CN106818901A - The medicament-fertilizer mixture of preventing and treating crops virus infection - Google Patents

The medicament-fertilizer mixture of preventing and treating crops virus infection Download PDF

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Publication number
CN106818901A
CN106818901A CN201611147600.6A CN201611147600A CN106818901A CN 106818901 A CN106818901 A CN 106818901A CN 201611147600 A CN201611147600 A CN 201611147600A CN 106818901 A CN106818901 A CN 106818901A
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parts
medicament
preventing
acid
fertilizer mixture
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王淼
张庆吉
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Xinchang County Agricultural Science And Technology Co Ltd Ao Ao
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Xinchang County Agricultural Science And Technology Co Ltd Ao Ao
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N29/00—Biocides, pest repellants or attractants, or plant growth regulators containing halogenated hydrocarbons
    • A01N29/02—Acyclic compounds or compounds containing halogen attached to an aliphatic side-chain of a cycloaliphatic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/10—Aromatic or araliphatic carboxylic acids, or thio analogues thereof; Derivatives thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
    • A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/14—Boron; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/16—Heavy metals; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/26—Phosphorus; Compounds thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05B—PHOSPHATIC FERTILISERS
    • C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80—Soil conditioners
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
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  • Plant Pathology (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
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  • Microbiology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Mycology (AREA)
  • Soil Sciences (AREA)
  • Virology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Fertilizers (AREA)

Abstract

A kind of medicament-fertilizer mixture for preventing and treating crops virus infection, it is characterised in that be made up of following raw material：Composite nano silver, methyl α-naphthyl acetate, potassium phosphate, agricultural active bacterium, Boron Nitride, three isooctyl acid glyceride, ferric citrate, ethephon (CEPHA),2-(chloroethyl) phosphonic acid, surfactant, dichloromethane, Achnatherum inebrians, humic acid, Nafusaku, heroubill.It is made by simple making step, manufacture craft of the present invention is simple, manufacturing process is environment friendly and pollution-free, the obtained medicine fertilizer batch mixing for preventing virus can effectively kill various pathogenic virus, its various nutriment needed for growing can also be provided for plant simultaneously, it is adapted to large-scale production, with good development prospect.

Description

The medicament-fertilizer mixture of preventing and treating crops virus infection
Technical field
The invention belongs to field of pesticide preparation, more particularly, to a kind of medicament-fertilizer mixture for preventing and treating crops virus infection.
Background technology
With continuing to develop for agriculture, gardens industry, there are various plants in the continuous growth of cultivated area in most plants Virosis, causes serious economic loss.The plant virus for damaging Horticultural crops includes cucumber mosaic virus (Cucumber Mosaic virus, CMV), tobacco mosaic virus (TMV) (Tobacco mosaic virus, TMV) and potato Y virus (Potato virus Y, PVY).In order to prevent and treat these viruses, develop agronomy prevention and controls and (for example use disease-free seed and training Educate those methods of antiviral new lines), but its effect is not notable.
The research for having many exploitation new microbe preparations recently prevents and treats plant virus using microorganism.In particular, micro- life Thing preparation is environment-friendly means, and it can keep natural ecosystems and nontoxic to mammal, thus to microorganism formulation Demand increase.
According to investigations, the whole world to the pathogenic microorganism of plant pest (fungi, strong bacterium, rickettsia, mycoplasma, virus, Algae etc.) there are more than 80,000 kinds, plant disease is brought about great losses to agricultural, and thus global crops are reduced every year on average Yield about 500Mt, once repeatedly occurred in history because certain plant disease epidemics and caused by serious famine, or even a large amount of populations die of hunger Calamity, the use of bactericide is a kind of cost-effective method of controlling plant diseases, existing bactericide is to prevent and treat phytopathy Harmful a kind of cost-effective method, although existing bactericide can kill pest and disease damage to a certain extent, sterilization Damage is produced to wheat simultaneously, its yield is influenceed, in addition, the residue of the bactericide of sprinkling produces harm, ring to environment, soil Guaranteed cost is poor.Therefore, it is necessary to invent a kind of environmental protection, even non-hazardous small to environmental hazard, while can have again Effect kills the bactericide of various pest and disease damages, so as to accomplish both to protect environment, various cereal crops can be made again from disease pest Infringement.
The content of the invention
For variety of problems present in above-mentioned background technology, prevent and treat what crops virus infected the invention provides a kind of Medicament-fertilizer mixture.The medicament-fertilizer mixture also can provide its normal life while plant main flow pathogenic virus are eliminated for plant The required various nutriment of length.
To achieve the above object, the scheme that uses of the present invention for：
A kind of medicament-fertilizer mixture for preventing and treating crops virus infection, is made up of following raw material and its parts by weight：Composite nano silver 20- 30 parts, methyl α-naphthyl acetate 3-9 parts, potassium phosphate 3-6 parts, 2-7 parts of agricultural active bacterium, Boron Nitride 3-7 parts, three isooctyl acid glyceride 0.001- 0.005 part, ferric citrate 0.001-0.003 parts, ethephon (CEPHA),2-(chloroethyl) phosphonic acid 1-3 parts, surfactant 10-15 parts, dichloromethane 10-15 Part, Achnatherum inebrians 10-15 parts, humic acid 3-6 parts, Nafusaku 8-15 parts, heroubill 2-8 parts.
Preferably, the medicament-fertilizer mixture of above-mentioned preventing and treating crops virus infection, is made up of following raw material and its parts by weight： 23 parts of composite nano silver, 4 parts of methyl α-naphthyl acetate, 4 parts of potassium phosphate, 5 parts of agricultural active bacterium, 4 parts of Boron Nitride, three isooctyl acid glyceride 0.002 part, it is 0.002 part of ferric citrate, 2 parts of ethephon (CEPHA),2-(chloroethyl) phosphonic acid, 12 parts of surfactant, 14 parts of dichloromethane, 14 parts of Achnatherum inebrians, rotten Grow 4 parts of acid, 8 parts of Nafusaku, 6 parts of heroubill.
Specifically, the preparation method of the composite nano silver is（1）, weigh silver nitrate solution in proportion and be placed in beaker, It is proportionally added into sodium hydroxide solution thereto again, is aged 36h, fully reaction is obtained predecessor；（2）, by step 1 before Thing filtering is driven, and it is multiple with milli-Q water；（3）, by step 2 gained filtering after predecessor be placed in baking oven, 80 DEG C baking Roasting 5h obtains clean filter residue；（4）, oxalic acid and zinc chloride are weighed according to formula rate, water saturation solution is each configured to, by grass The aqueous solution of acid and zinc chloride is mixed, and is sufficiently stirred for 50 min, and product is stood, and fully washing is extremely deposited without chlorion , 3~4 h of baking in 120 DEG C of baking ovens are then put into, obtain mix products；（5）, by the product in dry step 3 and Product in step 4 uniformly mixes and grinds, and is placed in Muffle furnace, 600 DEG C of holding 2h；（6）, cooling, grinding, be obtained nanometer Silver-ZnO fungicide mixture；（7）, by step 6 gained nanometer silver-ZnO fungicide mixture be added to silicic acid second It is fully hydrolyzed it in ester, is then placed on acidifying in hydrochloric acid, finally add the mixed liquor of isopropyl titanium and isopropanol, reacts 8- 16 hours, that is, obtain the nanometer silver-ZnO compound particle of titanium dioxide covering.
Specifically the agricultural active bacterium is：Agricultural active bacterium, edible oil monad, bacillus licheniformis.
It is specific as follows present invention also offers the preparation method of the medicament-fertilizer mixture of preventing and treating crops virus infection：
（1）, heroubill, Achnatherum inebrians are put into crushing, stirring in pulverizer, filter residue is carried out afterwards, obtain A mixtures；
（2）, A mixtures are poured into reactor and add methyl α-naphthyl acetate, potassium phosphate, Boron Nitride and surfactant, added It is stirred continuously in journey, mixing time is 10min, obtains B mixtures；
（3）, agricultural active bacterium, ethephon (CEPHA),2-(chloroethyl) phosphonic acid, dichloromethane, humic acid, Nafusaku, Yi Jibiao are sequentially added in B mixtures Face activating agent, is heated afterwards, and heating-up temperature is 35 DEG C -55 DEG C, and constant temperature 10min obtains C mixtures；
（4）, in C mixtures add composite nano silver and 1/3 surfactant, stirred after addition, be cooled to 60min is stood after normal temperature, that is, obtains preventing and treating the medicament-fertilizer mixture of crops virus infection.
Specifically, the application method of the medicament-fertilizer mixture of preventing and treating crops virus infection of the invention is, if making to crops With the dosage that can be pressed 1-5% mixes with water, sprinkling；If using trees, it can be mixed with water by the dosage of 1-3%, poured Filling is used.
Manufacture craft of the present invention is simple, manufacturing process is environment friendly and pollution-free, and the obtained medicine fertilizer batch mixing for preventing virus can have Effect kills various pathogenic virus, while various nutriment that can also be for needed for plant provides its growth, are adapted to large-scale production, tool There is good development prospect.
Specific embodiment
Embodiment 1
A kind of medicament-fertilizer mixture for preventing and treating crops virus infection, is made up of following raw material and its parts by weight：Composite nano silver 23 Part, 4 parts of methyl α-naphthyl acetate, 4 parts of potassium phosphate, 5 parts of agricultural active bacterium, 4 parts of Boron Nitride, 0.002 part of three isooctyl acid glyceride, ironic citrate 0.002 part of ammonium, 2 parts of ethephon (CEPHA),2-(chloroethyl) phosphonic acid, 12 parts of surfactant, 14 parts of dichloromethane, 14 parts of Achnatherum inebrians, 4 parts of humic acid, Nafusaku 8 parts, 6 parts of heroubill.
The medicament-fertilizer mixture of above-mentioned preventing and treating crops virus infection is prepared from by following steps：
（1）, heroubill, Achnatherum inebrians are put into crushing, stirring in pulverizer, filter residue is carried out afterwards, obtain A mixtures；
（2）, A mixtures are poured into reactor and add methyl α-naphthyl acetate, potassium phosphate, Boron Nitride and surfactant, added It is stirred continuously in journey, mixing time is 10min, obtains B mixtures；
（3）, sequentially add in B mixtures agricultural active bacterium, ethephon (CEPHA),2-(chloroethyl) phosphonic acid, dichloromethane, humic acid, Nafusaku, three different pungent Acid glyceride, ferric citrate and surfactant, are heated afterwards, and heating-up temperature is 35 DEG C -55 DEG C, constant temperature 10min, Obtain C mixtures；
（4）, in C mixtures add composite nano silver and 1/3 surfactant, stirred after addition, be cooled to 60min is stood after normal temperature, that is, obtains preventing and treating the medicament-fertilizer mixture of crops virus infection.
Embodiment 2
A kind of medicament-fertilizer mixture for preventing and treating crops virus infection, is made up of following raw material and its parts by weight：Composite nano silver 24 Part, 5 parts of methyl α-naphthyl acetate, 3 parts of potassium phosphate, 4 parts of agricultural active bacterium, 5 parts of Boron Nitride, 1 part of ethephon (CEPHA),2-(chloroethyl) phosphonic acid, 13 parts of surfactant, dichloro 13 parts of methane, 0.002 part of three isooctyl acid glyceride, 0.002 part of ferric citrate, 15 parts of Achnatherum inebrians, 4 parts of humic acid, methyl α-naphthyl acetate 10 parts of sodium, 5 parts of heroubill.
The medicament-fertilizer mixture of above-mentioned preventing and treating crops virus infection is prepared from by following steps：
（1）, heroubill, Achnatherum inebrians are put into crushing, stirring in pulverizer, filter residue is carried out afterwards, obtain A mixtures；
（2）, A mixtures are poured into reactor and add methyl α-naphthyl acetate, potassium phosphate, Boron Nitride and surfactant, added It is stirred continuously in journey, mixing time is 10min, obtains B mixtures；
（3）, agricultural active bacterium, ethephon (CEPHA),2-(chloroethyl) phosphonic acid, three isooctyl acid glyceride, ferric citrate, dichloromethane are sequentially added in B mixtures Alkane, humic acid, Nafusaku and surfactant, are heated afterwards, and heating-up temperature is 35 DEG C -55 DEG C, constant temperature 10min, Obtain C mixtures；
（4）, in C mixtures add composite nano silver and 1/3 surfactant, stirred after addition, be cooled to 60min is stood after normal temperature, that is, obtains preventing and treating the medicament-fertilizer mixture of crops virus infection.
Embodiment 3
A kind of medicament-fertilizer mixture for preventing and treating crops virus infection, is made up of following raw material and its parts by weight：Composite nano silver 23 It is part, 6 parts of methyl α-naphthyl acetate, 5 parts of potassium phosphate, 2 parts of agricultural active bacterium, 7 parts of Boron Nitride, 1 part of ethephon (CEPHA),2-(chloroethyl) phosphonic acid, 11 parts of surfactant, three different 0.002 part of glycerol caprylate, 0.002 part of ferric citrate, 14 parts of dichloromethane, 14 parts of Achnatherum inebrians, 4 parts of humic acid, methyl α-naphthyl acetate 11 parts of sodium, 4 parts of heroubill.A small amount of three isooctyl acid glyceride and ferric citrate composition, can be with dichloromethane, Achnatherum inebrians etc. Plant component material is combined, and can reduce illness rate, enhance immunity.
The medicament-fertilizer mixture of above-mentioned preventing and treating crops virus infection is prepared from by following steps：
（1）, heroubill, Achnatherum inebrians are put into crushing, stirring in pulverizer, filter residue is carried out afterwards, obtain A mixtures；
（2）, A mixtures are poured into reactor and add methyl α-naphthyl acetate, potassium phosphate, Boron Nitride and surfactant, added It is stirred continuously in journey, mixing time is 10min, obtains B mixtures；
（3）, sequentially add in B mixtures agricultural active bacterium, ethephon (CEPHA),2-(chloroethyl) phosphonic acid, dichloromethane, humic acid, Nafusaku, three different pungent Acid glyceride, ferric citrate and surfactant, are heated afterwards, and heating-up temperature is 35 DEG C -55 DEG C, constant temperature 10min, Obtain C mixtures；
（4）, in C mixtures add composite nano silver and 1/3 surfactant, stirred after addition, be cooled to 60min is stood after normal temperature, that is, obtains preventing and treating the medicament-fertilizer mixture of crops virus infection.
Described above not limitation of the present invention, the present invention is also not limited to the example above.The art it is common In essential scope of the invention, change, remodeling, addition or the replacement made should also belong to protection of the invention to technical staff Scope.

Claims (6)

1. it is a kind of to prevent and treat the medicament-fertilizer mixture that crops virus infects, it is characterised in that to be made up of following raw material and its parts by weight： Composite nano silver 20-30 parts, methyl α-naphthyl acetate 3-9 parts, potassium phosphate 3-6 parts, 2-7 parts of agricultural active bacterium, Boron Nitride 3-7 parts, it is three different pungent Acid glyceride 0.001-0.005 parts, ferric citrate 0.001-0.003 parts, ethephon (CEPHA),2-(chloroethyl) phosphonic acid 1-3 parts, surfactant 10-15 parts, Dichloromethane 10-15 parts, Achnatherum inebrians 10-15 parts, humic acid 3-6 parts, Nafusaku 8-15 parts, heroubill 2-8 parts.
2. it is according to claim 1 it is a kind of prevent and treat crops virus infection medicament-fertilizer mixture, it is characterised in that preferably by with Lower raw material and its parts by weight are constituted：23 parts of composite nano silver, 4 parts of methyl α-naphthyl acetate, 4 parts of potassium phosphate, 5 parts of agricultural active bacterium, nitric acid 4 parts of boron, 0.002 part of three isooctyl acid glyceride, 0.002 part of ferric citrate, 2 parts of ethephon (CEPHA),2-(chloroethyl) phosphonic acid, 12 parts of surfactant, dichloromethane 14 parts of alkane, 14 parts of Achnatherum inebrians, 4 parts of humic acid, 8 parts of Nafusaku, 6 parts of heroubill.
3. the medicament-fertilizer mixture that a kind of preventing and treating crops virus according to claim 1 infects, it is characterised in that described compound The preparation method of Nano Silver is：
1）Silver nitrate solution is weighed in proportion to be placed in beaker, then is proportionally added into sodium hydroxide solution thereto, be aged 36h, Fully reaction is obtained predecessor；
2）By in step 1 predecessor filtering, it is and multiple with milli-Q water；
3）Predecessor after the filtering of step 2 gained is placed in baking oven, 80 DEG C of baking 5h obtain clean filter residue；
4）Oxalic acid and zinc chloride are weighed according to formula rate, water saturation solution is each configured to, by the water-soluble of oxalic acid and zinc chloride Liquid is mixed, and is sufficiently stirred for 50 min, and product is stood, and fully washing exists to without chlorion, is then put into 120 DEG C 3~4 h are dried in baking oven, mix products are obtained；
5）Product in product and step 4 in dry step 3 is uniformly mixed and ground, is placed in Muffle furnace, 600 DEG C of guarantors Hold 2h；
6）Cooling, grinding, prepared nanometer silver-ZnO fungicide mixture；
7）The nanometer silver-ZnO fungicide mixture of step 6 gained is added in silester is fully hydrolyzed it, then Acidifying in hydrochloric acid is placed on, the mixed liquor of isopropyl titanium and isopropanol is finally added, reacted 8-16 hours, that is, obtain titanium dioxide The nanometer silver-ZnO compound particle of covering.
4. the medicament-fertilizer mixture that a kind of preventing and treating crops virus according to claim 1 infects, it is characterised in that described agricultural Active bacteria is：Agricultural active bacterium, edible oil monad, bacillus licheniformis.
5. the medicament-fertilizer mixture that a kind of preventing and treating crops virus according to claim 1 infects, it is characterised in that preparation method For：
1）, heroubill, Achnatherum inebrians are put into crushing, stirring in pulverizer, filter residue is carried out afterwards, obtain A mixtures；
2）, A mixtures are poured into reactor and add methyl α-naphthyl acetate, potassium phosphate, Boron Nitride and surfactant, adition process In be stirred continuously, mixing time is 10min, obtains B mixtures；
3）, agricultural active bacterium, ethephon (CEPHA),2-(chloroethyl) phosphonic acid, dichloromethane, humic acid, Nafusaku and surface are sequentially added in B mixtures Activating agent, is heated afterwards, and heating-up temperature is 35 DEG C -55 DEG C, and constant temperature 10min obtains C mixtures；
4）, in C mixtures add composite nano silver and 1/3 surfactant, stirred after addition, be cooled to often 60min is stood after temperature, that is, obtains preventing and treating the medicament-fertilizer mixture of crops virus infection.
6. the medicament-fertilizer mixture that a kind of preventing and treating crops virus according to claim 1 infects, it is characterised in that of the invention The application method of the medicament-fertilizer mixture of preventing and treating crops virus infection is, if using crops, by the dosage and water of 1-5% Mixing, sprinkling；If using trees, it can be mixed with water by the dosage of 1-3%, pouring is used.
CN201611147600.6A 2016-12-13 2016-12-13 The medicament-fertilizer mixture of preventing and treating crops virus infection Pending CN106818901A (en)

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CN106070357A (en) * 2016-06-20 2016-11-09 河南中天恒信生物化学科技有限公司 A kind of novel wheat field compound disinfectant and application thereof

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CN102210324A (en) * 2010-04-09 2011-10-12 中国科学院海洋研究所 Selective bactericide with composite nanoparticles as well as preparation and application thereof
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Application publication date: 20170613