according to following steps, and is counted by weight：
1st step：1900 parts of the ultra-pure water that electrical conductivity is 7.51 μ S/cm is added in a kettle., starts agitator in reactor, turn
Speed is 112rpm, starts heat pump, reactor temperature is risen to 116 DEG C；Sequentially add 4- [(5- cyano group -1,6- dihydros -
2- hydroxyl -1,4- dimethyl -6- oxo -3- pyridine radicals) azo] 113 parts of benzoic acid -2- phenoxyethyl acrylates, peroxide dioctyl phthalate -
171 parts of 4- (1,1- dimethylethyl) hexamethylene diester, 1- carbamic acids 3- (2- methoxycarbonyl phenoxies) -125 parts of 1,2-PD ester, stirring
To being completely dissolved, regulation pH value is 9.7, and agitator speed is adjusted into 182rpm, and temperature is 150 DEG C, esterification 13 hours；
2nd step：Take 2,2'- (the chloro- 1,1'- biphenyl -4,4'- bisazos of 3,3'- bis-) it is double [N- (2- methoxyphenyls) -3- oxos -
Butyramide] 250 parts, 6,6'(2,2'- dimethoxy-4 's, 4'- biphenylenes bisazo) the two-(naphthalene two of 5- hydroxyl -4- amino 1,3
Sodium sulfonate) 314 parts crushed, powder diameter is 1150 mesh；Add cyano group-(3- Phenoxyphenyls) methyl -3- (2,2- dichloros
Vinyl) 75 parts of -2,2- dimethyl cyclopropane carboxylic acids ester is well mixed, is laid in pallet, and tiling thickness is 35mm, using agent
Measure for 13.2kGy, energy for the alpha ray of 10.5MeV is irradiated 250 minutes, and Isodose β x ray irradiation xs 150 minutes；
3rd step：The mixed-powder processed through the 2nd step is dissolved in the N- (4- hydroxy phenyls methylene)-to methoxyl group that concentration is 76ppm
In 210 parts of aniline, reactor is added, agitator speed is 309rpm, and temperature is 218 DEG C, and starting vavuum pump makes the true of reactor
Reciprocal of duty cycle reaches 1.07MPa, keeps this state response 18 hours；Pressure release is simultaneously passed through radon gas, makes reacting kettle inner pressure for 2.01MPa,
Insulation stands 18 hours；Agitator speed is promoted to 395rpm, simultaneous reactions kettle pressure release to 0MPa；Sequentially add 3,5- it is double (1,
1- dimethyl ethyls) -4-HBA -2,4- double 310 parts of (1,1- dimethyl propyls) phenyl ester, 3,3'- [[3,3'- dimethyl
(1,1'- biphenyl) -4,4'- diyls] double (azos)] after double (4- amino -1-naphthalene sulfonic aicd) 333 parts of disodium salts are completely dissolved, add
112 parts of stirring mixing of crosslinking agent so that the hydrophilic lipophilic balance of reactor solution is 7.3, and insulation stands 17 hours；
4th step：Agitator speed be 224rpm when, sequentially add 115 parts of 4- hydroxy 3-methoxybenzenes ethanol, carbon peroxy acid-
255 parts of O, O- (1,1- dimethyl propyls)-O- (2- ethylhexyls) ester and 2,2- dimethyl -3- (2- methyl-1-propylenes base)-ring
248 parts of propanecarboxylic acid's cyano group (3- Phenoxyphenyls) methyl esters, lifts reactor pressure, reaches 2.19MPa, and temperature is 250
DEG C, polymerisation 30 hours；Reacting kettle inner pressure is down to 0MPa after the completion of reaction, 34 DEG C are cooled to, discharging enters molding press i.e.
Adhesive tape fast pulley 9-5-2 can be obtained.
The crosslinking agent is 3- methoxyl group dopamine hydrochlorides.
Reference examples
Reference examples are the adhesive tape fast pulley of commercially available certain brand.
Embodiment 4
The adhesive tape fast pulley described in adhesive tape fast pulley 9-5-2 and reference examples that embodiment 1~3 is prepared carries out using effect
Contrast.The two Poisson's ratio, elastic modelling quantity, heat distortion temperature, rate of ageing are counted, as a result as shown in table 1.
As seen from Table 1, adhesive tape fast pulley 9-5-2 of the present invention is its Poisson's ratio, elastic modelling quantity, heat distortion temperature, old
Change the product that the indexs such as speed are superior to prior art production.
Additionally, as shown in figure 5, being adhesive tape fast pulley 9-5-2 material fatigue performances of the present invention with use time
The statistics of change.Find out in figure, adhesive tape fast pulley 9-5-2 used by embodiment 1~3, its material fatigue performance is with use time
Intensity of variation is significantly better than existing product.
Claims (6)
1. a kind of carbon tetrachloride standard specimen automatic packaging system, including：Main body rack (1), master roller (2), control centre (3) is preceding
Auxiliary roller-way (4), clamping device (5), universal wheel (6) aids in electric machines for roller (7) afterwards, and roller-way (8), packaging mechanism are aided in afterwards
(9)；Characterized in that, the main body rack (1) is provided with master roller (2) and clamping device (5), master roller (2) and main body branch
Frame (1) rolls connection, and clamping device (5) is fixedly connected with main body rack (1)；Before the main body rack (1) is respectively arranged at two ends with
Auxiliary roller-way (4) and rear auxiliary roller-way (8), wherein auxiliary roller-way (8) side aids in electric machines for roller (7) afterwards after being disposed with, it is rear auxiliary
Electric machines for roller (7) are helped with rear auxiliary roller-way (8) drive connection；Clamping device (5) top is equipped with packaging mechanism (9), encapsulation
Mechanism (9) is fixedly connected with main body rack (1)；The universal wheel (6) is positioned at main body rack (1) corner, universal wheel (6) quantity
4, universal wheel (6) is welded and fixed with main body rack (1)；The control centre (3) is positioned at preceding auxiliary roller-way (4) bottom, control
Center (3) controls to be connected by wire with rear auxiliary electric machines for roller (7).
2. a kind of carbon tetrachloride standard specimen automatic packaging system according to claim 1, it is characterised in that the clamping device
(5) include：Grip block (5-1), belt motor (5-2), belt (5-3), power transmission shaft (5-4), clamping limiter (5-5), standard specimen
Detector (5-6), clamping board motor (5-7)；Grip block (5-1) quantity is 2, and wherein grip block (5-1) is provided with skin
Band (5-3)；Grip block (5-1) bottom end is provided with power transmission shaft (5-4), and power transmission shaft (5-4) is rolled with main body rack (1) and connected
Connect, grip block (5-1) bottom other end is provided with belt motor (5-2), belt motor (5-2) and belt (5-3) drive connection；Institute
State clamping board motor (5-7) and be located at power transmission shaft (5-4) one end, clamping board motor (5-7) is fixedly connected with main body rack (1)；Institute
State one of grip block (5-1) one end and be provided with clamping limiter (5-5) and standard specimen detector (5-6)；
The belt motor (5-2), clamping limiter (5-5), standard specimen detector (5-6) and clamping board motor (5-7) pass through
Wire controls to be connected with control centre (3).
3. a kind of carbon tetrachloride standard specimen automatic packaging system according to claim 1, it is characterised in that the packaging mechanism
(9) include：Upper packaging machine (9-1), upper packaging machine motor (9-2), upper packaging machine fixed mount (9-3), displacement traveller (9-
4), lower packaging machine (9-5), shield (9-6), manual spacing left regulation wheel (9-7), upper packaging machine limiter (9-8)；The displacement is slided
Pressure sensor is provided with inside post (9-4), displacement traveller (9-4) bottom center is provided with lower packaging machine (9-5), and top one end is provided with
Upper packaging machine motor (9-2), the top other end is provided with packaging machine limiter (9-8), wherein lower packaging machine (9-5) and position
Move traveller (9-4) to be fixedly connected, decrease speed sensor, upper packaging machine motor (9-2) are provided with inside lower packaging machine (9-5)
With displacement traveller (9-4) drive connection；Lower packaging machine (9-5) top is disposed with packaging machine fixed mount (9-3), upper encapsulation
Machine fixed mount (9-3) is provided with packaging machine (9-1), and rate of climb sensor is provided with inside upper packaging machine (9-1), wherein upper envelope
Installation fixed mount (9-3) is slidably connected with displacement traveller (9-4), and upper packaging machine (9-1) is fixed with upper packaging machine fixed mount (9-3)
Connection；Upper packaging machine fixed mount (9-3) the front side center is provided with shield (9-6), and shield (9-6) both sides are equipped with manual spacing tune
Section wheel (9-7), wherein manually spacing left regulation wheel (9-7) be slidably connected with upper packaging machine fixed mount (9-3), shield (9-6) with it is upper
Packaging machine fixed mount (9-3) is welded and fixed；
The pressure sensor, decrease speed sensor, rate of climb sensor, upper packaging machine motor (9-2) and upper envelope
Installation limiter (9-8) controls to be connected by wire with control centre (3).
4. a kind of carbon tetrachloride standard specimen automatic packaging system according to claim 3, it is characterised in that the lower packaging machine
(9-5) includes：Framework (9-5-1), adhesive tape fast pulley (9-5-2), regulation spring (9-5-3), tensioning wheel (9-5-4), cutter head (9-
5-5), stopper slot (9-5-6), directional wheel (9-5-7)；Framework (9-5-1) top is provided with adhesive tape fast pulley (9-5-2), glue
Speed probe is provided with inside band fast pulley (9-5-2), framework (9-5-1) bottom two ends are provided with tensioning wheel (9-5-4) and orientation
Wheel (9-5-7), wherein tensioning wheel (9-5-4) and framework (9-5-1) chain connection, are provided with rotating speed biography inside tensioning wheel (9-5-4)
Sensor；Described regulation spring (9-5-3) one end is located on tensioning wheel (9-5-4), and the other end is located on framework (9-5-1), regulation
Tensioned sensor is provided with inside spring (9-5-3)；Framework (9-5-1) bottom centre is provided with cutter head (9-5-5) and limit
Position groove (9-5-6), cutter head (9-5-5) and stopper slot (9-5-6) are fixedly connected with framework (9-5-1)；
Speed probe, tensioned sensor control to be connected by wire with control centre (3).
5. a kind of carbon tetrachloride standard specimen automatic packaging system according to claim 4, it is characterised in that the adhesive tape is fixed
Wheel (9-5-2) is molded by macromolecular material pressing mold, and the constituent and manufacturing process of adhesive tape fast pulley (9-5-2) are as follows：
First, adhesive tape fast pulley (9-5-2) constituent：
Count by weight, 4- [(5- cyano group -1,6- dihydros -2- hydroxyl-Isosorbide-5-Nitrae-dimethyl -6- oxo -3- pyridine radicals) azo]
72~155 parts of benzoic acid -2- phenoxyethyl acrylates, 128~215 parts of peroxide dioctyl phthalate -4- (1,1- dimethylethyl) hexamethylene diester,
1- carbamic acids 3- (2- methoxycarbonyl phenoxies) -86~165 parts of 1,2-PD ester, 2,2'- (3,3'- bis- chloro- 1,1'- biphenyl -4,
4'- bisazos) 213~288 parts of double [N- (2- methoxyphenyls) -3- oxo-butyramides], 6,6'(2,2'- dimethoxy-4 's,
4'- biphenylenes bisazo) 278~350 parts of two-(naphthalene disulfonate of 5- hydroxyl -4- amino 1,3), cyano group-(3- phenoxy group benzene
Base) methyl -3- (2,2- dichloroethylene) -66~81 parts of 2,2- dimethyl cyclopropane carboxylic acids ester, concentration is 67ppm~85ppm
N- (4- hydroxy phenyls methylene) 179~241 parts of-P-nethoxyaniline, 3,5- double (1,1- dimethyl ethyl) -4- hydroxy benzenes
Formic acid -2, double 254~367 parts of (1, the 1- dimethyl propyl) phenyl esters of 4-, 3,3'- [[3,3'- dimethyl (1,1'- biphenyl) -4,4'-
Diyl] double (azos)] double (4- amino -1-naphthalene sulfonic aicd) 269~398 parts of disodium salts, 70~154 parts of crosslinking agent, 4- hydroxyl -3- first
79~152 parts of epoxide benzyl carbinol, 230~281 parts of carbon peroxy acid-O, O- (1,1- dimethyl propyl)-O- (2- ethylhexyls) ester,
211~285 parts of 2,2- dimethyl -3- (2- methyl-1-propylenes base)-cyclopropane-carboxylic acid cyano group (3- Phenoxyphenyls) methyl esters；
The crosslinking agent is 5- benzyloxy -3- indolecarboxaldehydes, 3- methoxyl groups dopamine hydrochloride, 4- benzyloxy -3- indole acetonitriles
In any one；
2nd, the manufacturing process of adhesive tape fast pulley (9-5-2), comprises the steps of：
1st step：1350~2460 parts of ultra-pure water for adding electrical conductivity to be 6.56 μ S/cm~8.46 μ S/cm in a kettle., starts
Agitator in reactor, rotating speed is 98rpm~126rpm, starts heat pump, reactor temperature is risen to 89 DEG C~142
℃；Sequentially add 4- [(5- cyano group -1,6- dihydro -2- hydroxyl -1,4- dimethyl -6- oxo -3- pyridine radicals) azo] benzoic acid -
2- phenoxyethyl acrylates, peroxide dioctyl phthalate -4- (1,1- dimethylethyls) hexamethylene diester, 1- carbamic acids 3- (2- methoxycarbonyl phenoxies) -
1,2-PD ester, to being completely dissolved, regulation pH value is 8.8~10.6 for stirring, by agitator speed be adjusted to 152rpm~
213rpm, temperature is 124 DEG C~176 DEG C, esterification 8~18 hours；
2nd step：Take 2,2'- (the chloro- 1,1'- biphenyl -4,4'- bisazos of 3,3'- bis-) it is double [N- (2- methoxyphenyls) -3- oxos -
Butyramide], 6,6'(2,2'- dimethoxy-4 's, 4'- biphenylenes bisazo) the two-(naphthalenedisulfonic acid of 5- hydroxyl -4- amino 1,3
Sodium) to be crushed, powder diameter is 1000~1300 mesh；Add cyano group-(3- Phenoxyphenyls) methyl -3- (chloroethenes of 2,2- bis-
Alkenyl) -2,2- dimethyl cyclopropane carboxylic acids ester be well mixed, be laid in pallet, tiling thickness be 25mm~45mm, using agent
Measure for 10.3kGy~15.6kGy, energy for the alpha ray of 7.6MeV~13.5MeV is irradiated 200~300 minutes, and equal agent
The β x ray irradiation xs of amount 100~200 minutes；
3rd step：The mixed-powder processed through the 2nd step is dissolved in N- (4- hydroxy phenyls methylene)-P-nethoxyaniline, is added anti-
Kettle is answered, agitator speed is 263rpm~356rpm, and temperature is 168 DEG C~263 DEG C, and starting vavuum pump makes the vacuum of reactor
- 0.51MPa~2.65MPa is reached, this state response is kept 11~25 hours；Pressure release is simultaneously passed through radon gas, makes reacting kettle inner pressure
It is 1.37MPa~2.64MPa, insulation stands 15~24 hours；Agitator speed is promoted to 364rpm~420rpm, simultaneous reactions
Kettle pressure release is to 0MPa；Sequentially add 3,5- double (the 1,1- dimethyl propylenes of double (1,1- dimethyl ethyls) -4-HBA -2,4-
Base) phenyl ester, 3,3'- [[3,3'- dimethyl (1,1'- biphenyl) -4,4'- diyls] double (azos)] double (4- amino -1-naphthalene sulfonic aicd)
After disodium salt is completely dissolved, crosslinking agent stirring mixing is added so that the hydrophilic lipophilic balance of reactor solution is 6.2~8.4,
Insulation stands 13~22 hours；
4th step：When agitator speed is 284rpm~365rpm, 4- hydroxy 3-methoxybenzenes ethanol, carbon peroxide are sequentially added
Acid-O, O- (1,1- dimethyl propyls)-O- (2- ethylhexyls) esters and 2,2- dimethyl -3- (2- methyl-1-propylenes base)-ring third
Alkane carboxylic acid cyano group (3- Phenoxyphenyls) methyl esters, lifts reactor pressure, reaches 1.63MPa~2.75MPa, and temperature is
215 DEG C~286 DEG C, polymerisation 26~34 hours；Reacting kettle inner pressure is down to 0MPa after the completion of reaction, be cooled to 30 DEG C~
38 DEG C, discharging enters molding press and can be prepared by adhesive tape fast pulley (9-5-2).
6. a kind of method of work of carbon tetrachloride standard specimen automatic packaging system, it is characterised in that the method includes following step
Suddenly：
1st step：Power-on, now standard specimen detector (5-6) real-time detection whether there is standard specimen to pass through, as standard specimen detector (5-
6) when detecting standard specimen and pass through, standard specimen detector (5-6) produces electric signal transmission to control centre (3), control centre (3) control
Belt motor (5-2) and rear auxiliary electric machines for roller (7) start, and belt motor (5-2) drives standard specimen to move by belt (5-3)；
Packaging machine (9-1) and lower packaging machine (9-5) are now gone up as standard specimen movement is by tape-stripping to standard specimen specified location, and after passing through
Auxiliary roller-way (8) is delivered to next station；
2nd step：When standard specimen lateral dimension changes, now staff controls clamping device (5) by control centre (3)
Internal clamping board motor (5-7) starts, and clamping board motor (5-7) drives two grip blocks (5-1) remote by power transmission shaft (5-4)
From or be close to, realize the change of clamp distance；In grip block (5-1) displacement process, limiter (5-5) real-time monitoring is clamped
Two spacing of grip block (5-1), and produce electric signal to be sent to control centre (3), when grip block (5-1) is moved to limit position
When putting, clamping limiter (5-5) produces alarm signal to transmit to control centre (3), control centre (3) control clamping board motor
(5-7) shuts down；
3rd step：When standard specimen longitudinal size changes, now staff controls packaging mechanism (9) by control centre (3)
Internal upper packaging machine motor (9-2) starts, and upper packaging machine motor (9-2) is by displacement traveller (9-4) drive
Packaging machine fixed mount (9-3) is moved up and down, the change of packaging machine (9-1) and lower packaging machine (9-5) distance in realization；In upper encapsulation
In machine fixed mount (9-3) displacement process, the position of packaging machine fixed mount (9-3) in upper packaging machine limiter (9-8) real-time monitoring,
When upper packaging machine fixed mount (9-3) is moved to extreme position, upper packaging machine limiter (9-8) produces alarm signal to transmit to control
Center (3) processed, packaging machine motor (9-2) shuts down in control centre (3) control.
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| CN201611176120.2A CN106829071A (en) | 2016-12-19 | 2016-12-19 | A kind of carbon tetrachloride standard specimen automatic packaging system and its method of work |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107738781A (en) * | 2017-09-30 | 2018-02-27 | 贺碧先 | A kind of packing case sealing adhesive device |
| WO2019061459A1 (en) * | 2017-09-30 | 2019-04-04 | 贺碧先 | Packaging box adhesive tape sealing device |
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| US5735101A (en) * | 1996-08-05 | 1998-04-07 | Belcor Industries Inc | Tape management system |
| CN204750706U (en) * | 2015-05-27 | 2015-11-11 | 桐乡市红旗塑料包装袋厂 | Packing carton rubberizing closing device |
| CN204937565U (en) * | 2015-09-28 | 2016-01-06 | 赵世凯 | Automation carton folded package equipment |
| CN105691749A (en) * | 2016-03-28 | 2016-06-22 | 山东科技大学 | Automatic packaging machine with box sealing device |
| CN105923176A (en) * | 2016-06-15 | 2016-09-07 | 江南大学 | Semi-automatic adhesive tape box sealing device and box sealing method thereof |
| CN205591026U (en) * | 2016-03-09 | 2016-09-21 | 广东溢达纺织有限公司 | Automatic seal tape device |
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|---|---|---|---|---|
| US5735101A (en) * | 1996-08-05 | 1998-04-07 | Belcor Industries Inc | Tape management system |
| CN204750706U (en) * | 2015-05-27 | 2015-11-11 | 桐乡市红旗塑料包装袋厂 | Packing carton rubberizing closing device |
| CN204937565U (en) * | 2015-09-28 | 2016-01-06 | 赵世凯 | Automation carton folded package equipment |
| CN205591026U (en) * | 2016-03-09 | 2016-09-21 | 广东溢达纺织有限公司 | Automatic seal tape device |
| CN105691749A (en) * | 2016-03-28 | 2016-06-22 | 山东科技大学 | Automatic packaging machine with box sealing device |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107738781A (en) * | 2017-09-30 | 2018-02-27 | 贺碧先 | A kind of packing case sealing adhesive device |
| WO2019061459A1 (en) * | 2017-09-30 | 2019-04-04 | 贺碧先 | Packaging box adhesive tape sealing device |
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Application publication date: 20170613 |
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| RJ01 | Rejection of invention patent application after publication |