CN106757042A - A kind of stainless steel mirror board lapping liquid - Google Patents
A kind of stainless steel mirror board lapping liquid Download PDFInfo
- Publication number
- CN106757042A CN106757042A CN201611164497.6A CN201611164497A CN106757042A CN 106757042 A CN106757042 A CN 106757042A CN 201611164497 A CN201611164497 A CN 201611164497A CN 106757042 A CN106757042 A CN 106757042A
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- CN
- China
- Prior art keywords
- stainless steel
- lapping liquid
- mirror board
- steel mirror
- board lapping
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F3/00—Brightening metals by chemical means
- C23F3/04—Heavy metals
- C23F3/06—Heavy metals with acidic solutions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24B—MACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
- B24B37/00—Lapping machines or devices; Accessories
- B24B37/04—Lapping machines or devices; Accessories designed for working plane surfaces
- B24B37/042—Lapping machines or devices; Accessories designed for working plane surfaces operating processes therefor
- B24B37/044—Lapping machines or devices; Accessories designed for working plane surfaces operating processes therefor characterised by the composition of the lapping agent
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- ing And Chemical Polishing (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
Abstract
The invention mainly relates to chemical technology field, a kind of stainless steel mirror board lapping liquid is disclosed, be made up of following raw material：Malic acid, formic acid, oxalic acid, glycerine, sodium tripolyphosphate, double octadecyl phosphates, ricinoleic acid ethyl ester, calcium lignosulfonate, barium mahogany sulfonate, water；Raw material environmental protection, safety and Health will not damage health during use, grinding is quick, and the time shortens 1/2, hence it is evident that improve operating efficiency, and income improves 17.4%；Double octadecyl phosphates, ricinoleic acid ethyl ester, calcium lignosulfonate and barium mahogany sulfonate can strengthen heat resistance, anti-flammability and the rust-preventing characteristic of lapping liquid; keep stability of the lapping liquid in grinding; grinding rate is fast; surface is smooth; no marking, service life extension 18.3%, improves the use value of stainless steel mirror board; environmental protection, saves national resources.
Description
Technical field
The invention mainly relates to chemical technology field, more particularly to a kind of stainless steel mirror board lapping liquid.
Background technology
Mirror board, also known as 8K plates, are polished by polissoir with lapping liquid in stainless steel plate face, make plate face luminosity
Clear as mirror, any surface finish has plasticity higher, toughness and a mechanical strength, acid and alkali resistance gas, solution and other
The corrosion of medium, therefore, increasingly obtain the welcome of people.
, it is necessary to be ground polishing with lapping liquid in the process of stainless steel mirror board, make stainless steel plate face smooth and
Luminosity is clear as mirror, but because the hardness of stainless steel is big, grinding is difficult, and polishing is ground using existing lapping liquid
Time it is more long, and scratch occurs, decline the class of stainless steel mirror board, accordingly, it would be desirable to a kind of stainless steel mirror board
Quick lapping liquid.
The content of the invention
In order to make up the defect of prior art, it is an object of the invention to provide a kind of stainless steel mirror board lapping liquid.
A kind of stainless steel mirror board lapping liquid, is made up of the raw material of following weight portion：Malic acid 22 ~ 24, formic acid 6 ~ 8, grass
Acid 2 ~ 3, glycerine 24 ~ 26, dipotassium glycyrrhizinate 7 ~ 9, double octadecyl phosphates 5 ~ 7, ricinoleic acid ethyl ester 5 ~ 7, sulfomethylated lignin
Sour calcium 4 ~ 6, barium mahogany sulfonate 4 ~ 6, water 100 ~ 120.
Described water, is deionized water.
A kind of preparation method of stainless steel mirror board lapping liquid, specifically includes following steps：
（1）Malic acid, formic acid and dipotassium glycyrrhizinate are added to the water, 70 ~ 75 DEG C are heated to, insulated and stirred to being completely dissolved, plus
Fast dissolving and grinding to stainless steel, accelerates grinding and polishing speed, obtains mixture A；
（2）Glycerine, double octadecyl phosphates and ricinoleic acid ethyl ester are mixed, 30 ~ 35 are stirred under vacuum in 50 ~ 60 DEG C of insulations
Minute, the metal that suppression grinds away produces precipitation in lapping liquid, makes minute surface plate surface smooth, and no marking obtains mixture B；
（3）Mixture A and mixture B are well mixed, calcium lignosulfonate and barium mahogany sulfonate are added, in 50 ~ 60 DEG C of vacuum
The service life of stirring 40 ~ 50 minutes, fire resisting antirust, extension lapping liquid and stainless steel mirror board, obtains stainless steel mirror board grinding
Liquid；
（4）Vacuum packaging, obtains finished product.
The step（2）Vacuum stirring, vacuum is 0.1Mpa, and rotating speed is 110 ~ 130 revs/min.
The application method of the stainless steel mirror board lapping liquid, takes appropriate stainless steel mirror board lapping liquid when using, add
The water of 6 ~ 8 times of stainless steel mirror board lapping liquid weight amount, can be ground polishing, the ring of holding grinding and polishing after stirring
Border temperature is 20 ~ 25 DEG C, and sealing preserve is answered using remaining stainless steel mirror board lapping liquid.
It is an advantage of the invention that：A kind of stainless steel mirror board lapping liquid that the present invention is provided, raw material environmental protection, safety is strong
Health, will not damage health during use, grinding is quick, and the time shortens 1/2, hence it is evident that improve operating efficiency, income
Improve 17.4%；Double octadecyl phosphates, ricinoleic acid ethyl ester, calcium lignosulfonate and barium mahogany sulfonate can strengthen grinding
The heat resistance of liquid, anti-flammability and rust-preventing characteristic, keep stability of the lapping liquid in grinding, and grinding rate is fast, keep lapping liquid without
Precipitation, makes minute surface plate surface smooth, no marking, service life extension 18.3%, improves the use value of stainless steel mirror board, protects
Shield environmental resource.
Specific embodiment
Below the present invention is illustrated with specific embodiment.
Embodiment 1
A kind of stainless steel mirror board lapping liquid, is made up of the raw material of following weight portion：Malic acid 22, formic acid 6, oxalic acid 2, glycerine
24th, dipotassium glycyrrhizinate 7, double octadecyl phosphates 5, ricinoleic acid ethyl ester 5, calcium lignosulfonate 4, barium mahogany sulfonate 4, go from
Sub- water 100.
A kind of preparation method of stainless steel mirror board lapping liquid, specifically includes following steps：
（1）Malic acid, formic acid and dipotassium glycyrrhizinate are added to the water, 70 ~ 75 DEG C are heated to, insulated and stirred to being completely dissolved, plus
Fast dissolving and grinding to stainless steel, accelerates grinding and polishing speed, obtains mixture A；
（2）Glycerine, double octadecyl phosphates and ricinoleic acid ethyl ester are mixed, 30 points are stirred under vacuum in 50 ~ 60 DEG C of insulations
Clock, vacuum is 0.1Mpa, and rotating speed is 120 revs/min, and the metal that suppression grinds away produces precipitation in lapping liquid, makes minute surface
Plate surface is smooth, no marking, obtains mixture B；
（3）Mixture A and mixture B are well mixed, calcium lignosulfonate and barium mahogany sulfonate is added, in 60 DEG C of vacuum stirrings
50 minutes, fire resisting antirust extended the service life of lapping liquid and stainless steel mirror board, obtains stainless steel mirror board lapping liquid；
（4）Vacuum packaging, obtains finished product.
The application method of the stainless steel mirror board lapping liquid, takes appropriate stainless steel mirror board lapping liquid when using, add
The water of 8 times of stainless steel mirror board lapping liquid weight amount, can be ground polishing, the environment of holding grinding and polishing after stirring
Temperature is 20 ~ 25 DEG C, and sealing preserve is answered using remaining stainless steel mirror board lapping liquid.
Embodiment 2
A kind of stainless steel mirror board lapping liquid, is made up of the raw material of following weight portion：Malic acid 23, formic acid 7, oxalic acid 2.5, the third three
Alcohol 25, dipotassium glycyrrhizinate 8, double octadecyl phosphates 6, ricinoleic acid ethyl ester 6, calcium lignosulfonate 5, barium mahogany sulfonate 5, go
Ionized water 110.
Preparation and application, with embodiment 1.
Embodiment 3
A kind of stainless steel mirror board lapping liquid, is made up of the raw material of following weight portion：Malic acid 24, formic acid 8, oxalic acid 3, glycerine
26th, dipotassium glycyrrhizinate 9, double octadecyl phosphates 7, ricinoleic acid ethyl ester 7, calcium lignosulfonate 6, barium mahogany sulfonate 6, go from
Sub- water 120.
Preparation and application, with embodiment 1.
Comparative example 1
Removal malic acid and formic acid, remaining preparation and application, with embodiment 1.
Comparative example 2
Removal oxalic acid and glycerine, remaining preparation and application, with embodiment 1.
Comparative example 3
Removal dipotassium glycyrrhizinate, remaining preparation and application, with embodiment 1.
Comparative example 4
The double octadecyl phosphates of removal and ricinoleic acid ethyl ester, remaining preparation and application, with embodiment 1.
Comparative example 5
Removal calcium lignosulfonate and barium mahogany sulfonate, remaining preparation and application, with embodiment 1.
Comparative example 6
All raw materials are in step（1）Add, remaining preparation and application, with embodiment 1.
Comparative example 7
Existing commercially available stainless steel mirror board lapping liquid.
The grinding effect of embodiment and comparative example stainless steel mirror board lapping liquid：
Selection alundum (Al2O3) is abrasive material, is divided into equal-sized 100 pieces, is randomly divided into 10 groups, every group 10 pieces, every group of abrasive material point
Polishing is not ground with the stainless steel mirror board lapping liquid of the group, other processing routines are identical, after the completion for the treatment of, by each implementation
The salt acid soak that example is divided into A with the stainless steel mirror board of comparative example group and two groups of B, A group mass concentration are 10% 60 days, B groups are used
Mass concentration is that 10% sodium hydroxide solution soaks 60 days, detects rate of corrosion, and embodiment and comparative example stainless steel mirror board grind
The grinding effect of liquid is shown in Table 1.
Table 1：The grinding effect of embodiment and comparative example stainless steel mirror board lapping liquid
| Project | Milling time/(h) | Hcl corrosion rate/(%) | NaOH rate of corrosion/(%) |
| Embodiment 1 | 3~4 | 0.16 | 0.11 |
| Embodiment 2 | 3~4 | 0.19 | 0.13 |
| Embodiment 3 | 3~4 | 0.17 | 0.09 |
| Comparative example 1 | 6~7 | 1.51 | 1.23 |
| Comparative example 2 | 6~7 | 1.73 | 1.31 |
| Comparative example 3 | 5~6 | 1.62 | 1.62 |
| Comparative example 4 | 4~5 | 1.74 | 1.65 |
| Comparative example 5 | 4~5 | 1.36 | 1.44 |
| Comparative example 6 | 4~5 | 1.53 | 1.24 |
| Comparative example 7 | 8~9 | 1.67 | 1.27 |
As it can be seen from table 1 the stainless steel mirror board lapping liquid of embodiment, milling time is substantially short compared with comparative example, hcl corrosion
Rate and NaOH rate of corrosion are substantially low compared with comparative example, can extend the service life of stainless steel mirror board, illustrate that the present invention is carried
The stainless steel mirror board lapping liquid of confession has preferable grinding effect.
Claims (5)
1. a kind of stainless steel mirror board lapping liquid, it is characterised in that be made up of the raw material of following weight portion：Malic acid 22 ~ 24, first
Acid 6 ~ 8, oxalic acid 2 ~ 3, glycerine 24 ~ 26, sodium tripolyphosphate 7 ~ 9, double octadecyl phosphates 5 ~ 7, ricinoleic acid ethyl ester 5 ~ 7,
Calcium lignosulfonate 4 ~ 6, barium mahogany sulfonate 4 ~ 6, water 100 ~ 120.
2. stainless steel mirror board lapping liquid according to claim 1, it is characterised in that described water, is deionized water.
3. the preparation method of stainless steel mirror board lapping liquid described in a kind of claim 1, it is characterised in that specifically include following step
Suddenly：
（1）Malic acid, formic acid and sodium tripolyphosphate are added to the water, 70 ~ 75 DEG C are heated to, insulated and stirred is obtained to being completely dissolved
Mixture A；
（2）Glycerine, double octadecyl phosphates and ricinoleic acid ethyl ester are mixed, 30 ~ 35 are stirred under vacuum in 50 ~ 60 DEG C of insulations
Minute, obtain mixture B；
（3）Mixture A and mixture B are well mixed, calcium lignosulfonate and barium mahogany sulfonate are added, in 50 ~ 60 DEG C of vacuum
Stirring 40 ~ 50 minutes, obtains stainless steel mirror board lapping liquid；
（4）Vacuum packaging, obtains finished product.
4. the preparation method of stainless steel mirror board lapping liquid according to claim 3, it is characterised in that the step（2）'s
It is stirred under vacuum, vacuum is 0.1Mpa, rotating speed is 110 ~ 130 revs/min.
5. the application method of stainless steel mirror board lapping liquid described in a kind of any one of claim 1 ~ 4, it is characterised in that when using
Appropriate stainless steel mirror board lapping liquid is taken, 6 ~ 8 times of water of amount of stainless steel mirror board lapping liquid weight is added, after stirring
Polishing is ground, the environment temperature for keeping grinding and polishing is 20 ~ 25 DEG C, uses remaining stainless steel mirror board lapping liquid Ying Mi
Envelope is preserved.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611164497.6A CN106757042B (en) | 2016-12-16 | 2016-12-16 | A kind of stainless steel mirror board lapping liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611164497.6A CN106757042B (en) | 2016-12-16 | 2016-12-16 | A kind of stainless steel mirror board lapping liquid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106757042A true CN106757042A (en) | 2017-05-31 |
| CN106757042B CN106757042B (en) | 2019-07-12 |
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ID=58891597
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611164497.6A Active CN106757042B (en) | 2016-12-16 | 2016-12-16 | A kind of stainless steel mirror board lapping liquid |
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1480566A (en) * | 2002-09-03 | 2004-03-10 | 周国桢 | Electrochemical grind (polishing) method for stainless steel |
| CN101076395A (en) * | 2004-10-18 | 2007-11-21 | 精工爱普生株式会社 | Encapsulation product, process for producing the same, and ink composition |
| CN101649181A (en) * | 2008-08-13 | 2010-02-17 | 海门市森达装饰材料有限公司 | Mirror grinding material and preparation method thereof |
| CN102962731A (en) * | 2011-09-01 | 2013-03-13 | 沈阳远大铝业工程有限公司 | Stainless steel plate 8K mirror surface processing method |
| CN102965668A (en) * | 2011-09-01 | 2013-03-13 | 沈阳远大铝业工程有限公司 | Polishing solution for processing stainless steel plate material 8K mirror surface |
| CN105862044A (en) * | 2015-02-05 | 2016-08-17 | 盟智科技股份有限公司 | Chemical mechanical polishing slurry |
| KR20160100059A (en) * | 2015-02-13 | 2016-08-23 | 주식회사 케이씨텍 | Slurry composition for semiconductor polishing |
-
2016
- 2016-12-16 CN CN201611164497.6A patent/CN106757042B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1480566A (en) * | 2002-09-03 | 2004-03-10 | 周国桢 | Electrochemical grind (polishing) method for stainless steel |
| CN101076395A (en) * | 2004-10-18 | 2007-11-21 | 精工爱普生株式会社 | Encapsulation product, process for producing the same, and ink composition |
| CN101649181A (en) * | 2008-08-13 | 2010-02-17 | 海门市森达装饰材料有限公司 | Mirror grinding material and preparation method thereof |
| CN102962731A (en) * | 2011-09-01 | 2013-03-13 | 沈阳远大铝业工程有限公司 | Stainless steel plate 8K mirror surface processing method |
| CN102965668A (en) * | 2011-09-01 | 2013-03-13 | 沈阳远大铝业工程有限公司 | Polishing solution for processing stainless steel plate material 8K mirror surface |
| CN105862044A (en) * | 2015-02-05 | 2016-08-17 | 盟智科技股份有限公司 | Chemical mechanical polishing slurry |
| KR20160100059A (en) * | 2015-02-13 | 2016-08-23 | 주식회사 케이씨텍 | Slurry composition for semiconductor polishing |
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| Publication number | Publication date |
|---|---|
| CN106757042B (en) | 2019-07-12 |
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