CN106720242A - A kind of antistaling agent of red heart dragon fruit and preparation method thereof - Google Patents
A kind of antistaling agent of red heart dragon fruit and preparation method thereof Download PDFInfo
- Publication number
- CN106720242A CN106720242A CN201611044667.7A CN201611044667A CN106720242A CN 106720242 A CN106720242 A CN 106720242A CN 201611044667 A CN201611044667 A CN 201611044667A CN 106720242 A CN106720242 A CN 106720242A
- Authority
- CN
- China
- Prior art keywords
- extract
- extracting
- extract solution
- solution
- volume
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/14—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
- A23B7/153—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/14—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
- A23B7/153—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
- A23B7/154—Organic compounds; Microorganisms; Enzymes
Abstract
The present invention relates to technical field of preservation of fresh, more particularly to a kind of antistaling agent of red heart dragon fruit and preparation method thereof, antistaling agent of the invention, including the fresh-keeping composition of Chinese medicine and gel component, invention is using the flavones extracted in traditional Chinese medicine ingredients, volatile oil isoreactivity material carries out fresh-keeping to dragon fruit, simultaneously, also traditional Chinese medicine ingredients are mixed with gel component, it is fabricated to antistaling agent, in use, the antistaling agent also uses the film forming characteristics of gel component, air is come with the isolation of flue fruits, play bacterium in air-isolation, reduce the volatilization of dragon fruit internal moisture, can effectively play fresh-keeping, ensure the effect of the moisture of dragon fruit, and the fresh-keeping composition that the technical program is used is nontoxic natural traditional Chinese medicine, it is a kind of antistaling agent of environmental protection.
Description
【Technical field】
The present invention relates to technical field of preservation of fresh, more particularly to a kind of antistaling agent of red heart dragon fruit and preparation method thereof.
【Background technology】
Dragon fruit is tropical plants, and light shade tolerant, heat-resisting drought-enduring, happiness fertilizer are resistance to lean, and its stem is attached on rock can also be grown, and be planted
Thing strain wind resistance power is extremely strong, because dragon fruit is tasty, contains the rare vegetable albumin of general plant and anthocyanidin, Yi Jifeng
Rich vitamin and water-soluble dietary fiber, has turned into a kind of novel, excellent green health care food at present, but dragon fruit by
Larger in fruit, solid content is higher, at normal temperatures, places 1d pulp and begins to soften, and easily rots, conventional guarantor
Chemical composition content is more in fresh dose, often causes medicament residue, is unfavorable for food hygiene, and cryopreservation is relatively costly, and
And transport inconvenience, therefore, need to solve following problem in the preservation process of dragon fruit：(1) a kind of safe guarantor is used
Fresh dose, the fresh-keeping effect of dragon fruit is not interfered with, meanwhile, do not result in chemical composition residual yet；(2) can at normal temperatures to flue
Fruit is stored for a long time.
【The content of the invention】
In view of the above, it is necessary to provide a kind of antistaling agent of red heart dragon fruit and preparation method thereof, safety, nothing can be reached
Residual, while, moreover it is possible to the purpose of long-term storage is carried out to dragon fruit at normal temperatures.
To reach above-mentioned purpose, the technical solution adopted in the present invention is：
A kind of antistaling agent of red heart dragon fruit, including the fresh-keeping composition of Chinese medicine and gel component, the fresh-keeping composition of Chinese medicine with
Gel component volume ratio is 4-5:1, the fresh-keeping composition of Chinese medicine include percent by volume for 50%-60% red sage root extract and
Percent by volume is the A compositions of 40%-50%, and the A compositions are the following material composition of 0-20% by percent by volume：Radix Glycyrrhizae
Extract solution, galingal extract solution, fruit of a cubeb litsea tree extract solution, pine needle extract, wormwood extract solution, pitaya peel extract solution, lotus leaf are extracted
Liquid and pomelo peel extract solution；The gel component includes shitosan, the sodium alginate and B of 20wt-30wt% of 20wt-30wt%
Composition, the B component is the following material composition of 0-20wt% by percentage by weight：Carragheen, xanthans, konjac glucomannan and transparent
Matter acid.
Further, the fresh-keeping composition of the Chinese medicine includes at least 5 kinds A compositions.
Further, the gel component includes at least 2 kinds B components.
Further, the extracting method of the red sage root extract is：The dry product red sage root is by crushing, sieving, extracting, being concentrated to give
To extract solution；The screen sizes of the sieving process are the mesh of 40 mesh -50；The extracting solution that the leaching process is used is volume hundred
Fraction is 95% ethanol solution, and extraction time is 50min-80min, and extracting solution addition is 2 times -3 of crushed material volume
Times, extracting times are 2 times -4 times, are filtered after extraction, and merging filtrate obtains stoste；The concentration process is dense using water bath with thermostatic control
Contracting, bath temperature is 90 DEG C -100 DEG C, and concentration is stopped when being concentrated to the 1/5-1/3 that the volume of concentrate is stoste, and concentrate is institute
State red sage root extract.
Further, the licorice extract, pine needle extract, wormwood extract solution, pitaya peel extract solution, lotus leaf are extracted
Liquid, the extracting method of fruit of a cubeb litsea tree extract solution are to be ground Radix Glycyrrhizae, pine needle, wormwood, pitaya peel, lotus leaf, fruit of a cubeb litsea tree leaf respectively
Grind, extract, being filtrated to get extract solution, the extracting solution that the extraction is used is distilled water, and extracting solution addition is abrasive material
2 times -3 times of volume, the time of extraction is 48h-50h.
Further, the galingal extract solution, the extracting method of pomelo peel extract solution are by dry product galingal, dry product pomelo peel
Crushed respectively, sieved, being extracted, being distilled, condensed and obtain extract solution, the screen sizes of the sieving process are the mesh of 50 mesh -60,
The extracting solution that the leaching process is used is the NaOH that mass concentration is 5%, and extraction time is 30h-34h, and extracting solution adds
Dosage is 2-3 times of crushed material volume, and extracting times are 2 times -4 times, are filtered after extraction, and merging filtrate obtains stoste；The steaming
Evaporate process to be distilled using water bath with thermostatic control, distillation condensate liquid stops distillation when being the 1/3-1/2 of stoste volume, condensate liquid is described good
Ginger extract solution, pomelo peel extract solution.
Further, this programme additionally provides a kind of preparation method of red heart flue fresh-keeping agent of fruits, and methods described is included such as
Lower step：
(1) measure red sage root extract by the volume ratio and A compositions are thoroughly mixed, obtain mixed liquor；
(2) shitosan, sodium alginate and B component are weighed by the weight ratio to be sufficiently mixed, obtains solid mixture；
(3) after the mixed liquor of step (1) being heated into 50 DEG C -60 DEG C, the solid for adding step (2) by the volume ratio is mixed
Compound, is sufficiently stirred for, is cooled to 20 DEG C -30 DEG C and obtains the antistaling agent.
The present invention has the advantages that：
1st, the present invention uses Chinese medicine as the main component of antistaling agent, and fresh-keeping principle is using the flavones extracted in Chinese medicine
Very strong antioxidation can be played, the oxygen radical in dragon fruit body can be removed, prevent degeneration, the aging of cell, slowed down
The braiding time of dragon fruit, while there is volatile oil isoreactivity material in each traditional Chinese medicine ingredients, the effect of sterilization can be played, when
So, simply use Chinese medical extract dragon fruit is carried out it is fresh-keeping be it is inadequate, flue fruit volume is larger, and flavones, volatile oil
Isoreactivity composition is also not easy absorption on dragon fruit surface, and inventor's research finds that traditional Chinese medicine ingredients are mixed with gel component,
Layer protecting film is formed on dragon fruit surface, active component can be firmly adsorbed on dragon fruit surface, meanwhile, gel component is also
Layer protecting film is formd, air can be come with the isolation of flue fruits, play bacterium in air-isolation, reduced in dragon fruit
Portion's moisture evaporation, can effectively play moisture that is fresh-keeping, ensureing dragon fruit, it is ensured that the effect of dragon fruit freshness, and
The fresh-keeping composition that the technical program is used is nontoxic natural traditional Chinese medicine, is a kind of antistaling agent of environmental protection.
【Specific embodiment】
All features disclosed in this specification, or disclosed all methods or during the step of, except mutually exclusive
Feature and/or step beyond, can combine by any way.
Any feature disclosed in this specification (including any accessory claim, summary), unless specifically stated otherwise, each
Feature is an example in a series of equivalent or similar characteristics.
Embodiment 1：
1st, the fresh-keeping composition of the Chinese medicine of antistaling agent is：Percent by volume is 50% red sage root extract and percent by volume is
50% A compositions, wherein, A compositions are by licorice extract, 20% galingal extract solution, 20% that percent by volume is 20%
Fruit of a cubeb litsea tree extract solution, 20% pine needle extract, 20% wormwood extract solution composition.
2nd, the gel component of antistaling agent is：The shitosan of 30wt%, the sodium alginate of 30wt%, the carragheen of 20wt% and
The xanthans of 20wt%.
Wherein：
(1) extracting method of red sage root extract is：The dry product red sage root is by crushing, sieving, extracting, being concentrated to give extract solution；
The screen sizes of sieving process are 40 mesh；The extracting solution that leaching process is used is the ethanol solution that percentage by volume is 95%,
Extraction time is 50min, and extracting solution addition is 2 times of crushed material volume, and extracting times are 2 times, are filtered after extraction, are merged
Filtrate obtains stoste；Concentration process is concentrated using water bath with thermostatic control, and bath temperature is 90 DEG C, and it is stoste to be concentrated to the volume of concentrate
Stop concentration when 1/5, concentrate is red sage root extract.
(2) licorice extract, pine needle extract, wormwood extract solution, the extracting method of fruit of a cubeb litsea tree extract solution are by Radix Glycyrrhizae, pine
Pin, wormwood, fruit of a cubeb litsea tree leaf are ground, extract, being filtrated to get extract solution respectively, and the extracting solution that extraction is used is distilled water,
Extracting solution addition is 2 times of abrasive material volume, and the time of extraction is 48h.
(3) extracting method of galingal extract solution is to crush the galingal of dry product, sieve, extracting, distilling, condensing and obtain
Extract solution, the screen sizes of process of sieving are 50 mesh, and the extracting solution that leaching process is used is the NaOH that mass concentration is 5%,
Extraction time is 30h, and extracting solution addition is 2 times of crushed material volume, and extracting times are 2 times, are filtered after extraction, merge filter
Liquid obtains stoste；Still-process is distilled using water bath with thermostatic control, and distillation condensate liquid stops distillation, condensation when being the 1/3 of stoste volume
Liquid is galingal extract solution.
3rd, the preparation method of above-mentioned red heart flue fresh-keeping agent of fruits is：
(1) measure each Chinese medicine extract of the fresh-keeping composition of Chinese medicine respectively by 1 volume ratio, be thoroughly mixed, obtain
To mixed liquor；
(2) by 2 weight score another name amount gel component each composition, be thoroughly mixed, obtain solid mixing
Thing；
(3) it is by volume 4 after the mixed liquor of step (1) being heated into 50 DEG C:The 1 solid mixing for adding step (2)
Thing, is sufficiently stirred for, is cooled to 20 DEG C and obtains antistaling agent.
Embodiment 2：
1st, the fresh-keeping composition of the Chinese medicine of antistaling agent is：Percent by volume is 60% red sage root extract and percent by volume is
40% A compositions, A compositions are by pine needle extract, 20% wormwood extract solution, 20% dragon fruit that percent by volume is 20%
Skin extract solution, 20% Lotus Leaf Extracts and 20% pomelo peel extract solution composition.
2nd, the gel component of antistaling agent is：The shitosan of 30wt%, the sodium alginate of 30wt%, the hyaluronic acid of 20wt%
With 20wt% konjac glucomannans.
Wherein：
(1) extracting method of red sage root extract is：The dry product red sage root is by crushing, sieving, extracting, being concentrated to give extract solution；
The screen sizes of sieving process are 50 mesh；The extracting solution that leaching process is used is the ethanol solution that percentage by volume is 95%,
Extraction time is 80min, and extracting solution addition is 3 times of crushed material volume, and extracting times are 4 times, are filtered after extraction, are merged
Filtrate obtains stoste；Concentration process is concentrated using water bath with thermostatic control, and bath temperature is 100 DEG C, is concentrated to the volume of concentrate for stoste
1/3 when stop concentration, concentrate is red sage root extract.
(2) pine needle extract, wormwood extract solution, pitaya peel extract solution, the extracting method of Lotus Leaf Extracts be by pine needle,
Wormwood, pitaya peel, lotus leaf are ground, extract, being filtrated to get extract solution respectively, and the extracting solution that extraction is used is distillation
Water, extracting solution addition is 3 times of abrasive material volume, and the time of extraction is 50h.
(3) extracting method of pomelo peel extract solution be the pomelo peel of, dry product crushed, sieved, being extracted, being distilled, it is cold
Solidifying to obtain extract solution, the screen sizes of process of sieving are 60 mesh, and the extracting solution that leaching process is used is 5% for mass concentration
NaOH, extraction time is 34h, and extracting solution addition is 3 times of crushed material volume, and extracting times are 4 times, are filtered after extraction,
Merging filtrate obtains stoste；Still-process is distilled using water bath with thermostatic control, and distillation condensate liquid stops steaming when being the 1/2 of stoste volume
Evaporate, condensate liquid is galingal extract solution, pomelo peel extract solution.
3rd, the processing method of antistaling agent is processed according to the processing method of embodiment 1.
Embodiment 3：
1st, the fresh-keeping composition of the Chinese medicine of antistaling agent is：Percent by volume is 55% red sage root extract and percent by volume is
45% A compositions, A compositions are by licorice extract, 18% galingal extract solution, 18% fruit of a cubeb litsea tree that percent by volume is 15%
Extract solution, 17% pine needle extract, 18% wormwood extract solution, 14% pitaya peel extract solution.
2nd, the gel component of antistaling agent is：The shitosan of 25wt%, the sodium alginate of 25wt%, 15wt% carragheens,
18wt% xanthans and 17wt% konjac glucomannans.
Wherein：
(1) extracting method of red sage root extract is：The dry product red sage root is by crushing, sieving, extracting, being concentrated to give extract solution；
The screen sizes of sieving process are 40 mesh；The extracting solution that leaching process is used is the ethanol solution that percentage by volume is 95%,
Extraction time is 55in, and extracting solution addition is 2.5 times of crushed material volume, and extracting times are 3 times, are filtered after extraction, are closed
And filtrate obtains stoste；Concentration process is concentrated using water bath with thermostatic control, and bath temperature is 98 DEG C, is concentrated to the volume of concentrate for stoste
1/4 when stop concentration, concentrate is red sage root extract.
(2) licorice extract, pine needle extract, wormwood extract solution, pitaya peel extract solution, the extraction of fruit of a cubeb litsea tree extract solution
Method is to be ground Radix Glycyrrhizae, pine needle, wormwood, pitaya peel respectively, extract, being filtrated to get extract solution, the leaching that extraction is used
Solution is carried for distilled water, extracting solution addition is 2.5 times of abrasive material volume, and the time of extraction is 49h.
(3) extracting method of galingal extract solution is to crush the galingal of dry product, sieve, extracting, distilling, condensing and obtain
Extract solution, the screen sizes of process of sieving are 60 mesh, and the extracting solution that leaching process is used is the NaOH that mass concentration is 5%,
Extraction time is 32h, and extracting solution addition is 2.5 times of crushed material volume, and extracting times are 3 times, are filtered after extraction, are merged
Filtrate obtains stoste；Still-process is distilled using water bath with thermostatic control, and distillation condensate liquid stops distillation when being the 1/2 of stoste volume, cold
Lime set is galingal extract solution, pomelo peel extract solution.
3rd, the processing method of antistaling agent is processed according to the processing method of embodiment 1.
Embodiment 4：
1st, the fresh-keeping composition of the Chinese medicine of antistaling agent is：Percent by volume is 52% red sage root extract and percent by volume is
48% A compositions, A compositions are extracted by the licorice extract of percent by volume 20%, 20% fruit of a cubeb litsea tree extract solution, 20% pine needle
Liquid, 20% pitaya peel extract solution, 20% Lotus Leaf Extracts.
2nd, the gel component of antistaling agent is：The shitosan of 28wt%, the sodium alginate of 28wt%, the carragheen of 12wt%,
The xanthans of 12wt%, the konjac glucomannan of 14wt%, the hyaluronic acid of 6wt%
Wherein：
(1) extracting method of red sage root extract is：The dry product red sage root is by crushing, sieving, extracting, being concentrated to give extract solution；
The screen sizes of sieving process are 50 mesh；The extracting solution that leaching process is used is the ethanol solution that percentage by volume is 95%,
Extraction time is 70min, and extracting solution addition is 2.8 times of crushed material volume, and extracting times are 3 times, are filtered after extraction, are closed
And filtrate obtains stoste；Concentration process is concentrated using water bath with thermostatic control, and bath temperature is 97 DEG C, is concentrated to the volume of concentrate for stoste
1/4 when stop concentration, concentrate is red sage root extract.
(2) licorice extract, pine needle extract, pitaya peel extract solution, Lotus Leaf Extracts, the extraction of fruit of a cubeb litsea tree extract solution
Method is to be ground Radix Glycyrrhizae, pine needle, pitaya peel, lotus leaf, the fruit of a cubeb litsea tree respectively, extract, being filtrated to get extract solution, and extraction makes
Extracting solution is distilled water, and extracting solution addition is 2.5 times of abrasive material volume, and the time of extraction is 49h.
3rd, the preparation method of above-mentioned red heart flue fresh-keeping agent of fruits is：
(1) measure each Chinese medicine extract of the fresh-keeping composition of Chinese medicine respectively by 1 volume ratio, be thoroughly mixed, obtain
To mixed liquor；
(2) by 2 weight score another name amount gel component each composition, be thoroughly mixed, obtain solid mixing
Thing；
(3) it is by volume 5 after the mixed liquor of step (1) being heated into 60 DEG C:The 1 solid mixing for adding step (2)
Thing, is sufficiently stirred for, is cooled to 230 DEG C and obtains antistaling agent.
Embodiment 5：
1st, the fresh-keeping composition of the Chinese medicine of antistaling agent is：Percent by volume is 57% red sage root extract and percent by volume is
43% A compositions, A compositions including licorice extract that percent by volume is 16%, 14% fruit of a cubeb litsea tree extract solution, 12% it is good
Ginger extract solution, 12% pine needle extract, 18% wormwood extract solution, 17% pitaya peel extract solution, 11% lotus leaf are carried
Take liquid.
2nd, the gel component of antistaling agent is：The shitosan of gel component including 24wt%, the sodium alginate of 25wt%,
The carragheen of 18wt%, the xanthans of 17wt%, the hyaluronic acid of 16wt%.
Wherein：
(1) extracting method of red sage root extract is：The dry product red sage root is by crushing, sieving, extracting, being concentrated to give extract solution；
The screen sizes of sieving process are 50 mesh；The extracting solution that leaching process is used is the ethanol solution that percentage by volume is 95%,
Extraction time is 74min, and extracting solution addition is 3 times of crushed material volume, and extracting times are 4 times, are filtered after extraction, are merged
Filtrate obtains stoste；Concentration process is concentrated using water bath with thermostatic control, and bath temperature is 96 DEG C, and it is stoste to be concentrated to the volume of concentrate
Stop concentration when 1/4, concentrate is red sage root extract.
(2) licorice extract, pine needle extract, wormwood extract solution, pitaya peel extract solution, Lotus Leaf Extracts, the fruit of a cubeb litsea tree
The extracting method of extract solution is to be ground Radix Glycyrrhizae, pine needle, wormwood, pitaya peel, lotus leaf, the fruit of a cubeb litsea tree respectively, extract, filtering
Extract solution is obtained, the extracting solution that extraction is used is distilled water, and extracting solution addition is 2.5 times of abrasive material volume, is extracted
Time be 49h.
(3) extracting method of galingal extract solution is to crush the galingal of dry product, sieve, extracting, distilling, condensing and obtain
Extract solution, the screen sizes of process of sieving are 60 mesh, and the extracting solution that leaching process is used is the NaOH that mass concentration is 5%,
Extraction time is 33h, and extracting solution addition is 3 times of crushed material volume, and extracting times are 4 times, are filtered after extraction, merge filter
Liquid obtains stoste；Still-process is distilled using water bath with thermostatic control, and distillation condensate liquid stops distillation, condensation when being the 1/2 of stoste volume
Liquid is galingal extract solution, pomelo peel extract solution.
3rd, the processing method of antistaling agent is processed according to the processing method of embodiment 4.
Embodiment 6：
1st, the fresh-keeping composition of the Chinese medicine of antistaling agent is：Percent by volume is 52% red sage root extract and percent by volume is
48% A compositions, A is extracted by licorice extract that percent by volume is 12%, 17% galingal extract solution, 14% fruit of a cubeb litsea tree
Liquid, 8% pine needle extract, 16% wormwood extract solution, 12% pitaya peel extract solution, 12% Lotus Leaf Extracts and
9% pomelo peel extract solution composition.
2nd, the gel component of antistaling agent is：The shitosan of gel component including 27wt%, the sodium alginate of 27wt%,
The carragheen of 19wt%, 17wt% xanthans, 9wt% konjac glucomannans and 1wt% hyaluronic acids.
Wherein：
(1) extracting method of red sage root extract is：The dry product red sage root is by crushing, sieving, extracting, being concentrated to give extract solution；
The screen sizes of sieving process are 40 mesh；The extracting solution that leaching process is used is the ethanol solution that percentage by volume is 95%,
Extraction time is 74min, and extracting solution addition is 2.5 times of crushed material volume, and extracting times are 3 times, are filtered after extraction, are closed
And filtrate obtains stoste；Concentration process is concentrated using water bath with thermostatic control, and bath temperature is 96 DEG C, is concentrated to the volume of concentrate for stoste
1/4 when stop concentration, concentrate is red sage root extract.
(2) licorice extract, pine needle extract, wormwood extract solution, pitaya peel extract solution, Lotus Leaf Extracts, the fruit of a cubeb litsea tree
The extracting method of extract solution is to be ground Radix Glycyrrhizae, pine needle, wormwood, pitaya peel, lotus leaf, the fruit of a cubeb litsea tree respectively, extract, filtering
Extract solution is obtained, the extracting solution that extraction is used is distilled water, and extracting solution addition is 2.5 times of abrasive material volume, is extracted
Time be 49h.
(3) galingal extract solution, the extracting method of pomelo peel extract solution are to enter the pomelo peel of the galingal of dry product, dry product respectively
Row is crushed, sieved, extracting, distilling, condensation obtains extract solution, and the screen sizes of process of sieving are 60 mesh, what leaching process was used
Extracting solution is the NaOH that mass concentration is 5%, and extraction time is 32h, and extracting solution addition is the 2.5 of crushed material volume
Times, extracting times are 3 times, are filtered after extraction, and merging filtrate obtains stoste；Still-process is distilled using water bath with thermostatic control, is distilled cold
Stop distillation when lime set is stoste volume 1/3, condensate liquid is galingal extract solution, pomelo peel extract solution.
3rd, the processing method of antistaling agent is processed according to the processing method of embodiment 4.
Embodiment 7：
1st, the fresh-keeping composition of the Chinese medicine of antistaling agent is：Percent by volume is 56% red sage root extract and percent by volume is
44% A compositions, A compositions are by licorice extract, 17% fruit of a cubeb litsea tree extract solution, 17% pine needle that percent by volume is 17%
Extract solution, 17% wormwood extract solution, 7% pitaya peel extract solution, 10% Lotus Leaf Extracts, 15% pomelo peel are extracted
Liquid is constituted.
2nd, the gel component of antistaling agent is：The shitosan of 23wt%, the sodium alginate of 23wt%, the carragheen of 18wt%,
The xanthans of 19wt%, the konjac glucomannan of 7wt%, the hyaluronic acid of 10wt%.
Wherein：
(1) extracting method of red sage root extract is：The dry product red sage root is by crushing, sieving, extracting, being concentrated to give extract solution；
The screen sizes of sieving process are 50 mesh；The extracting solution that leaching process is used is the ethanol solution that percentage by volume is 95%,
Extraction time is 74min, and extracting solution addition is 3 times of crushed material volume, and extracting times are 3 times, are filtered after extraction, are merged
Filtrate obtains stoste；Concentration process is concentrated using water bath with thermostatic control, and bath temperature is 96 DEG C, and it is stoste to be concentrated to the volume of concentrate
Stop concentration when 1/3, concentrate is red sage root extract.
(2) licorice extract, pine needle extract, wormwood extract solution, pitaya peel extract solution, Lotus Leaf Extracts, the fruit of a cubeb litsea tree
The extracting method of extract solution is to be ground Radix Glycyrrhizae, pine needle, wormwood, pitaya peel, lotus leaf respectively, extract, being filtrated to get and carry
Take liquid, the extracting solution that extraction is used is distilled water, extracting solution addition is 3 times of abrasive material volume, the time of extraction is
48h。
(3) galingal extract solution, the extracting method of pomelo peel extract solution are to enter the pomelo peel of the galingal of dry product, dry product respectively
Row is crushed, sieved, extracting, distilling, condensation obtains extract solution, and the screen sizes of process of sieving are 50 mesh, what leaching process was used
Extracting solution is the NaOH that mass concentration is 5%, and extraction time is 33h, and extracting solution addition is 3 times of crushed material volume,
Extracting times are 3 times, are filtered after extraction, and merging filtrate obtains stoste；Still-process is distilled using water bath with thermostatic control, distills condensate liquid
For stoste volume 1/2 when stop distillation, condensate liquid be galingal extract solution, pomelo peel extract solution.
3rd, the preparation method of above-mentioned red heart flue fresh-keeping agent of fruits is：
(1) measure each Chinese medicine extract of the fresh-keeping composition of Chinese medicine respectively by 1 volume ratio, be thoroughly mixed, obtain
To mixed liquor；
(2) by 2 weight score another name amount gel component each composition, be thoroughly mixed, obtain solid mixing
Thing；
(3) it is by volume 5 after the mixed liquor of step (1) being heated into 55 DEG C:The 1 solid mixing for adding step (2)
Thing, is sufficiently stirred for, is cooled to 25 DEG C and obtains antistaling agent.
Embodiment 8：
1st, the fresh-keeping composition of the Chinese medicine of antistaling agent is：Percent by volume is 54% red sage root extract and percent by volume is
46% A compositions, A compositions are by licorice extract, 11% fruit of a cubeb litsea tree extract solution, 19% wormwood that percent by volume is 18%
Extract solution, 17% pitaya peel extract solution, 19% Lotus Leaf Extracts, 16% pomelo peel extract solution.
2nd, the gel component of antistaling agent is：The shitosan of 28wt%, the sodium alginate of 28wt%, 18wt% carragheens,
7wt% xanthans, 1wt% konjac glucomannans, 18wt% hyaluronic acids.
Wherein：
(1) extracting method of red sage root extract is：The dry product red sage root is by crushing, sieving, extracting, being concentrated to give extract solution；
The screen sizes of sieving process are 40 mesh；The extracting solution that leaching process is used is the ethanol solution that percentage by volume is 95%,
Extraction time is 71min, and extracting solution addition is 2 times of crushed material volume, and extracting times are 3 times, are filtered after extraction, are merged
Filtrate obtains stoste；Concentration process is concentrated using water bath with thermostatic control, and bath temperature is 92 DEG C, and it is stoste to be concentrated to the volume of concentrate
Stop concentration when 1/4, concentrate is red sage root extract.
(2) licorice extract, wormwood extract solution, pitaya peel extract solution, Lotus Leaf Extracts, the extraction of fruit of a cubeb litsea tree extract solution
Method is to be ground Radix Glycyrrhizae, wormwood, pitaya peel, lotus leaf, the fruit of a cubeb litsea tree respectively, extract, being filtrated to get extract solution, and extraction makes
Extracting solution is distilled water, and extracting solution addition is 3 times of abrasive material volume, and the time of extraction is 49h.
(3) extracting method of galingal extract solution is to crush the galingal of dry product respectively, sieve, extracting, distilling, condensing
Extract solution is obtained, the screen sizes of process of sieving are 50 mesh, and the extracting solution that leaching process is used is 5% for mass concentration
NaOH, extraction time is 31h, and extracting solution addition is 2 times of crushed material volume, and extracting times are 3 times, are filtered after extraction,
Merging filtrate obtains stoste；Still-process is distilled using water bath with thermostatic control, and distillation condensate liquid stops steaming when being the 1/3 of stoste volume
Evaporate, condensate liquid is galingal extract solution, pomelo peel extract solution.
3rd, the processing method of antistaling agent is processed according to the processing method of embodiment 7.
Embodiment 9：
1st, the fresh-keeping composition of the Chinese medicine of antistaling agent is：Percent by volume is 59% red sage root extract and percent by volume is
41% A compositions, A compositions are by licorice extract, 2% galingal extract solution, 19% fruit of a cubeb litsea tree that percent by volume is 20%
Extract solution, 19% pine needle extract, 17% wormwood extract solution, 18% pitaya peel extract solution, 12% lotus leaf are extracted
Liquid, 13% pomelo peel extract solution.
2nd, the gel component of antistaling agent is：The shitosan of gel component including 29wt%, the sodium alginate of 21wt%,
The carragheen of 17wt%, the xanthans of 18wt%, the konjac glucomannan of 19wt%, the hyaluronic acid of 13wt%.
Wherein：
(1) extracting method of red sage root extract is：The dry product red sage root is by crushing, sieving, extracting, being concentrated to give extract solution；
The screen sizes of sieving process are 40 mesh；The extracting solution that leaching process is used is the ethanol solution that percentage by volume is 95%,
Extraction time is 50min, and extracting solution addition is 2 times of crushed material volume, and extracting times are 2 times, are filtered after extraction, are merged
Filtrate obtains stoste；Concentration process is concentrated using water bath with thermostatic control, and bath temperature is 91 DEG C, and it is stoste to be concentrated to the volume of concentrate
Stop concentration when 1/5, concentrate is red sage root extract.
(2) licorice extract, pine needle extract, wormwood extract solution, pitaya peel extract solution, Lotus Leaf Extracts, the fruit of a cubeb litsea tree
The extracting method of extract solution is to be ground Radix Glycyrrhizae, pine needle, wormwood, pitaya peel, lotus leaf respectively, extract, being filtrated to get and carry
Liquid is taken, the extracting solution that extraction is used is distilled water, and extracting solution addition is 2.6 times of abrasive material volume, the time of extraction
It is 49.5h.
(3) galingal extract solution, the extracting method of pomelo peel extract solution are to enter the pomelo peel of the galingal of dry product, dry product respectively
Row is crushed, sieved, extracting, distilling, condensation obtains extract solution, and the screen sizes of process of sieving are 60 mesh, what leaching process was used
Extracting solution is the NaOH that mass concentration is 5%, and extraction time is 31.2h, and extracting solution addition is the 2.7 of crushed material volume
Times, extracting times are 3 times, are filtered after extraction, and merging filtrate obtains stoste；Still-process is distilled using water bath with thermostatic control, is distilled cold
Stop distillation when lime set is the 1/2 of stoste volume, condensate liquid is galingal extract solution, pomelo peel extract solution.
3rd, the processing method of antistaling agent is processed according to the processing method of embodiment 7.
Control group 1：
The formula for choosing embodiment 1 makes antistaling agent, but, 4 kinds of A compositions are selected, a kind of B component other materials ratio is entered
The corresponding adjustment of row, i.e.,：(1) the fresh-keeping composition of the Chinese medicine of antistaling agent is：Percent by volume is 50% red sage root extract and volume
Percentage is 50% A compositions, wherein, A compositions are extracted by licorice extract that percent by volume is 25%, 25% galingal
Liquid, 25% fruit of a cubeb litsea tree extract solution, 25% pine needle extract.(2) gel component of antistaling agent is：The shitosan of 30wt%,
The sodium alginate of 30wt%, the carragheen of 40wt%.
Control group 2：
Purchase fruit antistaling agent conventional on the market, is carried out according to operation instructions.
Control group 3：
Fruit antistaling agent is not used to carry out fresh-keeping.
Checking test：
The dragon fruit of maturation is won on the same day, dragon fruit is immersed in the antistaling agent of embodiment 1-9 and control group 1, soak
After 5-10min, dragon fruit is taken out, puts and store at normal temperatures, control group 2 according to the fruit antistaling agent bought on the market explanation
Book uses antistaling agent, then puts and is stored at normal temperatures, and control group 3 does not use antistaling agent, and dragon fruit directly is placed on into temperature
It is storage at a constant temperature in 5 DEG C of refrigerator-freezers.5d is observed and records, the concrete condition of 20d, 30d, 60d dragon fruit is shown in Table 1：
The fresh-keeping situation table of comparisons of the dragon fruit of table 1：
As seen from the above table, applied on dragon fruit using the preparation method of antistaling agent disclosed by the invention and antistaling agent, than
Commercially available antistaling agent effect more preferably, in A compositions up to 5 kinds, when B component is up to 3 kinds, can guarantee that the storage number of days of dragon fruit is more than or equal to
60 days, storage effect was good.
In sum, can play good fresh-keeping to dragon fruit using flue fresh-keeping agent of fruits of the invention and preparation method thereof
Effect, meanwhile, the fresh-keeping composition that this product is used is mostly pure natural traditional Chinese medicine ingredients, is a kind of good crude antistaling agent, energy
Play good fresh-keeping effect.
Embodiment described above only expresses several embodiments of the invention, and its description is more specific and detailed, but simultaneously
Therefore limitation of the scope of the invention can not be interpreted as.It should be pointed out that for the person of ordinary skill of the art,
Without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection model of the invention
Enclose.Therefore, protection scope of the present invention should be determined by the appended claims.
Claims (7)
1. a kind of antistaling agent of red heart dragon fruit, including the fresh-keeping composition of Chinese medicine and gel component, it is characterised in that the Chinese medicine is protected
Fresh composition is 4-5 with gel component volume ratio:1, the fresh-keeping composition of Chinese medicine includes that percent by volume is the red sage root of 50%-60%
Extract solution and percent by volume are the A compositions of 40%-50%, and the A compositions are the following material of 0-20% by percent by volume
Composition：Licorice extract, galingal extract solution, fruit of a cubeb litsea tree extract solution, pine needle extract, wormwood extract solution, pitaya peel extract solution,
Lotus Leaf Extracts and pomelo peel extract solution；The gel component includes shitosan, the sea of 20wt-30wt% of 20wt-30wt%
Mosanom and B component, the B component are the following material composition of 0-20wt% by percentage by weight：Carragheen, xanthans, evil spirit
Taro glue and hyaluronic acid.
2. the antistaling agent of a kind of red heart dragon fruit according to claim 1, it is characterised in that the Chinese medicine is fresh-keeping into subpackage
Containing at least 5 kinds A compositions.
3. the antistaling agent of a kind of red heart dragon fruit according to claim 1, it is characterised in that the gel component is comprising extremely
Few 2 kinds of B components.
4. the antistaling agent of a kind of red heart dragon fruit according to claim 1, it is characterised in that the red sage root extract is carried
The method of taking is：The dry product red sage root is by crushing, sieving, extracting, being concentrated to give extract solution；The screen sizes of the sieving process are 40
The mesh of mesh -50；The extracting solution that the leaching process is used is the ethanol solution that percentage by volume is 95%, and extraction time is
50min-80min, extracting solution addition is 2 times -3 times of crushed material volume, and extracting times are 2 times -4 times, are filtered after extraction,
Merging filtrate obtains stoste；The concentration process is concentrated using water bath with thermostatic control, and bath temperature is 90 DEG C -100 DEG C, is concentrated to concentration
Liquid product stops concentration when being the 1/5-1/3 of stoste, concentrate is the red sage root extract.
5. the antistaling agent of a kind of red heart dragon fruit according to claim 1, it is characterised in that the licorice extract, pine
Pin extract solution, wormwood extract solution, pitaya peel extract solution, Lotus Leaf Extracts, the extracting method of fruit of a cubeb litsea tree extract solution be, will be sweet
Grass, pine needle, wormwood, pitaya peel, lotus leaf, fruit of a cubeb litsea tree leaf are ground, extract, being filtrated to get extract solution, the extraction respectively
The extracting solution for using is distilled water, and extracting solution addition is 2 times -3 times of abrasive material volume, and the time of extraction is 48h-
50h。
6. the antistaling agent of a kind of red heart dragon fruit according to claim 1, it is characterised in that the galingal extract solution, shaddock
The extracting method of sub- skin extract solution is to crush dry product galingal, dry product pomelo peel respectively, sieve, extracting, distilling, condensing
To extract solution, the screen sizes of the sieving process are the mesh of 50 mesh -60, and the extracting solution that the leaching process is used is that quality is dense
The NaOH for 5% is spent, extraction time is 30h-34h, and extracting solution addition is 2-3 times of crushed material volume, and extracting times are 2
Secondary -4 times, filtered after extraction, merging filtrate obtains stoste；The still-process is distilled using water bath with thermostatic control, and distillation condensate liquid is
Stop distillation during the 1/3-1/2 of stoste volume, condensate liquid is the galingal extract solution, pomelo peel extract solution.
7. the preparation method of a kind of red heart flue fresh-keeping agent of fruits according to claim 1-6 any one, it is characterised in that
Methods described comprises the following steps：
(1) measure red sage root extract by the volume ratio and A compositions are thoroughly mixed, obtain mixed liquor；
(2) shitosan, sodium alginate and B component are weighed by the weight ratio to be sufficiently mixed, obtains solid mixture；
(3) after the mixed liquor of step (1) being heated into 50 DEG C -60 DEG C, the solid for adding step (2) by the volume ratio mixes
Thing, is sufficiently stirred for, is cooled to 20 DEG C -30 DEG C and obtains the antistaling agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611044667.7A CN106720242A (en) | 2016-11-24 | 2016-11-24 | A kind of antistaling agent of red heart dragon fruit and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611044667.7A CN106720242A (en) | 2016-11-24 | 2016-11-24 | A kind of antistaling agent of red heart dragon fruit and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106720242A true CN106720242A (en) | 2017-05-31 |
Family
ID=58975232
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611044667.7A Pending CN106720242A (en) | 2016-11-24 | 2016-11-24 | A kind of antistaling agent of red heart dragon fruit and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106720242A (en) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107318972A (en) * | 2017-08-11 | 2017-11-07 | 贵州省果树科学研究所 | A kind of dragon fruit normal temperature antistaling agent and preparation method thereof and preservation method |
| CN107333877A (en) * | 2017-07-31 | 2017-11-10 | 周海腾 | Melon and fruit antistaling agent prepared by a kind of glycyrrhiza glabra extract |
| CN107494712A (en) * | 2017-09-25 | 2017-12-22 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of longan seed essential oil fresh applied to banana and preparation method thereof |
| CN107801772A (en) * | 2017-10-31 | 2018-03-16 | 博白县富山水果种植专业合作社 | A kind of granulated sugar tangerine antistaling agent and preparation method thereof |
| CN107927151A (en) * | 2017-12-08 | 2018-04-20 | 刘艳蓉 | A kind of natural long-acting fruit and vegetable fresh-keeping agent and preparation method thereof |
| CN107927150A (en) * | 2017-12-08 | 2018-04-20 | 杨坚 | A kind of natural composite antistaling agent for vegetables and preparation method thereof |
| CN108077829A (en) * | 2018-01-10 | 2018-05-29 | 山东青果食品有限公司 | A kind of processing method based on reduction vegetables nutrient loss |
| CN108294105A (en) * | 2018-01-29 | 2018-07-20 | 广西壮族自治区农业科学院 | Antistaling agent of threshing and preparation method thereof and application after a kind of inhibition grape harvest |
| CN108782746A (en) * | 2018-04-28 | 2018-11-13 | 徐州工程学院 | The fresh-keeping plastics of Fresh-cut apple and its application |
| CN108850145A (en) * | 2018-06-11 | 2018-11-23 | 南阳道地金木瓜生物科技股份有限公司 | A kind of method for storing and refreshing of pawpaw |
| CN111357808A (en) * | 2018-12-25 | 2020-07-03 | 山东摩卡智能科技有限公司 | Fresh-cut potato preservative |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101637199A (en) * | 2008-08-01 | 2010-02-03 | 上海健音食品科技有限公司 | Purely natural betelnut capsula preservative |
| CN102972507A (en) * | 2012-12-13 | 2013-03-20 | 浙江海洋学院 | Traditional Chinese medicine extracting solution for freshness preservation of fish flesh |
| CN103462174A (en) * | 2013-09-27 | 2013-12-25 | 青岛大学 | Compound preservative, preparing method of compound preservative and purpose of compound preservative |
| CN103828907A (en) * | 2012-11-25 | 2014-06-04 | 董书阁 | Winter jujube Chinese herbal medicine fresh-keeping agent and preparation method thereof |
| CN105053174A (en) * | 2015-09-17 | 2015-11-18 | 邯郸学院 | Preparation method and application of plant source complex preservative |
| CN105123913A (en) * | 2015-08-27 | 2015-12-09 | 太仓市永发农场专业合作社 | Composite preservative for blueberries |
| CN105325536A (en) * | 2015-11-06 | 2016-02-17 | 广西南宁胜祺安科技开发有限公司 | Pitaya antistaling agent and preparation method thereof |
| CN105613725A (en) * | 2015-12-23 | 2016-06-01 | 广西绿希望农业发展有限公司 | Preservation method of pitaya fruit |
-
2016
- 2016-11-24 CN CN201611044667.7A patent/CN106720242A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101637199A (en) * | 2008-08-01 | 2010-02-03 | 上海健音食品科技有限公司 | Purely natural betelnut capsula preservative |
| CN103828907A (en) * | 2012-11-25 | 2014-06-04 | 董书阁 | Winter jujube Chinese herbal medicine fresh-keeping agent and preparation method thereof |
| CN102972507A (en) * | 2012-12-13 | 2013-03-20 | 浙江海洋学院 | Traditional Chinese medicine extracting solution for freshness preservation of fish flesh |
| CN103462174A (en) * | 2013-09-27 | 2013-12-25 | 青岛大学 | Compound preservative, preparing method of compound preservative and purpose of compound preservative |
| CN105123913A (en) * | 2015-08-27 | 2015-12-09 | 太仓市永发农场专业合作社 | Composite preservative for blueberries |
| CN105053174A (en) * | 2015-09-17 | 2015-11-18 | 邯郸学院 | Preparation method and application of plant source complex preservative |
| CN105325536A (en) * | 2015-11-06 | 2016-02-17 | 广西南宁胜祺安科技开发有限公司 | Pitaya antistaling agent and preparation method thereof |
| CN105613725A (en) * | 2015-12-23 | 2016-06-01 | 广西绿希望农业发展有限公司 | Preservation method of pitaya fruit |
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107333877A (en) * | 2017-07-31 | 2017-11-10 | 周海腾 | Melon and fruit antistaling agent prepared by a kind of glycyrrhiza glabra extract |
| CN107318972A (en) * | 2017-08-11 | 2017-11-07 | 贵州省果树科学研究所 | A kind of dragon fruit normal temperature antistaling agent and preparation method thereof and preservation method |
| CN107494712A (en) * | 2017-09-25 | 2017-12-22 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of longan seed essential oil fresh applied to banana and preparation method thereof |
| CN107801772A (en) * | 2017-10-31 | 2018-03-16 | 博白县富山水果种植专业合作社 | A kind of granulated sugar tangerine antistaling agent and preparation method thereof |
| CN107927151A (en) * | 2017-12-08 | 2018-04-20 | 刘艳蓉 | A kind of natural long-acting fruit and vegetable fresh-keeping agent and preparation method thereof |
| CN107927150A (en) * | 2017-12-08 | 2018-04-20 | 杨坚 | A kind of natural composite antistaling agent for vegetables and preparation method thereof |
| CN108077829A (en) * | 2018-01-10 | 2018-05-29 | 山东青果食品有限公司 | A kind of processing method based on reduction vegetables nutrient loss |
| CN108294105A (en) * | 2018-01-29 | 2018-07-20 | 广西壮族自治区农业科学院 | Antistaling agent of threshing and preparation method thereof and application after a kind of inhibition grape harvest |
| CN108782746A (en) * | 2018-04-28 | 2018-11-13 | 徐州工程学院 | The fresh-keeping plastics of Fresh-cut apple and its application |
| CN108782746B (en) * | 2018-04-28 | 2022-04-08 | 徐州工程学院 | Film coating agent for fresh-cut broccoli preservation and application thereof |
| CN108850145A (en) * | 2018-06-11 | 2018-11-23 | 南阳道地金木瓜生物科技股份有限公司 | A kind of method for storing and refreshing of pawpaw |
| CN108850145B (en) * | 2018-06-11 | 2021-08-20 | 南阳道地金木瓜生物科技股份有限公司 | Papaya storage and preservation method |
| CN111357808A (en) * | 2018-12-25 | 2020-07-03 | 山东摩卡智能科技有限公司 | Fresh-cut potato preservative |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106720242A (en) | A kind of antistaling agent of red heart dragon fruit and preparation method thereof | |
| CN105010519B (en) | A kind of antistaling agent and preparation method thereof of Qarnet Chinese yam | |
| CN101768514B (en) | Alhagi sparsifolia extract and preparation method and application thereof | |
| CN101933533A (en) | Plant source preservative and preparation method and application thereof | |
| CN103918780B (en) | Waxberry preservative | |
| CN104920600A (en) | Preservative for longan and preparation method and preservation method thereof | |
| CN107897357A (en) | A kind of Siraitia grosvenori preservative and its preservation method | |
| CN105360434B (en) | Preparation method of jujube black tea | |
| CN104688930A (en) | Anti-fatigue ginseng and deer bone health care wine and preparation method thereof | |
| CN105123912A (en) | Preservative for honey peaches | |
| CN108522684A (en) | A kind of Huanghua pear dark tea and preparation method thereof | |
| KR100894636B1 (en) | A manufacturing process of the beverage including yam extract | |
| CN111528381A (en) | Heat-clearing fire-reducing sore-throat-relieving plant beverage and preparation method thereof | |
| KR20100104331A (en) | Composition of health beverage | |
| CN104068166A (en) | Camphor flavored green tea and preparation method thereof | |
| CN108523121A (en) | A kind of functional food and preparation method thereof of anti-haze clearing lung-heat | |
| CN108497056B (en) | Guava preservative and preparation method thereof | |
| KR100755728B1 (en) | Health food composition for asthma and preparation process of the same | |
| CN105284963B (en) | Cock skin fruit tree special plant fungicide and its production method | |
| CN107094868A (en) | A kind of red bayberry preservative being combined based on plant extracts | |
| CN106962468A (en) | It is a kind of to extend red bayberry and go mouldy the cold nebulization preservation method of rotten time | |
| CN103704409B (en) | A kind of cold tea and preparation method thereof | |
| KR101950983B1 (en) | Composition of elderberry and mehod of making beverage using the same | |
| CN106332993A (en) | Quick-acting tea leaves with full aroma and preparation method thereof | |
| KR101971422B1 (en) | Process for preparing bellflower pear juice composition and bellflower pear juice prepared by the composition |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170531 |