CN106813955B - Canned sample gas sampling device in petroleum and natural gas exploration laboratory - Google Patents

Canned sample gas sampling device in petroleum and natural gas exploration laboratory Download PDF

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Publication number
CN106813955B
CN106813955B CN201710078779.2A CN201710078779A CN106813955B CN 106813955 B CN106813955 B CN 106813955B CN 201710078779 A CN201710078779 A CN 201710078779A CN 106813955 B CN106813955 B CN 106813955B
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cup
bowl
inner sleeve
screw rod
tank
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CN201710078779.2A
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CN106813955A (en
Inventor
明晓峰
赵建勇
吴刚
孙道武
李淑慧
田辉
解永华
刘艳
杨冰
李冬
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Shengli Geological Logging Co Of Sinopec Jingwei Co ltd
Sinopec Oilfield Service Corp
Sinopec Shengli Petroleum Engineering Corp
Sinopec Jingwei Co Ltd
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Shengli Geological Logging Co Of Sinopec Jingwei Co ltd
Sinopec Oilfield Service Corp
Sinopec Shengli Petroleum Engineering Corp
Sinopec Jingwei Co Ltd
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Priority to CN201710078779.2A priority Critical patent/CN106813955B/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/22Devices for withdrawing samples in the gaseous state
    • G01N1/2226Sampling from a closed space, e.g. food package, head space

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention provides a canned sample gas taking device for an oil and gas exploration laboratory, which belongs to the technical field of oil and gas exploration, and has the structure that a tank cup is fixedly arranged on the upper surface of a chassis, the bottom edge of the tank cup is fixedly welded with the chassis, a canned sample tank is seamlessly seated in the tank cup, an outer sleeve cup is sleeved on the periphery of the tank cup, an outer sleeve bowl is arranged above the outer sleeve cup, and a flat top cover is arranged at the top of the outer sleeve bowl; the center of the screw rod is provided with an air passage which is vertically communicated; the lower end of the screw rod is fixedly connected with an inner sleeve bowl, the top end of the inner sleeve bowl is fixedly connected with the screw rod and communicated with the air passage, and the top end of the screw rod is fixedly connected with an air outlet quick lock joint. The petroleum and natural gas exploration laboratory canned sample gas taking device fully eliminates adverse factors of gas taking by a drainage method in specific application, improves scientific high efficiency of gas taking of a laboratory canned sample tank, improves quality of light hydrocarbon logging of tank top gas, and powerfully supports achievement of maximization of oil and gas exploration benefits.

Description

Canned sample gas sampling device in petroleum and natural gas exploration laboratory
Technical Field
The invention relates to the technical field of petroleum and natural gas exploration, in particular to a canned sample gas taking device for a petroleum and natural gas exploration laboratory.
Background
In oil and gas exploration, the identification and evaluation of an oil and gas water layer are one of important links in oil and gas exploration and development work, and the application of new logging technology has recently attracted more and more attention from domestic and foreign specialists and scholars. In recent years, along with the gradual deep exploration of oil fields, the objects of resource exploration are more diversified, including shale gas, coalbed methane and the like, the oil-gas-water relationship of exploration blocks is more and more complex, and higher requirements are put forward on the oil-gas reservoir identification and evaluation technology. Especially, the judgment difficulty of the light oil layer, the residual oil layer, the high mud-containing reservoir and the volcanic gas-water layer is higher, and the requirement of fine evaluation cannot be met only by means of the conventional single logging technology for qualitative interpretation of the oil-gas layer. Through the continuous efforts of a large number of logging workers, the logging has moved from the traditional logging to a new stage of modern comprehensive evaluation logging, forms a new modern logging technology integrating on-site data acquisition, data, processing and hydrocarbon reservoir interpretation and evaluation, and plays an increasingly important role in the exploration and development of hydrocarbon resources. Through technical innovation and development, the comprehensive logging technology, the under-lens fluorescence analysis technology, the interpretation and evaluation technology and the like are sequentially applied to the on-site logging, so that the comprehensive logging realizes the crossover development. Meanwhile, a complete set of evaluation technical systems for light oil layer, residual oil layer, high mud-containing reservoir, gas-water layer recognition evaluation and the like are formed by overcoming the technical problems of complex oil-gas-water layer recognition evaluation.
The method for quantitatively evaluating the hydrocarbon reservoir by comprehensively using the new logging technology is a very difficult problem, and not only is the application of the new technology required, but also the synthesis of multiple disciplines such as geological logging, logging and the like is required. The gas light hydrocarbon logging on the top of the tank is an important work, and the basis of the work is collection and operation work of the gas dissipated by the tank sample.
The tank top gas is a mixed gas of hydrocarbon and air which is stored in the top space of the canned rock debris (core) and reaches gas-liquid phase balance with the liquid at the lower part, wherein the hydrocarbon is naturally desorbed from the rock debris (core). The light hydrocarbon logging of the tank top gas is to inject a tank top gas sample into a gas chromatograph for analysis, so that the light hydrocarbon components of the tank top gas are completely separated, and the light logging method of the oil gas light hydrocarbon components is obtained. The top gas of the tank detects common C1-C7 hydrocarbon components in crude oil, including 7 normal paraffins, 13 isoparaffins, 8 naphthenes and 1 aromatic hydrocarbon (benzene), and 29 monomer components. Compared with the gas logging which can only detect C1-C5 hydrocarbon components, the light hydrocarbon information obtained by the gas logging on the tank top is more abundant and comprehensive. The light hydrocarbon is partially volatilized and dissipated before the rock scraps (cores) are canned, so that the light hydrocarbon in the tank top gas is substantially the result of natural desorption and dissipation of the residual light hydrocarbon after the light hydrocarbon in the rock scraps (cores) is partially volatilized. Compared with the light hydrocarbon in the original stratum, the light hydrocarbon composition (component number) of the tank top gas is basically the same, the composition of the stratum light hydrocarbon is reflected, and the abundance of the tank top gas light hydrocarbon is closely related to the abundance of the stratum light hydrocarbon and the light hydrocarbon escape and volatilization degree of the sample tank. The relative content of the light hydrocarbon in the tank top gas is the result of the combined action of the light hydrocarbon in the stratum on the physical properties of the oil layer, the property of the crude oil, the light hydrocarbon content in the crude oil, the performance of the drilling fluid and other factors. The gas-light hydrocarbon logging on the top of the tank is based on the abundance of light hydrocarbon, the composition of light hydrocarbon is used as a reference, the relative content of light hydrocarbon is used as a main basis to judge the activity degree of light hydrocarbon, then the activity degree of hydrocarbon reservoir is pushed out through the activity degree of light hydrocarbon, and finally the aim of judging hydrocarbon reservoir is achieved, so the gas-light hydrocarbon logging on the top of the tank plays a very important role in oil and gas exploration, and as mentioned above, the laboratory gas-taking work of the rock debris (core) tank sample is a key basic work because the gas-taking work is an important link, namely the quantity, affecting the analysis of the gas-light hydrocarbon on the top of the tank.
The collection of gas from a laboratory in a chip (core) can sample is a critical operation for ensuring the complete collection of light hydrocarbon components. In general, in a drainage and air extraction method used by a laboratory operator in a conventional air extraction mode, namely, a canning sample tank for collecting and canning on site is vertically arranged (the canning sample tank is stored and transported upside down after being collected on site, so as to prevent air from volatilizing from a tank cover), the canning sample tank is placed into water, a tank body is held by one hand, a plastic bag is held by the other hand, the tank cover is rotated by the hand for holding the plastic bag, and light hydrocarbon gas which is scattered from rock debris (cores) after the tank cover is unscrewed and accumulated in the top space in the tank can enter the plastic bag (because the gas is insoluble in water); then, the operator takes out the plastic bag from the water and tightens the plastic bag, then the plastic bag is pumped out of the plastic bag by the injector, and the gas is injected into the analysis equipment for detection and analysis, and the gas taking operation steps are repeated after the analysis is finished. This type of gas extraction is original and is also commonly used because there is no better method and apparatus for extracting gas from a canned sample tank. However, this gas extraction method has a number of disadvantages, which directly affect the tank top gas analysis. In summary, there are several disadvantages:
1. the plastic bag is covered, the cover is screwed to take out air, so that the plastic bag is damaged, and the air can escape into the atmosphere after the plastic bag is damaged, so that the canned sample air is wasted, the irreparable data loss is caused, and the exploration benefit is reduced;
2. clean fresh water is used for draining and taking gas, and is a waste of fresh water resources; meanwhile, plastic garbage is formed after the plastic bag is damaged, so that the environment is polluted;
3. the space volume of the plastic bag is not quantitative, so that the gas extracted by the injector cannot be quantitative, and the analysis working quality is affected;
4. after the plastic bag is drained and gas is taken out, the plastic bag is required to be contacted with air when being taken out from the water, and the gas collected in the period is required to be diluted to different degrees, so that the gas analysis quality and the oil-gas exploration benefit are affected;
5. the drill cuttings (cores) in the tank are mixed with the drilling fluid, so that when an operator unscrews the tank cover, the drilling fluid is mixed with the drill cuttings (cores) to infect fresh water, and hands are corroded after being immersed for a long time, so that occupational health of the operator is damaged;
6. the tank body is smooth, the periphery of the tank cover is provided with shallow threads, and under the condition that the tank cover is very tight, operators can hardly unscrew the tank cover, which is time-consuming and labor-consuming;
7. in winter, the temperature of water is low, and the operator can soak hands in cold water for a long time, which is more unfavorable for physical health.
In short, according to the conventional laboratory drainage gas extraction method, various possible situations can occur in the gas extraction process, and meanwhile, the necessity such as gas dilution, loss and the like also exists, and all the problems affect the scientificity and the high efficiency of the final light hydrocarbon analysis, so that the benefit of oil and gas exploration is directly affected.
Disclosure of Invention
The invention aims to solve the defects of the prior art and provides a canned sample gas taking device for an oil and gas exploration laboratory.
The technical scheme of the invention is realized in the following manner that the oil and gas exploration laboratory canning sample gas sampling device structurally comprises a chassis, a can cup, an outer sleeve cup, an inner sleeve bowl and an outer sleeve bowl;
the upper surface of the chassis is fixedly provided with a tank cup, the bottom edge of the tank cup is fixedly welded with the chassis, a tank sample tank is seamlessly arranged in the tank cup, and the wall of the tank cup is provided with an inner sleeve wire hole;
the periphery edge of the upper surface of the chassis is provided with a bearing lock catch on the same circumference, and the inner periphery of the bearing lock catch is provided with an annular sealing ring; the bottom edge of the tank cup is arranged at the inner periphery of the sealing ring;
the periphery of the pot cup is sleeved with an outer sleeve cup, the outer sleeve cup is arranged in a hollow column shape, and the periphery of the bottom edge of the outer sleeve cup is provided with a clamping lock catch; the clamping lock catch corresponds to the bearing lock catch, the outer cup is fixedly connected with the chassis through the rotary lock catch of the clamping lock catch and the bearing lock catch, the bottom edge of the outer cup is in pressure lock fit and is arranged on the sealing ring, and the outer cup is in sealing connection with the chassis;
the side wall of the outer sleeve cup is provided with a through hole which is coaxially matched with the inner sleeve wire hole and internally and externally corresponds to the inner sleeve wire hole;
an inner sleeve screw cap is fixedly welded on the outer wall of the through hole, and a fastening screw rod is screwed into the inner sleeve screw cap, passes through the through hole and is screwed into the inner sleeve screw hole of the can cup;
an outer sleeve bowl is arranged above the outer sleeve cup, the bottom outer wall of the outer sleeve bowl and the top outer wall of the outer sleeve cup are fixed and integrally welded, and the outer sleeve bowl is in a conical cylinder shape with the upper end reduced in diameter and the lower end expanded in diameter;
the top of the coat bowl is provided with a flat top cover; the center of the flat top cover is provided with a hole, a nut seat is horizontally welded above the hole, the nut seat is screwed with a screw rod, the screw rod penetrates up and down and protrudes out of the nut seat,
the center of the screw rod is provided with an air passage which is vertically communicated;
the lower end of the screw rod is fixedly connected with an inner sleeve bowl, the inner sleeve bowl is arranged in the inner cavity of the outer sleeve bowl, and the inner sleeve bowl is in a cone shape with a reduced top end and an expanded bottom end;
the top end of the inner sleeve bowl is fixedly connected with the screw rod and communicated with the air passage,
an inner sleeve bowl circular hoop is welded at the bottom end of the inner sleeve bowl; the inner ring of the inner sleeve bowl circular hoop is uniformly provided with vertical sleeve teeth which are matched with tooth grooves at the top of the canned sample tank; the inner sleeve bowl circular hoop is vertically sleeved with teeth and a tooth slot at the top of the canned sample pot form an airflow passage;
the top end of the screw rod is fixedly connected with an air outlet quick lock joint; the air outlet quick lock joint is communicated with the air passage;
a disc-shaped rocking disc is fixedly arranged on the neck of the screw rod below the air outlet quick lock joint; the rocking disc, the screw rod and the inner sleeve bowl are fixedly connected into a whole, and the rocking disc rotates to drive the screw rod to rotate, so that the inner sleeve bowl is pushed in and out of the inner sleeve bowl by threads, and the inner sleeve bowl slides up and down in the inner cavity of the outer sleeve bowl.
The outer wall of the inner sleeve bowl is in airtight sliding sleeve joint with the inner wall of the outer sleeve bowl.
The air outlet quick lock joint is internally provided with an air flow pressing opening and closing valve.
The chassis, the outer cup and the outer bowl form an airtight space.
The nut seat is in airtight threaded connection with the screw rod; the fastening screw rod is in airtight threaded connection with the inner sleeve screw cap.
The outer wall of the outer cup is provided with a lock catch clamping holding lug.
Compared with the prior art, the invention has the following beneficial effects:
the petroleum and natural gas exploration laboratory canning sample gas sampling device fully eliminates adverse factors of gas sampling by a drainage method in specific application, improves scientific and high-efficiency of gas sampling by a laboratory canning sample tank, protects occupational health of operators, saves fresh water resources, reduces material loss, protects environment, improves quality of light hydrocarbon logging of tank top gas, and powerfully supports achievement of maximization of oil and gas exploration benefits.
The canned sample gas sampling device for the petroleum and natural gas exploration laboratory has the following performances and advantages:
1. the sealed tank body gas taking eliminates the situation that the gas can not be collected again due to dissipation after the plastic bag is damaged in the drainage gas taking, avoids data loss and improves exploration benefits;
2. the drainage method is not used for taking air, so that fresh water resources are saved; no plastic bag is used, so that the pollution of plastic garbage to the environment is reduced;
3. the space volume of the sealed tank body is quantitative, so that the quantification of the gas extracted by the injector is realized, and the gas analysis working quality is ensured;
4. the gas dissipated into the sealed tank body is not contacted with surrounding air, and the collected gas is not diluted by air, so that the gas analysis is more real and reliable, and the oil and gas exploration benefit is improved;
5. operators do not need to contact polluted liquid, so that the corrosion of hands is avoided, and the occupational health of practitioners is strongly protected;
6. the tank body is firmly fixed in a certain space range with a certain volume, and the mechanical screwing is more convenient to operate, and saves time and labor;
7. because no water source is needed, the problem of winter and summer water temperature is not needed to be considered, the cost is saved, and the cost reduction and synergy are realized.
The canned sample gas taking device in the petroleum and natural gas exploration laboratory is an invention design which is high-efficiency and reliable in application, can play a positive and remarkable role in the operation of canned sample gas taking, and can be used in the working field similar to canned sample gas taking.
The canned sample gas sampling device for the petroleum and natural gas exploration laboratory has the advantages of reasonable design, simple structure, safety, reliability, convenient use, easy maintenance and good popularization and use values.
Drawings
Fig. 1 is a schematic diagram of the structure of the present invention.
The reference numerals in the drawings denote:
1. chassis, 2, can cup, 3, can sample can, 4, inner sleeve screw hole, 5, bearing lock catch, 6, sealing ring,
7. an outer sleeve cup 8, a clamping lock catch 9, a through hole 10, an inner sleeve screw cap 11, a fastening screw rod,
12. the outer bowl, 13, the flat top cover, 14, the hole, 15, the nut seat, 16, the screw rod, 17, the air passage, 18, the inner bowl, 19, the inner bowl circular hoop, 20, the vertical sleeve tooth, 21, the tooth socket, 22 and the air flow passage,
23. the air outlet quick lock joint, 24, the rocking disc, 25, the air flow pressing opening and closing valve, 26 and the lock catch clamping holding lug.
Detailed Description
The canned sample gas sampling device for petroleum and natural gas exploration laboratories of the present invention is described in detail below with reference to the accompanying drawings.
As shown in the attached drawing, the canned sample gas taking device for the petroleum and natural gas exploration laboratory structurally comprises a chassis, a can cup, an outer sleeve cup, an inner sleeve bowl and an outer sleeve bowl;
the upper surface of the chassis 1 is fixedly provided with a pot cup 2, the bottom edge of the pot cup 2 is fixedly welded with the chassis 1, a pot sample pot 3 is seamlessly seated in the pot cup 2, and the wall of the pot cup 2 is provided with an inner sleeve wire hole 4;
the periphery edge of the upper surface of the chassis 1 is provided with a bearing lock catch 5 on the same circumference, and the inner periphery of the bearing lock catch 5 is provided with an annular sealing ring 6; the bottom edge of the tank cup is arranged at the inner periphery of the sealing ring;
the outer periphery of the pot cup 2 is sleeved with an outer sleeve cup 7, the outer sleeve cup 7 is arranged in a hollow column shape, and the periphery of the bottom edge of the outer sleeve cup 7 is provided with a clamping lock catch 8; the clamping lock catch 8 corresponds to the bearing lock catch 5, the outer cup 7 is fixedly connected with the chassis 1 through the rotary lock catch of the clamping lock catch 8 and the bearing lock catch 5, the bottom edge pressure lock of the outer cup 7 is buckled and arranged on the sealing ring 6, and the outer cup 7 is in sealing connection with the chassis 1;
the side wall of the outer sleeve cup 7 is provided with a through hole 9, and the through hole 9 is coaxially matched with the inner sleeve wire hole 4 and internally and externally corresponds to the inner sleeve wire hole;
an inner sleeve screw cap 10 is fixedly welded on the outer wall of the through hole 9, and a fastening screw rod 11 is screwed into the inner sleeve screw cap 10, passes through the through hole 9 and is screwed into the inner sleeve screw hole 4 of the can cup;
an outer sleeve bowl 12 is arranged above the outer sleeve cup 7, the bottom outer wall of the outer sleeve bowl 12 and the top outer wall of the outer sleeve cup 7 are fixed and integrally welded, and the outer sleeve bowl 12 is in a conical cylinder shape with the upper end reduced in diameter and the lower end expanded in diameter;
the top of the coat bowl 12 is provided with a flat top cover 13; the center of the flat top cover 13 is provided with a hole, a nut seat 15 is horizontally welded above the hole 14, a screw rod 16 is screwed on the nut seat 15, the screw rod 16 penetrates up and down and protrudes out of the nut seat 15,
an air passage 17 which is vertically communicated is formed in the center of the screw rod 16;
the lower end of the screw rod 16 is fixedly connected with an inner sleeve bowl 18, the inner sleeve bowl 18 is arranged in the inner cavity of the outer sleeve bowl, and the inner sleeve bowl is in a cone shape with a reduced top end and an expanded bottom end;
the top end of the inner sleeve bowl 18 is fixedly connected with the screw rod and communicated with the air passage,
an inner bowl circular hoop 19 is welded at the bottom end of the inner bowl 18; the inner ring of the inner sleeve bowl circular hoop 19 is uniformly provided with vertical sleeve teeth, and the vertical sleeve teeth 20 are matched with tooth grooves 21 at the top of the canned sample pot; the inner bowl circular hoop 19 is vertically sleeved with teeth and a tooth slot 21 at the top of the canned sample pot 3 to form an airflow passage 22;
the top end of the screw rod 16 is fixedly connected with an air outlet quick lock joint 23; the air outlet quick lock joint 23 is communicated with the air passage 17;
a disc-shaped rocking disc 24 is fixedly arranged on the neck of the screw rod below the air outlet quick lock joint 23; the rocking disc, the screw rod and the inner sleeve bowl are fixedly connected into a whole, and the rocking disc rotates to drive the screw rod to rotate, so that the inner sleeve bowl is pushed in and out of the inner sleeve bowl by threads, and the inner sleeve bowl slides up and down in the inner cavity of the outer sleeve bowl.
The outer wall of the inner sleeve bowl 18 is in airtight sliding sleeve connection with the inner wall of the outer sleeve bowl 12.
The air outlet quick lock joint 23 is internally provided with an air flow pressing opening and closing valve 25.
The chassis 1, the coat cup 7 and the coat bowl 12 form an airtight space.
The nut seat 15 and the screw rod 16 are in airtight threaded connection; the fastening screw rod 11 is in airtight threaded connection with the inner sleeve screw cap 10.
The outer wall of the outer cup is provided with a lock catch clamping holding lug 26.
The whole canned sample gas taking device of the petroleum and natural gas exploration laboratory is made of stainless steel, the sealing rubber cushion is used for sealing, and the main components comprise a chassis, a tank cup, an outer sleeve cup, an inner sleeve bowl, an outer sleeve bowl, a screw rod, a rocking disc and a gas outlet quick-locking joint.
And (5) a chassis. The chassis is a disc, the thickness is 5mm, the diameter is 300mm, 4 fixing bolt holes are formed in the periphery of the disc, the aperture is 6mm, and the chassis can be fixed on other supports. Three locks are arranged on the chassis, and when the outer sleeve cup sits in the sealing rubber pad, the holding lug is twisted to be buckled and sealed with the lock catch on the outer sleeve cup.
And (5) filling the pot cup. The tank cup is welded at the center of the chassis, the hollow cone-shaped tank is hollow, the top inner diameter is 83mm, the bottom inner diameter is 80mm, the wall thickness is 5mm, the height is 95mm, and the canned sample tank can be seamlessly seated. A sleeve thread hole with the diameter of 8mm is formed at the position 47.5mm away from the bottom edge on one side of the middle part of the cylinder body of the pot cup. The periphery of the pot cup is provided with a plastic deformation sealing rubber cushion, and the mantle fiber cup can be sealed and located in the rubber cushion.
⒊ outer cup. The outer cup is a hollow column with the height of 200mm, the inner diameter of 110mm and the wall thickness of 5mm. Three locks are uniformly arranged on the bottom edge of the outer cup and are used for being in sealing butt joint with the locks on the chassis. One side of the outer cup is provided with a hole with the diameter of 8mm at the position 47.5mm away from the bottom edge, the outer wall is provided with a screw cap, and a fastening screw rod passes through the threading hole of the cup through the hole to fix the canning sample pot. After the outer sleeve cup and the tank cup are connected and sealed through the lock catch, the two holes are exactly and completely matched, and an drift diameter is formed for fastening the sleeve wire rod. After the gas is taken out, the tightening force on the canned sample tank is removed by screwing the sleeve screw rod, then the holding lug is held for reverse rotation, the connection between the sleeve cup and the tank cup can be removed, and then the next canned sample gas taking operation is performed.
4. And (5) a bowl is sleeved outside. The outer bowl and the outer cup are connected in the path and can be used as a whole. The outer bowl is conical with a narrow upper part and a wide lower part, the lower part and the outer cup have the through diameters of 110mm in inner diameter and 5mm in wall thickness; the inner diameter of the upper part is 70mm, and the height of the outer bowl is 100mm. The top of the coat bowl is a flat top cover, a hole is formed in the middle of the coat bowl, the aperture is 25mm, and a screw cap with the aperture of 25mm is welded above the hole. The screw rod is screwed in and out through the screw cap.
5. And a screw rod. The screw rod is a screw rod with the diameter of 25mm, the whole length of 150mm and the no-wire length of 50mm. The center of the screw rod is hollow to form an air passage, the air passage is communicated with the inner sleeve bowl, the hollow drift diameter is 5mm, the top of the screw rod is connected with an air outlet quick lock joint, a passage is formed with the air passage, a flexible pipeline can be connected to the quick lock joint, and the flexible pipeline can be directly connected to gas analysis equipment. The quick-locking connector is divided into a male connector and a female connector, the male connector is inserted into the female connector, a locking ring on the female connector can be pressed to be ejected, and a screw rod of the female connector is fixedly sleeved. A round rocking disc is welded at the position 20mm away from the top of the whole screw rod at the non-screw position of the upper screw rod, the rocking disc is 10mm thick and 150mm in diameter, anti-skid threads are arranged on the gripping surface of the rocking disc, the screw rod is rotated by hands, and the screw rod drives the inner sleeve bowl to rotate.
6. And (5) an inner sleeve bowl. The inner sleeve bowl can be rotated high and low in a cavity formed by the outer sleeve bowl and the outer sleeve cup by rotating the screw rod, the inner diameter of the upper part of the inner sleeve bowl is 30mm, and the wall thickness is 3mm; the outer diameter of the lower part is 108mm, and the height of the inner sleeve bowl is 80mm. The top of the inner sleeve bowl is welded with the screw rod and is also connected with the air passage. The lower part of the inner sleeve bowl is welded with an inner sleeve bowl mantle fiber.
7. The bowl is sleeved with the wire. The lower part of the inner sleeve bowl is welded with a hollow round hoop (inner sleeve bowl threading), the outer diameter of the round hoop is 108mm, the inner diameter is 98mm, the wall thickness is 5mm, and the height is 25mm. 13 vertical sleeve teeth are uniformly distributed on the inner ring of the circular hoop, the tooth height is 20mm, the tooth depth is 1mm, the sleeve teeth can be eaten into tooth grooves on the tank cover, and the tooth grooves between the sleeve teeth and the tooth grooves of the tank cover form a gas circulation passage. The screw rod rotates to drive the inner sleeve bowl sleeve wire to rotate, and the tank cover is unscrewed under the action of torsion. After the tank cover is unscrewed, gas escapes, high pressure is formed in the sealed tank body device, the quick-locking joint is pressed, and the gas can move from the high pressure to the low pressure along the air passage.
The laboratory canned sample gas sampling device has reasonable design, is easy and convenient to operate, and does not need special maintenance. The canned sample can body is placed in the can cup and is seamlessly accommodated in the can cup, and the can cover is fastened by the fastening sleeve wire rod, so that the can cover can be unscrewed more conveniently. The outer sleeve cup and the tank cup are tightly sealed, so that gas cannot escape into the surrounding atmosphere, and the gas is taken out through the gas outlet quick-locking connector, so that the quantification of the gas taking is realized. The hand shaking plate drives the inner sleeve bowl threading to rotate, so that the tank cover can be conveniently detached, and the reverse shaking plate can be lifted off the tank cover. The outer sleeve cup is tightly buckled with the sealing rubber pad, the lock catch is connected with the outer sleeve cup and the tank cup, gas dissipated after the tank cover is unscrewed is completely limited in the whole limited space range, and the gas for tank top gas analysis is purer, and the analysis result is more real and accurate.

Claims (3)

1. The canned sample gas taking device for the petroleum and natural gas exploration laboratory is characterized by comprising a chassis, a can cup, an outer sleeve cup, an inner sleeve bowl and an outer sleeve bowl;
the upper surface of the chassis is fixedly provided with a tank cup, the bottom edge of the tank cup is fixedly welded with the chassis, a tank sample tank is seamlessly arranged in the tank cup, and the wall of the tank cup is provided with an inner sleeve wire hole;
the periphery edge of the upper surface of the chassis is provided with a bearing lock catch on the same circumference, and the inner periphery of the bearing lock catch is provided with an annular sealing ring; the bottom edge of the tank cup is arranged at the inner periphery of the sealing ring;
the periphery of the pot cup is sleeved with an outer sleeve cup, the outer sleeve cup is arranged in a hollow column shape, and the periphery of the bottom edge of the outer sleeve cup is provided with a clamping lock catch; the clamping lock catch corresponds to the bearing lock catch, the outer cup is fixedly connected with the chassis through the rotary lock catch of the clamping lock catch and the bearing lock catch, the bottom edge of the outer cup is in pressure lock fit and is arranged on the sealing ring, and the outer cup is in sealing connection with the chassis;
the side wall of the outer sleeve cup is provided with a through hole which is coaxially matched with the inner sleeve wire hole and internally and externally corresponds to the inner sleeve wire hole;
fixedly welding an inner sleeve wire nut on the outer wall of the through hole, fastening a screw rod, screwing the inner sleeve wire nut into the through hole, and screwing the screw rod into the inner sleeve wire hole of the can cup;
an outer sleeve bowl is arranged above the outer sleeve cup, the bottom outer wall of the outer sleeve bowl and the top outer wall of the outer sleeve cup are fixed and integrally welded, and the outer sleeve bowl is in a conical cylinder shape with the upper end reduced in diameter and the lower end expanded in diameter;
the top of the coat bowl is provided with a flat top cover; the center of the flat top cover is provided with a hole, a nut seat is horizontally welded above the hole, the nut seat is screwed with a screw rod, the screw rod penetrates up and down and protrudes out of the nut seat,
the center of the screw rod is provided with an air passage which is vertically communicated;
the lower end of the screw rod is fixedly connected with an inner sleeve bowl, the inner sleeve bowl is arranged in the inner cavity of the outer sleeve bowl, and the inner sleeve bowl is in a cone shape with a reduced top end and an expanded bottom end;
the top end of the inner sleeve bowl is fixedly connected with the screw rod and communicated with the air passage,
an inner sleeve bowl circular hoop is welded at the bottom end of the inner sleeve bowl; the inner ring of the inner sleeve bowl circular hoop is uniformly provided with vertical sleeve teeth which are matched with tooth grooves at the top of the canned sample tank; the inner sleeve bowl circular hoop is vertically sleeved with teeth and a tooth slot at the top of the canned sample pot form an airflow passage;
the top end of the screw rod is fixedly connected with an air outlet quick lock joint; the air outlet quick lock joint is communicated with the air passage;
a disc-shaped rocking disc is fixedly arranged on the neck of the screw rod below the air outlet quick lock joint; the rocking disc, the screw rod and the inner sleeve bowl are fixedly connected into a whole, and the rocking disc rotates to drive the screw rod to rotate, so that the inner sleeve bowl is pushed in and out of the inner sleeve bowl by threads, and the inner sleeve bowl slides up and down in the inner cavity of the outer sleeve bowl;
the outer wall of the inner sleeve bowl is in airtight sliding sleeve joint with the inner wall of the outer sleeve bowl;
the air outlet quick lock joint is internally provided with an air flow pressing opening and closing valve;
the chassis, the outer cup and the outer bowl form an airtight space.
2. The petroleum and natural gas exploration laboratory canned sample gas extraction apparatus of claim 1, wherein: the nut seat is in airtight threaded connection with the screw rod; the fastening screw rod is in airtight threaded connection with the inner sleeve screw cap.
3. The petroleum and natural gas exploration laboratory canned sample gas extraction apparatus of claim 1, wherein: the outer wall of the outer cup is provided with a lock catch clamping holding lug.
CN201710078779.2A 2017-02-14 2017-02-14 Canned sample gas sampling device in petroleum and natural gas exploration laboratory Active CN106813955B (en)

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CN108181138B (en) * 2017-12-29 2019-12-24 中国科学院广州地球化学研究所 Gas taking device of hydrocarbon source rock hydrocarbon generation thermal simulation reaction kettle
CN109991350B (en) * 2019-03-25 2023-09-12 中国石油化工股份有限公司 Gas chromatography analysis method for light hydrocarbon in top gas of rock debris tank and gas sampling and sampling device

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