CN106818923A - A kind of micro-capsule suspension for trapping and killing citrus fruit fly - Google Patents

A kind of micro-capsule suspension for trapping and killing citrus fruit fly Download PDF

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Publication number
CN106818923A
CN106818923A CN201710052189.2A CN201710052189A CN106818923A CN 106818923 A CN106818923 A CN 106818923A CN 201710052189 A CN201710052189 A CN 201710052189A CN 106818923 A CN106818923 A CN 106818923A
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CN
China
Prior art keywords
capsule suspension
citrus fruit
fruit fly
micro
trap
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710052189.2A
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Chinese (zh)
Inventor
吴少华
李永裕
陈晓丹
王波
廖正萍
杨贝贝
邹丽婷
颜悦
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Fujian Agriculture and Forestry University
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Fujian Agriculture and Forestry University
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Application filed by Fujian Agriculture and Forestry University filed Critical Fujian Agriculture and Forestry University
Priority to CN201710052189.2A priority Critical patent/CN106818923A/en
Publication of CN106818923A publication Critical patent/CN106818923A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/26Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests in coated particulate form
    • A01N25/28Microcapsules or nanocapsules
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/36Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Plant Pathology (AREA)
  • Environmental Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Dentistry (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Biotechnology (AREA)
  • Pest Control & Pesticides (AREA)
  • Toxicology (AREA)
  • Botany (AREA)
  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention relates to a kind of micro-capsule suspension for trapping and killing citrus fruit fly, it is to add cyclodextrin to form in essential oil is compounded, and compounding essential oil is 1 with the weight ratio of cyclodextrin:5.25~24.The micro-capsule suspension also includes Ricinate, thickener, antifreeze, preservative, synergist and water, and it can lentamente discharge active material, preferably extend its lasting period, and solvent for use is water, to environment, human body, the equal nonhazardous effect of livestock.

Description

A kind of micro-capsule suspension for trapping and killing citrus fruit fly
Technical field
Quarantine and Prevention Technique field the present invention relates to citrus fruit fly, and in particular to a kind of micro- glue of trapping citrus fruit fly Capsule suspending agent.
Background technology
Plants essential oil typically has fragrance, can play the effect such as anti-oxidant, antibacterial, expelling parasite, desinsection, is widely used in doctor The fields such as medicine, cosmetics, commodity.But plants essential oil exist photodissociation volatile, not easy to maintain, easy, to it is thermo-responsive it is easy decompose etc. Problem.Microcapsules technology can well protect essential oil not by external environmental interference, without the original quality of influence essential oil, Physicochemical property and activity.
The features such as microcapsule formulations agricultural chemicals has low toxicity, efficient, the lasting period is long, portion also compares in the market at present It is few(The developmental research of micro-capsule suspension, Chinese agricultural chemicals, 2012, (08): 22-26), it is that the development of pesticide in future formulation becomes Gesture.In order that essential oil microcapsules can play preferable bioactivity, it is necessary to be processed into corresponding formulation.Suspending agent is application In those water insoluble or relatively low active materials of solubility in water, need to add some auxiliary agents in preparation process, it is such as wet Profit dispersant, thickener, antifreeze etc., make gained preparation have good mobility, dispersiveness, frost resistance and suspension Deng.LC essential oils are prepared into micro-capsule suspension by rich happiness with β-CD, and by simulant storehouse, the 30%LC/ β-CD with 100 times of liquid are micro- After capsule suspension processes 10 d to cacac moth, prevention effect up to 76.81%, more than control DDT EC(Natural products LC Bioactivity and its slow release formulation research to cacac moth, Kweiyang:Guizhou University, 2008).
The content of the invention
In order to overcome the above-mentioned deficiencies of the prior art, the invention provides a kind of the micro- of long-acting lasting trapping citrus fruit fly Capsule suspension.
The technical solution adopted in the present invention is:
The micro-capsule suspension of the trapping citrus fruit fly that the present invention is provided, it is cyclodextrin to be added in essential oil is compounded and is prepared into Suspending agent.
The micro-capsule suspension of described trapping citrus fruit fly includes:Compounding essential oil, cyclodextrin, Ricinate, increasing Thick dose, antifreeze, preservative, synergist and water, wherein:
Described compounding essential oil is 1 with the weight ratio of cyclodextrin: 5.25 ~ 24.
Content of the compounding essential oil in suspending agent is 10.0-30.0 wt%;
Content of the Ricinate in suspending agent is 1.0-5.0 wt%;
Content of the thickener in suspending agent is 0.1-0.5 wt%;
Content of the antifreeze in suspending agent is 1.0-5.0 wt%;
Content of the preservative in suspending agent is 1.0-5.0 wt%;
Content of the synergist in suspending agent is 10.0-30.0wt%;
Balance of water.
The compounding essential oil is thousand layers of aurin oil and lemon by weight 1:1 ~ 7 and 1 ~ 7:1 mixing;
The cyclodextrin is beta-schardinger dextrin;
The Ricinate be polyvinylpyrrolidone, lauryl sodium sulfate and neopelex in one kind or Several mixing;
The thickener is the one kind or several in xanthans, aluminium-magnesium silicate, polyvinyl alcohol, sodium carboxymethylcellulose and sodium alginate The mixing planted;
The antifreeze is the mixing of one or more in polyethylene glycol, 1,2- propane diols, urea and sodium chloride;
The preservative is Sodium Benzoate;
The synergist is peptone.
The micro-capsule suspension of the trapping citrus fruit fly that the present invention is provided is directed to active component has volatile characteristic, It is prepared into micro-capsule suspension.
Compared with prior art, the invention has the advantages that:
1) by adding cyclodextrin, compounding essential oil is made to be coated by cyclodextrin, so as to improve its suspendability and sustained release performance.Make out Send out consumption low, high efficiency, the citrus fruit fly attractant micro-capsule suspension of lasting period long are possibly realized, substantially reduce its consumption and Use cost, improves its application level.
2)The cyclodextrin has good coating function to active component, and can be discharged well in water activity into Point.
3)The micro-capsule suspension is respectively provided with good attractant effect to the female male worm of citrus fruit fly.
Specific embodiment
The present invention is explained further with reference to specific embodiment, but not to the present invention any type of limitation of composition.Remove Have outside specified otherwise, the method and step and reagent in following examples are commonly used in the art.
Embodiment 1:
A kind of citrus fruit fly attractant micro-capsule suspension, its composition is made by weight percentage, by compounding essential oil(Thousand layers of aurin Oil:Lemon=1:3.5)1.6wt%, cyclodextrin 8.4wt%, peptone 10.0wt%, Ricinate 1.0wt%, thickener 0.1wt%, antifreeze 1.0wt% and preservative 1.0wt%, water 76.9wt%.
Embodiment 2:
A kind of citrus fruit fly attractant micro-capsule suspension, it is characterised in that its composition is made by weight percentage, by compounding essence Oil(Thousand layers of aurin oil:Lemon=1:5.0)1.82wt%, cyclodextrin 18.2wt%, peptone 20.0wt%, Ricinate 3.0wt%, thickener 0.2wt%, antifreeze 3.0wt% and preservative 3.0wt%, water 50.8wt%.
Embodiment 3:
A kind of citrus fruit fly attractant micro-capsule suspension, it is characterised in that its composition is made by weight percentage, by compounding essence Oil(Thousand layers of aurin oil:Lemon=2.5:1)1.43wt%, cyclodextrin 28.6wt%, peptone 25.0wt%, Ricinate 4.0wt%, thickener 0.3wt%, antifreeze 2.0wt% and preservative 4.0wt%, water 39.7wt%.
Embodiment 4:
A kind of citrus fruit fly attractant micro-capsule suspension, it is characterised in that its composition is made by weight percentage, by compounding essence Oil(Thousand layers of aurin oil:Lemon=6.0:1)1.2wt%, cyclodextrin 28.8wt%, peptone 30.0wt%, Ricinate 5.0wt%, thickener 0.5wt%, antifreeze 5.0wt% and preservative 5.0wt%, water 24.5wt%.
The indoor attractant effect that citrus fruit fly is carried out to above-described embodiment 1-4 using Y-shaped smell sensing apparatus is tested.Experiment repeats 3 Secondary, test result is as follows:
Note:Data are average ± standard error in table, are shown with different lowercase letter Analysis of variance differences behind column data Write(P<0.05).
The foregoing is only presently preferred embodiments of the present invention, all impartial changes done according to scope of the present invention patent with Modification, should all belong to covering scope of the invention.

Claims (9)

1. it is a kind of trap and kill citrus fruit fly micro-capsule suspension, it is characterised in that:It is made up of following raw material:Compounding essential oil, ring paste Essence, Ricinate, thickener, antifreeze, preservative, synergist and water.
2. it is according to claim 1 it is a kind of trap and kill citrus fruit fly micro-capsule suspension, it is characterised in that:Raw material is by following Component is made:
Content of the compounding essential oil in suspending agent is 10.0-30.0 wt%;
The compounding essential oil is 1 with the weight ratio of cyclodextrin:5.25 ~ 24;
Content of the Ricinate in suspending agent is 1.0-5.0 wt%;
Content of the thickener in suspending agent is 0.1-0.5 wt%;
Content of the antifreeze in suspending agent is 1.0-5.0 wt%;
Content of the preservative in suspending agent is 1.0-5.0 wt%;
Content of the synergist in suspending agent is 10.0-30.0wt%;
Balance of water.
3. it is according to claim 1 it is a kind of trap and kill citrus fruit fly micro-capsule suspension, it is characterised in that:The compounding Essential oil is thousand layers of aurin oil and lemon by weight 1:1 ~ 7 and 1 ~ 7:1 mixing.
4. it is according to claim 1 it is a kind of trap and kill citrus fruit fly micro-capsule suspension, it is characterised in that:The cyclodextrin It is beta-schardinger dextrin.
5. it is according to claim 1 it is a kind of trap and kill citrus fruit fly micro-capsule suspension, it is characterised in that:The moistening point Powder is one or more in polyvinylpyrrolidone, lauryl sodium sulfate and neopelex.
6. it is according to claim 1 it is a kind of trap and kill citrus fruit fly micro-capsule suspension, it is characterised in that:The thickener It is one or more in xanthans, aluminium-magnesium silicate, polyvinyl alcohol, sodium carboxymethylcellulose and sodium alginate.
7. it is according to claim 1 it is a kind of trap and kill citrus fruit fly micro-capsule suspension, it is characterised in that:The antifreeze It is one or more in polyethylene glycol, 1,2- propane diols, urea and sodium chloride.
8. it is according to claim 1 it is a kind of trap and kill citrus fruit fly micro-capsule suspension, it is characterised in that:The preservative It is Sodium Benzoate.
9. it is according to claim 1 it is a kind of trap and kill citrus fruit fly micro-capsule suspension, it is characterised in that:The synergist It is peptone.
CN201710052189.2A 2017-01-24 2017-01-24 A kind of micro-capsule suspension for trapping and killing citrus fruit fly Pending CN106818923A (en)

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CN201710052189.2A CN106818923A (en) 2017-01-24 2017-01-24 A kind of micro-capsule suspension for trapping and killing citrus fruit fly

Applications Claiming Priority (1)

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CN201710052189.2A CN106818923A (en) 2017-01-24 2017-01-24 A kind of micro-capsule suspension for trapping and killing citrus fruit fly

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116035003A (en) * 2023-01-12 2023-05-02 福建省农业科学院植物保护研究所 Biodegradable thrips attracting and smearing adhesive and application method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009001076A1 (en) * 2007-06-25 2008-12-31 Syngenta Participation Ag Pesticide compositions
CN101589728A (en) * 2009-06-30 2009-12-02 福建农林大学 Protein attractant for Bactrocera dorsalis Hendel and preparation method thereof
CN103548826A (en) * 2013-11-04 2014-02-05 吴小毅 Bactrocera dorsalis amphoteric attractant as well as preparation method and application thereof
CN105724455A (en) * 2016-04-19 2016-07-06 福建农林大学 Composite attractant used for attracting both male and female bactrocera thailandica
CN105815344A (en) * 2016-04-19 2016-08-03 福建农林大学 Composite attractant for citrus fruit flies

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009001076A1 (en) * 2007-06-25 2008-12-31 Syngenta Participation Ag Pesticide compositions
CN101589728A (en) * 2009-06-30 2009-12-02 福建农林大学 Protein attractant for Bactrocera dorsalis Hendel and preparation method thereof
CN103548826A (en) * 2013-11-04 2014-02-05 吴小毅 Bactrocera dorsalis amphoteric attractant as well as preparation method and application thereof
CN105724455A (en) * 2016-04-19 2016-07-06 福建农林大学 Composite attractant used for attracting both male and female bactrocera thailandica
CN105815344A (en) * 2016-04-19 2016-08-03 福建农林大学 Composite attractant for citrus fruit flies

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周一万: "冬青油微囊悬浮剂的制备及其杀蚜活性研究", 《农药学学报》 *
周一万: "植物源农药制剂加工关键技术研究", 《中国博士学位论文全文数据库 农业科技辑》 *
师迎春 等编: "《无公害菜园首选农药100种(第2版)》", 31 January 2016, 中国农业出版社 *
饶喜: "天然产物LC对烟草粉螟的生物活性及其缓释剂型研究", 《中国优秀硕士学位论文全文数据库 农业科技辑》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116035003A (en) * 2023-01-12 2023-05-02 福建省农业科学院植物保护研究所 Biodegradable thrips attracting and smearing adhesive and application method thereof

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SE01 Entry into force of request for substantive examination
CB03 Change of inventor or designer information
CB03 Change of inventor or designer information

Inventor after: Li Yongyu

Inventor after: Wu Shaohua

Inventor after: Chen Xiaodan

Inventor after: Wang Bo

Inventor after: Liao Zhengping

Inventor after: Yang Beibei

Inventor after: Zou Liting

Inventor after: Yan Yue

Inventor before: Wu Shaohua

Inventor before: Li Yongyu

Inventor before: Chen Xiaodan

Inventor before: Wang Bo

Inventor before: Liao Zhengping

Inventor before: Yang Beibei

Inventor before: Zou Liting

Inventor before: Yan Yue

RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20170613