CN106719804A - A kind of metope mildew removing agent and preparation method thereof - Google Patents
A kind of metope mildew removing agent and preparation method thereof Download PDFInfo
- Publication number
- CN106719804A CN106719804A CN201710026324.6A CN201710026324A CN106719804A CN 106719804 A CN106719804 A CN 106719804A CN 201710026324 A CN201710026324 A CN 201710026324A CN 106719804 A CN106719804 A CN 106719804A
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- China
- Prior art keywords
- removing agent
- parts
- mildew removing
- metope
- sodium
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
- A01N31/16—Oxygen or sulfur directly attached to an aromatic ring system with two or more oxygen or sulfur atoms directly attached to the same aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/02—Amines; Quaternary ammonium compounds
- A01N33/12—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/10—Aromatic or araliphatic carboxylic acids, or thio analogues thereof; Derivatives thereof
Abstract
The invention discloses a kind of metope mildew removing agent and preparation method thereof, the metope mildew removing agent it is main by 5~10 parts of sodium chlorites, 5~10 parts of hydrogen peroxide, 0.05~0.1 part of EDETATE DISODIUM, 0.05~0.5 part of bleeding agent, 0.5~1 part of sodium metasilicate, 0.1~0.5 part of mould inhibitor and the agitated dissolvings of deionized water after, adjust pH to 11~12 using 10wt% sodium hydroxide solutions and be obtained.The characteristics of mildew removing agent that the present invention is provided has safe and nontoxic, is mainly used in removing the mould on the surfaces such as cement, fragment of brick, ceramic tile, glass, and long-term mould proof effect is played while having and suppressing fungus growth.
Description
Technical field
The invention belongs to mildew removing agent technical field, it is related to a kind of mildew removing agent and preparation method thereof, more particularly to cement, brick
The mildew removing agent of the metopes such as block, ceramic tile, glass.
Technical background
With the improvement of living condition, the finishing of metope is increasingly popularized, wall surfacing while visual sense of beauty is brought,
Also the nutritional ingredient required for having carried a large amount of suitable fungus growths secretly, under appropriate conditions, mycotic spore can just grow simultaneously
Rapid breeding spreads to form mould spot.Mildew not only makes metope become ugly, but also can serious harm person health.There is research table
Bright Long Term Contact and suction mould, can trigger breathing problem and allergic symptom, such as bronchitis, tonsillitis, Hay Fever,
Asthma etc.；The low people of immunity is also possible to therefore cause headache, fever etc., while can also hide a large amount of hepatitis viruses in mould
And influenza virus etc..Many people are erased using rag or whitewashed a wall again and tackle the metope of mildew, but this can not be killed
Mould, can recur again under the suitable conditions.There is more mould remover product on the market at present, it is main to use hypochlorite by mould
Oxidation Decomposition, but because hypochlorite stability is poor, should not preserve for a long time, without mildew-proof function after decomposition.
Patent 201410615237.0 discloses a kind of preparation method of metope mildew removing agent, and main component is that 84 thimerosals are same
When also compounded plant extracts, this can reduce the stability of product.Except being also had using various sterilization agent using hypochlorite
The method configuration mildew removing agent of compounding, patent 201010131603.7 discloses a kind of mildew-proof mildew-eliminating agent for walls, using hydroxyl hexichol
Ether, Biphenthrin, borax, alcohol etc. are configured, and have preferable anti-mold effect, but except mould speed is slow.
The content of the invention
The technical problems to be solved by the invention are to overcome existing technical deficiency, there is provided it is a kind of it is stable in properties, except mould effect
Really the mildew removing agent of good, safety and environmental protection with and preparation method thereof.
First technical problem to be solved by this invention is to provide a kind of metope mildew removing agent, the mildew removing agent it is main by with
The raw material of lower parts by weight is obtained：5~10 parts of sodium chlorite, 5~10 parts of hydrogen peroxide, 0.05~0.1 part of EDETATE DISODIUM, infiltration
0.05~0.5 part of agent, 0.5~1 part of sodium metasilicate, 0.1~0.5 part of mould inhibitor, solvent is deionized water.
Wherein, in above-mentioned metope mildew removing agent, the sodium chlorite is 80wt% sodium chlorites solid and 50wt% chlorous acid
At least one in sodium liquid.
Wherein, in above-mentioned metope mildew removing agent, the mass concentration of the hydrogen peroxide is 27.5%.
Wherein, in above-mentioned metope mildew removing agent, the bleeding agent is Phosphate of Polyoxyethylene Isooctyl Ether, dimethyl
At least one in base glycine betaine and water-soluble azone.
Wherein, in above-mentioned metope mildew removing agent, the mould inhibitor is benzalkonium chloride, triclosan, potassium sorbate and methyl hydroxybenzoate
In at least one.
Second technical problem to be solved by this invention is to provide the preparation method of above-mentioned metope mildew removing agent, the method tool
Body is comprised the following steps：
(1), to 65~75 parts of deionized waters, 5~10 parts of sodium chlorites, 0.05~0.1 part of EDTA bis- of addition in reactor
Sodium salt and 0.5~1 part of sodium metasilicate, stirring to all of solid are completely dissolved；
(2), under stirring condition, to added in step (1) described reactor 5~10 parts of hydrogen peroxide, 0.05~0.5 part ooze
Saturating agent, 0.1~0.5 part of mould inhibitor, continue to stir 25~35min, obtain mixed liquor；
(3), to the sodium hydroxide solution that mass fraction 8~12% is added dropwise in above-mentioned mixed liquor, by the pH of the mixed liquor
11~12 are adjusted to, then add deionized water, constant volume.
Wherein, the preparation method of above-mentioned metope mildew removing agent, in step (1), the time of the stirring is 30min.
The beneficial effects of the invention are as follows：The characteristics of mildew removing agent that the present invention is provided has safe and nontoxic, using low in formula
The sodium chlorite and hydrogen peroxide of concentration are used as mildew removing agent, good stability, while compound stabilizer and bleeding agent, improve mildew removing agent
Stability, permeability, can effectively oxidation Decomposition mould and its spore；The addition of mould inhibitor, also extends mycete on wall
Recurrence time, plays the purpose of long-acting mould-proof.
Brief description of the drawings
Fig. 1 is the metope mildew removing agent that uses embodiment 1 to prepare, and except comparison diagram before and after mould, (a figures are except before mould, b figures are except mould
Afterwards).
Specific embodiment
The invention provides a kind of metope mildew removing agent, the mildew removing agent is mainly obtained by the raw material of following parts by weight：It is sub-
5~10 parts of sodium chlorate, 5~10 parts of hydrogen peroxide, 0.05~0.1 part of EDETATE DISODIUM, 0.05~0.5 part of bleeding agent, sodium metasilicate 0.5
~1 part, 0.1~0.5 part of mould inhibitor, solvent is deionized water；The sodium chlorite be 80wt% sodium chlorites solid and
At least one in 50wt% sodium chlorite liquid；The mass concentration of the hydrogen peroxide is 27.5%；The bleeding agent is different pungent
At least one in alcohol polyoxyethylene ether phosphate, dodecyldimethylammonium hydroxide inner salt and water-soluble azone；It is described mould proof
Agent is at least one in benzalkonium chloride, triclosan, potassium sorbate and methyl hydroxybenzoate.
Further, present invention also offers the preparation method of above-mentioned metope mildew removing agent, the method specifically includes following step
Suddenly：
(1), to 65~75 parts of deionized waters, 5~10 parts of sodium chlorites, 0.05~0.1 part of EDTA bis- of addition in reactor
Sodium salt and 0.5~1 part of sodium metasilicate, stirring to all of solid are completely dissolved；
(2), under stirring condition, to added in step (1) described reactor 5~10 parts of hydrogen peroxide, 0.05~0.5 part ooze
Saturating agent, 0.1~0.5 part of mould inhibitor, continue to stir 25~35min, obtain mixed liquor；
(3), to the sodium hydroxide solution that mass fraction 8~12% is added dropwise in above-mentioned mixed liquor, by the pH of the mixed liquor
11~12 are adjusted to, then add deionized water, be settled to 100 parts.
Wherein, the preparation method of above-mentioned metope mildew removing agent, in step (1), the time of the stirring is 30min.
Mildew removing agent provided by the present invention is applied to the metopes such as cement, fragment of brick, ceramic tile, glass, and low concentration is used in formula
Sodium chlorite and hydrogen peroxide as mildew removing agent, good stability, while compound stabilizer and bleeding agent, improve the steady of mildew removing agent
Qualitative, permeability, can effectively oxidation Decomposition mould and its spore；The addition of mould inhibitor, also extends the recurrence of mycete on wall
Time, play the purpose of long-acting mould-proof.
The present invention is made further explanation and description below in conjunction with specific embodiment, but and is not so limited the present invention
Protection domain.
Embodiment 1
The preparation method of metope mildew removing agent, comprises the following steps：
(1), to added in the reactor equipped with agitator 70 parts of deionized waters, 6 parts of sodium chlorite solids (80wt%),
0.05 part of EDETATE DISODIUM and 0.5 part of sodium metasilicate, stirring 30min to all of solid are completely dissolved；
(2), under stirring condition, to adding 6 parts of hydrogen peroxide (mass concentrations of hydrogen peroxide in step (1) described reactor
For 27.5%), 0.1 part of bleeding agent-Phosphate of Polyoxyethylene Isooctyl Ether, 0.2 part of mould inhibitor-triclosan, continue stir
30min, obtains mixed liquor；
(3), to the sodium hydroxide solution that mass fraction 10% is added dropwise in above-mentioned mixed liquor, the pH of the mixed liquor is adjusted to
11, then add deionized water, it is settled to 100 parts.
Embodiment 2
The preparation method of metope mildew removing agent, comprises the following steps：
(1), to added in the reactor equipped with agitator 70 parts of deionized waters, 8 parts of sodium chlorite solids (80wt%),
0.08 part of EDETATE DISODIUM and 0.8 part of sodium metasilicate, stirring 30min to all of solid are completely dissolved；
(2), under stirring condition, to adding 4 parts of hydrogen peroxide (mass concentrations of hydrogen peroxide in step (1) described reactor
For 27.5%), 0.1 isooctanol part bleeding agent polyoxyethylene ether phosphate, 0.2 part of mould inhibitor-triclosan, continue to stir 30min,
Obtain mixed liquor；
(3), to the sodium hydroxide solution that mass fraction 10% is added dropwise in above-mentioned mixed liquor, the pH of the mixed liquor is adjusted to
11, then add deionized water, it is settled to 100 parts.
Embodiment 3
The preparation method of metope mildew removing agent, comprises the following steps：
(1), to added in the reactor equipped with agitator 70 parts of deionized waters, 10 parts of sodium chlorite solids (80wt%),
0.08 part of EDETATE DISODIUM and 0.8 part of sodium metasilicate, stirring 30min to all of solid are completely dissolved；
(2), under stirring condition, to adding 2 parts of hydrogen peroxide (mass concentrations of hydrogen peroxide in step (1) described reactor
For 27.5%), the poly- part bleeding agent oxygen ethene ether phosphate of 0.1- isooctanol, 0.2 part of mould inhibitor-triclosan, continue stir
30min, obtains mixed liquor；
(3), to the sodium hydroxide solution that mass fraction 10% is added dropwise in above-mentioned mixed liquor, the pH of the mixed liquor is adjusted to
11, then add deionized water, it is settled to 100 parts.
Embodiment 4
The preparation method of metope mildew removing agent, comprises the following steps：
(1), to added in the reactor equipped with agitator 70 parts of deionized waters, 8 parts of sodium chlorite solids (80wt%),
0.08 part of EDETATE DISODIUM and 0.8 part of sodium metasilicate, stirring 30min to all of solid are completely dissolved；
(2), under stirring condition, to adding 4 parts of hydrogen peroxide (mass concentrations of hydrogen peroxide in step (1) described reactor
For 27.5%), 0.1 part of bleeding agent-dodecyldimethylammonium hydroxide inner salt, -0.2 part of benzalkonium chloride of mould inhibitor and 0.2 part of benzoic acid,
Continue to stir 30min, obtain mixed liquor；
(3), to the sodium hydroxide solution that mass fraction 10% is added dropwise in above-mentioned mixed liquor, the pH of the mixed liquor is adjusted to
11, then add deionized water, it is settled to 100 parts.
Embodiment 5
The preparation method of metope mildew removing agent, comprises the following steps：
(1), to added in the reactor equipped with agitator 70 parts of deionized waters, 8 parts of sodium chlorite solids (80wt%),
0.08 part of EDETATE DISODIUM and 0.8 part of sodium metasilicate, stirring 30min to all of solid are completely dissolved；
(2), under stirring condition, to adding 4 parts of hydrogen peroxide (mass concentrations of hydrogen peroxide in step (1) described reactor
For 27.5%), 0.1 part of bleeding agent-water solubility azone, -0.2 part of triclosan of mould inhibitor and 0.2 part of Sodium Benzoate, continue to stir
30min is mixed, mixed liquor is obtained；
(3), to the sodium hydroxide solution that mass fraction 10% is added dropwise in above-mentioned mixed liquor, the pH of the mixed liquor is adjusted to
11, then add deionized water, it is settled to 100 parts.
Embodiment 1~5 is respectively provided with good except mould and anti-mold effect：Above-mentioned mildew removing agent is smeared or is sprayed on and has been undergone
Onto the common metope of ball spore cladosporium pollution, after 8~15min, you can substantially find that the mould of wall surface is oxidized and decompose；
Also, 4~6 months persistently are observed, the mouldy metope treated through mould inhibitor of the present invention is not infected by mycotic spore again.
The above is the preferred embodiments of the present invention, it is noted that for a person skilled in the art, is not being taken off
On the premise of structure of the present invention, various modifications and improvements can be made, these should also be as being considered as protection scope of the present invention,
The practicality of these effects implemented all without the influence present invention and this patent.
Claims (7)
1. metope mildew removing agent, it is characterised in that the mildew removing agent is mainly obtained by the raw material of following parts by weight：Sodium chlorite 5
~10 parts, 5~10 parts of hydrogen peroxide, 0.05~0.1 part of EDETATE DISODIUM, 0.05~0.5 part of bleeding agent, 0.5~1 part of sodium metasilicate,
0.1~0.5 part of mould inhibitor, solvent is deionized water.
2. metope mildew removing agent according to claim 1, it is characterised in that the sodium chlorite is 80wt% sodium chlorite solids
With at least one in 50wt% sodium chlorite liquid.
3. metope mildew removing agent according to claim 1, it is characterised in that the mass concentration of the hydrogen peroxide is 27.5%.
4. metope mildew removing agent according to claim 1, it is characterised in that the bleeding agent is isooctanol polyethoxylate phosphoric acid
At least one in ester, dodecyldimethylammonium hydroxide inner salt and water-soluble azone.
5. metope mildew removing agent according to claim 1, it is characterised in that the mould inhibitor is benzalkonium chloride, triclosan, sorb
At least one in sour potassium and methyl hydroxybenzoate.
6. the preparation method of metope mildew removing agent described in any one of Claims 1 to 5, it is characterised in that the method specifically include with
Lower step：
(1), to 65~75 parts of deionized waters, 5~10 parts of sodium chlorites, 0.05~0.1 part of EDETATE DISODIUM of addition in reactor
With 0.5~1 part of sodium metasilicate, stir to all of solid and be completely dissolved；
(2), under stirring condition, to added in step (1) described reactor 5~10 parts of hydrogen peroxide, 0.05~0.5 part infiltration
Agent, 0.1~0.5 part of mould inhibitor, continue to stir 25~35min, obtain mixed liquor；
(3), to the sodium hydroxide solution that mass fraction 8~12% is added dropwise in above-mentioned mixed liquor, the pH of the mixed liquor is adjusted to
11~12, then add deionized water, it is settled to 100 parts.
7. the preparation method of metope mildew removing agent according to claim 6, it is characterised in that in step (1), the stirring when
Between be 30min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710026324.6A CN106719804A (en) | 2017-01-13 | 2017-01-13 | A kind of metope mildew removing agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710026324.6A CN106719804A (en) | 2017-01-13 | 2017-01-13 | A kind of metope mildew removing agent and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN106719804A true CN106719804A (en) | 2017-05-31 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710026324.6A Pending CN106719804A (en) | 2017-01-13 | 2017-01-13 | A kind of metope mildew removing agent and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108576035A (en) * | 2018-05-07 | 2018-09-28 | 广州佳伲思抗菌材料有限公司 | A kind of mildew removing agent and preparation method thereof |
| CN108659709A (en) * | 2018-04-10 | 2018-10-16 | 广西南疆科技服务有限公司 | It is a kind of to remove mould mildew removing agent and preparation method thereof for metope |
| CN114503981A (en) * | 2022-01-07 | 2022-05-17 | 上海膜益信息科技有限公司 | Non-layering mildew preventive and preparation method and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101623002A (en) * | 2008-07-07 | 2010-01-13 | 刘铁刚 | Wall mould fungus remover and preparation method thereof |
| CN103798284A (en) * | 2013-10-15 | 2014-05-21 | 刘强 | Mold cleaning agent |
| CN105309474A (en) * | 2014-07-29 | 2016-02-10 | 崔起龙 | Wall mold cleaning spray |
| CN105994357A (en) * | 2016-05-21 | 2016-10-12 | 杨勇 | Compound mildew preventive |
-
2017
- 2017-01-13 CN CN201710026324.6A patent/CN106719804A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101623002A (en) * | 2008-07-07 | 2010-01-13 | 刘铁刚 | Wall mould fungus remover and preparation method thereof |
| CN103798284A (en) * | 2013-10-15 | 2014-05-21 | 刘强 | Mold cleaning agent |
| CN105309474A (en) * | 2014-07-29 | 2016-02-10 | 崔起龙 | Wall mold cleaning spray |
| CN105994357A (en) * | 2016-05-21 | 2016-10-12 | 杨勇 | Compound mildew preventive |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108659709A (en) * | 2018-04-10 | 2018-10-16 | 广西南疆科技服务有限公司 | It is a kind of to remove mould mildew removing agent and preparation method thereof for metope |
| CN108576035A (en) * | 2018-05-07 | 2018-09-28 | 广州佳伲思抗菌材料有限公司 | A kind of mildew removing agent and preparation method thereof |
| CN114503981A (en) * | 2022-01-07 | 2022-05-17 | 上海膜益信息科技有限公司 | Non-layering mildew preventive and preparation method and application thereof |
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