CN106723052A - A kind of preparation method of the linseed oil nanoemulsions rich in ω 3 - Google Patents
A kind of preparation method of the linseed oil nanoemulsions rich in ω 3 Download PDFInfo
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- CN106723052A CN106723052A CN201611235189.8A CN201611235189A CN106723052A CN 106723052 A CN106723052 A CN 106723052A CN 201611235189 A CN201611235189 A CN 201611235189A CN 106723052 A CN106723052 A CN 106723052A
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- linseed oil
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- nanoemulsions
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- 239000000944 linseed oil Substances 0.000 title claims abstract description 47
- 235000021388 linseed oil Nutrition 0.000 title claims abstract description 47
- 239000007908 nanoemulsion Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000003921 oil Substances 0.000 claims abstract description 34
- 235000019198 oils Nutrition 0.000 claims abstract description 34
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 11
- 239000000839 emulsion Substances 0.000 claims abstract description 7
- 235000013336 milk Nutrition 0.000 claims description 11
- 239000008267 milk Substances 0.000 claims description 11
- 210000004080 milk Anatomy 0.000 claims description 11
- 229920000223 polyglycerol Polymers 0.000 claims description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 4
- 238000000199 molecular distillation Methods 0.000 claims description 3
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 2
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims description 2
- 239000002202 Polyethylene glycol Substances 0.000 claims description 2
- 229930006000 Sucrose Natural products 0.000 claims description 2
- 235000011187 glycerol Nutrition 0.000 claims description 2
- 229920001223 polyethylene glycol Polymers 0.000 claims description 2
- 235000010958 polyglycerol polyricinoleate Nutrition 0.000 claims description 2
- 239000003996 polyglycerol polyricinoleate Substances 0.000 claims description 2
- 229920000136 polysorbate Polymers 0.000 claims description 2
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 2
- 229940083466 soybean lecithin Drugs 0.000 claims description 2
- 239000005720 sucrose Substances 0.000 claims description 2
- -1 sucrose ester Chemical class 0.000 claims description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims 2
- 229940075507 glyceryl monostearate Drugs 0.000 claims 1
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 claims 1
- 238000003754 machining Methods 0.000 abstract description 4
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 235000004431 Linum usitatissimum Nutrition 0.000 description 37
- 241000208202 Linaceae Species 0.000 description 33
- 235000004426 flaxseed Nutrition 0.000 description 9
- 240000006240 Linum usitatissimum Species 0.000 description 8
- 239000000835 fiber Substances 0.000 description 6
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 4
- 238000013019 agitation Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000012467 final product Substances 0.000 description 3
- 239000008236 heating water Substances 0.000 description 3
- 230000001954 sterilising effect Effects 0.000 description 3
- 239000003643 water by type Substances 0.000 description 3
- ULDSUTWYOBXEBV-UHFFFAOYSA-N 5-phenyl-1,3-oxazolidine-2-thione Chemical compound O1C(=S)NCC1C1=CC=CC=C1 ULDSUTWYOBXEBV-UHFFFAOYSA-N 0.000 description 2
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 229960004488 linolenic acid Drugs 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000002689 soil Substances 0.000 description 2
- MJYQFWSXKFLTAY-OVEQLNGDSA-N (2r,3r)-2,3-bis[(4-hydroxy-3-methoxyphenyl)methyl]butane-1,4-diol;(2r,3r,4s,5s,6r)-6-(hydroxymethyl)oxane-2,3,4,5-tetrol Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O.C1=C(O)C(OC)=CC(C[C@@H](CO)[C@H](CO)CC=2C=C(OC)C(O)=CC=2)=C1 MJYQFWSXKFLTAY-OVEQLNGDSA-N 0.000 description 1
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- 240000000491 Corchorus aestuans Species 0.000 description 1
- 235000011777 Corchorus aestuans Nutrition 0.000 description 1
- 235000010862 Corchorus capsularis Nutrition 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000208204 Linum Species 0.000 description 1
- 244000236527 Linum perenne Species 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- OGBUMNBNEWYMNJ-UHFFFAOYSA-N batilol Chemical class CCCCCCCCCCCCCCCCCCOCC(O)CO OGBUMNBNEWYMNJ-UHFFFAOYSA-N 0.000 description 1
- 235000005370 blue flax Nutrition 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 210000004602 germ cell Anatomy 0.000 description 1
- 238000005286 illumination Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 239000008347 soybean phospholipid Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/1528—Fatty acids; Mono- or diglycerides; Petroleum jelly; Paraffine; Phospholipids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biophysics (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Edible Oils And Fats (AREA)
Abstract
The present invention discloses a kind of preparation method of the linseed oil nanoemulsions rich in ω 3, comprises the following steps：1）Linseed oil and emulsifying agent are weighed respectively, both quality respectively account for 1% the 20% of stoste gross mass, linseed oil and emulsifying agent stirs at 25 40 DEG C and is allowed to well mixed, formation oil phase；2）Water soluble emulsifier is added to the water, stirs to form water phase, the amount of water soluble emulsifier accounts for the % of 0.1 % 10 of stoste gross mass, the quality of water accounts for 50% the 90% of stoste gross mass；3）The water synthermal with oil phase is mutually slowly added into oil phase, after stirring, is added in setting pressure as the high pressure homogenizer of the MPa of 30 MPa 80 and is circulated homogeneous 1 10 times；4）The emulsion that will be obtained is cooled to room temperature, you can must be rich in the linseed oil nanoemulsions of ω 3.The preparation method of the linseed oil nanoemulsions rich in ω 3 of the invention is easy to operate, high in machining efficiency.
Description
Technical field
The present invention relates to a kind of preparation method of the linseed oil nanoemulsions rich in ω -3.
Background technology
Linseed oil is produced by linseed and formed, and linseed is the seed of flax, belongs to flax family (Linaceae), and have another name called flax, because it is former
Originate in East India area, Han dynasty Zhang Qian send as an envoy to the Western Regions when, flax is taken back into China through the Silk Road, mainly plant in old times Xiongnu
One band, is the area of " Notherna barbarin tribes in ancient China " aggregation, therefore and gains the name.Linseed belongs to traditional oil crops in China, and flax is divided into oil
With flax, with flax, oil seed flax seed mainly originates from Changbai Mountain song-Nen plain and black in China for Oil and Fibre Flax and fiber
Longjiang area, the Inner Mongol, from Liupan Mountain of Ningxia area, Zhangjiakou Ba Shang Zhangbei County；Inner Mongolian grassland distribution is most, and northeast is a small amount of
Plantation etc..It is " weather that cools, plentiful soil, sufficient as oil seed flax although flax possesses anti-barren habit
Three conditions of illumination " must be indispensable.Plantation is cultivated within thousand by locals to find：The Northwest's day and night temperature is balanced, fertile
The natural ecological environments such as the sunlight of soil and abundance are best suitable for the plantation of the special oil crops such as flax, and the category whole nation is without industry
Contaminated zone, northwest ground Xinjiang, Gansu, up to more than 56%, wherein alpha-linolenic acid contains the linseed oil oil content that is produced from West Inner Mongolia area
Amount is even more and is far above other growing areas, and linseed oil activity is also to top the list.The ground such as Xinjiang, Gansu, Ningxia, Inner Mongol, Shanxi, it is local
Also known as siritch, mainly due to being that ancient times Han dynasty Zhang Qian sends as an envoy to the incoming China in Middle East.Cold pressed flax seed oil contains abundant
Alpha-linolenic acid, be the linolenic most effectual way of supplement.Linseed oil is the oils that linseed is squeezed, and linseed is also known as recklessly
Numb seed, is annual or herbaceos perennial flax the seed of flax family (Linaceae), linum.Flax is most ancient in the world
One of fibre crops, kind is more, but is broadly divided into 3 classes:Oil seed flax, fiber flax and oil fibre mean flax,
Its seed can extract oil, and as one of big oil crops in the world ten, its yield accounts for the 7th.Oil seed flax is mainly originated in and added
Put on airs, China, Argentina, the U.S..China is the flax taken back when the Western Regions are sent as an envoy to by Han dynasty special envoy Zhang Qian in B.C. 2nd century
Seed, in Xinjiang, Gansu, the ground such as Ningxia, Heilungkiang, Jilin, the Inner Mongol, Shanxi, northeast starts plantation, and initial linseed is main
Make medicinal, just extracted oil [3] with its seed until 16th century, be nowadays one of main economic crops in China, be also China of China
North, northwest, the main oil crops of Northeast Heavy Frigid Region of China plantation.China's northeast latitude is high close with Canadian latitude, produces Asia
Numb seed is best suitable for industrial production linseed oil, inedibility.
The mankind cultivate and using flax history can trace back to more than 8000 years before.Utilization of the China to flax has more than 2000
The history in year, is referred to as " flax ", " Ya fiber crops ", " tick flax " etc. in history, oil seed flax is also called jute by indivedual areas,
" flax " appellation is then used till today always.Record of the ancient Chinese on " flax ", what is mainly said is oil seed flax, and China is fine
The cultivation for tieing up flax started from for 20 beginnings of the century.Opinions vary for the Origin on flax, have originate from the Near East, Mediterranean it
Say have and originate in saying for the ground such as middle Asia, the Near East, have and originate in saying for western part of Asia and W. Asia, also originate in
Asia says,《German Economy flora》Then explicitly point out original Asia.Chinese scholar advocates many archeologies of world flax, recognizes
Germline is cultivated for China Flax to be developed by wild species, China is one of flax original producton location.
The preparation method inconvenient operation of current existing linseed oil nanoemulsions, processing efficiency is not high.
The content of the invention
In view of this, it is an object of the present invention to provide a kind of easy to operate, high in machining efficiency linseed oil rich in ω -3
The preparation method of nanoemulsions.
In order to solve the above-mentioned technical problem, the technical scheme is that：
A kind of preparation method of the linseed oil nanoemulsions rich in ω -3, comprises the following steps：
1）Linseed oil and emulsifying agent are weighed respectively, and both quality respectively account for the 1% -20% of stoste gross mass, by linseed oil
Stirred at 25-40 DEG C with emulsifying agent and be allowed to well mixed, form oil phase；
2）Water soluble emulsifier is added to the water, stirs to form water phase, the amount of water soluble emulsifier accounts for stoste gross mass
0.1 % -10 %, the quality of water accounts for the 50% -90% of stoste gross mass；
3）The water synthermal with oil phase is mutually slowly added into oil phase, after stirring, is added to and is set pressure as 30 MPa-
Homogeneous is circulated in the high pressure homogenizer of 80 MPa 1-10 times；
4）The emulsion that will be obtained is cooled to room temperature, you can must be rich in the linseed oil nanoemulsions of ω -3.
Preferably, described emulsifying agent includes primary emulsion and assistant for emulsifying agent, primary emulsion includes polyglycereol list oleic acid
In ester, polyglycereol monolaurate, polyglycerol monostearate, molecular distillation monoglyceride, soybean lecithin, sucrose ester and tween
One or more；Assistant for emulsifying agent includes the one kind or several in sapn, polyglycerol polyricinoleate, propane diols, glycerine and polyethylene glycol
Kind.
Preferably, the processing condition of the pressure homogenizer can regulate and control.
Preferably, the described linseed oil nanoemulsions rich in ω -3 are added in milk.
The technology of the present invention effect major embodiment is in the following areas：Linseed rich in ω -3 can be obtained using above method
Oil nano emulsions, it is easy to operate, it is high in machining efficiency.
Specific embodiment
Embodiment 1
A kind of preparation method of the linseed oil nanoemulsions rich in ω -3, comprises the following steps：
1）Prepare oil phase：Weigh 10 g linseed oil, the polyglycerol monooleates of 8 g ten, 2 g sorbester p17s, under 30 DEG C of water-baths,
Stirred with machine mixer with the rotating speed of 400 r/min；
2）Prepare water phase：80 g deionized waters, and heating water bath are weighed to 30 DEG C；
3）Prepare nanoemulsions：Deionized water is poured slowly into oil phase, after stirring, high pressure homogenizer pressure 60 is set to
MPa, mixed liquor is circulated 8 times by high pressure homogenizer, and the linseed oil nanoemulsions rich in ω -3 are obtained after cooling；
4）Prepare the linseed oil milk rich in ω -3：Linseed oil nanoemulsions and 230 of 20 g rich in ω -3 are weighed respectively
G milk, mechanical agitation is uniform, and 18 MPa descended high pressure homogenizer to circulate 2 times, and the linseed oil ox rich in ω -3 is obtained final product after sterilizing
Milk.
Embodiment 2
A kind of preparation method of the linseed oil nanoemulsions rich in ω -3, comprises the following steps：
1）Prepare oil phase：Weigh 10 g linseed oil, the polyglycerol monooleates of 6 g ten, 2 g polysorbas20s, 1 g sorbester p17s, 30
Under DEG C water-bath, stirred with machine mixer with the rotating speed of 400 r/min；
2）Prepare water phase：Weigh 2 g molecular distillation monoglycerides, 79 g deionized waters, heating water bath is to 30 DEG C and stirs；
3）Prepare nanoemulsions：Water is mutually poured slowly into oil phase, after stirring, high pressure homogenizer pressure 60 MPa is set to,
Mixed liquor is circulated 8 times by high pressure homogenizer, the linseed oil nanoemulsions rich in ω -3 are obtained after cooling；
4）Prepare the linseed oil milk rich in ω -3：Linseed oil nanoemulsions and 230 of 20 g rich in ω -3 are weighed respectively
G milk, mechanical agitation is uniform, and 18 MPa descended high pressure homogenizer to circulate 2 times, and the linseed oil ox rich in ω -3 is obtained final product after sterilizing
Milk.
Embodiment 3
A kind of preparation method of the linseed oil nanoemulsions rich in ω -3, comprises the following steps：
1) oil phase is prepared:10 g linseed oil are weighed, the polyglycerol monooleates of 6 g ten, 2.5 g powdered soybean phospholipids, 2.5 g tell
Temperature 80, under 30 DEG C of water-baths, is stirred with the rotating speed of 400 r/min with machine mixer；
2) water phase is prepared:79 g deionized waters, and heating water bath are weighed to 30 DEG C；
3) nanoemulsions are prepared:Deionized water is poured slowly into oil phase, after stirring, high pressure homogenizer pressure 60 is set to
MPa, mixed liquor is circulated 8 times by high pressure homogenizer, and the linseed oil nanoemulsions rich in ω -3 are obtained after cooling；
4) the linseed oil milk rich in ω -3 is prepared:Linseed oil nanoemulsions and 230 of 20 g rich in ω -3 are weighed respectively
G milk, mechanical agitation is uniform, and 18 MPa descended high pressure homogenizer to circulate 2 times, and the linseed oil ox rich in ω -3 is obtained final product after sterilizing
Milk.
The technology of the present invention effect major embodiment is in the following areas：Linseed rich in ω -3 can be obtained using above method
Oil nano emulsions, it is easy to operate, it is high in machining efficiency.
Certainly, it is more than representative instance of the invention, in addition, the present invention can also have other various specific implementations
The technical scheme that mode, all use equivalents or equivalent transformation are formed, all falls within the scope of protection of present invention.
Claims (4)
1. a kind of preparation method of the linseed oil nanoemulsions rich in ω -3, it is characterised in that：Comprise the following steps：
1）Linseed oil and emulsifying agent are weighed respectively, and both quality respectively account for the 1% -20% of stoste gross mass, by linseed oil
Stirred at 25-40 DEG C with emulsifying agent and be allowed to well mixed, form oil phase；
2）Water soluble emulsifier is added to the water, stirs to form water phase, the amount of water soluble emulsifier accounts for stoste gross mass
0.1 % -10 %, the quality of water accounts for the 50% -90% of stoste gross mass；
3）The water synthermal with oil phase is mutually slowly added into oil phase, after stirring, is added to and is set pressure as 30 MPa-
Homogeneous is circulated in the high pressure homogenizer of 80 MPa 1-10 times；
4）The emulsion that will be obtained is cooled to room temperature, you can must be rich in the linseed oil nanoemulsions of ω -3.
2. the preparation method of the linseed oil nanoemulsions rich in ω -3 according to claim 1, it is characterised in that：It is described
Emulsifying agent include primary emulsion and assistant for emulsifying agent, primary emulsion includes polyglycerol monooleate, polyglycereol monolaurate, poly-
One or more in glyceryl monostearate, molecular distillation monoglyceride, soybean lecithin, sucrose ester and tween；Assistant for emulsifying agent bag
Include one or more in sapn, polyglycerol polyricinoleate, propane diols, glycerine and polyethylene glycol.
3. the preparation method of the linseed oil nanoemulsions rich in ω -3 according to claim 1, it is characterised in that：It is described
Pressing the processing condition of homogenizer can regulate and control.
4. the preparation method of the linseed oil nanoemulsions rich in ω -3 according to claim 1, it is characterised in that：It is described
The linseed oil nanoemulsions rich in ω -3 be added in milk.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611235189.8A CN106723052A (en) | 2016-12-28 | 2016-12-28 | A kind of preparation method of the linseed oil nanoemulsions rich in ω 3 |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611235189.8A CN106723052A (en) | 2016-12-28 | 2016-12-28 | A kind of preparation method of the linseed oil nanoemulsions rich in ω 3 |
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| Publication Number | Publication Date |
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| CN106723052A true CN106723052A (en) | 2017-05-31 |
Family
ID=58923743
Family Applications (1)
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|---|---|---|---|
| CN201611235189.8A Pending CN106723052A (en) | 2016-12-28 | 2016-12-28 | A kind of preparation method of the linseed oil nanoemulsions rich in ω 3 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108553419A (en) * | 2018-05-24 | 2018-09-21 | 安阳工学院 | A kind of Alpha-ethyl linolenate microemulsion and preparation method thereof |
| CN113667140A (en) * | 2021-09-06 | 2021-11-19 | 陕西科技大学 | Degradable high-molecular emulsion, preparation method thereof and application thereof in preparation of composite paper |
| CN115251363A (en) * | 2022-08-04 | 2022-11-01 | 蕴能(大连)生物科技有限公司 | Nano emulsion taking milk phospholipid as emulsifier and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1915045A (en) * | 2006-09-07 | 2007-02-21 | 广州风行牛奶有限公司 | Method for adding polyunsaturated fatty acid in animal milk |
| CN101843336A (en) * | 2010-04-22 | 2010-09-29 | 王京南 | Linseed oil fat emulsion oral solution, beverage and manufacturing method thereof |
-
2016
- 2016-12-28 CN CN201611235189.8A patent/CN106723052A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1915045A (en) * | 2006-09-07 | 2007-02-21 | 广州风行牛奶有限公司 | Method for adding polyunsaturated fatty acid in animal milk |
| CN101843336A (en) * | 2010-04-22 | 2010-09-29 | 王京南 | Linseed oil fat emulsion oral solution, beverage and manufacturing method thereof |
Non-Patent Citations (5)
| Title |
|---|
| 姜兆华: "《应用表面化学》", 28 February 2009, 哈尔滨工业大学出版社 * |
| 孟胜男: "《药剂学》", 30 September 2011, 上海科学技术出版社 * |
| 武杰: "《新型果蔬食品加工工艺与配方》", 31 January 2001, 科学技术文献出版社 * |
| 阎芳: "《基础化学》", 31 August 2014, 山东人民出版社 * |
| 黄文: "《食品添加剂》", 30 November 2006, 中国计量出版社 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108553419A (en) * | 2018-05-24 | 2018-09-21 | 安阳工学院 | A kind of Alpha-ethyl linolenate microemulsion and preparation method thereof |
| CN113667140A (en) * | 2021-09-06 | 2021-11-19 | 陕西科技大学 | Degradable high-molecular emulsion, preparation method thereof and application thereof in preparation of composite paper |
| CN113667140B (en) * | 2021-09-06 | 2022-11-15 | 陕西科技大学 | Degradable high-molecular emulsion, preparation method thereof and application thereof in preparation of composite paper |
| CN115251363A (en) * | 2022-08-04 | 2022-11-01 | 蕴能(大连)生物科技有限公司 | Nano emulsion taking milk phospholipid as emulsifier and preparation method and application thereof |
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