CN106732304A - Modified form ammonium paratungstate decomposer - Google Patents

Modified form ammonium paratungstate decomposer Download PDF

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Publication number
CN106732304A
CN106732304A CN201611150681.5A CN201611150681A CN106732304A CN 106732304 A CN106732304 A CN 106732304A CN 201611150681 A CN201611150681 A CN 201611150681A CN 106732304 A CN106732304 A CN 106732304A
Authority
CN
China
Prior art keywords
cell body
exhaust
decomposer
dwell chamber
sealing top
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611150681.5A
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Chinese (zh)
Inventor
贺建昌
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
South-East Nonferrous Metal Ltd Hengyang Hunan
Original Assignee
South-East Nonferrous Metal Ltd Hengyang Hunan
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by South-East Nonferrous Metal Ltd Hengyang Hunan filed Critical South-East Nonferrous Metal Ltd Hengyang Hunan
Priority to CN201611150681.5A priority Critical patent/CN106732304A/en
Publication of CN106732304A publication Critical patent/CN106732304A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/74General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/86Catalytic processes
    • B01D53/8678Removing components of undefined structure
    • B01D53/8681Acidic components
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G41/00Compounds of tungsten

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Exhaust Gas Treatment By Means Of Catalyst (AREA)

Abstract

The invention discloses a kind of modified form ammonium paratungstate decomposer, including decomposing cell body, sealing top is set at the top of the decomposition cell body, space forms exhaust dwell chamber between the sealing top and the reactive tank for decomposing cell body bottom, interleaved is provided with some spoilers successively from the bottom to top in the exhaust dwell chamber, the surface of the spoiler is coated with exhaust gas catalyst, temperature detector is provided with the exhaust dwell chamber, pressure detector, the decomposer is set and the temperature detector in vitro, the control device of pressure detector connection, a blast pipe for being connected with the exhaust dwell chamber and being connected with waste gas recovering device is provided with the sealing top, the control valve being connected with the control device is provided with the blast pipe.The present invention will decompose and sealing top be set at the top of cell body, will react the waste gas for producing and carries out centralized recovery discharge, and realize full automatic working according to pressure and temperature, safe and reliable.

Description

Modified form ammonium paratungstate decomposer
Technical field
The present invention relates to ammonium paratungstate production apparatus field, more particularly to a kind of modified form ammonium paratungstate decomposer.
Background technology
Ammonium paratungstate (APT) is the important intermediate compound for producing tungsten powder, tungsten filament, tungsten-bast alloy and all tungsten materials, is also Large exporting of China.The one of step for producing ammonium paratungstate is exactly that wolframic acid is decomposed, and current wolframic acid decomposer is big Majority uses opened type structure, and waste gas pollutes environment from air discharge high in causing decomposable process.
The content of the invention
A kind of above-mentioned not enough and defect it is an object of the invention to be directed to prior art, there is provided modified form ammonium paratungstate point Solution groove, to solve the above problems.
Technical problem solved by the invention can be realized using following technical scheme:
Modified form ammonium paratungstate decomposer, including decompose cell body, it is characterised in that it is set at the top of the decomposition cell body Sealing top, space forms exhaust dwell chamber between the sealing top and the reactive tank for decomposing cell body bottom, and the waste gas stops Stay in chamber that interleaved is provided with some spoilers successively from the bottom to top, the surface of the spoiler is coated with exhaust gas catalyst, Temperature detector, pressure detector are provided with the exhaust dwell chamber, the decomposer sets examined with the temperature in vitro Survey device, the control device of pressure detector connection, be provided with sealing top one connected with the exhaust dwell chamber and with The blast pipe of waste gas recovering device connection, is provided with the control valve being connected with the control device on the blast pipe.
As a result of technical scheme as above, the present invention will decompose and sealing top be set at the top of cell body, will react The waste gas of generation carries out centralized recovery discharge, and realizes full automatic working according to pressure and temperature, safe and reliable.Furthermore, when Waste gas is first neutralized when exhaust dwell chamber stops with the exhaust gas catalyst reaction on spoiler, reduces acidity when waste gas is discharged.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing The accompanying drawing to be used needed for having technology description is briefly described, it should be apparent that, drawings in the following description are only this Some embodiments of invention, for those of ordinary skill in the art, on the premise of not paying creative work, can be with Other accompanying drawings are obtained according to these accompanying drawings.
Fig. 1 is the structural representation of an embodiment of the present invention.
Specific embodiment
In order that technological means, creation characteristic, reached purpose and effect that the present invention is realized are easy to understand, enter below One step illustrates the present invention.
Modified form ammonium paratungstate decomposer shown in Figure 1, including cell body 100 is decomposed, the top for decomposing cell body 100 sets Sealing top 110 is set to, space forms exhaust dwell chamber between sealing top 110 and the reactive tank 120 for decomposing the bottom of cell body 100 130.Interleaved is provided with some spoilers 131 successively from the bottom to top in exhaust dwell chamber 130, and the surface of spoiler 131 applies Exhaust gas catalyst is covered with, when waste gas is stopped in exhaust dwell chamber 130, in the exhaust gas catalyst reaction first and on spoiler 131 With acidity when reduction waste gas is discharged.Temperature detector 210, pressure detector 220 are provided with exhaust dwell chamber 130, point Solution cell body 100 sets outward the control device 300 being connected with temperature detector 210, pressure detector 220.Set on sealing top 110 A blast pipe 400 for being connected with exhaust dwell chamber 130 and being connected with waste gas recovering device 500 is equipped with, is provided with blast pipe 400 The control valve 410 being connected with control device 300.
Operation principle of the invention is as follows:
The waste gas that the reaction of reactive tank 120 is produced is detained in the exhaust dwell chamber 130 after rising, when temperature detector 210, After the air pressure and temperature that pressure detector 220 is detected in exhaust dwell chamber 130 reach predetermined parameter, control device 300 is controlled Control valve processed 410 is opened so that the waste gas in exhaust dwell chamber 130 is concentrated from blast pipe 400 and is expelled to waste gas recovery dress 500 are put to be recycled.
General principle of the invention and principal character and advantages of the present invention has been shown and described above.The technology of the industry Personnel it should be appreciated that the present invention is not limited to the above embodiments, simply explanation described in above-described embodiment and specification this The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appending claims and its Equivalent thereof.

Claims (1)

1. modified form ammonium paratungstate decomposer, including decomposition cell body, it is characterised in that be set at the top of the decomposition cell body close Bind portion, space forms exhaust dwell chamber, the exhaust dwell between the sealing top and the reactive tank for decomposing cell body bottom Interleaved is provided with some spoilers successively from the bottom to top in chamber, and the surface of the spoiler is coated with exhaust gas catalyst, Temperature detector, pressure detector are provided with the exhaust dwell chamber, the decomposer is set and the temperature detection in vitro Device, the control device of pressure detector connection, be provided with sealing top one connect with the exhaust dwell chamber and with give up The blast pipe of gas recovering device connection, is provided with the control valve being connected with the control device on the blast pipe.
CN201611150681.5A 2016-12-14 2016-12-14 Modified form ammonium paratungstate decomposer Pending CN106732304A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611150681.5A CN106732304A (en) 2016-12-14 2016-12-14 Modified form ammonium paratungstate decomposer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611150681.5A CN106732304A (en) 2016-12-14 2016-12-14 Modified form ammonium paratungstate decomposer

Publications (1)

Publication Number Publication Date
CN106732304A true CN106732304A (en) 2017-05-31

Family

ID=58887457

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611150681.5A Pending CN106732304A (en) 2016-12-14 2016-12-14 Modified form ammonium paratungstate decomposer

Country Status (1)

Country Link
CN (1) CN106732304A (en)

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6277954B2 (en) * 1999-09-14 2001-08-21 Kaneka Corporation Method of stripping for latex of vinyl chloride paste resin, stripping apparatus, and vinyl chloride paste resin latex having low concentration of residual monomer
CN1726163A (en) * 2002-12-12 2006-01-25 巴斯福股份公司 Method for the production of chlorine by means of gas phase oxidation of hydrogen chloride
CN101402055A (en) * 2008-10-30 2009-04-08 重庆大学 Ribbed catalyst structure
CN102941006A (en) * 2012-11-30 2013-02-27 吴江市万事达环保溶剂有限公司 Chemical waste gas treatment device
CN103016113A (en) * 2011-09-26 2013-04-03 江苏中盛建设集团有限公司 Catalytic-type automobile tail-air purification device
CN203123829U (en) * 2013-04-08 2013-08-14 郑州大学 Formaldehyde purifying device based on photochemical catalysis
CN204973857U (en) * 2015-04-13 2016-01-20 天津八通化工有限公司 Porcelain enamel reaction kettle
CN206508986U (en) * 2016-12-14 2017-09-22 衡阳市南东有色金属有限公司 Modified form ammonium paratungstate decomposer

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6277954B2 (en) * 1999-09-14 2001-08-21 Kaneka Corporation Method of stripping for latex of vinyl chloride paste resin, stripping apparatus, and vinyl chloride paste resin latex having low concentration of residual monomer
CN1726163A (en) * 2002-12-12 2006-01-25 巴斯福股份公司 Method for the production of chlorine by means of gas phase oxidation of hydrogen chloride
CN101402055A (en) * 2008-10-30 2009-04-08 重庆大学 Ribbed catalyst structure
CN103016113A (en) * 2011-09-26 2013-04-03 江苏中盛建设集团有限公司 Catalytic-type automobile tail-air purification device
CN102941006A (en) * 2012-11-30 2013-02-27 吴江市万事达环保溶剂有限公司 Chemical waste gas treatment device
CN203123829U (en) * 2013-04-08 2013-08-14 郑州大学 Formaldehyde purifying device based on photochemical catalysis
CN204973857U (en) * 2015-04-13 2016-01-20 天津八通化工有限公司 Porcelain enamel reaction kettle
CN206508986U (en) * 2016-12-14 2017-09-22 衡阳市南东有色金属有限公司 Modified form ammonium paratungstate decomposer

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Application publication date: 20170531

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