CN106802083A - A kind of antimony reduction furnace - Google Patents

A kind of antimony reduction furnace Download PDF

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Publication number
CN106802083A
CN106802083A CN201510832202.7A CN201510832202A CN106802083A CN 106802083 A CN106802083 A CN 106802083A CN 201510832202 A CN201510832202 A CN 201510832202A CN 106802083 A CN106802083 A CN 106802083A
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CN
China
Prior art keywords
furnace
reduction
reduction furnace
wastewater treatment
quartz ampoule
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Pending
Application number
CN201510832202.7A
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Chinese (zh)
Inventor
李贺成
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Hengyang Heng Rong Gaochun Semiconductor Materials Co Ltd
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Hengyang Heng Rong Gaochun Semiconductor Materials Co Ltd
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Application filed by Hengyang Heng Rong Gaochun Semiconductor Materials Co Ltd filed Critical Hengyang Heng Rong Gaochun Semiconductor Materials Co Ltd
Priority to CN201510832202.7A priority Critical patent/CN106802083A/en
Publication of CN106802083A publication Critical patent/CN106802083A/en
Pending legal-status Critical Current

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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/25Process efficiency

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  • Waste-Gas Treatment And Other Accessory Devices For Furnaces (AREA)

Abstract

The invention discloses a kind of antimony reduction furnace, including quartz ampoule, resistance furnace and reduction furnace furnace shell, resistance furnace is placed in reduction furnace furnace shell, quartz ampoule is horizontally through the axis of reduction furnace furnace shell, and be positioned in resistance furnace, quartz ampoule includes reduction inner tube, exhaust pipe and discharge nozzle, reduction inner tube is inclined in the quartz ampoule, exhaust pipe is connected with emission-control equipment, emission-control equipment includes process tank, demarcation strip is provided with process tank, process tank is separated into demarcation strip the exhaust level and lower floor's wastewater treatment layer on upper strata, the through hole that exhaust level is communicated with wastewater treatment layer, the water containing activated carbon is contained with wastewater treatment layer, exhaust pipe extension is inserted into wastewater treatment layer bottom.By the waste gas of antimony reduction furnace of the present invention by from wastewater treatment layer bottom through the charcoal absorption exhaust-gas treatment in water after, discharged through the through hole of division board one end, so as to extend time of the waste water in by treatment water, improve the purifying rate after exhaust-gas treatment.

Description

A kind of antimony reduction furnace
Technical field
The present invention relates to a kind of antimony reduction furnace, more particularly to a kind of assembly of reduction furnace of high pure metal antimony, belong to high pure metal purifying plant technical field.
Background technology
High purity antimony refers to the high pure metal antimony of more than 5N, and mainly for the preparation of semi-conducting material, it can form the compound semiconductors such as aluminium antimonide, gallium antimonide, indium antimonide;As the dopant of the monocrystalline such as semiconductor Germanium, silicon, N-type semiconductor is formed it into;Furthermore it is also possible to be used as to prepare other high pure metal alloys.In some photoelectric fields, such as infrared acquisition, piezoelectricity, pressure-sensitive electronic original part, property material based on it typically require metal purity in 5-7N.The preparation of high purity antimony is mainly realized by processes such as chlorination, rectifying, reduction, distillations.Due to traditional high purity antimony reduction furnace operationally, some pernicious gases can be generated, this pernicious gas is for during general making to let go unchecked, so that workshop smoke pollution is serious, smell is pungent unpleasant, healthy to Manufacturing Worker causes serious threat, and the present invention is called on and solving above-mentioned technical problem.
The content of the invention
The invention aims to solve the problems, such as to be previously mentioned in above-mentioned background technology, there is provided a kind of antimony reduction furnace.
To achieve these goals, technical scheme is as follows:
A kind of antimony reduction furnace,Including quartz ampoule,Resistance furnace and reduction furnace furnace shell,The resistance furnace is placed in the reduction furnace furnace shell,The quartz ampoule is horizontally through the axis of reduction furnace furnace shell,And be positioned in resistance furnace,The quartz ampoule includes reduction inner tube,Exhaust pipe and discharge nozzle,The reduction inner tube is inclined in the quartz ampoule,Charging aperture is provided with the reduction inner tube,The quartz ampoule reveal to the reduction furnace furnace shell outside side be provided with discharge nozzle and exhaust pipe,The exhaust pipe is connected with emission-control equipment,The emission-control equipment includes process tank,Demarcation strip is provided with the process tank,The process tank is separated into the demarcation strip exhaust level and lower floor's wastewater treatment layer on upper strata,The through hole that the exhaust level is communicated with wastewater treatment layer,The water containing activated carbon is contained with the wastewater treatment layer,The exhaust pipe extension is inserted into wastewater treatment layer bottom.
Further, the position of the position of the through hole and exhaust pipe insertion wastewater treatment layer is respectively arranged on the both sides of the process tank.
Further, the center line of the reduction inner tube and the center line of quartz ampoule into 30 ° of overturning angles.
Further, also including servicing unit, the servicing unit includes suspension ring and lifting motor, and the suspension ring are fixed on reduction furnace furnace shell, and one end and the suspension ring of lifting motor are mounted.
Further, also including support meanss, support meanss are the bearing for supporting reduction furnace furnace shell.
Compared with prior art, beneficial effects of the present invention are as follows:
1, the present invention is by setting emission-control equipment, its emission-control equipment includes process tank, demarcation strip is provided with its process tank, process tank is separated into demarcation strip the exhaust level and lower floor's wastewater treatment layer on upper strata, the through hole that exhaust level is communicated with wastewater treatment layer, the water containing activated carbon is contained with wastewater treatment layer, exhaust pipe extension is inserted into wastewater treatment layer bottom, set by this, the waste gas of antimony reduction furnace by from wastewater treatment layer bottom after the charcoal absorption exhaust-gas treatment in water, discharged through the through hole of division board one end, so as to extend time of the waste water in by treatment water, improve the purifying rate after exhaust-gas treatment.
2nd, by antimony reduction furnace of the invention, the waste gas of its discharge has met and exceeded relevant national standard, works well, and a comfortable production environment of health is provided to plant personnel, has ensured the physical and mental health of workpeople.
Brief description of the drawings
Technical scheme in order to illustrate more clearly the embodiments of the present invention, the accompanying drawing to be used needed for being described to embodiment below is briefly described, apparently, drawings in the following description are only some embodiments of the present invention, for those of ordinary skill in the art, without having to pay creative labor, other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is the structural representation in the present embodiment.
Specific embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made belongs to the scope of protection of the invention.
Specific embodiment:
A kind of antimony reduction furnace with reference to shown in Fig. 1,Including quartz ampoule 1,Resistance furnace and reduction furnace furnace shell 2,Resistance furnace is placed in reduction furnace furnace shell 2,Quartz ampoule 1 is horizontally through the axis of reduction furnace furnace shell 2,And be positioned in resistance furnace,Quartz ampoule 1 includes reduction inner tube 3,Exhaust pipe 4 and discharge nozzle 5,Reduction inner tube 3 is inclined in quartz ampoule 1,Charging aperture 6 is provided with reduction inner tube 3,Quartz ampoule 1 reveals to the outside side of reduction furnace furnace shell 2 and is provided with discharge nozzle 5 and exhaust pipe 4,Exhaust pipe 4 is connected with emission-control equipment 8,Emission-control equipment includes process tank,Demarcation strip 9 is provided with process tank,Process tank is separated into demarcation strip the exhaust level 10 and lower floor's wastewater treatment layer 11 on upper strata,The through hole 12 that exhaust level 10 is communicated with wastewater treatment layer 11,The water containing activated carbon is contained with wastewater treatment layer 11,The extension of exhaust pipe 4 is inserted into 11 bottom of wastewater treatment layer.
In the present embodiment, the position of the position of through hole 12 and the insertion wastewater treatment of exhaust pipe 4 layer 11 is respectively arranged on the both sides of process tank.
The present embodiment by set the waste gas of above-mentioned emission-control equipment antimony reduction furnace by from 11 bottom of wastewater treatment layer after the charcoal absorption exhaust-gas treatment in water, discharged through the through hole 12 of the one end of division board 9, so as to extend time of the waste water in by treatment water, the purifying rate after exhaust-gas treatment is improve.
By antimony reduction furnace of the invention, the waste gas of its discharge has met and exceeded relevant national standard, has worked well, and a comfortable production environment of health is provided to plant personnel, has ensured the physical and mental health of workpeople.
In the present embodiment, the center line of inner tube 3 is reduced with the center line of quartz ampoule 1 into 30 ° of overturning angles.
In the present embodiment, also including servicing unit, servicing unit includes suspension ring 13 and lifting motor 14, and suspension ring 13 are fixed on reduction furnace furnace shell 2, and one end and the suspension ring 13 of lifting motor 14 are mounted.Set by this and be easy to antimony to reduce furnace discharge.
In the present embodiment, also including support meanss, support meanss 15 are the bearing of support reduction furnace furnace shell.
Presently preferred embodiments of the present invention is the foregoing is only, is not intended to limit the invention, all any modification, equivalents made within the scope of the present invention etc. should be included within the scope of the present invention.

Claims (5)

1. a kind of antimony reduction furnace,Including quartz ampoule,Resistance furnace and reduction furnace furnace shell,The resistance furnace is placed in the reduction furnace furnace shell,The quartz ampoule is horizontally through the axis of reduction furnace furnace shell,And be positioned in resistance furnace,It is characterized in that,The quartz ampoule includes reduction inner tube,Exhaust pipe and discharge nozzle,The reduction inner tube is inclined in the quartz ampoule,Charging aperture is provided with the reduction inner tube,The quartz ampoule reveal to the reduction furnace furnace shell outside side be provided with discharge nozzle and exhaust pipe,The exhaust pipe is connected with emission-control equipment,The emission-control equipment includes process tank,Demarcation strip is provided with the process tank,The process tank is separated into the demarcation strip exhaust level and lower floor's wastewater treatment layer on upper strata,The through hole that the exhaust level is communicated with wastewater treatment layer,The water containing activated carbon is contained with the wastewater treatment layer,The exhaust pipe extension is inserted into wastewater treatment layer bottom.
2. antimony reduction furnace according to claim 1, it is characterised in that the position of the position of the through hole and exhaust pipe insertion wastewater treatment layer is respectively arranged on the both sides of the process tank.
3. antimony reduction furnace according to claim 1, it is characterised in that the center line of the reduction inner tube and the center line of quartz ampoule into 30 ° of overturning angles.
4. antimony reduction furnace according to claim 1, it is characterised in that also including servicing unit, the servicing unit includes suspension ring and lifting motor, and the suspension ring are fixed on reduction furnace furnace shell, and one end and the suspension ring of lifting motor are mounted.
5. antimony reduction furnace according to claim 1, it is characterised in that also including support meanss, support meanss are the bearing for supporting reduction furnace furnace shell.
CN201510832202.7A 2015-11-25 2015-11-25 A kind of antimony reduction furnace Pending CN106802083A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510832202.7A CN106802083A (en) 2015-11-25 2015-11-25 A kind of antimony reduction furnace

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510832202.7A CN106802083A (en) 2015-11-25 2015-11-25 A kind of antimony reduction furnace

Publications (1)

Publication Number Publication Date
CN106802083A true CN106802083A (en) 2017-06-06

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113089030A (en) * 2021-04-03 2021-07-09 深圳市红火火机械装备有限公司 Electrolytic aluminum waste gas processing apparatus

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101844229A (en) * 2010-03-24 2010-09-29 峨嵋半导体材料研究所 Preparation method and production equipment of high-purity antimony particles
CN202061524U (en) * 2011-04-11 2011-12-07 攀枝花源丰钛业有限公司 Kiln waste gas treatment device for producing high-purity titanium dioxide
CN103968388A (en) * 2014-05-27 2014-08-06 浙江华川实业集团有限公司 Paper mill waste disposal equipment and operating method thereof
CN204255077U (en) * 2014-10-31 2015-04-08 峨嵋半导体材料研究所 A kind of antimony reduction furnace
CN204485632U (en) * 2015-03-12 2015-07-22 湖北万丰化工有限公司 A kind of emission-control equipment

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101844229A (en) * 2010-03-24 2010-09-29 峨嵋半导体材料研究所 Preparation method and production equipment of high-purity antimony particles
CN202061524U (en) * 2011-04-11 2011-12-07 攀枝花源丰钛业有限公司 Kiln waste gas treatment device for producing high-purity titanium dioxide
CN103968388A (en) * 2014-05-27 2014-08-06 浙江华川实业集团有限公司 Paper mill waste disposal equipment and operating method thereof
CN204255077U (en) * 2014-10-31 2015-04-08 峨嵋半导体材料研究所 A kind of antimony reduction furnace
CN204485632U (en) * 2015-03-12 2015-07-22 湖北万丰化工有限公司 A kind of emission-control equipment

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113089030A (en) * 2021-04-03 2021-07-09 深圳市红火火机械装备有限公司 Electrolytic aluminum waste gas processing apparatus

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Application publication date: 20170606