CN106823432A - A kind of distilling apparatus - Google Patents
A kind of distilling apparatus Download PDFInfo
- Publication number
- CN106823432A CN106823432A CN201710257344.4A CN201710257344A CN106823432A CN 106823432 A CN106823432 A CN 106823432A CN 201710257344 A CN201710257344 A CN 201710257344A CN 106823432 A CN106823432 A CN 106823432A
- Authority
- CN
- China
- Prior art keywords
- distilling apparatus
- vaporization chamber
- chamber
- even hot
- hot chamber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
Abstract
This application provides a kind of distilling apparatus, for required material to be separated from mixed material, including heater element, vaporization chamber, condenser and even hot chamber, it is characterized in that, the heater element is used for the medium heating in the even hot chamber, charging aperture, discharging opening, slag-drip opening are provided with the vaporization chamber, the discharging opening is connected by pipeline with condenser, the vaporization chamber outside is provided with housing, the housing forms even hot chamber with vaporization chamber outside, and is provided with medium inlet and media outlet on the even hot chamber.The distilling apparatus that the application is provided can be such that mixed material is heated evenly during distillation, accelerate the speed that low-boiling point material is separated from mixed material, improve operating efficiency.
Description
Technical field
It is especially a kind of that low-boiling point material is separated from various mixtures the present invention relates to distillation technique field
Distilling apparatus.
Background technology
Distillation is a kind of thermodynamic (al) separating technology, and it is different using each component boiling point in mixing liquid or liquid-solid system,
Low boiling component is evaporated, then condenses to separate the unit process of whole component, be to evaporate and condense two kinds of unit operations
Joint.With other separation means, such as extraction, filtering for crystallizing compare, its advantage be without the use of system components with
Other outer solvents, so as to ensure that new impurity will not be introduced.
At present, distillation is the Main Means for being applied to cuts separation.However, in still-process, mixture is received
Heat is uneven, and while will further result in a part of low-boiling point material and separated, another part low-boiling point material is not because adding
Heat and do not separated yet, have impact on production efficiency.
The content of the invention
In order to solve the above technical problems, the present invention provides a kind of distilling apparatus, the distilling apparatus can make in heating process
Mixed material is heated evenly, improve production efficiency.
The technical scheme that the present invention is provided is as follows：
A kind of distilling apparatus, for required material to be separated from mixed material, including heater element, vaporization chamber,
Condenser and even hot chamber, it is characterised in that the heater element is used for the medium heating in the even hot chamber, the vaporization chamber
On be provided with charging aperture, discharging opening, slag-drip opening, the discharging opening is connected by pipeline with condenser, and vaporization chamber outside sets
Housing is equipped with, the housing forms even hot chamber with vaporization chamber outside, and is provided with medium inlet and Jie on the even hot chamber
Matter is exported.
Preferably, be additionally provided with slag-drip opening on the vaporization chamber, slag-drip opening at be provided with control valve.
Preferably, also including rabbling mechanism, the rabbling mechanism includes motor and mixing component, the motor and institute
State mixing component to be connected by shaft coupling, the motor drives the mixing component to be stirred in the vaporization chamber.
Preferably, the mixing component includes agitating shaft and the stirring parts being arranged on agitating shaft, and the stirring parts are with spiral shell
The mode for revolving precession is arranged along the agitating shaft.
Preferably, the rabbling mechanism also includes reductor, and the reductor is connected with the motor, for reducing
State the speed of motor.
Preferably, the rabbling mechanism also includes spring bearing, and the bearing support is separately positioned on the agitating shaft two
End, wherein the spring bearing of one end is connected with the motor by shaft coupling.
Preferably, the rabbling mechanism also includes water-cooling bearing block, and the water-cooling bearing block is used to cool down the support shaft
Hold.
Preferably, also including heat-insulation layer, the heat-insulation layer is arranged on even hot chamber outside.
Preferably, the heater element is Elema.
The distilling apparatus that the present invention is provided, mixed material enters vaporization chamber from charging aperture, and heat transfer medium enters from medium inlet
Enter even hot chamber, full of whole even hot chamber, heater element is heated to the heat transfer medium in even hot chamber, simultaneously because heat transfer is made
With the heat transfer of heat transfer medium is to the mixed material in vaporization chamber.Low-boiling point material is after its boiling point is reached from mixed material
In separate in gaseous form, by entering pipeline after discharging opening, eventually enter into the condensation chamber that be connected with pipeline and condense.By
Vaporization chamber outside is coated in even hot chamber, the area that heat transfer medium transmits heat is increased so that heat transfer medium can be by heat
Transmit evenly improves the production efficiency of industrial production low-boiling point material to the mixed material in vaporization chamber.
Brief description of the drawings
In order to illustrate more clearly of the embodiment of the present application or technical scheme of the prior art, below will be to embodiment or existing
The accompanying drawing to be used needed for having technology description is briefly described, it should be apparent that, drawings in the following description are only this
Some embodiments described in application, for those of ordinary skill in the art, on the premise of not paying creative work,
Other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is the front view of distilling apparatus provided in an embodiment of the present invention；
Fig. 2 is the structural representation of the mixing component of distilling apparatus provided in an embodiment of the present invention.
Specific embodiment
In order that those skilled in the art more fully understand the technical scheme in the application, below in conjunction with the application reality
The accompanying drawing in example is applied, the technical scheme in the embodiment of the present application is clearly and completely described, it is clear that described implementation
Example is only some embodiments of the present application, rather than whole embodiments.Based on the embodiment in the application, this area is common
The every other embodiment that technical staff is obtained under the premise of creative work is not made, should all belong to the application protection
Scope.
The embodiment of the present invention is write using progressive mode.
As shown in figure 1, a kind of distilling apparatus provided in an embodiment of the present invention, for required material to be divided from mixed material
Separate out and, including heater element 1, vaporization chamber 2, condenser 3 and even hot chamber 4, heater element 1 is for the medium in even hot chamber 4
Heating, is provided with charging aperture 21, discharging opening 22, slag-drip opening 23 on vaporization chamber 2, discharging opening 22 is connected by pipeline with condenser 3,
The outside of vaporization chamber 2 is provided with housing, and housing forms even hot chamber 4 with the outside of vaporization chamber 2, and is provided with medium inlet on even hot chamber 4
41 and media outlet 42.
Heat transfer medium enters even hot chamber 4, the full whole even hot chamber 4 of filling from medium inlet 41.Specifically, heat transfer medium is
The water of 70% flake caustic mixing 30%, caustic soda will be gradually dissolved in water, while the caustic soda water after 1 pair of dissolving of heater element
Heating, as the temperature of caustic soda water is raised, moisture is evaporated, until being heated to the caustic soda liquid of predetermined temperature in even hot chamber 4
Fill.Meanwhile, mixed material enters vaporization chamber 2 from charging aperture 21, and the caustic soda liquid for being heated to predetermined temperature passes through heat transfer
Effect transfers heat to mixed material in vaporization chamber 2, and mixed material is heated continuously, until low-boiling point material is from mixture
Evaporation is separated in material, and the low-boiling point material separated enters discharging opening 22 in gaseous form, is eventually entered into along pipeline
Condensing tube condensation.When distilling apparatus is stopped using, heat transfer medium can be discharged from media outlet 42, it is to avoid heat transfer medium is long
Phase rests on causes corrosion in soaking chamber to device.Because even hot chamber 4 is housing and the outside of vaporization chamber 2 on the outside of vaporization chamber 2
Between the chamber that is formed, therefore, even hot chamber 4 is coated on the outside of vaporization chamber 2, and the caustic soda liquid in even hot chamber 4 will also be coated on vaporization chamber 2
Outside, caustic soda liquid can by heat from all directions Transmit evenly to the mixed material in vaporization chamber 2 so that mixed material is each
Part is heated and is heated evenly simultaneously, shortens the time that distillation obtains required low-boiling point material, has saved energy consumption, improves life
Produce efficiency.
Specifically, heater element 1 set predetermined temperature so that distilling apparatus continuous firing 500 DEG C to 550 DEG C it
Between, separated until the low-boiling point material by boiling point between 260 DEG C -480 DEG C all evaporates from mixed material.Set
Predetermined temperature needed for distillation so that distilling apparatus continuous firing then keeps low-boiling point material between 500 DEG C to 550 DEG C
While sustainable evaporation, other materials will not again occur and be evaporated.Therefore, the low-boiling point material purity obtained by distillation compared with
It is high.
Wherein, control valve 24 is provided with slag-drip opening 23, after the low-boiling point material in mixed material is distilled totally,
Control valve 24 is opened to discharge residual residue from slag-drip opening 23.
The embodiment of the present invention also includes rabbling mechanism 5, and rabbling mechanism 5 includes motor 52 and mixing component 51, motor
52 drive the agitation in vaporization chamber 2 of mixing component 51.Motor 52 replaces artificial implementation stirring work, improves operating efficiency；
And the agitation mixed material in vaporization chamber 2 of mixing component 51 so that mixed material various pieces are all even with the outside of vaporization chamber 2
Hot chamber 4 contacts, therefore mixed material in vaporization chamber 2 has further obtained uniform and sufficiently heating.
Specifically, as described in Figure 2, mixing component 51 includes agitating shaft 511 and the stirring parts being arranged on agitating shaft 511
512, stirring parts 512 are arranged in the way of being screwed onto along agitating shaft 511.Agitating shaft 511 passes across the center of vaporization chamber 2, stirring
Stirring parts 512 are provided with axle 511, during stirring, stirring parts 512 are rotated with agitating shaft 511 and be able to will mixed in the short time
Compound material is spread out, and the mixture material for spreading out is evenly distributed in vaporization chamber 2, is uniformly heated and fully, is carried
Distillation efficiency high.Also, stirring parts 512 are in the way of being screwed onto along the axial arranging of agitating shaft 511, the scope of lead angle
It it is 7 ° to 9 °, when agitating shaft 511 is rotated, the stirring parts 512 arranged in certain lead angle mode on agitating shaft 511 can push away thing
Material is moved towards slag-drip opening 23.
Specifically, stirring parts 512 are rake teeth or blade.In other embodiments, selection can be needed according to actual production
The species of stirring parts 512, as long as identical technique effect can be reached, within the scope of the present invention.
Wherein, rabbling mechanism 5 also includes reductor 53, and reductor 53 is connected with motor 52, and reductor 53 is defeated by its
Enter the gear wheel on the few gear engagement output shaft of the number of teeth on axle to reduce the speed of the motor 52 for running at high speed, so as to drop
The output speed of low motor 52
Wherein, rabbling mechanism 5 also includes spring bearing 55, and bearing support 55 is separately positioned on the two ends of agitating shaft 511, is used for
Support agitating shaft 511 is stably stirred in vaporization chamber.Specifically, the spring bearing 55 of the wherein one end of agitating shaft 511 with it is electronic
Machine 52 is connected by shaft coupling 54, and shaft coupling 54 is Hooks coupling universal coupling.
Specifically, rabbling mechanism 5 also includes water-cooling bearing block 56, cooling water enters bearing from the interface of water-cooling bearing block 56
In seat, the bearing support 55 to the two ends of agitating shaft 511 is lowered the temperature, and the cooling water for completing cooling work is arranged from bearing block delivery port
Go out, into cooling pond.The setting of water-cooling bearing block 56 prevents rabbling mechanism 5 to overheat and produce deformation, and influences its normal
Work.
The embodiment of the present invention also includes heat-insulation layer 6, and heat-insulation layer 6 is arranged on the outside of even hot chamber 4.
Specifically, the material of heat-insulation layer 6 can be polystyrene foam, foam cement and aeroge, in other implementations
In example, can need voluntarily to select the material category of heat-insulation layer 6 according to actual production, as long as identical technique effect can be reached
, within the scope of the present invention.
Wherein, heater element 1 be Elema, can also be Si-Mo rod or PTC heatings, in other embodiments, can
Needed to select the species of heater element 1 according to actual production, as long as identical technique effect can be reached, in this hair
In bright protection domain.
The foregoing description of the disclosed embodiments, enables professional and technical personnel in the field to realize or uses the present invention.
Various modifications to these embodiments will be apparent for those skilled in the art, as defined herein
General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, the present invention
The embodiments shown herein is not intended to be limited to, and is to fit to and principles disclosed herein and features of novelty phase one
The scope most wide for causing.
Claims (9)
1. a kind of distilling apparatus, for required material to be separated from mixed material, including heater element (1), vaporization chamber
(2), condenser (3) and even hot chamber (4), it is characterised in that the heater element is used for the medium heating in the even hot chamber,
Charging aperture (21), discharging opening (22), slag-drip opening (23) are provided with the vaporization chamber (2), the discharging opening (22) is by pipeline
It is connected with condenser (3), vaporization chamber (2) outside is provided with housing, the housing forms even with the vaporization chamber (2) outside
Medium inlet (41) and media outlet (42) are provided with hot chamber (4), and the even hot chamber (4).
2. distilling apparatus as claimed in claim 1, it is characterised in that slag-drip opening (23) place on the vaporization chamber (2) sets
It is equipped with control valve (24).
3. distilling apparatus as claimed in claim 1, it is characterised in that also including rabbling mechanism (5), the rabbling mechanism (5)
Including motor (52) and mixing component (51), the motor (52) is connected with the mixing component (51) by shaft coupling (54)
Connect, the motor (52) drives the mixing component (51) agitation in the vaporization chamber (2).
4. distilling apparatus as claimed in claim 3, it is characterised in that the mixing component (51) including agitating shaft (511) and
The stirring parts (512) on agitating shaft are arranged on, the stirring parts (512) are in the way of being screwed onto along the agitating shaft (511)
Axially arrangement.
5. distilling apparatus as claimed in claim 3, it is characterised in that the rabbling mechanism (5) also includes reductor (53), institute
State reductor (53) to be connected with the motor (52), the speed for reducing the motor (52).
6. distilling apparatus as claimed in claim 4, it is characterised in that the rabbling mechanism (5) also includes spring bearing (55),
The bearing support (55) is separately positioned on the agitating shaft (511) two ends, the wherein spring bearing (55) and the electricity of one end
Motivation (52) is connected by shaft coupling (54).
7. distilling apparatus as claimed in claim 6, it is characterised in that the rabbling mechanism (5) also includes water-cooling bearing block
(56), the water-cooling bearing block (56) is for cooling down the spring bearing (55).
8. distilling apparatus as claimed in claim 1, it is characterised in that also including heat-insulation layer (6), the heat-insulation layer (6) is set
In even hot chamber (4) outside.
9. distilling apparatus as claimed in claim 1, it is characterised in that the heater element (1) is Elema.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710257344.4A CN106823432A (en) | 2017-04-19 | 2017-04-19 | A kind of distilling apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710257344.4A CN106823432A (en) | 2017-04-19 | 2017-04-19 | A kind of distilling apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106823432A true CN106823432A (en) | 2017-06-13 |
Family
ID=59147498
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710257344.4A Pending CN106823432A (en) | 2017-04-19 | 2017-04-19 | A kind of distilling apparatus |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106823432A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109499417A (en) * | 2018-12-05 | 2019-03-22 | 飞翼股份有限公司 | A kind of crude tailings Paste mixer drive mechanism |
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| CN1119959A (en) * | 1994-08-31 | 1996-04-10 | 拜尔公司 | A process and a device for seperating a solid residue from its solution in a strirred bed of material |
| CN201342252Y (en) * | 2009-01-06 | 2009-11-11 | 邹平福海科技发展有限公司 | Desolvation device for sticky thermal sensitive materials |
| CN201890854U (en) * | 2010-12-01 | 2011-07-06 | 宁波大发化纤有限公司 | Quality and viscosity regulation system for waste plastic |
| CN203044003U (en) * | 2013-01-22 | 2013-07-10 | 安徽銮威化工科技开发有限公司 | Defoamer synthesis reaction kettle |
| CN203170309U (en) * | 2013-02-27 | 2013-09-04 | 上海亚杜润滑材料有限公司 | Heating and cooling system of reaction kettle |
| CN204380295U (en) * | 2014-12-30 | 2015-06-10 | 江西嘉源香料有限公司 | A kind of distillation still |
| CN204522340U (en) * | 2015-03-19 | 2015-08-05 | 江西盛伟实业有限公司 | A kind of novel distillation still |
| CN105276811A (en) * | 2015-11-04 | 2016-01-27 | 苏俊兰 | Tubular efficient heating furnace |
| CN206660635U (en) * | 2017-04-19 | 2017-11-24 | 长沙科力威蒸馏技术有限公司 | A kind of distilling apparatus |
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2017
- 2017-04-19 CN CN201710257344.4A patent/CN106823432A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1119959A (en) * | 1994-08-31 | 1996-04-10 | 拜尔公司 | A process and a device for seperating a solid residue from its solution in a strirred bed of material |
| CN201342252Y (en) * | 2009-01-06 | 2009-11-11 | 邹平福海科技发展有限公司 | Desolvation device for sticky thermal sensitive materials |
| CN201890854U (en) * | 2010-12-01 | 2011-07-06 | 宁波大发化纤有限公司 | Quality and viscosity regulation system for waste plastic |
| CN203044003U (en) * | 2013-01-22 | 2013-07-10 | 安徽銮威化工科技开发有限公司 | Defoamer synthesis reaction kettle |
| CN203170309U (en) * | 2013-02-27 | 2013-09-04 | 上海亚杜润滑材料有限公司 | Heating and cooling system of reaction kettle |
| CN204380295U (en) * | 2014-12-30 | 2015-06-10 | 江西嘉源香料有限公司 | A kind of distillation still |
| CN204522340U (en) * | 2015-03-19 | 2015-08-05 | 江西盛伟实业有限公司 | A kind of novel distillation still |
| CN105276811A (en) * | 2015-11-04 | 2016-01-27 | 苏俊兰 | Tubular efficient heating furnace |
| CN206660635U (en) * | 2017-04-19 | 2017-11-24 | 长沙科力威蒸馏技术有限公司 | A kind of distilling apparatus |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109499417A (en) * | 2018-12-05 | 2019-03-22 | 飞翼股份有限公司 | A kind of crude tailings Paste mixer drive mechanism |
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| PB01 | Publication | ||
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170613 |
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| RJ01 | Rejection of invention patent application after publication |