CN106800888A - Carrying magnetic polishing composite powder and preparation method thereof - Google Patents

Carrying magnetic polishing composite powder and preparation method thereof Download PDF

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Publication number
CN106800888A
CN106800888A CN201611173218.2A CN201611173218A CN106800888A CN 106800888 A CN106800888 A CN 106800888A CN 201611173218 A CN201611173218 A CN 201611173218A CN 106800888 A CN106800888 A CN 106800888A
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CN
China
Prior art keywords
powder
polishing
composite powder
magnetic
content
Prior art date
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Pending
Application number
CN201611173218.2A
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Chinese (zh)
Inventor
吴志雄
胡少刚
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Weilishi Fine Chemical Co Ltd
Original Assignee
Suzhou Weilishi Fine Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suzhou Weilishi Fine Chemical Co Ltd filed Critical Suzhou Weilishi Fine Chemical Co Ltd
Priority to CN201611173218.2A priority Critical patent/CN106800888A/en
Publication of CN106800888A publication Critical patent/CN106800888A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09GPOLISHING COMPOSITIONS; SKI WAXES
    • C09G1/00Polishing compositions
    • C09G1/02Polishing compositions containing abrasives or grinding agents

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)

Abstract

Carrying magnetic polishes composite powder, it is characterised in that:Obtained by following mass ratio formula and method:Formula Magnaglo content 60% 80%;Engineering plastics content is 5% 10%;Polishing powder content 5% 10%;Plasticizer about total amount 1.5% 2%;Preparation method:First, according to the formula, with engineering plastics as carrier, Magnaglo, polishing powder is added to be well mixed;2nd, 200 220 DEG C are heated, is kneaded 30 40 minutes with mixing kneader and extremely mediated uniformly;3rd, plasticizer is added, continues to knead 30 40 minutes afterwards;4th, the composite powder crushing pulverizer that will be kneaded is ground to wherein 95% above section granularity and reaches 250 μm 2500 μm;5th, sub-sieve is carried out with vibratory sieve to go out less than the 2500 μm composite powders of granularity and then pack.Utilizing works plastics of the present invention carry out mixing cladding to magnetic conductive material or magnetic material, lift the magnetic powder life-span, and further reduction scratches, and adjustable granularity and then can reach and require that degree of conformity is high to workpiece polishing, and it is possessed recuperability.

Description

Carrying magnetic polishing composite powder and preparation method thereof
Technical field
Formula of composite powder and preparation method thereof is polished with carrying magnetic the present invention relates to a kind of MRF.
Background technology
MRF polishes the curved surface polishing to be overcome to conventional planar, there is provided overall technique is reformed, with Constantly bringing forth new ideas for workpiece, has played great effect.Magnetorheological devices are main to be polished cell body by work piece holder, band magnetic force and is thrown Light powder and slurry are constituted, then when being polished, using magnetic-adsorption band magnetic force polishing powder, workpiece are pressed on what polishing powder, are done and are revolved Turn workpiece is carried out it is smooth, while workpiece is played polishing (adding lustre to) act on.Owner will be using magnetic force by again in polishing process Close powder and fix what bottom, formation can throw the burnishing surface of curved surface, then with the engineering plastics and polishing powder in composite powder composition, to workpiece Get leveling and highlighting process.
MRF has played very big key effect to curved surface polishing technique, and carrying magnetic polishing composite powder and slurry are even more The core of the technique, carrying magnetic polishing composite powder and slurry are good to improving polishing speed, precision in technique to traditional magnetic powder Rate, even more a quantum jump.
The existing Magnaglo of tradition is not protected, and slurry has necessarily influence, polishing condition on it, and particle size does not have can Scalability is low to workpiece requirement conformability.Also having some has a way coated to particle, but still with the life-span is shorter, bag Cover the defects, such as Northeastern University's Master's thesis such as rear removal force difference particle diameter is non-adjustable and workpiece requirement degree of conformity is low, not recyclable 《The synthesis of reduced iron powder Magnetorheologicai polishing liquid and performance study》Described in the cladding to reduced iron powder be using silane coupled Agent is that surfactant prepares well mixed with isopropanol as solvent again, and effect is to improve its dispersion effect in carrier fluid, Do not change Magnaglo polishing efficiency, yield, and particle size itself does not have adjustable, it is poor for applicability;Grinding in addition The active ingredient in composite powder is polished in polishing process and can increase over time to act on and gradually decayed, and magnetic property can produced Raw influence.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of carrying magnetic polishing composite powder, except possessing magnetic conductive material or magnetic Property material outside, have certain protection and lifting magnetic powder life-span to magnetic conductive material or magnetic material, possess removal force outer to work Part further reduces scuffing, and adjustable granularity is high to workpiece requirement degree of conformity, and carrying magnetic polishes composite powder more for that can return The property received, overcomes many defects of conventional magnetic powder.
In order to solve the above technical problems, the present invention is adopted the following technical scheme that:Carrying magnetic polishes composite powder and its preparation side Method, carrying magnetic polishing composite powder, it is characterised in that:Obtained by following mass ratio formula and method:
Formula
Magnaglo content 60%-80%;
Engineering plastics content is 5%-10%;
Polishing powder content 5%-10%;
Plasticizer about total amount 1.5%-2%;
Preparation method:
First, it is formulated according to it, with engineering plastics as carrier, adds Magnaglo, polishing powder to be well mixed;
2nd, 200-220 DEG C is heated, 30-40 minutes is kneaded to mediating uniformly with mixing kneader, Magnaglo is wrapped Treatment is covered, the composite powder of greater particle size is tentatively manufactured into;
3rd, plasticizer is added, continues to knead 30-40 minutes afterwards;
4th, the composite powder crushing pulverizer that will be kneaded be ground to wherein 95% above section granularity reach 250 μm- The composite powder of 2500 μm of relatively small particle;
5th, sub-sieve is carried out with vibratory sieve to go out less than the 2500 μm composite powder finished products of granularity and then pack.
Preferably, its Magnaglo can be the magnetic material of iron, cobalt, nickel or iron, cobalt, nickel, the compound of rubidium or oxide Or permeability magnetic material.
Preferably, its polishing powder is the media with grinding effect such as silica, aluminum oxide, zirconium oxide.
The beneficial effects of the present invention are possessing outside magnetic conductive material or magnetic material, utilizing works plastics are to magnetic conductivity material Material or magnetic material carry out mixing cladding, it is obtained certain protection and lifting magnetic powder life-span, outer right possessing removal force Workpiece further reduces scuffing, and manufacture itself needs to be crushed again by kneading, the particle diameter of finished breaking is reached adjustable particle Spend and then can reach and degree of conformity is high to be required to workpiece polishing, and carrying magnetic polishing composite powder overcomes more for recuperability Many defects of conventional magnetic powder.
Specific embodiment
Embodiment 1:
Formula
Iron content 60%;
Engineering plastics content is 5%;
Silica polishes powder content 5%;
Mineral oil total amount 1.5%;
Preparation method:
First, according to the formula, with engineering plastics as carrier, iron powder is added, is well mixed;
2nd, 200 DEG C are heated, are kneaded to kneading uniformly with mixing kneader,
3rd, add mineral oil and continue uniform with 200 DEG C of heating mixings;
4th, the composite powder crushing pulverizer that will be kneaded is ground to wherein 95% above section granularity and reaches 250 μm;
5th, sub-sieve is carried out with vibratory sieve to go out less than the 250 μm composite powders of granularity and then pack.
Embodiment 2:
Carrying magnetic polishes composite powder, it is characterised in that:Obtained by following mass ratio formula and method:
Formula
Magnaglo content 80%;
Engineering plastics content is 10%;
Polishing powder content 8%;
Plasticizer about total amount 2%;
Preparation method:
First, it is formulated according to it, with engineering plastics as carrier, adds Magnaglo, polishing powder to be well mixed;
2nd, 220 DEG C are heated, 40 minutes are kneaded to mediating uniformly with mixing kneader, cladding treatment is carried out to Magnaglo, The preliminary composite powder for being manufactured into greater particle size;
3rd, plasticizer is added, continues to knead 40 minutes afterwards;
4th, the composite powder crushing pulverizer that will be kneaded is ground to wherein 95% above section granularity and reaches 2500 μm Compared with the composite powder of small particle;
5th, sub-sieve is carried out with vibratory sieve to go out less than the 2500 μm composite powder finished products of granularity and then pack.
Embodiment 3:
Carrying magnetic polishes composite powder, it is characterised in that:Obtained by following mass ratio formula and method:
Formula
Magnaglo content 80%;
Engineering plastics content is 8%;
Polishing powder content 10%;
Plasticizer about total amount 2%;
Preparation method:
First, it is formulated according to it, with engineering plastics as carrier, adds Magnaglo, polishing powder to be well mixed;
2nd, 210 DEG C are heated, 35 minutes are kneaded to mediating uniformly with mixing kneader, cladding treatment is carried out to Magnaglo, The preliminary composite powder for being manufactured into greater particle size;
3rd, plasticizer is added, continues to knead 35 minutes afterwards;
4th, the composite powder crushing pulverizer that will be kneaded is ground to wherein 95% above section granularity and reaches 1000 μm Compared with the composite powder of small particle;
5th, sub-sieve is carried out with vibratory sieve to go out less than the 1000 μm composite powder finished products of granularity and then pack.
Specific embodiment of the invention is the foregoing is only, reference explanation feasible specific embodiment party of the invention is only used as Method, is not intended as limitation of the invention, and any those skilled in the art are not departing from claims of the present invention and specification Addition or the wherein inessential and neccessary composition of improvement in the case of principle, spirit, or take similar processing mode to be regarded as Equal replacement of the invention, similarly comprising within the scope of the present invention, specific protection domain is defined by claims.

Claims (3)

1. carrying magnetic polishes composite powder, it is characterised in that:Obtained by following mass ratio formula and method:
Formula
Magnaglo content 60%-80%;
Engineering plastics content is 5%-10%;
Polishing powder content 5%-10%;
Plasticizer about total amount 1.5%-2%;
Preparation method:
First, according to the formula, with engineering plastics as carrier, Magnaglo, polishing powder is added to be well mixed;
2nd, 200-220 DEG C is heated, is kneaded 30-40 minutes with mixing kneader and extremely mediated uniformly;
3rd, plasticizer is added, continues to knead 30-40 minutes afterwards;
4th, the composite powder crushing pulverizer that will be kneaded is ground to wherein 95% above section granularity and reaches 250 μm of -2500 μ m;
5th, sub-sieve is carried out with vibratory sieve to go out less than the 2500 μm composite powders of granularity and then pack.
2. according to claim 1, its carrying magnetic polishes composite powder and preparation method thereof, it is characterised in that the Magnaglo can It is the magnetic material or permeability magnetic material of iron, cobalt, nickel or iron, cobalt, nickel, the compound of rubidium or oxide.
3. carrying magnetic according to claim 1 polishing composite powder and preparation method thereof, it is characterised in that the polishing powder is The medium with grinding effect such as silica, aluminum oxide, zirconium oxide.
CN201611173218.2A 2016-12-18 2016-12-18 Carrying magnetic polishing composite powder and preparation method thereof Pending CN106800888A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611173218.2A CN106800888A (en) 2016-12-18 2016-12-18 Carrying magnetic polishing composite powder and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611173218.2A CN106800888A (en) 2016-12-18 2016-12-18 Carrying magnetic polishing composite powder and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106800888A true CN106800888A (en) 2017-06-06

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Country Status (1)

Country Link
CN (1) CN106800888A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110508803A (en) * 2019-09-12 2019-11-29 兰州理工大学 Nanometer cuts the preparation method at first iron-based magnetic force essence polishing powder end

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101294061A (en) * 2008-06-25 2008-10-29 湖南大学 Magnetic abrasive material
CN103965832A (en) * 2013-01-30 2014-08-06 比亚迪股份有限公司 Polishing abrasive and preparation method thereof
CN105131906A (en) * 2015-09-08 2015-12-09 沈阳化工大学 Flexible magnetic abrasive

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101294061A (en) * 2008-06-25 2008-10-29 湖南大学 Magnetic abrasive material
CN103965832A (en) * 2013-01-30 2014-08-06 比亚迪股份有限公司 Polishing abrasive and preparation method thereof
CN105131906A (en) * 2015-09-08 2015-12-09 沈阳化工大学 Flexible magnetic abrasive

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
张广成 等: "《塑料成型加工技术》", 30 September 2015 *
林建中: "《高分子加工与工程》", 1 February 1969 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110508803A (en) * 2019-09-12 2019-11-29 兰州理工大学 Nanometer cuts the preparation method at first iron-based magnetic force essence polishing powder end
CN110508803B (en) * 2019-09-12 2020-06-30 兰州理工大学 Preparation method of nano cutting element iron-based magnetic fine polishing powder

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Application publication date: 20170606