CN106729878A - solid air freshening agent and preparation method thereof - Google Patents

solid air freshening agent and preparation method thereof Download PDF

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Publication number
CN106729878A
CN106729878A CN201611198174.9A CN201611198174A CN106729878A CN 106729878 A CN106729878 A CN 106729878A CN 201611198174 A CN201611198174 A CN 201611198174A CN 106729878 A CN106729878 A CN 106729878A
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CN
China
Prior art keywords
weight portions
content
solid air
freshening agent
air freshening
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
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CN201611198174.9A
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Chinese (zh)
Inventor
郭常青
吴学军
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Anhui Leking Environment Technology Co Ltd
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Anhui Leking Environment Technology Co Ltd
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Priority to CN201611198174.9A priority Critical patent/CN106729878A/en
Publication of CN106729878A publication Critical patent/CN106729878A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • A61L9/013Deodorant compositions containing animal or plant extracts, or vegetable material
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L9/00Disinfection, sterilisation or deodorisation of air
    • A61L9/01Deodorant compositions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D49/00Separating dispersed particles from gases, air or vapours by other methods

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Epidemiology (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Botany (AREA)
  • Zoology (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The invention discloses a kind of solid air freshening agent, the solid air freshening agent is made up of agar powder, deionized water, ethanol, aromatic, active alundum (Al2O3) and ethylene glycol monobutyl ether;Wherein, relative to the agar powder of 100 weight portions, the content of deionized water is 100 500 weight portions, the content of ethanol is 50 150 weight portions, the content of aromatic is 10 20 weight portions, and the content of active alundum (Al2O3) is 15 weight portions, and the content of ethylene glycol monobutyl ether is 13 weight portions.The solid air freshening agent can be continued for indoor or closing workplace purification of air, pure and fresh.The manufacture craft of the solid air freshening agent is simple and raw material is simple and easy to get can realize quantifying production.

Description

Solid air freshening agent and preparation method thereof
Technical field
The present invention relates to solid air freshening agent, in particular it relates to a kind of solid air freshening agent and preparation method thereof.
Background technology
To the healthy most important of human body, the problem of environmental pollution for especially taking place frequently in recent years more allows people to IAQ Begin to focus on air quality.Indoor such as many public places cannot lead to more due to causing room air poor, flow of the people of divulging information The air circulation of itself is crossed to realize purification of air;And the accumulation floating of dust and smouldering so that people is in room for various smells It is interior to produce uncomfortable sensation, and easily produce courses of infection.Therefore, the control of indoor air quality is most important.Generally People can kill using with antivirus effect, simple, the easy-operating liquid spray solid air freshening agent with aromatic odor Go out the germ in air, improve peculiar smell.
At present, the complicated component various in style and most of of commercially available solid air freshening agent, depositing dust bactericidal effect is poor, also Peculiar smell is easily produced to cause that indoor groups of people feel is uncomfortable.And most solid air freshening agent is liquid spray, it is impossible to even It is continuous automatically to carry out air purification, it is necessary to artificial carrying out is sprayed and then play effect with fresh air;And some are conventional Indoor place or closed workplace such as compartment in need the lasting air purification that carries out, therefore provide a kind of empty The solid air freshening agent of gas good purification.
The content of the invention
It is an object of the invention to provide a kind of solid air freshening agent, the solid air freshening agent can be continued for room Interior or closing workplace purification of air, pure and fresh.The manufacture craft of the solid air freshening agent is simple and raw material is simple and easy to get Can realize quantifying production.
To achieve these goals, the invention provides a kind of solid air freshening agent, the solid air freshening agent is by fine jade Cosmetics, deionized water, ethanol, aromatic, active alundum (Al2O3) and ethylene glycol monobutyl ether composition;
Wherein, relative to the agar powder of 100 weight portions, the content of deionized water is 100-500 weight portions, the content of ethanol It is 50-150 weight portions, the content of aromatic is 10-20 weight portions, and the content of active alundum (Al2O3) is 1-5 weight portions, second two The content of alcohol monobutyl ether is 1-3 weight portions.
In the present invention, the aromatic for using can be selected in scope wide, but in order that obtained solid air is clear New agent low manufacture cost, environment-protecting asepsis, it is harmless to the human body and can guarantee that it is excellent using indoor interior air quality, preferably Ground, aromatic is prepared by following methods:Peppermint, dried orange peel, chrysanthemum, aloe are smashed to pieces, the mixture after then smashing to pieces Be added in ethanol heated, stir, filter, except color obtains the aromatic.
In the preparation process of above-mentioned aromatic, in order that obtain peppermint, dried orange peel, chrysanthemum, aloe can fully extract after smashing to pieces Take, be added to after smashing to pieces and heated, stirred and in order to improve extraction efficiency, it is preferable that the temperature of heating is 25-30 DEG C, plus The time of heat is 0.5-1.0h.
Being heated, stir, filter after, the filtrate for obtaining can remain the color of plant leaf blade, made in order to improve Aromatic degree of purity, the filtrate of gained is carried out except color treatment, it is preferable that as follows the step of except color:By activated carbon plus In entering the filtrate being filtrated to get, then system is sealed and activated carbon is taken out after standing 5-10h.
In the present invention, in order that obtaining obtained solid air freshening agent there is good dust-laying effect further to improve sky The effect of gas purification, with the addition of active alundum (Al2O3), in order to further improve active alundum (Al2O3) with other components Dispersion mixing is improving air purification effect, it is preferable that the particle diameter of active alundum (Al2O3) is 50-100nm.
Present invention also offers a kind of method of the preparation of above-mentioned solid air freshening agent, first agar powder is added to Heated in ionized water, stir and obtain agar dispersion liquid;Then, aromatic, alundum (Al2O3), ethylene glycol monobutyl ether are added It is stirred in ethanol and obtains mixed liquor;Finally, mixed liquor is added to agar when agar dispersion liquid is cooled to 30-35 DEG C It is stirred in dispersion liquid, mixed, natural cooling solidification obtains solid air freshening agent;
Wherein, relative to the agar powder of 100 weight portions, the content of deionized water is 100-500 weight portions, the content of ethanol It is 50-150 weight portions, the content of aromatic is 10-20 weight portions, and the content of active alundum (Al2O3) is 1-5 weight portions, second two The content of alcohol monobutyl ether is 1-3 weight portions.
In above-mentioned preparation method, in order to improve the dispersion effect of each component and then improve obtained solid air freshening agent Depositing dust, the effect of sterilizing and purifying air, mixing is stirred to each component, it is preferable that the rotating speed of stirring be 2000- 3000rpm, the time of stirring is 1.0-1.5h.
By such scheme, the present invention is added in ethanol by by aromatic, alundum (Al2O3), ethylene glycol monobutyl ether Row stirring obtains mixed liquor, and finally mixed liquor is added in agar dispersion liquid carries out scattered adsorption, finally treats agar solution nature Solid air freshening agent is obtained after cooled and solidified.The aluminum oxide nanoparticles of addition can have drop well to air Dirt effect, improves the air purification effect of solid air freshening agent;And aromatic can then volatilize and play fresh air, removal The effect of peculiar smell.
Other features and advantages of the present invention will be described in detail in subsequent specific embodiment part.
Specific embodiment
Specific embodiment of the invention is described in detail below.It should be appreciated that described herein specific Implementation method is merely to illustrate and explain the present invention, and is not intended to limit the invention.
Embodiment 1
First the agar powder of 100kg is added in the deionized water of 100kg and is heated, stirred and obtain agar dispersion liquid;
Then, the ethylene glycol monobutyl ether of the aromatic of 10kg, the alundum (Al2O3) (50nm) of 1kg, 1kg is added to 50kg Ethanol in, selection rotating speed obtain mixed liquor for 2000rpm is stirred 1.5h;
Finally, stirred in mixed liquor being added to agar dispersion liquid when the agar dispersion liquid is cooled to 30-35 DEG C Mix, mix, natural cooling solidification obtains the solid air freshening agent, is denoted as A1;Wherein, aromatic used is by following sides Method is prepared:First peppermint, dried orange peel, chrysanthemum, aloe are smashed to pieces, the mixture after then smashing to pieces is added in ethanol at 25 DEG C Middle heating 1.0h, is followed by stirring for, filters, then by activated carbon be added in the filtrate through being filtrated to get and closed system stand 5h remove Color obtains the aromatic.
Embodiment 2
First the agar powder of 100kg is added in the deionized water of 300kg and is heated, stirred and obtain agar dispersion liquid;
Then, the ethylene glycol monobutyl ether of the aromatic of 15kg, the alundum (Al2O3) (80nm) of 3kg, 2kg is added to In the ethanol of 100kg, selection rotating speed obtains mixed liquor for 2500rpm is stirred 1.2h;
Be stirred during mixed liquor finally, to be added to agar dispersion liquid when the agar dispersion liquid is cooled to 35 DEG C, Mixing, natural cooling solidification obtains the solid air freshening agent, is denoted as A2;Wherein, aromatic used is by following methods It is prepared:First peppermint, dried orange peel, chrysanthemum, aloe are smashed to pieces, the mixture after then smashing to pieces is added in ethanol in 28 DEG C 0.8h is heated, is followed by stirring for, filtered, then activated carbon is added in the filtrate through being filtrated to get simultaneously closed system and stand 8h except color Obtain the aromatic.
Embodiment 3
First the agar powder of 100kg is added in the deionized water of 500kg and is heated, stirred and obtain agar dispersion liquid;
Then, the ethylene glycol monobutyl ether of the aromatic of 20kg, the alundum (Al2O3) (100nm) of 5kg, 3kg is added to In the ethanol of 150kg, selection rotating speed obtains mixed liquor for 3000rpm is stirred 1.0h;
Be stirred during mixed liquor finally, to be added to agar dispersion liquid when the agar dispersion liquid is cooled to 35 DEG C, Mixing, natural cooling solidification obtains solid air freshening agent, is denoted as A3;Wherein, aromatic used is prepared by following methods And obtain:First peppermint, dried orange peel, chrysanthemum, aloe are smashed to pieces, the mixture after then smashing to pieces is heated in being added to ethanol in 30 DEG C 1.0h, is followed by stirring for, filters, then by activated carbon be added in the filtrate through being filtrated to get and closed system stand 10h except color is obtained To the aromatic.
Comparative example 1
Solid air freshening agent is obtained according to the method for embodiment 1 and is denoted as B1, the difference is that not adding active alundum (Al2O3).
Comparative example 2
Solid air freshening agent is obtained according to the method for embodiment 1 and is denoted as B2, the difference is that not adding ethylene glycol monobutyl ether.
Comparative example 3
Solid air freshening agent is obtained according to the method for embodiment 1 and is denoted as B3, the difference is that not adding aromatic.
In the present invention, solid air freshening agent obtained by embodiment 1-3 effectively indoor air can be played purification, Pure and fresh effect;Rear free from extraneous odour with fresh air is used in addition, and manufacture craft is simple, raw material is easy to get can realize batch metaplasia Produce.The aluminum oxide nanoparticles that the using effect of solid air freshening agent obtained in comparative example 1-3 indicates addition can There is good dust-laying effect to air, the air purification effect of solid air freshening agent is improve;And aromatic can then be waved Initiate to fresh air, go the effect that eliminates the unusual smell.
The preferred embodiment of the present invention described in detail above, but, the present invention is not limited in above-mentioned implementation method Detail, in range of the technology design of the invention, various simple variants can be carried out to technical scheme, this A little simple variants belong to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned specific embodiment, in not lance In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to it is various can The combination of energy is no longer separately illustrated.
Additionally, can also be combined between a variety of implementation methods of the invention, as long as it is without prejudice to originally The thought of invention, it should equally be considered as content disclosed in this invention.

Claims (8)

1. a kind of solid air freshening agent, it is characterised in that the solid air freshening agent by agar powder, deionized water, ethanol, Aromatic, active alundum (Al2O3) and ethylene glycol monobutyl ether composition;
Wherein, relative to the agar powder of 100 weight portions, the content of the deionized water is 100-500 weight portions, the ethanol Content is 50-150 weight portions, and the content of the aromatic is 10-20 weight portions, and the content of the active alundum (Al2O3) is 1- 5 weight portions, the content of the ethylene glycol monobutyl ether is 1-3 weight portions.
2. solid air freshening agent according to claim 1, wherein, the aromatic is prepared by following methods: Peppermint, dried orange peel, chrysanthemum, aloe are smashed to pieces, the mixture after then smashing to pieces heated in being added to ethanol, stirred, filtered, Except color obtains the aromatic.
3. solid air freshening agent according to claim 2, wherein, the temperature of the heating is 25-30 DEG C, heating when Between be 0.5-1.0h.
4. the solid air freshening agent according to Claims 2 or 3, wherein, it is described except color the step of it is as follows:By activated carbon plus In entering the filtrate being filtrated to get, then system is sealed and activated carbon is taken out after standing 5-10h.
5. solid air freshening agent according to claim 4, wherein, the particle diameter of the alundum (Al2O3) is 50-100nm.
6. the preparation method of the solid air freshening agent in a kind of 1-5 such as claim as described in any one, it is characterised in that first Agar powder is added in deionized water and is heated, stirred and obtain agar dispersion liquid;Then, by aromatic, alundum (Al2O3), Ethylene glycol monobutyl ether is added in ethanol to be stirred and obtains mixed liquor;Finally, treat that the agar dispersion liquid is cooled to 30-35 DEG C When the mixed liquor is added in the agar dispersion liquid is stirred, mixes, natural cooling solidification obtains the solid Air freshener;
Wherein, relative to the agar powder of 100 weight portions, the content of the deionized water is 100-500 weight portions, the ethanol Content is 50-150 weight portions, and the content of the aromatic is 10-20 weight portions, and the content of the active alundum (Al2O3) is 1- 5 weight portions, the content of the ethylene glycol monobutyl ether is 1-3 weight portions.
7. preparation method according to claim 6, wherein, the rotating speed of the stirring is 2000-3000rpm.
8. preparation method according to claim 7, wherein, the time of the stirring is 1.0-1.5h.
CN201611198174.9A 2016-12-22 2016-12-22 solid air freshening agent and preparation method thereof Pending CN106729878A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611198174.9A CN106729878A (en) 2016-12-22 2016-12-22 solid air freshening agent and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201611198174.9A CN106729878A (en) 2016-12-22 2016-12-22 solid air freshening agent and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106729878A true CN106729878A (en) 2017-05-31

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107519519A (en) * 2017-09-15 2017-12-29 海门市琴键农产品有限公司 A kind of solid air freshening agent

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102743777A (en) * 2011-04-19 2012-10-24 南通宏利达针织有限公司 Refrigerator smell removal agent and preparation method thereof
CN103349789A (en) * 2013-06-18 2013-10-16 上海市静安区教育学院附属学校 Solid air freshening agent and its preparation method
CN104383574A (en) * 2014-10-22 2015-03-04 青岛克立克信息技术有限公司 Long-acting refreshing air purifying agent

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102743777A (en) * 2011-04-19 2012-10-24 南通宏利达针织有限公司 Refrigerator smell removal agent and preparation method thereof
CN103349789A (en) * 2013-06-18 2013-10-16 上海市静安区教育学院附属学校 Solid air freshening agent and its preparation method
CN104383574A (en) * 2014-10-22 2015-03-04 青岛克立克信息技术有限公司 Long-acting refreshing air purifying agent

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107519519A (en) * 2017-09-15 2017-12-29 海门市琴键农产品有限公司 A kind of solid air freshening agent

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Application publication date: 20170531