CN106734805B - Φ 500~650mm Cr6 swaged forging Electro Slag Remelting Steel cold roll blank forging deformation techniques - Google Patents

Φ 500~650mm Cr6 swaged forging Electro Slag Remelting Steel cold roll blank forging deformation techniques Download PDF

Info

Publication number
CN106734805B
CN106734805B CN201611104319.4A CN201611104319A CN106734805B CN 106734805 B CN106734805 B CN 106734805B CN 201611104319 A CN201611104319 A CN 201611104319A CN 106734805 B CN106734805 B CN 106734805B
Authority
CN
China
Prior art keywords
forging
temperature
fire
roll
swaged
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201611104319.4A
Other languages
Chinese (zh)
Other versions
CN106734805A (en
Inventor
于瑞芝
张岩
李颇
李瑛�
唐刚
刘洪波
姚凤祥
崔连进
刘向军
贾俊林
张程
毛威昂
李艾
李庆斌
李明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jianlong Beiman Special Steel Co Ltd
Original Assignee
Jianlong Beiman Special Steel Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jianlong Beiman Special Steel Co Ltd filed Critical Jianlong Beiman Special Steel Co Ltd
Priority to CN201611104319.4A priority Critical patent/CN106734805B/en
Publication of CN106734805A publication Critical patent/CN106734805A/en
Application granted granted Critical
Publication of CN106734805B publication Critical patent/CN106734805B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • B21J5/06Methods for forging, hammering, or pressing; Special equipment or accessories therefor for performing particular operations
    • B21J5/08Upsetting
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J1/00Preparing metal stock or similar ancillary operations prior, during or post forging, e.g. heating or cooling
    • B21J1/06Heating or cooling methods or arrangements specially adapted for performing forging or pressing operations
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21JFORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
    • B21J5/00Methods for forging, hammering, or pressing; Special equipment or accessories therefor
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/26Methods of annealing
    • C21D1/28Normalising
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/26Methods of annealing
    • C21D1/32Soft annealing, e.g. spheroidising
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/06Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires
    • C21D8/065Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires of ferrous alloys
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/22Ferrous alloys, e.g. steel alloys containing chromium with molybdenum or tungsten
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/24Ferrous alloys, e.g. steel alloys containing chromium with vanadium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Forging (AREA)

Abstract

The invention discloses a kind of 500~650mm of Φ Cr6 swaged forgings Electro Slag Remelting Steel cold roll blank forging deformation technique, the technique includes the following steps:Converter smelting+LF refining+VD vacuum → continuous cast round billets material → electrode blank hot sending annealing → cleaning → electroslag remelting → ESR ingot annealing → forging → forging rear annealing, wherein forging is produced using four fiery modes, first fire time is using jumping-up, the mode of texturing of pulling, second fire time is forged using heavy reduction, the 3rd fire to the 4th fiery forging and molding.The temperature and soaking time of crucial control High temperature diffusion in forging process, that forges every fire time returns stove holding temperature and time, per the control of the secondary deflection of fire and final forging temperature.2~3 grades of the spherodized structure of Cr6 swaged forgings Electro Slag Remelting Steel cold roll roller stock produced by the invention, carbide network≤2.0 grade, below carbide strip, 1.0 grades of liquation, non-metallic inclusion summation≤2.0 grade, flaw detection qualification rate has been increased to 95% by original 75%, and distribution of carbides is tiny, disperse, and service life is long.

Description

Φ 500~650mm Cr6 swaged forging Electro Slag Remelting Steel cold rolls blank forging deforms Technique
Technical field
The invention belongs to metallurgical technology fields, are related to a kind of Cr6 swaged forgings Electro Slag Remelting Steel cold roll blank forging deformation Technique.
Background technology
The cold roll material that the country uses before 2008 is mainly Cr2, Cr3 and Cr5 series, domestic cold to promote It rolls working roll to be updated with steel, improves wearability, roughness retentivity and the anti-roll marks performance of cold roll roller stock, from Start within 2008 the full special steel in north and cold roll steel of the Baosteel roll company co-production exploitation containing Cr6%.The steel grade roller Base alloy content is higher, carbide segregation weight, and especially big specification roller stock, ultrasonic examination is difficult to meet the requirements, and production is qualified Rate is relatively low.
Cr6 type roller stocks are on the basis of MC5 steel grades, and C is slightly improved, Si and Mo contents increase, and Cr contents add 1%, since alloy content is higher, steel ingot is also easy to produce serious segregation, and Forging Plasticity is poor, and it is larger to manufacture difficulty.Roller stock is used The requirements such as carbide network, banding, liquation and the field trash of steel, gas, flaw detection are all very stringent.Existing Cr6 is added using electric furnace External refining and the mode Electrode for remelting blank of vacuum outgas pour into a mould 10.4 tons of (Φ 680mm) electrode ingots by the way of molding. Φ 865mm~Φ 960mm electroslag ingots are produced using electroslag remelting mode.It is forged using 3000 tons of hydraulic presses, forging is advanced The processing of row high temperature homogenization is produced using the mode of 3 fiery mode finished products, the first fire time upper mounting plate jumping-up, pulling, steel ingot end Easily generate shrinkage cavity, the first fire time reduction in pass and deformation rate is excessive be easy to cause body of roll transverse fissure osculum.The second fire time body of roll Reduction in pass is excessive to be easy to cause body of roll transverse fissure osculum, when roll neck deforms between 800~900 DEG C, roll neck deformation rate is excessive, Deformation temperature is too low to be easy to cause internal carbides line of segragation cracking.3rd fire time body of roll deflection is smaller, body of roll coarse grains, Carbide network is serious.Roll neck deformation temperature is high, and it is inclined that local deformation rate is big, deformation velocity be easy to cause roll neck internal carbides soon Analysis area generated fire check.
The content of the invention
The object of the present invention is to provide a kind of 500~650mm of Φ Cr6 swaged forgings Electro Slag Remelting Steel cold roll blank forgings Deformation technique, the product quality of the technique productions are stablized, and production testing qualification rate reaches more than 95%.Cr6 type cold rolls It is compared after coming into operation with MC5 cold rolls since roll change rate has dropped 10% caused by roll marks defect, improves cold-reduced sheet Surface quality and milling train work efficiency.
The purpose of the present invention is what is be achieved through the following technical solutions:
A kind of 500~650mm of Φ Cr6 swaged forgings Electro Slag Remelting Steel cold roll blank forging deformation technique, including walking as follows Suddenly:Converter smelting+LF refining+VD vacuum → continuous cast round billets material → electrode blank hot sending annealing → cleaning → electroslag remelting → electroslag Ingot annealing → forging → forging rear annealing, wherein:
High temperature homogenization processing is carried out before forging, control heating temperature as 1190 DEG C~1210 DEG C, soaking time is 30~ 42h。
It is produced, is as follows using four fiery modes during forging:
First fire:Using the upward jumping-up of arc upset plate Steel ingot feeder head, upset ratio is controlled between 1.5~2.0, then adopted With flat anvil, lower V-type anvil pull out, reduction in pass be 30~50mm, deformation rate be 15~20%, return stove soaking time 2.5~ 3.5h returns 1190~1210 DEG C of furnace temperature;
Second fire:The body of roll pulls out finished product forging's block dimension and adds 50mm surpluses, and reduction in pass is 60~80mm, deformation rate 25 ~30%, it returns stove and keeps the temperature 1~2h, return 1170~1190 DEG C of furnace temperature;
3rd fire:Upper flat anvil is constant, and lower anvil forges one end roll neck using small V-type anvil, and deformation rate is 20~60%, passage pressure Lower amount carries out in a manner that high temperature stops forging 3 seconds between 30~80mm, returns stove soaking time 50~70 minutes, return furnace temperature 1170~1190 DEG C;
4th fire:Forge other end roll neck, the rest and reorganization body of roll, body of roll deflection between 7~8%, roll neck forging method and 3rd fire is the same;
Above each fire time final forging temperature is 850~900 DEG C, and less than 900 DEG C are rest and reorganization temperature;
It is heat-treated after forging, controls normalizing temperature:1020℃;Spheroidizing temperature:840℃、740℃:Expand hydrogen to move back Fiery temperature:680℃.
The present invention is produced in forging using four fiery modes, and the first fire uses the upward jumping-up of arc upset plate Steel ingot feeder head, Reduce the generation of shrinkage cavity, while improve lumber recovery;And first fire time reduction in pass be reduced to 30 by 80~100mm~ 50mm light reductions are touched, and deformation rate is also reduced to 15~20% by 25~30%, are reduced the body of roll and are generated transverse fissure osculum.Second fire The secondary body of roll pulls out finished product forging's block dimension and adds 50mm surpluses, and reduction in pass is 60~80mm, between deformation rate is 25~30%, road Secondary drafts reduces, and reduces the generation of body of roll crackle.3rd fire time forging one end roll neck, deformation rate is 20~60%, road Secondary drafts carries out between 30~80mm in a manner that high temperature stops forging 3 seconds, i.e., upper anvil pauses 3 seconds again when touching forging Pressure reduces roll neck internal carbides line of segragation caused by since deflection is excessive and crosses fire check;Roll neck deformation temperature 900 DEG C with On, reduce the internal cleavage that roll neck is formed due to cryogenic forging.4th fire time forging other end roll neck, the rest and reorganization body of roll, the body of roll Deflection is between 7~8%, and roll neck forging method is as the 3rd fire.First fire returns stove and keeps the temperature 2.5~3.5h, the second fire It returns stove and keeps the temperature 1~2h, the 3rd fire returns stove 50~70 minutes.Final forging temperature is 850~900 DEG C, and less than 900 DEG C are rest and reorganization temperature, It is not allow for large deformation.Increase by 1 fire, the roll neck of the second fire forging is changed to the 3rd fire and is forged, ensures forging temperature, reduces Due to internal cleavage caused by cryogenic forging.
A diameter of 500~650mm of Cr6 swaged forgings Electro Slag Remelting Steel cold roll roller stock produced by the invention, spherodized structure 2 ~3 grades, carbide network≤2.0 grade, below carbide strip, 1.0 grades of liquation, non-metallic inclusion summation≤2.0 grade, flaw detection Qualification rate has been increased to 95% by original 75%, and distribution of carbides is tiny, disperse, and service life is long.It is domestic at present precious The large-sized rolling mills of the Large Steel ironworks such as steel, Shoudu Iron and Steel Co, Anshan iron and steel plant start the cold roll using Cr6 section bar matter, using effect compared with Good, Cr6 types roller stock will progressively replace MC5 series cold rolls, the product wide market, can give enterprise in the near future Industry brings considerable economic benefit.Cr6 type roller stock ton steel profit is 4200 yuan or so, and the full year output in north is 2000 tons of left sides at present The right side can make a profit 8,400,000 yuan every year.Trial-produceing successfully for this product establishes solid base for the update of domestic cold roll material Plinth.
Description of the drawings
Fig. 1 is 1 grade of Cr6 roller stocks Cold Roll, the high power picture of 0 grade of liquation (100 ×);
Fig. 2 is the high power picture of 1 grade of Cr6 roller stocks net carbide (500 ×);
Fig. 3 is the high power picture of 2 grades of Cr6 roller stocks spherodized structure (500 ×);
Fig. 4 is the high temperature hot deformation resistance curve of Cr6;
Fig. 5 is the high-temp plastic figure of Cr6.
Specific embodiment
Technical scheme is further described below in conjunction with the accompanying drawings, but is not limited thereto, it is every to this Inventive technique scheme is modified or replaced equivalently, and without departing from the spirit and scope of technical solution of the present invention, should all be covered In protection scope of the present invention.
The present invention provides a kind of 500~650mm of Φ Cr6 swaged forging Electro Slag Remelting Steel cold rolls blank forgings to deform work Skill produces electrode blank by the way of converter smelting, ladle refining, vacuum outgas, then using electroslag remelting mode into one Cleaning molten steel is walked, by the segregation for controlling the state modulators ESR ingot such as melting rate in esr process.Rational electricity Slag ingot homogenization temperature and time, using the forging method of light-weight-light during forging, ESR ingot starting stage touch, then big pressure The forging of lower amount (30~50mm light reductions are touched during direct drawing out after jumping-up, come out of the stove again after stove heat preservation is returned pulling when can 60~ 80mm heavy reductions forge), each passage mutually overturning in 90 °, the body of roll reserves correction amount, and roll neck is given birth to by the way of finished product at twice Production, forging temperature are modified when being less than 900 DEG C, quick water-spraying control control net carbide after forging.The present invention passes through to molten steel Degree of purity, ESR ingot segregation, forging before high temperature homogenization temperature and time, forging deformation process, final forging temperature and controll cooling after forging, Heat treatment after forging etc. carries out priority control, and product is finally trial-produceed successfully, and the high power photo of product is shown in Fig. 1-Fig. 3.Particular technique side Case is as follows:
First, production process route is as follows:
Converter smelting+LF+VD → continuous cast round billets material → electrode blank hot sending annealing → cleaning → electroslag remelting → ESR ingot Annealing → forging → forging rear annealing → smooth surface, flaw detection → inspection (high and low times, gas) → are submitted.
2nd, each production process critical control point and technical principle are as follows:
A, converter smelting and LF refining+VD vacuum
For the chemical composition requirement of Cr6 type roller stocks, and consider to carry out the scaling loss of easy scaling loss element during electroslag remelting Amount, sets the internal control batch components of the steel grade, is specifically shown in Table 1 first.
Cr6 types roller stock is selected strictly to control harmful elements Pb, Sn, As, Sb, Bi content during furnace charge with the smelting of steel.Turn Stove initial smelting period ensures that molten steel takes off P, and in addition priority control terminal C content >=0.12%, prevents Molten Steel over-oxidation;When P content accords with It closes requirement and liquid steel temperature is suitable, slag-stopping tapping is carried out using slag retaining cone and control the lower quantity of slag, when slag thickness of slag layer is more than 150mm will carry out deslagging after deslagging processing or LF heatings;Tapping process carries out alloying, and main component control is in lower limit, tapping Heat lime and refining slag simultaneously;Ladle is to electricity heating is given behind LF refining position, and heating samples after a certain period of time, according to analysis result Adjusting component meets the requirements.When molten steel temperature is suitable, bits are white, deoxidation well carries out vacuum refining afterwards.Below 67 pa of vacuum degree, It is kept for 15 minutes, soft argon blowing 15 minutes after vacuum breaker.Continuous casting electrode blank selects the suitable casting degree of superheat in process of production And pulling rate.Electrode blank is annealed, and annealing is cleared up after coming out of the stove, and carries out electroslag remelting.
1 BGCr6 standards of table and blank chemical component requirement (%)
B, electroslag remelting and ESR ingot annealing
During electroslag remelting, first have to strengthen the baking to slag charge, it is ensured that the heating temperature of slag charge and heating time;And changing During slag, slag charge will equably be added portionwise, and to ensure slugging quality, metal electrode of being allowed for access after scorification is clear is refined.Especially It, to ensure to realize that shrinkage cavity depth is minimum, volume is minimum, improves the lumber recovery of ESR ingot it is noted that the control of feeding phase operation. According to the control melting rate of ingot shape size reasonable in esr process, ensure melting rate equalization stable.ESR ingot is annealed Processing, carry out cleaning sampling after annealing, then go to forge plant heated, forging process.
C, heating, forging and heat treatment after forging
ESR ingot is packed into stove preheating to be expected, after forging temperature is risen to, carries out high temperature homogenization processing, its purpose is to Improve or eliminate the uneven components formed in metallurgical process, forged after heat preservation.Its forging characteristic of Cr6 steel than MC3 and MC5 are weaker.Using jumping-up, the forging method of pulling, meet the requirement of forging ratio >=3, fully broken coarse branch Shape carbide.First fire time is using jumping-up, the mode of texturing of pulling, using the small deformation amount of 30~50mm, the second fire during pulling Secondary that the forging of 60~80mm heavy reductions can be used, abundant soldering internal flaw, temperature can light reduction finishing when being less than 900 DEG C. 3rd fire to the 4th fiery forging and molding.The temperature and soaking time of crucial control High temperature diffusion, are forged per fire in forging process Return stove holding temperature and time, per fire time deflection and final forging temperature control.
Heat treatment after forging is actually conditioning treatment, and emphasis is to complete three tasks:First, eliminate netted carbonization Object second is that eliminating stress softening tissue obtains globular pearlite tissue, third, to reduce hydrogen content in steel, prevents the production of white point It is raw.Therefore, heat treatment cycle curve is also made of three parts:Normalizing+spheroidizing+expansion hydrogen annealing.Annealing process by Two sections of compositions, the molten disconnected effect of carbide is played in 840 DEG C of nodularizations, and 740 DEG C of nodularization then determines final nodularization effect.
3rd, process parameter test is studied
1st, forging range is definite
To grope optimal smithing technological parameter, the sampling progress high temperature thermoplasticity experiment on Cr6 type roller stocks is groped optimal Forging range, provide theoretical foundation for big production.
Gleeble experiments are carried out using 3500 equipment of GLEEBLE at different temperature.Specific test temperature is as follows:Choosing Select 800 DEG C, 850 DEG C, 900 DEG C, 950 DEG C, 1000 DEG C, 1050 DEG C, 1100 DEG C, 1120 DEG C, 1140 DEG C, 1160 DEG C, 1180 DEG C, 1200 DEG C, 1220 DEG C, 1240 DEG C amount to 14 different temperatures, each two samples of temperature.
As seen in Figure 4, at 850 DEG C, resistance of deformation is larger, and resistance of deformation drastically declines at 900 DEG C, with change The rise of shape temperature, resistance of deformation is on a declining curve, to 1100~1200 DEG C between resistance of deformation variation it is smaller, curve is in gentle Trend, deformation temperature are more than that 1200 DEG C of resistances of deformation drastically decline again.It is seen from fig 5 that 800~1200 DEG C of plasticity compared with Good, more than 1200 DEG C plasticity drastically decline.
Generally between 1170~1190 DEG C, final forging temperature is controlled at 850~900 DEG C initial forging temperature during Cr6 blank forgings Between, light reduction finishing is carried out below 900 DEG C.It is found according to above analysis of experiments, the forging temperature model that we select Enclose that comparison is reasonable, substantial amounts of production practices also fully demonstrate the reasonability of Cr6 type blank forgings temperature range selection, high temperature modeling Property experiment theoretical foundation further is provided to the forging temperature reasonability of Cr6 type roller stocks.
2nd, normalizing temperature is definite
In order to verify the netted raised situation of change with heating temperature of Cr6 roller stocks, choose netted 3.5 grades of Cr6 12 Sample keeps the temperature oil cooling in 30 minutes at a temperature of 6 different heatings and examines netted situation of change, and inspection result is shown in Table 2.
Table 2
From table 2 it can be seen that with the raising of hardening heat, net level continuously decreases.950 DEG C do not change, 970 DEG C Improve unobvious, 990 DEG C start to have clear improvement, and there is no closing carbide networks, and 1050 DEG C netted to be reduced to 1.5 grades.
Because soaking time is shorter during experiment, therefore present invention normalizing temperature in production selects 1020 DEG C.
4th, 500~650mm of Φ Cr6 swaged forgings Electro Slag Remelting Steel cold roll roller stock manufacturing process is as follows:
1st, the chemical Composition Control of steel exists:C:0.85~0.95%, Mn:0.20~0.50%, Si:0.80~1.20%, S:≤ 0.015%, P:≤ 0.020%, Cr:5.50~6.00%, Mo:0.30~0.50%, V:0.05~0.15%, oxygen content ≤20×10-6, hydrogen content≤1.5 × 10-6, nitrogen content≤120 × 10-6, remaining is Fe.
2nd, steel is smelted using converter smelting+LF refining+VD vacuum+ESR electro-slag re-melting methods, electroslag ingot:Φ 865~ 960mm;
(1) using converter smelting+LF refining+VD vacuum technologies production Φ 650mm electrode bars when, LF refining furnace refining is in vain Slag method, soft blow argon >=15 minute after the degassing of VD stoves.
(2) in the smelting of Φ 865mm and Φ 960mm electroslag ingots, electrode bar remelting input power is controlled respectively 1300 ~1400kW and 1700~1800kW;Packing stage input power is continuously decreased with being not more than the speed of 100kW/h.
3rd, steel ingot carries out high temperature homogenization processing before forging, and heating temperature is 1190 DEG C~1210 DEG C, soaking time root It is controlled according to ingot shape by 30~42h.
4th, using more fire time forgings, it is divided into four steps:
First fire:Using the upward jumping-up of arc upset plate Steel ingot feeder head, upset ratio is controlled between 1.5~2.0, then adopted It is pulled out with flat anvil, lower V-type anvil, reduction in pass is 30~50mm, and deformation rate is 15~20%.Stove is returned according to steel ingot size to protect Between warm 2.5~3.5h of time, 1190~1210 DEG C of furnace temperature is returned.
Second fire:The body of roll pulls out finished product forging's block dimension and adds 50mm surpluses, and reduction in pass is 60~80mm, deformation rate 25 ~30%.It returns stove and keeps the temperature 1~2h, return 1170~1190 DEG C of furnace temperature.
3rd fire:Upper flat anvil is constant, and lower anvil forges one end roll neck using small V-type anvil, and deformation rate is 20~60%, passage pressure Lower amount carries out between 30~80mm in a manner that high temperature stops forging 3 seconds.It returns stove and keeps the temperature 50~70 minutes, return furnace temperature 1170 ~1190 DEG C.
4th fire:Forge other end roll neck, the rest and reorganization body of roll, body of roll deflection between 7~8%, roll neck forging method and 3rd fire is the same.
Above each fire time final forging temperature is 850~900 DEG C, and less than 900 DEG C are rest and reorganization temperature, are not allow for large deformation.
5th, water cooling after 3~4 minutes, is heat-fed annealing after the forging of finished product roller stock after air-cooled to 350~400 DEG C.
6th, heat treatment after forging process curve is also made of three parts:1020 DEG C of normalizing;Spheroidizing:840 DEG C of carbide Molten disconnected, 740 DEG C form globular carbide and grow up, and 680 DEG C of expansion hydrogen and globular carbide are further grown up.
Cr6 swaged forgings Electro Slag Remelting Steel cold roll roller stock carbide strip produced by the invention and liquation are according to GB/ The 8th, 9 rank figures are assessed as≤1.0 grades in T18254-2002 standards, and net carbide is according in GB/T1299-2014 standards Three rank figures are assessed as≤2.0 grades, and spherodized structure is assessed as 2 grades -3 grades according to second level figure in GB/T1299-2014 standards, For roller stock after roughing according to requiring to detect a flaw in GB/T13314-2008, credit rating meets A grades of requirements in Table A .2.

Claims (4)

1. a kind of 500~650mm of Φ Cr6 swaged forgings Electro Slag Remelting Steel cold roll blank forging deformation technique, including walking as follows Suddenly:Converter smelting+LF refining+VD vacuum → continuous cast round billets material → electrode blank hot sending annealing → cleaning → electroslag remelting → electroslag Ingot annealing → forging → forging rear annealing, it is characterised in that the forging is produced using four fiery modes, is as follows:
First fire:Using the upward jumping-up of arc upset plate Steel ingot feeder head, upset ratio is controlled between 1.5~2.0, then using upper Flat anvil, the pulling of lower V-type anvil, reduction in pass are 30~50mm, and deformation rate is 15~20%, returns stove 2.5~3.5h of soaking time, Return 1190~1210 DEG C of furnace temperature;
Second fire:The body of roll pulls out finished product forging's block dimension and adds 50mm surpluses, and reduction in pass is 60~80mm, deformation rate for 25~ 30%, it returns stove and keeps the temperature 1~2h, return 1170~1190 DEG C of furnace temperature;
3rd fire:Upper flat anvil is constant, and lower anvil forges one end roll neck using small V-type anvil, and deformation rate is 20~60%, reduction in pass Between 30~80mm, carried out in a manner that high temperature stops forging 3 seconds, return stove soaking time 50~70 minutes, return furnace temperature 1170 ~1190 DEG C;
4th fire:Other end roll neck is forged, the rest and reorganization body of roll, body of roll deflection is between 7~8%, roll neck forging method and the 3rd It is fiery the same;
Above each fire time final forging temperature is 850~900 DEG C, and less than 900 DEG C are rest and reorganization temperature.
2. 500~650mm of Φ Cr6 swaged forging Electro Slag Remelting Steel cold rolls blank forging according to claim 1 deforms work Skill, it is characterised in that high temperature homogenization processing is carried out before the forging, it is 1190 DEG C~1210 DEG C control heating temperature, during heat preservation Between be 30~42h.
3. 500~650mm of Φ Cr6 swaged forging Electro Slag Remelting Steel cold rolls blank forging according to claim 1 deforms work Skill, it is characterised in that be heat-treated after the forging, it is 1020 DEG C to control normalizing temperature.
4. 500~650mm of Φ Cr6 swaged forging Electro Slag Remelting Steel cold rolls blank forging according to claim 1 deforms work Skill, it is characterised in that the chemical Composition Control of the Cr6 swaged forgings Electro Slag Remelting Steel cold roll roller stock exists:C:0.85~ 0.95%th, Mn:0.20~0.50%, Si:0.80~1.20%, S:≤ 0.015%, P:≤ 0.020%, Cr:5.50~ 6.00%th, Mo:0.30~0.50%, V:0.05~0.15%, oxygen content≤20 × 10-6, hydrogen content≤1.5 × 10-6, nitrogen contains Amount≤120 × 10-6, remaining is Fe.
CN201611104319.4A 2016-12-05 2016-12-05 Φ 500~650mm Cr6 swaged forging Electro Slag Remelting Steel cold roll blank forging deformation techniques Active CN106734805B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611104319.4A CN106734805B (en) 2016-12-05 2016-12-05 Φ 500~650mm Cr6 swaged forging Electro Slag Remelting Steel cold roll blank forging deformation techniques

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611104319.4A CN106734805B (en) 2016-12-05 2016-12-05 Φ 500~650mm Cr6 swaged forging Electro Slag Remelting Steel cold roll blank forging deformation techniques

Publications (2)

Publication Number Publication Date
CN106734805A CN106734805A (en) 2017-05-31
CN106734805B true CN106734805B (en) 2018-05-22

Family

ID=58874061

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611104319.4A Active CN106734805B (en) 2016-12-05 2016-12-05 Φ 500~650mm Cr6 swaged forging Electro Slag Remelting Steel cold roll blank forging deformation techniques

Country Status (1)

Country Link
CN (1) CN106734805B (en)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108723268A (en) * 2018-04-19 2018-11-02 河南中原特钢装备制造有限公司 Small deformation amount improves the forging method of continuous casting billet forging hollow object General Loosen
CN108728606B (en) * 2018-05-09 2020-09-29 石家庄钢铁有限责任公司 Production process of cold roll steel electroslag blank
CN108672625B (en) * 2018-05-28 2019-09-27 建龙北满特殊钢有限责任公司 A kind of processing method using diameter forging machine production multi-step cold roll base
CN108942093B (en) * 2018-07-05 2020-02-18 建龙北满特殊钢有限责任公司 Manufacturing method of sector plate forge piece for economical coiler drum
CN108950134B (en) * 2018-08-21 2021-01-26 成都先进金属材料产业技术研究院有限公司 Remelting method of electroslag ingot for cold roll
CN111167986B (en) * 2020-02-26 2022-02-01 建龙北满特殊钢有限责任公司 Forging method for improving net shape of roller blank by using radial forging machine
CN111534755B (en) * 2020-06-17 2022-05-10 江苏良工精密合金钢有限公司 High-temperature-resistant water-free roller and preparation method thereof
CN111715829B (en) * 2020-06-29 2022-03-15 建龙北满特殊钢有限责任公司 Forging method for improving ultrasonic flaw detection qualification rate of large-step-difference roller blank
CN112126743B (en) * 2020-08-19 2021-12-14 石钢京诚装备技术有限公司 Production method of low-aluminum-content Cr5 steel ingot for supporting roll
CN114410977B (en) * 2021-12-27 2023-07-25 河钢股份有限公司 Preparation method of large-size high-strength invar forging
CN114836675B (en) * 2022-04-20 2023-06-06 山西太钢不锈钢股份有限公司 Preparation method of high-end structural steel 30CrMnSiNi2A
CN115537640B (en) * 2022-10-14 2023-03-10 唐山志威科技有限公司 ZW931 roller of lithium ion battery pole piece rolling mill and preparation method thereof
CN116855703B (en) * 2023-07-13 2024-03-08 广东韶铸精锻有限公司 Forging process method of blank
CN116949260B (en) * 2023-09-20 2023-12-19 成都先进金属材料产业技术研究院股份有限公司 Steel ingot for P91 seamless steel tube and thermal deformation method thereof

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1686666A (en) * 2005-04-18 2005-10-26 宝钢集团上海五钢有限公司 Production method of large high chromium steel cold roll blank
CN101381844B (en) * 2008-09-11 2011-01-05 山东中天模具有限公司 Production technology of cold working die steel material
DE102009049398C5 (en) * 2009-10-14 2015-05-07 Benteler Automobiltechnik Gmbh Method for producing a structural component for a motor vehicle and structural component
CN101709427A (en) * 2009-11-26 2010-05-19 上海大学 Low-cost, high-strength, high-toughness and high-abrasion resistance cold-working die steel and preparation method thereof
CN102418042B (en) * 2011-11-16 2013-06-05 抚顺特殊钢股份有限公司 Novel manufacturing process of phi 300 mm-phi 700 mm high-carbon high-chromium cold-working die steel forged round steel
JP6394319B2 (en) * 2014-11-21 2018-09-26 新日鐵住金株式会社 Hot forging
CN105755391A (en) * 2016-05-16 2016-07-13 昆山双儒模具科技有限公司 Novel high-speed steel material and preparation process thereof

Also Published As

Publication number Publication date
CN106734805A (en) 2017-05-31

Similar Documents

Publication Publication Date Title
CN106734805B (en) Φ 500~650mm Cr6 swaged forging Electro Slag Remelting Steel cold roll blank forging deformation techniques
CN109112408B (en) Manufacturing method of large-specification P92 heat-resistant steel forging
CN106947908B (en) A kind of method of continuous casting electroslag production 4Cr5MoSiV1 die steels
CN102418042B (en) Novel manufacturing process of phi 300 mm-phi 700 mm high-carbon high-chromium cold-working die steel forged round steel
CN100519813C (en) High-strength toughness cold working die steel and method of producing the same
CN101787492B (en) Manufacturing method of high quality and large size mandril blank
CN110935827B (en) Forging method of large-specification fine-grain austenitic stainless steel SNCrW bar
CN105088094B (en) A kind of manufacture method for controlling nitrogen austenitic stainless steel heavy forging
CN101660098A (en) Hot-rolling seamless steel pipe applicable to high temperature of 580-620 DEG C and high pressure of 24-30MPa and production method thereof
CN105839028B (en) Austenite heat-resistance Valve Steel manufacture method
CN1686666A (en) Production method of large high chromium steel cold roll blank
CN112695255B (en) Preparation method of ferrite martensite steel clad tube
CN112375982B (en) Process for forging round steel by using superfine chromium-molybdenum hot-working die steel
CN105177264B (en) A kind of manufacturing method of stainless steel forging round steel
CN102000954A (en) Method for manufacturing continuous pipe mill retained mandrel
CN106636861B (en) The preparation technology of high-alloy hot work mould steel
CN105522085A (en) Manufacturing method for large section forgings of high-speed tool steel
JP2023542427A (en) Low-cost, high-performance Q500 bridge steel and production method
CN102337462A (en) Production method for GCr15 bearing steel pipe
CN103147009B (en) N80Q steel-grade oil casing and manufacture method thereof
CN106825463A (en) A kind of method that billet caster produces low-carbon (LC) Ni Mo steel alloys
CN104404356B (en) A kind of return material method of smelting of impeller martensitic stain less steel
CN105543653A (en) Plastic die steel with high intensity, high toughness and high corrosion resistance and production method thereof
CN107641775A (en) Ship axle high intensity austenite magnetism-free stainless steel and preparation method thereof
CN106591683B (en) The processing method of cold roll tool steel

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
CB02 Change of applicant information
CB02 Change of applicant information

Address after: 161041, No. 7, red shore street, Fulaerji District, Heilongjiang, Qigihar

Applicant after: Jianlong Beiman Special Steel Co. Ltd.

Address before: 161041, No. 7, red shore street, Fulaerji District, Heilongjiang, Qigihar

Applicant before: DONGBEI SPECIAL STEEL GROUP BEIMAN SPECIAL STEEL CO., LTD.

GR01 Patent grant
GR01 Patent grant