CN106810591A - A kind of equipment that glycyrrhizic acid is extracted from Radix Glycyrrhizae - Google Patents
A kind of equipment that glycyrrhizic acid is extracted from Radix Glycyrrhizae Download PDFInfo
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- CN106810591A CN106810591A CN201710042925.6A CN201710042925A CN106810591A CN 106810591 A CN106810591 A CN 106810591A CN 201710042925 A CN201710042925 A CN 201710042925A CN 106810591 A CN106810591 A CN 106810591A
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- Prior art keywords
- tank body
- glycyrrhizic acid
- radix glycyrrhizae
- interior
- airduct
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07J—STEROIDS
- C07J63/00—Steroids in which the cyclopenta(a)hydrophenanthrene skeleton has been modified by expansion of only one ring by one or two atoms
- C07J63/008—Expansion of ring D by one atom, e.g. D homo steroids
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- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Extraction Or Liquid Replacement (AREA)
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Abstract
The invention discloses a kind of equipment that glycyrrhizic acid is extracted from Radix Glycyrrhizae, including：Extractor, ultrasonic oscillator and hot-gas system, the extractor include outer tank body and interior tank body, and the outer tank body is weldingly fixed on inner canister in vitro, and the ultrasonic oscillator is located in inner canister body；The hot-gas system includes air blower, heating tank, airduct and helix tube, the air blower connects heating tank by airduct, heater is set in the heating tank, heating tank is connected by airduct with helix tube, the helix tube is arranged on interior tank base, and the tube wall upper surface of helix tube is uniformly arranged stomata；Interior tank body top is also connected with steam outlet pipe, and the steam outlet pipe connects condenser pipe, and the condenser pipe is in serpentine, and condenser pipe is immersed in the cooling water in cooling cylinder.Homogeneous heating of the present invention is rapid, can quickly separate out glycyrrhizic acid and extract, and improves extraction efficiency and processing efficiency.
Description
Technical field
The present invention relates to glycyrrhizic acid extractive technique field, specifically a kind of equipment that glycyrrhizic acid is extracted from Radix Glycyrrhizae.
Background technology
Radix Glycyrrhizae is a kind of beneficial bowl spares herbal medicine, and medicinal part is root and rhizome, and Medicinal Materials Characters root is in cylinder, long by 25~
100cm, 0.6~3.5cm of diameter, indication is clearing heat and detoxicating, expelling phlegm and arresting coughing, gastral cavity abdomen etc..Happiness sunlight is abundant, and sunshine temperature long is low
Dry climate.Radix Glycyrrhizae is also widely used for food industry, refines candy, preserved fruit and chewing gum etc..
Radix Glycyrrhizae contains various chemical compositions, and main component has glycyrrhizic acid, liquiritin etc..The chemical composition of Radix Glycyrrhizae is extremely multiple
Miscellaneous, the compound isolated from Radix Glycyrrhizae so far has glycyrrhizin, enoxolone, liquiritin, isoliquiritin, new Radix Glycyrrhizae
Glucoside, neoisoliquiritin, glycyrrhizin, isoliquiritigenin and licoricidin, glycyrol, isoglycyrol, 7- methylcoumarins essence, umbrella shape flower
The tens of kinds of compounds such as lactone, wherein, glycyrrhizic acid is topmost active component in Radix Glycyrrhizae.Glycyrrhizic acid and its series of products, it is right
Sarcoma, papillomavirus, growth of cancer cells have inhibitory action, and the inhibiting rate to AIDS is more up to 90%, there is stronger increase people
Body immunity function is acted on, and is also good food additives and perfumery base.
It is that Radix Glycyrrhizae is dipped into water based on boiling method that the method for extraction Radix Glycyrrhizae is main from Radix Glycyrrhizae, and heating is boiled straight
The extraction of row glycyrrhizic acid is tapped into, such method is time-consuming more long, typically palpus 5-6 hours, and complicated component in extract solution, starch,
The impurity contents such as colloid, flavones are high, are that the treatment that is further purified of glycyrrhizic acid brings trouble, therefore the present invention to glycyrrhizic acid
Extracting method and equipment are improved, to improve the efficiency and production efficiency of glycyrrhizic acid extraction.
The content of the invention
It is an object of the invention to provide a kind of equipment that glycyrrhizic acid is extracted from Radix Glycyrrhizae, with solving above-mentioned background technology
The problem of proposition.
To achieve the above object, the present invention provides following technical scheme：
A kind of equipment that glycyrrhizic acid is extracted from Radix Glycyrrhizae, including：Extractor, ultrasonic oscillator and hot-gas system, it is described to carry
Taking tank includes outer tank body and interior tank body, and the outer tank body is weldingly fixed on inner canister in vitro, ultrasonic oscillator is installed in outer tank body
Controller, the ultrasonic oscillator controller is electrically connected with ultrasonic oscillator, and the ultrasonic oscillator is located at interior tank body
It is interior；The hot-gas system includes air blower, heating tank, airduct and helix tube, and the air blower connects heating tank by airduct,
Heater is set in the heating tank, and heating tank is connected by airduct with helix tube, and the helix tube is arranged on interior tank body bottom
Portion, the tube wall upper surface of helix tube is uniformly arranged stomata；Interior tank body top is also connected with steam outlet pipe, and the steam outlet pipe connection is cold
Solidifying pipe, the condenser pipe is in serpentine, and condenser pipe is immersed in the cooling water in cooling cylinder.
As further scheme of the invention：Vacuum chamber is left between the interior tank body and outer tank body.
As further scheme of the invention：The valve to pumping in it is provided on the vacuum chamber.
As further scheme of the invention：The diameter with diameter greater than airduct of the heating tank.
As further scheme of the invention：The heater is carbon fibre heating tube.
As further scheme of the invention：Purifying box is also set up between the heating tank and air blower, in the purifying box
Some groups of filter cottons are set.
As further scheme of the invention：Temperature detection rod is also set up in the inner canister body.
As further scheme of the invention：The temperature detection rod is arranged on the underface that steam goes out tube inlet.
As further scheme of the invention：The condenser pipe lower section sets collecting box.
Compared with prior art, the beneficial effects of the invention are as follows：Bubble is bloated by helix tube to be stirred mixed liquor,
And the heat in the air after heating gradually is mixed liquid and absorbs, gradually rise mixeding liquid temperature, bubble is contacted with mixed liquor
Compare fully, therefore be not in local temperature high and be charred, the low Radix Glycyrrhizae acid substance of local temperature is difficult to the problem for separating out, and works as temperature
When being increased to the fluidizing point of glycyrrhizic acid, glycyrrhizic acid enters in steam outlet pipe degree with air-flow, and in condenser pipe inner condensat liquid, most
Collection in collecting box is flowed into eventually, additionally, ultrasonic oscillator can carry out ultrasonic oscillation to mixed liquor, further speeds up Radix Glycyrrhizae each
Component seperation, makes glycyrrhizic acid be more easy to, from precipitation, improve extraction efficiency.
Brief description of the drawings
Fig. 1 is structural representation of the invention.
Specific embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation is described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.It is based on
Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of creative work is not made
Embodiment, belongs to the scope of protection of the invention.
Fig. 1 is referred to, in the embodiment of the present invention, a kind of equipment that glycyrrhizic acid is extracted from Radix Glycyrrhizae, including：It is extractor, super
Acoustic wave oscillator 5 and hot-gas system, the extractor include outer tank body 21 and interior tank body 22, and the outer tank body 21 is welded and fixed
Outside interior tank body 22, ultrasonic oscillator controller 1, the ultrasonic oscillator controller 1 and ultrasound are installed in outer tank body 21
Wave oscillator 5 is electrically connected, and the ultrasonic oscillator 5 is located in interior tank body 22；The hot-gas system includes air blower 6, heating
Tank 7, airduct 8 and helix tube 9, the air blower 6 are connected by airduct 8 and set in heating tank 7, the heating tank 7 heating dress
71 are put, heating tank 7 is connected by airduct 8 with helix tube 9, the helix tube 9 is arranged on the bottom of interior tank body 22, the pipe of helix tube 9
Wall upper surface is uniformly arranged stomata, can bloat air-flow from the stomata；The top of interior tank body 22 is also connected with steam outlet pipe 12, the steaming
Vapour outlet pipe 12 connects condenser pipe 13, and the condenser pipe 13 is in serpentine, and condenser pipe 13 is immersed in the cooling water in cooling cylinder 14.
Left between the interior tank body 22 and outer tank body 21 in vacuum chamber 4, vacuum chamber 4 and vacuumized, to completely cut off the air in it,
Lack the heat insulating ability that air can be improved in interior tank body 22 as heat-conducting medium, reducing energy consumption.
The valve 3 to pumping in it is provided on the vacuum chamber 4.
The diameter with diameter greater than airduct 8 of the heating tank 7, makes air-flow flow velocity reduction in heating tank 7, longer to obtain
Heat time.
The heater 71 is carbon fibre heating tube, and carbon fibre heating tube has the advantages that heat radiation is high, it is fast to generate heat, can
Quickly air-flow is set to be heated to uniform temperature.
Also set up between the heating tank 7 and air blower 6 and some groups of filter cottons be set in purifying box 61, the purifying box 61,
Air-flow can be filtered, prevent impurity from entering in extractor.
Temperature detection rod 11 is also set up in the interior tank body 22.
The temperature detection rod 11 is arranged on the underface of the entrance of steam outlet pipe 12, for detecting vapor (steam) temperature, prevents steam temperature
Spend height.
The lower section of the condenser pipe 13 sets collecting box 15, for collecting condensed glycyrrhizic acid.
Operation principle of the invention is：Air-flow is bloated by air blower 6, and enters heating in heating tank 7, then from spiral
Sprayed in the stomata of pipe 9, be stirred and produce bubble to mixed liquor, and the heat in air after heating gradually is mixed liquid
Absorb, gradually rise mixeding liquid temperature, bubble is contacted relatively fully with mixed liquor, therefore is not in local temperature high and burnt
Paste, the low Radix Glycyrrhizae acid substance of local temperature is difficult to the problem for separating out, when temperature is increased to the fluidizing point of glycyrrhizic acid, glycyrrhizic acid with
Air-flow enters in steam outlet pipe 12, and in the inner condensat liquid of condenser pipe 13, collection in collecting box 15 is finally flowed into, additionally, ultrasonic
Wave oscillator 5 can carry out ultrasonic oscillation to mixed liquor, further speed up the separation of Radix Glycyrrhizae each component, glycyrrhizic acid is more easy to from analysis
Go out, improve extraction efficiency.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be in other specific forms realized.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires to be limited rather than described above, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.Any reference in claim should not be considered as the claim involved by limitation.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each implementation method is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should
Specification an as entirety, the technical scheme in each embodiment can also be formed into those skilled in the art through appropriately combined
May be appreciated other embodiment.
Claims (9)
1. it is a kind of from Radix Glycyrrhizae extract glycyrrhizic acid equipment, including：Extractor, ultrasonic oscillator（5）And hot-gas system, institute
Stating extractor includes outer tank body（21）With interior tank body（22）, the outer tank body（21）It is weldingly fixed on interior tank body（22）Outward, it is special
Levy and be：Outer tank body（21）Upper installation ultrasonic oscillator controller（1）, the ultrasonic oscillator controller（1）With ultrasound
Wave oscillator（5）Electrical connection, the ultrasonic oscillator（5）Positioned at interior tank body（22）It is interior；The hot-gas system includes air blower
（6）, heating tank（7）, airduct（8）And helix tube（9）, the air blower（6）By airduct（8）Connection heating tank（7）, it is described
Heating tank（7）Interior setting heater（71）, heating tank（7）By airduct（8）With helix tube（9）Connection, the helix tube（9）
It is arranged on interior tank body（22）Bottom, helix tube（9）Tube wall upper surface be uniformly arranged stomata；Interior tank body（22）Top is also connected with steaming
Vapour outlet pipe（12）, the steam outlet pipe（12）Connection condenser pipe（13）, the condenser pipe（13）In serpentine, condenser pipe（13）Leaching
In cooling cylinder（14）In interior cooling water.
2. it is according to claim 1 it is a kind of from Radix Glycyrrhizae extract glycyrrhizic acid equipment, it is characterised in that：The interior tank body
（22）And outer tank body（21）Between leave vacuum chamber（4）.
3. it is according to claim 2 it is a kind of from Radix Glycyrrhizae extract glycyrrhizic acid equipment, it is characterised in that：The vacuum chamber
（4）On be provided for pumping in it valve（3）.
4. it is according to claim 1 it is a kind of from Radix Glycyrrhizae extract glycyrrhizic acid equipment, it is characterised in that：The heating tank
（7）With diameter greater than airduct（8）Diameter.
5. it is according to claim 1 it is a kind of from Radix Glycyrrhizae extract glycyrrhizic acid equipment, it is characterised in that：The heater
（71）It is carbon fibre heating tube.
6. it is according to claim 1 it is a kind of from Radix Glycyrrhizae extract glycyrrhizic acid equipment, it is characterised in that：The heating tank
（7）With air blower（6）Between also set up purifying box（61）, the purifying box（61）Some groups of filter cottons of interior setting.
7. it is according to claim 1 it is a kind of from Radix Glycyrrhizae extract glycyrrhizic acid equipment, it is characterised in that：The interior tank body
（22）Inside also set up temperature detection rod（11）.
8. it is according to claim 7 it is a kind of from Radix Glycyrrhizae extract glycyrrhizic acid equipment, it is characterised in that：The temperature detection rod
（11）It is arranged on steam outlet pipe（12）The underface of entrance.
9. it is according to claim 1 it is a kind of from Radix Glycyrrhizae extract glycyrrhizic acid equipment, it is characterised in that：The condenser pipe
（13）Lower section sets collecting box（15）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710042925.6A CN106810591B (en) | 2017-01-20 | 2017-01-20 | A kind of equipment for extracting glycyrrhizic acid from Radix Glycyrrhizae |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710042925.6A CN106810591B (en) | 2017-01-20 | 2017-01-20 | A kind of equipment for extracting glycyrrhizic acid from Radix Glycyrrhizae |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106810591A true CN106810591A (en) | 2017-06-09 |
| CN106810591B CN106810591B (en) | 2019-09-13 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710042925.6A Expired - Fee Related CN106810591B (en) | 2017-01-20 | 2017-01-20 | A kind of equipment for extracting glycyrrhizic acid from Radix Glycyrrhizae |
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| CN (1) | CN106810591B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113842667A (en) * | 2020-09-17 | 2021-12-28 | 湖南食尚康农业股份有限公司 | Sealwort extract product preparation equipment |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103800866A (en) * | 2012-11-01 | 2014-05-21 | 美梭生技股份有限公司 | Preparation method of Xiaoyao drink |
| CN204428881U (en) * | 2015-01-15 | 2015-07-01 | 漯河医学高等专科学校 | A kind of Radix Glycyrrhizae extraction element |
| CN204447387U (en) * | 2014-12-12 | 2015-07-08 | 成都彼斯特生物科技有限公司 | Ultrasonic wave multitple extraction Radix Glycyrrhizae solution containment |
| CN104983778A (en) * | 2015-06-29 | 2015-10-21 | 宁夏中汇天颐生物科技有限公司 | Method for continuously and comprehensively extracting liquorice ingredient with high pressure |
-
2017
- 2017-01-20 CN CN201710042925.6A patent/CN106810591B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103800866A (en) * | 2012-11-01 | 2014-05-21 | 美梭生技股份有限公司 | Preparation method of Xiaoyao drink |
| CN204447387U (en) * | 2014-12-12 | 2015-07-08 | 成都彼斯特生物科技有限公司 | Ultrasonic wave multitple extraction Radix Glycyrrhizae solution containment |
| CN204428881U (en) * | 2015-01-15 | 2015-07-01 | 漯河医学高等专科学校 | A kind of Radix Glycyrrhizae extraction element |
| CN104983778A (en) * | 2015-06-29 | 2015-10-21 | 宁夏中汇天颐生物科技有限公司 | Method for continuously and comprehensively extracting liquorice ingredient with high pressure |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113842667A (en) * | 2020-09-17 | 2021-12-28 | 湖南食尚康农业股份有限公司 | Sealwort extract product preparation equipment |
| CN113842667B (en) * | 2020-09-17 | 2023-01-24 | 湖北鄂达生物科技有限公司 | Sealwort extract product preparation equipment |
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| Publication number | Publication date |
|---|---|
| CN106810591B (en) | 2019-09-13 |
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| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20190819 Address after: 017008 Pharmaceutical Industrial Park, Hantai Town, Dongsheng District, Ordos City, Inner Mongolia Autonomous Region Applicant after: INNER MONGOLIA YILI PHARMACEUTICAL Co.,Ltd. Address before: 321000 Wucheng City, Jinhua Province Industrial and commercial district of Zhejiang City, building 3-302 room 3 Applicant before: JINHUA MINGZHENG TECHNOLOGY Co.,Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
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Granted publication date: 20190913 Termination date: 20220120 |
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| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190913 |