CN106748527A - A kind of production method of organic water-soluble fertilizer - Google Patents
A kind of production method of organic water-soluble fertilizer Download PDFInfo
- Publication number
- CN106748527A CN106748527A CN201710028583.2A CN201710028583A CN106748527A CN 106748527 A CN106748527 A CN 106748527A CN 201710028583 A CN201710028583 A CN 201710028583A CN 106748527 A CN106748527 A CN 106748527A
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- China
- Prior art keywords
- soluble fertilizer
- organic water
- liquid
- production method
- cholesterol
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Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
Abstract
The invention belongs to Water soluble fertilizer production field, specifically related to a kind of manufacturing technique method of organic water-soluble fertilizer, reacted after turf, feather, cholesterol and alkali lye are sufficiently mixed, then neutralize, separation of solid and liquid, addition nitrogenous fertilizer, potash fertilizer, phosphate fertilizer compound, organic water-soluble fertilizer is dried to obtain by condensing crystallizing, the organic water-soluble fertilizer of present invention production can improve soil physical and chemical property, increase soil fertility;Promote the activity of edaphon;Fertilizer cost is reduced, maintain and promotes soil nutrient balance.
Description
Technical field
The invention belongs to field, especially a kind of production method of organic water-soluble fertilizer.
Background technology
Water soluble fertilizer be it is a kind of can be with completely soluble polyelement composite fertilizer, it can promptly be dissolved in the water, more
Easily it is absorbed by crops, and its absorption rate is of a relatively high, and more crucially it can apply to be sprayed the facilities such as filling
Agricultural, realizes water-fertilizer integral, reaches the efficiency that water-saving saves fertile saving of labor.
The water soluble fertilizer that there is current standard in current China has:It is a great number of elements water-soluble fertilizer, moderate-element water-soluble fertilizer, micro-
Secondary element water-soluble fertilizer, water-soluble fertilizer containing amino acid, containing humic acid water-soluble fertilizer, wherein largely, Medium-microelements Water soluble fertilizer
Material only has definitive requirement to a large amount of, Medium-microelements content, and content requirement is not done to dissolved organic matter;Contain ammonia simultaneously
An Ji Suan≤10%, Fu Zhi Suan≤3% limited in base acid, humic acid water-soluble fertilizer, above-mentioned content's index are relatively low, are that plant carries
The absorbable organic matter negligible amounts for supplying, the effect for do not reach and improve product quality, increasing soil fertility.
It is contemplated that the absorbable content of organic matter in water-soluble fertilizer is improved to the control of more than 30%, NPK contents existing
Less than 20%, and increase the content of the benefit materials such as peptide, enzyme, trace element, reach improvement soil, regulation microbial balance,
Improve the effect of product quality.
The content of the invention
The present invention is achieved by the following technical programs:
To solve the above problems, the present invention provides a kind of production method of organic water-soluble fertilizer, comprises the following steps:
(1) crush:Turf, feather are crushed to 10~100 mesh, cholesterol crushes powdering or pulpous state.
(2) react:By turf, feather, cholesterol and mass percent for 1~20% alkali lye mixes according to a certain percentage,
At a certain temperature in reaction kettle for reaction 0.5~3 hour, liquid A is obtained.
(3) neutralize:Regulation pH value is 6~8 during acid and conditioning agent are added into liquid A.Then separation of solid and liquid obtains liquid B.
(4) concentrate:Liquid B and additive are carried out into hybrid reaction according to a certain percentage, is then dried by condensing crystallizing
Obtain organic water-soluble fertilizer.
Turf, feather, cholesterol, alkali lye proportioning are 1t according to quality, quality, quality, volume in the step:0.1~
2t:0.01~1t:0.5~2m3Hybrid reaction is carried out, reaction temperature is 80~250 DEG C.
The step cholesterol is one or more mixing in animal brain, animal kidney, animal pancreas, eggs.
The step alkali lye is at least one of NaOH, potassium hydroxide, ammoniacal liquor.
The step acid is one kind in sulfuric acid, nitric acid or both mixing, and conditioning agent is ferric sulfate, manganese sulfate, sulfuric acid
At least one of copper, zinc sulfate.
The step additive is potassium nitrate, potassium sulfate, potassium chloride, potassium dihydrogen phosphate, ammonium sulfate, urea, phosphoric acid hydrogen two
The various mixing of a kind of the latter in potassium, magnesium sulfate.
Beneficial effect
Turf, feather are rich in the necessary humic acid of plant and amino acid, and humic acid contains various active group, network easily occurs
Close reaction, but its complex compound that metal is generated with calcium, magnesium, iron, aluminium etc. is hard to tolerate in water, by highly basic medium, by turf
Water and combined humus soluble in water are insoluble in in feather ash, humate soluble in water is disposably complexed into,
The improvement of technique so that production cost reduction, while improving plant absorption efficiency;Amino acid provides nutrients for the growth of plant
Matter, aggravates the accumulation of dry and from plant root or leaf portion to the running speed at other positions and quantity, adjusts a great number of elements,
The ratio and poised state of micro- and various nutriments, and then play a part of coordinate plant growth, amino acid is also
Chelatropic reaction can occur with a great number of elements such as N, P, K, the trace element such as Zn, Fe, Cu, Mn, B, Mo, to element needed for crop
Protective effect is produced, and generates the chelate that solubility is good, be easily absorbed by crops, so as to be conducive to plant absorption;It is solid rich in courage
The material of alcohol is hydrolyzed into peptide, enzyme under the high temperature conditions can promote absorption of the plant to NPK and organic matter, micro- in increase soil
Biological content, regulation geobiont balance.
The invention belongs to Water soluble fertilizer production field, and in particular to a kind of manufacturing technique method of organic water-soluble fertilizer, by turf,
Feather, cholesterol and alkali lye react after being sufficiently mixed, and then neutralize, separation of solid and liquid, addition nitrogenous fertilizer, potash fertilizer, phosphate fertilizer compound, pass through
Condensing crystallizing is dried to obtain organic water-soluble fertilizer, and the organic water-soluble fertilizer of present invention production can improve soil physical and chemical property, carry
Soil fertility high;Promote the activity of edaphon;Fertilizer cost is reduced, maintain and promotes soil nutrient balance.
Specific embodiment
Embodiment 1
(1) crush:Turf, feather are crushed to 10 mesh, cholesterol crushes powdering or pulpous state;
(2) react:By turf, feather, cholesterol and mass percent for 5% alkali lye mixes according to a certain percentage, one
Determine at temperature in reaction kettle for reaction 0.5 hour, obtain liquid A;
(3) neutralize:Regulation pH value is 6 during acid and conditioning agent are added into liquid A.Then separation of solid and liquid obtains liquid B;
(4) concentrate:Liquid B and additive are carried out into hybrid reaction according to a certain percentage, is then dried by condensing crystallizing
Obtain organic water-soluble fertilizer;
Turf, feather, cholesterol, alkali lye proportioning are 1t according to quality, quality, quality, volume in the step:0.5:
0.06:0.8m carries out hybrid reaction, and reaction temperature is 80 DEG C.
Embodiment 2
(1) crush:Turf, feather are crushed to 100 mesh, cholesterol crushes powdering or pulpous state;
(2) react:By turf, feather, cholesterol and mass percent for 20% alkali lye mixes according to a certain percentage, one
Determine at temperature in reaction kettle for reaction 3 hours, obtain liquid A;
(3) neutralize:Regulation pH value is 8 during acid and conditioning agent are added into liquid A, and then separation of solid and liquid obtains liquid B;
(4) concentrate:Liquid B and additive are carried out into hybrid reaction according to a certain percentage, is then dried by condensing crystallizing
Obtain organic water-soluble fertilizer;
Turf, feather, cholesterol, alkali lye proportioning are 1t according to quality, quality, quality, volume in the step:2t:1t:
2m carries out hybrid reaction, and reaction temperature is 170 DEG C.
Embodiment 3
(1) crush:Turf, feather are crushed to 50 mesh, cholesterol crushes powdering or pulpous state;
(2) react:By turf, feather, cholesterol and mass percent for 10% alkali lye mixes according to a certain percentage, one
Determine at temperature in reaction kettle for reaction 1.5 hours, obtain liquid A;
(3) neutralize:Regulation pH value is 7 during acid and conditioning agent are added into liquid A, and then separation of solid and liquid obtains liquid B;
(4) concentrate:Liquid B and additive are carried out into hybrid reaction according to a certain percentage, is then dried by condensing crystallizing
Obtain organic water-soluble fertilizer;
Turf, feather, cholesterol, alkali lye proportioning are 1t according to quality, quality, quality, volume in the step:2t:
0.01:0.5m carries out hybrid reaction, and reaction temperature is 100 DEG C.
Embodiment 4
(1) crush:Turf, feather are crushed to 80 mesh, cholesterol crushes powdering or pulpous state;
(2) react:By turf, feather, cholesterol and mass percent for 15% alkali lye mixes according to a certain percentage, one
Determine at temperature in reaction kettle for reaction 1 hour, obtain liquid A;
(3) neutralize:Regulation pH value is 6.5 during acid and conditioning agent are added into liquid A, and then separation of solid and liquid obtains liquid B;
(4) concentrate:Liquid B and additive are carried out into hybrid reaction according to a certain percentage, is then dried by condensing crystallizing
Obtain organic water-soluble fertilizer;
Turf, feather, cholesterol, alkali lye proportioning are 1t according to quality, quality, quality, volume in the step:1.3t:
0.7t:1.5m carries out hybrid reaction, and reaction temperature is 200 DEG C.
Embodiment 5
(1) crush:Turf, feather are crushed to 60 mesh, cholesterol crushes powdering or pulpous state;
(2) react:By turf, feather, cholesterol and mass percent for 17% alkali lye mixes according to a certain percentage, one
Determine at temperature in reaction kettle for reaction 2.5 hours, obtain liquid A;
(3) neutralize:Regulation pH value is 7.5 during acid and conditioning agent are added into liquid A, and then separation of solid and liquid obtains liquid B;
(4) concentrate:Liquid B and additive are carried out into hybrid reaction according to a certain percentage, is then dried by condensing crystallizing
Obtain organic water-soluble fertilizer;
Turf, feather, cholesterol, alkali lye proportioning are 1t according to quality, quality, quality, volume in the step:1.2t:
0.5t:1.2m carries out hybrid reaction, and reaction temperature is 80~250 DEG C.
Embodiment 6
(1) crush:Turf, feather are crushed to 90 mesh, cholesterol crushes powdering or pulpous state;
(2) react:By turf, feather, cholesterol and mass percent for 8% alkali lye mixes according to a certain percentage, one
Determine at temperature in reaction kettle for reaction 1 hour, obtain liquid A;
(3) neutralize:Regulation pH value is 8 during acid and conditioning agent are added into liquid A, and then separation of solid and liquid obtains liquid B;
(4) concentrate:Liquid B and additive are carried out into hybrid reaction according to a certain percentage, is then dried by condensing crystallizing
Obtain organic water-soluble fertilizer;
Turf, feather, cholesterol, alkali lye proportioning are 1t according to quality, quality, quality, volume in the step:0.1t:
0.01t:2m carries out hybrid reaction, and reaction temperature is 230 DEG C.
Claims (6)
1. a kind of production method of organic water-soluble fertilizer, it is characterised in that the water-soluble fertilizer production method is comprised the following steps:
(1) crush:Turf, feather are crushed to 10~100 mesh, cholesterol crushes powdering or pulpous state;
(2) react:By turf, feather, cholesterol and mass percent for 1~20% alkali lye mixes according to a certain percentage, one
Determine at temperature in reaction kettle for reaction 0.5~3 hour, obtain liquid A;
(3) neutralize:Regulation pH value is 6~8 during acid and conditioning agent are added into liquid A, and then separation of solid and liquid obtains liquid B;
(4) concentrate:Liquid B and additive are carried out into hybrid reaction according to a certain percentage, is then dried to obtain by condensing crystallizing
Organic water-soluble fertilizer.
2. according to power require profit 1 described in a kind of organic water-soluble fertilizer production method, it is characterised in that step (2) medium-height grass
Charcoal, feather, cholesterol, alkali lye proportioning are 1t according to quality, quality, quality, volume:0.1~2t:0.01~1t:0.5~2m3
Hybrid reaction is carried out, reaction temperature is 80~250 DEG C.
3. according to power require profit 1 described in a kind of organic water-soluble fertilizer production method, it is characterised in that what the step (2) referred to
Cholesterol is one or more mixing in animal brain, animal kidney, animal pancreas, eggs.
4. according to power require profit 1 described in a kind of organic water-soluble fertilizer production method, it is characterised in that what the step (2) referred to
Alkali lye is at least one of NaOH, potassium hydroxide, ammoniacal liquor.
5. according to power require profit 1 described in a kind of organic water-soluble fertilizer production method, it is characterised in that referred in the step (3)
Acid be one kind in sulfuric acid, nitric acid or both mixing, conditioning agent be in ferric sulfate, manganese sulfate, copper sulphate, zinc sulfate at least
It is a kind of.
6. according to power require profit 1 described in a kind of organic water-soluble fertilizer production method, it is characterised in that what the step (4) referred to
Additive is the one kind in potassium nitrate, potassium sulfate, potassium chloride, potassium dihydrogen phosphate, ammonium sulfate, urea, dipotassium hydrogen phosphate, magnesium sulfate
The various mixing of the latter.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107814663A (en) * | 2017-11-30 | 2018-03-20 | 广州雨蔬农业科技有限公司 | A kind of vegetables and fruits organic formula fertilizer and its preparation and application method |
CN108299093A (en) * | 2018-03-15 | 2018-07-20 | 河南博联农业研究院有限公司 | A kind of multi-element water soluble fertilizer and preparation method |
CN108314537A (en) * | 2018-03-28 | 2018-07-24 | 王珍珍 | A kind of weight-reducing synergic water soluble fertilizer and preparation method |
CN111285738A (en) * | 2020-03-06 | 2020-06-16 | 湛江市农海科技有限公司 | Biological fulvic acid water-soluble fertilizer and preparation method thereof |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101712581A (en) * | 2009-11-18 | 2010-05-26 | 陕西科技大学 | Method for preparing organic/inorganic humate foliar fertilizer |
CN105985178A (en) * | 2015-12-29 | 2016-10-05 | 芜湖润蓝生物科技有限公司 | Efficient fertilizer with additional modified osmanthus fragrans essential oil and double-release effects for Chinese cabbage and method for preparing efficient fertilizer |
-
2017
- 2017-01-16 CN CN201710028583.2A patent/CN106748527A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101712581A (en) * | 2009-11-18 | 2010-05-26 | 陕西科技大学 | Method for preparing organic/inorganic humate foliar fertilizer |
CN105985178A (en) * | 2015-12-29 | 2016-10-05 | 芜湖润蓝生物科技有限公司 | Efficient fertilizer with additional modified osmanthus fragrans essential oil and double-release effects for Chinese cabbage and method for preparing efficient fertilizer |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107814663A (en) * | 2017-11-30 | 2018-03-20 | 广州雨蔬农业科技有限公司 | A kind of vegetables and fruits organic formula fertilizer and its preparation and application method |
CN108299093A (en) * | 2018-03-15 | 2018-07-20 | 河南博联农业研究院有限公司 | A kind of multi-element water soluble fertilizer and preparation method |
CN108314537A (en) * | 2018-03-28 | 2018-07-24 | 王珍珍 | A kind of weight-reducing synergic water soluble fertilizer and preparation method |
CN111285738A (en) * | 2020-03-06 | 2020-06-16 | 湛江市农海科技有限公司 | Biological fulvic acid water-soluble fertilizer and preparation method thereof |
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