CN106807307A - Transparent tubular reactor - Google Patents
Transparent tubular reactor Download PDFInfo
- Publication number
- CN106807307A CN106807307A CN201710075391.7A CN201710075391A CN106807307A CN 106807307 A CN106807307 A CN 106807307A CN 201710075391 A CN201710075391 A CN 201710075391A CN 106807307 A CN106807307 A CN 106807307A
- Authority
- CN
- China
- Prior art keywords
- tubular reactor
- pipe support
- transparent tubular
- ring stand
- reactor according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
- B01J8/067—Heating or cooling the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
- B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00389—Controlling the temperature using electric heating or cooling elements
- B01J2208/00398—Controlling the temperature using electric heating or cooling elements inside the reactor bed
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00389—Controlling the temperature using electric heating or cooling elements
- B01J2208/00415—Controlling the temperature using electric heating or cooling elements electric resistance heaters
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses a kind of transparent tubular reactor, including body, the entrance and exit on body, body is made up of transparent material；Integrally formed with depressed part on body, heating rod is installed in depressed part；Multiple convex portions are provided with inboard wall of tube body；Positioned at the support frame on convex portion top, support frame is made up of the pillar of upper frame, underframe and connection upper frame and underframe, and upper frame includes ring stand pillar one, pipe support one and the pipe support two that ring stand one and ring stand one are weldingly connected；Underframe includes the ring stand pillar two and pipe support three that ring stand two and ring stand two are weldingly connected, and the axle center of pipe support one and pipe support three is located on same axis；Through the pipe sleeve that pipe support one and bottom contact with pipe support three；It is arranged at the thermocouple inside pipe sleeve；Through pipe support three and insert the temperature sensor in catalyst；It is positioned over the silica wool between convex portion and depressed part.The transparent tubular reactor that the present invention is provided can allow observer to observe the change of catalyst condition and color in time, very convenient.
Description
Technical field
The present invention relates to laboratory apparatus technical field, more particularly to a kind of transparent tubular reactor.
Background technology
Catalyst, refers to that can change reactant chemical reaction rate in chemical reaction without changing chemical balance, and
The material that the weight and chemical property of itself all do not change before and after chemical reaction, using very wide in chemical experiment
It is general.
Fixed bed is widely used in the sign of catalyst reaction performance.At present, fixed bed typically uses external heating
The mode of stove heat, reaction tube is in heating furnace, therefore, catalyst condition and color cannot be observed during the course of the reaction
Change, it is impossible to the state of catalyst is judged from visual perception.
Therefore, how the problem that a kind of reactor of convenient observation is those skilled in the art's urgent need to resolve is provided.
The content of the invention
In view of this, the invention provides a kind of transparent tubular reactor, conveniently can be observed during the course of the reaction.
To achieve these goals, the present invention is adopted the following technical scheme that：
A kind of transparent tubular reactor, including：Body, the entrance and exit on the body, the body is by saturating
Bright material is made；Integrally formed with depressed part on the body, heating rod is installed in the depressed part；On the inboard wall of tube body
It is provided with multiple convex portions；Positioned at the support frame on the convex portion top, wherein support frame as described above is main by upper frame, underframe and connection
The pillar composition of the upper frame and the underframe, the ring that the upper frame includes ring stand one, is weldingly connected with the ring stand one successively
Post setting one, pipe support one and pipe support two；The ring stand pillar that the underframe includes ring stand two, is weldingly connected with the ring stand two successively
Two and pipe support three, and the axle center of the pipe support one and the pipe support three is located on same axis；Through the pipe support one and
The pipe sleeve that bottom contacts with the pipe support three；It is arranged at the thermocouple inside the pipe sleeve；Through the pipe support three and insertion urge
Temperature sensor in agent；It is positioned over the silica wool between the convex portion and the depressed part.
Optionally, the material of the body includes but is not limited to quartz, hard glass.
Optionally, the bottom of the body is at least provided with three supporting legs.
Optionally, the convex portion is integrally formed with the body.
Optionally, multiple convex portions are symmetricly set on the inboard wall of tube body.
Optionally, it is provided with valve in the entrance and the outlet.
Optionally, the valve includes：Magnetic valve, hand-operated valve or pneumatic operated valve.
Optionally, it is additionally provided with scale on the body.
Optionally, also include：It is arranged at the pressure inductor on the inboard wall of tube body.
Optionally, the pillar at least includes two.
Understood via above-mentioned technical scheme, it is compared with prior art, anti-the present disclosure provides a kind of transparent tubular type
Device is answered, the transparent tubular reactor is made of transparent material, catalyst can be observed during being chemically reacted
The change of state and color, can in time observe the change of catalyst, very convenient.Additionally, depressed part be designed to increase
Plus the contact area of heating rod and hydrogen-catalyst reactor so that heat faster, and depressed part and body are integrally formed, both letters
Clean and practicality.
Therefore, the transparent tubular reactor that the present invention is provided is very practical, has a good application prospect.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing
The accompanying drawing to be used needed for having technology description is briefly described, it should be apparent that, drawings in the following description are only this
Inventive embodiment, for those of ordinary skill in the art, on the premise of not paying creative work, can also basis
The accompanying drawing of offer obtains other accompanying drawings.
The structural representation of the transparent tubular reactor that Fig. 1 accompanying drawings are provided for the present invention；
A kind of structural representation of support frame in the transparent tubular reactor that Fig. 2 accompanying drawings are provided for the present invention；
Another structural representation of support frame in the transparent tubular reactor that Fig. 3 accompanying drawings are provided for the present invention；
The schematic diagram of the transparent tubular reactor high scale that Fig. 4 accompanying drawings are provided for the present invention；
The profile of the depressed part that Fig. 5 accompanying drawings are provided for the present invention；
The side view of the depressed part that Fig. 6 accompanying drawings are provided for the present invention.
Specific embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation is described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.It is based on
Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of creative work is not made
Embodiment, belongs to the scope of protection of the invention.
The embodiment of the invention discloses a kind of transparent tubular reactor, catalyst can be observed in chemical reaction process
State and color, observe the change of catalyst in time, very convenient, directly perceived.
The invention discloses a kind of transparent tubular reactor, including：Body 1, entrance 2 and outlet 3 on body 1,
Body 1 is made up of transparent material；Integrally formed with depressed part 4 on body 1, heating rod 5 is installed in depressed part 4；The inwall of body 1
On be provided with multiple convex portions 6；Positioned at the support frame 7 on the top of convex portion 6, wherein support frame 7 mainly by upper frame 71, underframe 72 and connects
The pillar 73 for connecing upper frame 71 and underframe 72 is constituted, the ring that upper frame 71 includes ring stand 1, is weldingly connected with ring stand 1 successively
Post setting 1, pipe support 1 and pipe support 2 714；Underframe 72 is weldingly connected including ring stand 2 721, successively with ring stand 2 721
Ring stand pillar 2 722 and pipe support 3 723, and pipe support 1 and pipe support 3 723 axle center be located at same axis on；Pass through
The pipe sleeve 8 that pipe support 1 and bottom contact with pipe support 3 723；It is arranged at the thermocouple 9 inside pipe sleeve 8；Through pipe support three
723 and insert the temperature sensor 10 in catalyst；It is positioned over the silica wool 11 between convex portion 6 and depressed part 4.
The transparent tubular reactor that the present invention is provided is made of transparent material, can be during being chemically reacted
The change of the state and color of catalyst is observed, the change of catalyst is observed in time, understood with the change that will pass through catalyst
Whether reaction is being carried out, very convenient.Secondly as pipe support is provided with support frame, when using the transparent tubular reactor,
Can be by support frame come the thermocouple in stable sockets and pipe sleeve so that reactor is more stable, handy.Additionally, depressed part
The contact area for being designed to increase heating rod and hydrogen-catalyst reactor so that heating faster, and depressed part and body one
Body formed, it is not only succinct but also practical.
Also need to illustrate, the chemistry that the transparent tubular reactor that the present invention is provided can either adapt to gas is anti-
Should, the chemical reaction of liquid is can adapt to again, using than wide.And in the specific implementation, the specific embodiment bag of support frame
Include but be not limited to accompanying drawing 2 and the support frame shown in accompanying drawing 3.
In order to further optimize above-mentioned technical proposal, the material of body 1 includes but is not limited to quartz, hard glass.
When the transparent tubular reactor of present invention offer is implemented, it is possible to use quartz or hard glass make
The quality of transparent tubular reactor, quartz and hard glass is relatively adapted to chemical experiment, is difficult to be ruptured in chemical reaction process.
Also need to illustrate is, it would however also be possible to employ other transparent materials make the transparent tubular reactor that the present invention is provided, as long as
Chemical experiment can be adapted to just can be with.
In order to further optimize above-mentioned technical proposal, the bottom of body 1 is at least provided with three supporting legs 12.
In the bottom of body, supporting leg is set, can be using transparent tubular reactor an as reaction that can independently stand
Device, it is not necessary to which other support bases, purposes is more extensive.
In order to further optimize above-mentioned technical proposal, convex portion 6 is integrally formed with body 1.
As the material of convex portion is with the material of body, and body is integrally formed, equally be can adapt to chemical anti-
Should, additionally it is possible to play a part of to support support frame, prevent support frame from dropping, when support frame is not used, due to having
The setting of convex portion, very easily can take out support frame.
In order to further optimize above-mentioned technical proposal, multiple convex portions 6 are symmetricly set on the inwall of body 1.
There is multiple convex portion on body, uniformly can be arranged on body, plays a part of to support support frame.
In order to further optimize above-mentioned technical proposal, valve 13 is provided with entrance 2 and outlet 3.
During being chemically reacted, can be by the big of the valve regulated air inlet on entrance and exit or feed liquor
It is small, chemical reaction can be controlled in time.
In order to further optimize above-mentioned technical proposal, valve 13 includes：Magnetic valve, hand-operated valve or pneumatic operated valve.
In order to further optimize above-mentioned technical proposal, scale 14 is additionally provided with body 1.
Scale is set on body, the amount of reactant intuitively can be substantially observed very much, especially to carry out liquid anti-
When answering, the volume of reactant can be found out by reading scale, it is very convenient.
In order to further optimize above-mentioned technical proposal, also include：It is arranged at the pressure inductor 15 on the inwall of body 1.
When gas reaction is carried out, the pressure in body can be detected by pressure sensor, in specific implementation
When, pressure sensor and temperature sensor can be connected to background controller, it becomes possible to realize it is long-range check data and
Control, high degree of automation.
In order to further optimize above-mentioned technical proposal, pillar 73 at least includes two.
Each embodiment is described by the way of progressive in this specification, and what each embodiment was stressed is and other
The difference of embodiment, between each embodiment identical similar portion mutually referring to.For device disclosed in embodiment
For, because it is corresponded to the method disclosed in Example, so description is fairly simple, related part is said referring to method part
It is bright.
The foregoing description of the disclosed embodiments, enables professional and technical personnel in the field to realize or uses the present invention.
Various modifications to these embodiments will be apparent for those skilled in the art, as defined herein
General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, the present invention
The embodiments shown herein is not intended to be limited to, and is to fit to and principles disclosed herein and features of novelty phase one
The scope most wide for causing.
Claims (10)
1. a kind of transparent tubular reactor, including：Body (1), entrance (2) and outlet (3) on the body (1), its
It is characterised by, the body (1) is made up of transparent material；Integrally formed with depressed part (4), the depression on the body (1)
Heating rod (5) is installed in portion (4)；Multiple convex portions (6) are provided with body (1) inwall；Positioned at the convex portion (6) top
Support frame (7), wherein support frame as described above (7) is main by upper frame (71), underframe (72) and connects the upper frame (71) and institute
Pillar (73) composition of underframe (72) is stated, the upper frame (71) is welded including ring stand one (711), successively with the ring stand one (711)
Connect connected ring stand pillar one (712), pipe support one (713) and pipe support two (714)；The underframe (72) including ring stand two (721),
The ring stand pillar two (722) and pipe support three (723) being weldingly connected with the ring stand two (721) successively, and the pipe support one
(713) and the pipe support three (723) axle center be located at same axis on；Through the pipe support one (713) and bottom and the pipe
The pipe sleeve (8) of the contact of frame three (723)；It is arranged at the internal thermocouple (9) of the pipe sleeve (8)；Through the pipe support three (723) and
Temperature sensor (10) in insertion catalyst；It is positioned over the silica wool between the convex portion (6) and the depressed part (4)
(11)。
2. transparent tubular reactor according to claim 1, it is characterised in that the material of the body (1) is included but not
It is limited to quartz, hard glass.
3. transparent tubular reactor according to claim 1, it is characterised in that the bottom of the body (1) at least provided with
There are three supporting legs (12).
4. transparent tubular reactor according to claim 1, it is characterised in that the convex portion (6) and the body (1)
It is body formed.
5. transparent tubular reactor according to claim 1, it is characterised in that multiple convex portions (6) are symmetricly set in
On body (1) inwall.
6. transparent tubular reactor according to claim 1, it is characterised in that on the entrance (2) and the outlet (3)
It is provided with valve (13).
7. transparent tubular reactor according to claim 6, it is characterised in that the valve (13) includes：Magnetic valve, hand
Dynamic valve or pneumatic operated valve.
8. transparent tubular reactor according to claim 1, it is characterised in that be additionally provided with scale on the body (1)
(14)。
9. transparent tubular reactor according to claim 1, it is characterised in that also include：It is arranged in the body (1)
Pressure inductor (15) on wall.
10. transparent tubular reactor according to claim 1, it is characterised in that the pillar (73) at least includes two.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710075391.7A CN106807307B (en) | 2017-02-10 | 2017-02-10 | Transparent tubular reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710075391.7A CN106807307B (en) | 2017-02-10 | 2017-02-10 | Transparent tubular reactor |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106807307A true CN106807307A (en) | 2017-06-09 |
| CN106807307B CN106807307B (en) | 2019-11-26 |
Family
ID=59111782
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710075391.7A Expired - Fee Related CN106807307B (en) | 2017-02-10 | 2017-02-10 | Transparent tubular reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106807307B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE759541A (en) * | 1969-12-04 | 1971-05-27 | Basf Ag | MIXING DEVICE FOR CARRYING OUT CHEMICAL REACTIONS |
| CN203000580U (en) * | 2012-05-24 | 2013-06-19 | 广州市豪昱净水设备有限公司 | A hot water flask and a heating module thereof |
| CN104162385A (en) * | 2013-05-20 | 2014-11-26 | 黄华 | Transparent tubular reactor |
-
2017
- 2017-02-10 CN CN201710075391.7A patent/CN106807307B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE759541A (en) * | 1969-12-04 | 1971-05-27 | Basf Ag | MIXING DEVICE FOR CARRYING OUT CHEMICAL REACTIONS |
| CN203000580U (en) * | 2012-05-24 | 2013-06-19 | 广州市豪昱净水设备有限公司 | A hot water flask and a heating module thereof |
| CN104162385A (en) * | 2013-05-20 | 2014-11-26 | 黄华 | Transparent tubular reactor |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106807307B (en) | 2019-11-26 |
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| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20200713 Address after: 410000 room 101A, building B6, Lugu Yuyuan, No.27 Wenxuan Road, high tech Development Zone, Changsha City, Hunan Province Patentee after: Hunan Weiling Instrument Co.,Ltd. Address before: 100000 Beijing city Haidian District Road No. 9, non-ferrous metal industry talent center Patentee before: Huang Hua |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20191126 Termination date: 20220210 |