CN106752711A - A kind of hydraulic oil container fire resistant anticorrosive paint and preparation method thereof - Google Patents
A kind of hydraulic oil container fire resistant anticorrosive paint and preparation method thereof Download PDFInfo
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- CN106752711A CN106752711A CN201611196037.1A CN201611196037A CN106752711A CN 106752711 A CN106752711 A CN 106752711A CN 201611196037 A CN201611196037 A CN 201611196037A CN 106752711 A CN106752711 A CN 106752711A
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- parts
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- anticorrosive paint
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
- C09D5/082—Anti-corrosive paints characterised by the anti-corrosive pigment
- C09D5/084—Inorganic compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a kind of hydraulic oil container fire resistant anticorrosive paint, the fire resistant anticorrosive paint includes following components according to the mass fraction:Epoxy resin：30 40 parts, sodium cellulose glycolate：10 15 parts, polytetrafluoroethylene (PTFE)：24 parts, sodium bentonite：36 parts, nano silicon：10 18 parts, nano titanium oxide：9 13 parts, barium sulfate：47 parts, zinc oxide：35 parts, filler：10 15 parts, calcium oxide：37 parts, dimethylbenzene：23 parts, butyl ester：34 parts, pigment：8 11 parts, hexone：36 parts, accelerator：35 parts, coupling agent：45 parts；The present invention has good wear resistence, high temperature resistant and corrosion resistance.
Description
Technical field
The present invention relates to a kind of coating and preparation method thereof, and in particular to a kind of high temperature resistant for protecting hydraulic oil container is prevented
Etching ground and preparation method thereof.
Background technology
With continuing to develop for China's modern industry, particularly in metallurgy, petrochemical industry, the energy, new material and hydraulic pressure casting etc.
The application of industry, high-temperature service and auxiliary facility is more and more, however metal material in the hot environment easily with air in oxygen
There is oxidation reaction in gas, produce corrosion phenomena, so that metal material gradually loses intensity and causes structural missing, as each
The hidden danger of the accident of kind.Therefore, high-temperature service surface is typically necessary application fire-resistant anticorrosion paint and is protected, to prevent metal
Material oxidation is corroded, and extends the service life of high-temperature service；Specific to hydraulic oil container in hydraulic system due to exposing in the environment
Easily corrosion.
Coating common now is susceptible to thermal degradation and carbonization under the high temperature conditions, it is impossible to protection is played to base material and is made
With, and high-temperature resistant coating can keep not embrittlement under the high temperature conditions, not with base material peel off, not bubbling while keep certain
Physics and chemistry and mechanical performance so that object can grind at high temperature from the influence of the undesirable conditions such as chemical attack, oxidation corrosion
Sending out a kind of can effectively protect the coating of hydraulic oil container in hydraulic system as those skilled in the art's technical problem urgently to be resolved hurrily.
The content of the invention
The technical problems to be solved by the invention are, for the shortcoming that above prior art is present, propose a kind of hydraulic oil
Case fire resistant anticorrosive paint and preparation method thereof, the coating wear resistence prepared is good, high temperature resistant and excellent corrosion resistance.
In order to solve the above technical problems, the present invention provides a kind of hydraulic oil container fire resistant anticorrosive paint, it is described resistance to
High-temp anti-corrosion coating includes following components according to the mass fraction:Epoxy resin：30-40 parts, sodium cellulose glycolate：10-15
Part, polytetrafluoroethylene (PTFE)：2-4 parts, sodium bentonite：3-6 parts, nano silicon：10-18 parts, nano titanium oxide： 9-13
Part, barium sulfate：4-7 parts, zinc oxide：3-5 parts, filler：10-15 parts, calcium oxide：3-7 parts, dimethylbenzene：2-3 parts, butyl ester：3-4
Part, pigment：8-11 parts, hexone：3-6 parts, accelerator：3-5 parts, coupling agent：4-5 parts；
Described filler includes following components according to the mass fraction：Glass dust：30-40 parts, talcum powder：15-20 parts, mica powder：10-
15 parts, carbon black：10-20 parts, clay：6-8 parts；The pigment is the mixture of titanium dioxide and aluminium triphosphate；The accelerator
It is compound bifunctional silane, the coupling agent is silane coupler.
Further limits scheme of the invention：
Foregoing fire resistant anticorrosive paint includes following components according to the mass fraction:Epoxy resin：33 parts, hydroxymethyl cellulose
Sodium：11 parts, polytetrafluoroethylene (PTFE)：2 parts, sodium bentonite：3 parts, nano silicon：10 parts, nano titanium oxide：10 parts,
Barium sulfate：4 parts, zinc oxide：3 parts, filler：11 parts, calcium oxide：4 parts, dimethylbenzene：2 parts, butyl ester：3 parts, pigment：8 parts, methyl
Isobutyl ketone：3 parts, accelerator：3 parts, coupling agent：4 parts；
Described filler includes following components according to the mass fraction：Glass dust：35 parts, talcum powder：15 parts, mica powder：11 parts, carbon
It is black：13 parts, clay：6 parts；The pigment is the mixture of titanium dioxide and aluminium triphosphate；The accelerator is compound couple of official
Silane can be rolled into a ball, the coupling agent is silane coupler.
Foregoing fire resistant anticorrosive paint includes following components according to the mass fraction:Epoxy resin：36 parts, methylol fibre
The plain sodium of dimension：13 parts, polytetrafluoroethylene (PTFE)：4 parts, sodium bentonite：5 parts, nano silicon：13 parts, nano titanium oxide： 12
Part, barium sulfate：5 parts, zinc oxide：4 parts, filler：13 parts, calcium oxide：6 parts, dimethylbenzene：3 parts, butyl ester：4 parts, pigment：10 parts,
Hexone：5 parts, accelerator：4 parts, coupling agent：5 parts；
Described filler includes following components according to the mass fraction：Glass dust：37 parts, talcum powder：18 parts, mica powder：13 parts, carbon
It is black：15 parts, clay：7 parts；The pigment is the mixture of titanium dioxide and aluminium triphosphate；The accelerator is compound couple of official
Silane can be rolled into a ball, the coupling agent is silane coupler.
The present invention also designs a kind of preparation method of hydraulic oil container fire resistant anticorrosive paint, and the fire resistant anticorrosive is applied
The preparation method of material specifically includes following steps：
Step one：Dimethylbenzene, hexone and butyl ester are mixed according to said ratio, is stirred with 100-200r/min
20-30min, makes it stir, and is subsequently adding epoxy resin, polytetrafluoroethylene (PTFE), and temperature rises to 95-105 DEG C, then temperature drop
To 60-70 DEG C, sodium cellulose glycolate, sodium bentonite, calcium oxide and zinc oxide are added, continue to be stirred with 200-300r/min
2-3h, it is standby；
Step 2：According to said ratio by filler, nano silicon, nano titanium oxide attrition grinding, sulfuric acid is subsequently adding
Barium and pigment mix, and 30-40min is stirred with 200-300r/min, standby；
Step 3：Step one and step 2 are mixed, 1-2h is stirred with 100-200r/min, accelerator and idol are added while stirring
Connection agent, you can.
The beneficial effects of the invention are as follows：
Compound bifunctional silane accelerator is added in coating of the invention, with reactivity high, heat-resisting quantity
And good storage stability；Nano silicon, nano titanium oxide are added in coating, corrosion resistance and intensity is improved, together
When nano material fine size so that coating seems more fine and smooth, using titanium dioxide and aluminium triphosphate, improves the resistance to of coating
Corrosive nature；Addition sodium bentonite, obtains after hydrophily montmorillonite is readily wetted by water in bentonite and expands, so that coating has touching
Denaturation and caking property；Glass dust, talcum powder, mica powder and carbon black are with the addition of in auxiliary agent, glass dust is added, it is possible to increase corrosion resistant
Corrosion energy, the addition of talcum powder can change the linear expansion coefficient of coating, improve under the room temperature alternation performance and high temperature of coating
Anti- cracking performance, improves water resistance, heat-resisting quantity and the wearability of film；Mica powder significantly improves the intensity of coating.
Specific embodiment
Embodiment 1
The present embodiment provides a kind of hydraulic oil container corrosion resistance coating, and fire resistant anticorrosive paint includes with the following group according to the mass fraction
Point:Epoxy resin：33 parts, sodium cellulose glycolate：11 parts, polytetrafluoroethylene (PTFE)：2 parts, sodium bentonite：3 parts, nanometer titanium dioxide
Silicon：10 parts, nano titanium oxide：10 parts, barium sulfate：4 parts, zinc oxide：3 parts, filler：11 parts, calcium oxide：4 parts, diformazan
Benzene：2 parts, butyl ester：3 parts, pigment：8 parts, hexone：3 parts, accelerator：3 parts, coupling agent：4 parts；
Described filler includes following components according to the mass fraction：Glass dust：35 parts, talcum powder：15 parts, mica powder：11 parts, carbon
It is black：13 parts, clay：6 parts；The pigment is the mixture of titanium dioxide and aluminium triphosphate；The accelerator is compound couple of official
Silane can be rolled into a ball, the coupling agent is silane coupler.
The present embodiment also provides the preparation method of the corrosion resistant metal coating for hydraulic cylinder, and specific preparation method is as follows：
Step one：Dimethylbenzene, hexone and butyl ester are mixed according to said ratio, is stirred with 100r/min
30min, makes it stir, and is subsequently adding epoxy resin, polytetrafluoroethylene (PTFE), and temperature rises to 98 DEG C, and then temperature is down to 68 DEG C,
Sodium cellulose glycolate, sodium bentonite, calcium oxide and zinc oxide are added, continues to stir 3h with 200r/min, it is standby；
Step 2：According to said ratio by filler, nano silicon, nano titanium oxide attrition grinding, sulfuric acid is subsequently adding
Barium and pigment mix, and 40min is stirred with 200r/min, standby；
Step 3：Step one and step 2 are mixed, 2h are stirred with 100r/min, accelerator and coupling agent are added while stirring,
.
Embodiment 2
The present embodiment provides a kind of hydraulic oil container fire resistant anticorrosive paint, and fire resistant anticorrosive paint is wrapped according to the mass fraction
Include following components:Epoxy resin：36 parts, sodium cellulose glycolate：13 parts, polytetrafluoroethylene (PTFE)：4 parts, sodium bentonite：5 parts, receive
Rice silica：13 parts, nano titanium oxide：12 parts, barium sulfate：5 parts, zinc oxide：4 parts, filler：13 parts, calcium oxide：6
Part, dimethylbenzene：3 parts, butyl ester：4 parts, pigment：10 parts, hexone：5 parts, accelerator：4 parts, coupling agent：5 parts；
Described filler includes following components according to the mass fraction：Glass dust：37 parts, talcum powder：18 parts, mica powder：13 parts, carbon
It is black：15 parts, clay：7 parts；The pigment is the mixture of titanium dioxide and aluminium triphosphate；The accelerator is compound couple of official
Silane can be rolled into a ball, the coupling agent is silane coupler.
The present embodiment also provides the preparation method of the corrosion resistant metal coating for hydraulic cylinder, and specific preparation method is as follows：
Step one：Dimethylbenzene, hexone and butyl ester are mixed according to said ratio, is stirred with 200r/min
20min, makes it stir, and is subsequently adding epoxy resin, polytetrafluoroethylene (PTFE), and temperature rises to 103 DEG C, and then temperature is down to 65
DEG C, sodium cellulose glycolate, sodium bentonite, calcium oxide and zinc oxide are added, continue to stir 2h with 300r/min, it is standby；
Step 2：According to said ratio by filler, nano silicon, nano titanium oxide attrition grinding, sulfuric acid is subsequently adding
Barium and pigment mix, and 30min is stirred with 300r/min, standby；
Step 3：Step one and step 2 are mixed, 1h are stirred with 200r/min, accelerator and coupling agent are added while stirring,
.
In addition to the implementation, the present invention can also have other embodiment.All use equivalents or equivalent transformation shape
Into technical scheme, all fall within the protection domain of application claims.
Claims (4)
1. a kind of hydraulic oil container fire resistant anticorrosive paint, it is characterised in that the fire resistant anticorrosive paint presses mass parts
Number meter includes following components:Epoxy resin：30-40 parts, sodium cellulose glycolate：10-15 parts, polytetrafluoroethylene (PTFE)：2-4 parts, sodium
Base bentonite：3-6 parts, nano silicon：10-18 parts, nano titanium oxide：9-13 parts, barium sulfate：4-7 parts, oxidation
Zinc：3-5 parts, filler：10-15 parts, calcium oxide：3-7 parts, dimethylbenzene：2-3 parts, butyl ester：3-4 parts, pigment：8-11 parts, methyl it is different
Butyl ketone：3-6 parts, accelerator：3-5 parts, coupling agent：4-5 parts；
Described filler includes following components according to the mass fraction：Glass dust：30-40 parts, talcum powder：15-20 parts, mica powder：10-
15 parts, carbon black：10-20 parts, clay：6-8 parts；The pigment be titanium dioxide, aluminium triphosphate, iron oxide red or carbon black it is a kind of or
It is several；The accelerator is compound bifunctional silane, and the coupling agent is silane coupler.
2. hydraulic oil container fire resistant anticorrosive paint according to claim 1, it is characterised in that the high temperature resistant is prevented
Etching ground includes following components according to the mass fraction:Epoxy resin：33 parts, sodium cellulose glycolate：11 parts, polytetrafluoroethyl-ne
Alkene：2 parts, sodium bentonite：3 parts, nano silicon：10 parts, nano titanium oxide：10 parts, barium sulfate：4 parts, oxidation
Zinc：3 parts, filler：11 parts, calcium oxide：4 parts, dimethylbenzene：2 parts, butyl ester：3 parts, pigment：8 parts, hexone：3 parts,
Accelerator：3 parts, coupling agent：4 parts；
Described filler includes following components according to the mass fraction：Glass dust：35 parts, talcum powder：15 parts, mica powder：11 parts, carbon
It is black：13 parts, clay：6 parts；The pigment is the mixture of titanium dioxide and aluminium triphosphate；The accelerator is compound couple of official
Silane can be rolled into a ball, the coupling agent is silane coupler.
3. hydraulic oil container fire resistant anticorrosive paint according to claim 1, it is characterised in that the high temperature resistant is prevented
Etching ground includes following components according to the mass fraction:Epoxy resin：36 parts, sodium cellulose glycolate：13 parts, polytetrafluoroethyl-ne
Alkene：4 parts, sodium bentonite：5 parts, nano silicon：13 parts, nano titanium oxide：12 parts, barium sulfate：5 parts, oxidation
Zinc：4 parts, filler：13 parts, calcium oxide：6 parts, dimethylbenzene：3 parts, butyl ester：4 parts, pigment：10 parts, hexone：5 parts,
Accelerator：4 parts, coupling agent：5 parts；
Described filler includes following components according to the mass fraction：Glass dust：37 parts, talcum powder：18 parts, mica powder：13 parts, carbon
It is black：15 parts, clay：7 parts；The pigment is the mixture of titanium dioxide and aluminium triphosphate；The accelerator is compound couple of official
Silane can be rolled into a ball, the coupling agent is silane coupler.
4. according to any described hydraulic oil container corrosion-and high-temp-resistant preparation method for coating of claim 1-3, it is characterised in that
Specifically include following steps：
Step one：Dimethylbenzene, hexone and butyl ester are mixed according to said ratio, is stirred with 100-200r/min
20-30min, makes it stir, and is subsequently adding epoxy resin, polytetrafluoroethylene (PTFE), and temperature rises to 95-105 DEG C, then temperature drop
To 60-70 DEG C, sodium cellulose glycolate, sodium bentonite, calcium oxide and zinc oxide are added, continue to be stirred with 200-300r/min
2-3h, it is standby；
Step 2：According to said ratio by filler, nano silicon, nano titanium oxide attrition grinding, sulfuric acid is subsequently adding
Barium and pigment mix, and 30-40min is stirred with 200-300r/min, standby；
Step 3：Step one and step 2 are mixed, 1-2h is stirred with 100-200r/min, accelerator and idol are added while stirring
Connection agent, you can.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611196037.1A CN106752711A (en) | 2016-12-22 | 2016-12-22 | A kind of hydraulic oil container fire resistant anticorrosive paint and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611196037.1A CN106752711A (en) | 2016-12-22 | 2016-12-22 | A kind of hydraulic oil container fire resistant anticorrosive paint and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107501871A (en) * | 2017-10-18 | 2017-12-22 | 徐宏伟 | A kind of Novel composite heat resistance material and preparation method thereof |
| CN108047786A (en) * | 2017-12-15 | 2018-05-18 | 苏州赛斯德工程设备有限公司 | A kind of fire resistant anticorrosive paint and preparation method thereof |
| CN108546497A (en) * | 2018-05-09 | 2018-09-18 | 常州市华菱新材料有限公司 | A kind of self-drying type epoxy coating and preparation method thereof and application method |
| CN111808501A (en) * | 2020-07-16 | 2020-10-23 | 杭州烯创科技有限公司 | Anti-aging graphene hydrophobic coating for windscreen wiper and preparation method of anti-aging graphene hydrophobic coating |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107501871A (en) * | 2017-10-18 | 2017-12-22 | 徐宏伟 | A kind of Novel composite heat resistance material and preparation method thereof |
| CN108047786A (en) * | 2017-12-15 | 2018-05-18 | 苏州赛斯德工程设备有限公司 | A kind of fire resistant anticorrosive paint and preparation method thereof |
| CN108546497A (en) * | 2018-05-09 | 2018-09-18 | 常州市华菱新材料有限公司 | A kind of self-drying type epoxy coating and preparation method thereof and application method |
| CN111808501A (en) * | 2020-07-16 | 2020-10-23 | 杭州烯创科技有限公司 | Anti-aging graphene hydrophobic coating for windscreen wiper and preparation method of anti-aging graphene hydrophobic coating |
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Application publication date: 20170531 |