CN106716118A - Oil degradation meter and method for evaluating oil degradation - Google Patents
Oil degradation meter and method for evaluating oil degradation Download PDFInfo
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- CN106716118A CN106716118A CN201580049990.0A CN201580049990A CN106716118A CN 106716118 A CN106716118 A CN 106716118A CN 201580049990 A CN201580049990 A CN 201580049990A CN 106716118 A CN106716118 A CN 106716118A
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- Prior art keywords
- grease
- dielectric constant
- acid number
- oil
- memory cell
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- 238000000034 method Methods 0.000 title abstract description 10
- 230000015556 catabolic process Effects 0.000 title abstract 5
- 238000006731 degradation reaction Methods 0.000 title abstract 5
- 238000005259 measurement Methods 0.000 claims abstract description 7
- 239000004519 grease Substances 0.000 claims description 118
- 239000002253 acid Substances 0.000 claims description 56
- 230000032683 aging Effects 0.000 claims description 45
- 230000015654 memory Effects 0.000 claims description 25
- 238000011156 evaluation Methods 0.000 claims description 17
- 230000006399 behavior Effects 0.000 claims description 10
- 235000013305 food Nutrition 0.000 abstract description 6
- 230000002378 acidificating effect Effects 0.000 abstract 1
- 239000000463 material Substances 0.000 description 9
- 239000008157 edible vegetable oil Substances 0.000 description 5
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 239000004973 liquid crystal related substance Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 230000006641 stabilisation Effects 0.000 description 2
- 238000011105 stabilization Methods 0.000 description 2
- 238000002479 acid--base titration Methods 0.000 description 1
- 150000001491 aromatic compounds Chemical class 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000002847 impedance measurement Methods 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
- G01N27/02—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance
- G01N27/22—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating capacitance
- G01N27/221—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating capacitance by investigating the dielectric properties
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/02—Food
- G01N33/03—Edible oils or edible fats
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/26—Oils; Viscous liquids; Paints; Inks
- G01N33/28—Oils, i.e. hydrocarbon liquids
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/26—Oils; Viscous liquids; Paints; Inks
- G01N33/28—Oils, i.e. hydrocarbon liquids
- G01N33/2805—Oils, i.e. hydrocarbon liquids investigating the resistance to heat or oxidation
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Immunology (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Pathology (AREA)
- Food Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Investigating Or Analyzing Materials By The Use Of Electric Means (AREA)
Abstract
Provided are an oil degradation meter and a method for evaluating oil degradation, which allow a user to set an arbitrary level of degradation of an oil/fat using acidic value (AV) as an indicator, regardless of differing parameters such as the moisture content of foods to be fried, so as to allow the user to know, easily and with reliable repeatability, when to change the oil/fat. According to a setting procedure, the user: sets the acidity value (AV0) of unused oil/fat as 0; measures and records the dielectric constant (D0) of the oil/fat at this time; measures the dielectric constant (D100) of the oil/fat at the time of changing under specific oil/fat usage conditions; and records this dielectric constant (D100) along with the acidity value (AV100) at this time. According to a measurement procedure, the user measures the dielectric constant (Dn) of a sample oil/fat, and calculates the acidity value (AVn) of said sample oil/fat on the basis of the dielectric constants (D0, D100) and the acidity value (AV100) recorded during the setting procedure, using the formula AVn = AV100 x ((Dn - D0) / (D100 - D0)).
Description
Technical field
The present invention relates to the state by evaluating grease grease it is aging based on and grease Degree of Ageing evaluation method.
Background technology
As the index of refined and rotten (Degree of Ageing) of edible oil and fat, polar compound amount (Total Polar are used
Materials (total polar substances):Hereinafter referred to as " TPM values ".), acid number (Acid Value:Hereinafter referred to as " AV values ") etc..
TPM values are, with the amount of the general name of following material i.e. polar compound (TPM) as target value is referred to, to be somebody's turn to do in edible oil and fat
Material be produced by the moisture in food materials (Fried Fishes) free fatty, because of heating increased aromatic compound, with
And because aoxidizing material of generation etc. with air contact.The TPM values can be derived from the measurement result of the dielectric constant of grease.
Amount of the AV values as the potassium hydroxide (KOH) in order in and required for the free fatty present in 1g edible oil and fat
(mg) define.
Additionally, in Europe using TPM as index, and in Japan using AV values as index.
Prior art literature
Non-patent literature
Non-patent literature 1:Nagoya unity and coherence in writing great Ji wants No. 12 (2012) (P.121-P.13) city river and clear " edible oil
Plus Hot Lieization Evaluation value-PV/CV/AV Zhi と Very compound Liang Xiang Seki-" (Nagoya unity and coherence in writing university summary the 12nd
(2012) (P.121-P.13) city river and it is clear " evaluation-PV/CV/AV of the heat ageing of edible oil value and polar compound amount
Correlation ").
The content of the invention
The invention problem to be solved
Due to can easily obtain the dielectric constant of grease by the measure of the impedance of grease, therefore, easily determine TPM
Value.On the other hand, in order to neutralize the measure of the amount of the potassium hydroxide required for free fatty, it is necessary to dripped by neutralizing
It is fixed to carry out, so being not easy.
Also, it is uncorrelated between the dielectric constant of grease and AV values, can be because of bars such as the moistures in food materials (Fried Fishes)
Part and turn into entirely different value.Therefore, using AV values as in the case of index, the measure of AV values is not easy to, therefore, present situation
It is to change grease limit point is empirically found out from color and smell of grease etc..
Therefore, the present invention is to propose in view of the foregoing, it is therefore intended that provide a kind of aging meter of grease and grease is old
Change degree evaluation method, even if in the case of the condition difference such as moisture in food materials (Fried Fishes), it is also possible to by user
Any Degree of Ageing for setting the grease with acid number (AV values) as index, can easily know grease according to the repeatability of stabilization
Replacing period.
Means for solving the problems
In order to solve above-mentioned problem and realize above-mentioned purpose, the aging meter of grease of the invention has following structure.
[structure 1]
Structure 1 is characterised by, possesses the Dielectric Coefficient unit, right being measured to the dielectric constant of sample grease
Memory cell that the dielectric constant determined by Dielectric Coefficient unit is stored, input acid number will be simultaneously input into
Acid number stores input block to memory cell, carries out the fortune of the computing based on the dielectric constant and acid number stored in memory cell
Unit and the control unit being controlled to Dielectric Coefficient unit, input block, memory cell and arithmetic element are calculated,
Under setting pattern, control unit is by the acid number (AV of unused grease0) 0 is set to, determine dielectric constant (D now0) and store
In the memory unit, the dielectric constant (D of the grease for changing period under specific grease behaviour in service is determined100), together with now
Acid number (AV100) be collectively stored in memory cell, under mode determination, control unit determines the dielectric constant of sample grease
(Dn), by its measurement result (Dn) store in the memory unit, and according to the dielectric for being stored under setting pattern in the memory unit
Constant (D0, D100) and acid number (AV100), arithmetic expression [AV is passed through by arithmetic elementn=AV100×{(Dn-D0)/(D100-D0)], meter
Calculate the acid number (AV of sample greasen)。
[structure 2]
In the aging meter of grease with structure 1, it is characterised by the acid number (AV of the grease in the period of replacing100) be defined as
100。
Also, grease Degree of Ageing evaluation method of the invention has following structure.
[structure 3]
Structure 3 is characterised by, in operation is set, by the acid number (AV of unused grease0) 0 is set to, determine now
Dielectric constant (D0) and recorded, determine the dielectric constant of the grease for changing period under specific grease behaviour in service
(D100), together with acid number (AV now100) recorded together, in mensuration operation, determine the dielectric constant of sample grease
(Dn), according to the dielectric constant (D recorded in setting operation0, D100) and acid number (AV100), by arithmetic expression [AVn=AV100×
{(Dn-D0)/(D100-D0)], calculate the acid number (AV of sample greasen)。
[structure 4]
In the grease Degree of Ageing evaluation method with structure 3, it is characterised by the acid number of the grease in the period of replacing
(AV100) it is defined as 100.
The effect of invention
In the aging meter of grease of the invention, under setting pattern, storage is not used the acid number (AV of grease0) and dielectric
Constant (D0), and store under specific grease behaviour in service replacing period grease acid number (AV100) and dielectric constant
(D100), under mode determination, determine the dielectric constant (D of sample greasen), by arithmetic expression [AVn=AV100×{(Dn-D0)/
(D100-D0)], calculate the acid number (AV of sample greasen)。
Additionally, in grease Degree of Ageing evaluation method of the invention, in operation is set, record is not used the acid number of grease
(AV0) and dielectric constant (D0), and record under specific grease behaviour in service replacing period grease acid number (AV100) with
And dielectric constant (D100), in mensuration operation, determine the dielectric constant (D of sample greasen), by arithmetic expression [AVn=AV100×
{(Dn-D0)/(D100-D0)], calculate the acid number (AV of sample greasen)。
If additionally, by change period grease acid number (AV100) be defined as 100, then can be according to the sample oil for determining
Dielectric constant (the D of fatn), calculate the percentage untill replacing period.
Therefore, in the aging meter of grease of the invention and grease Degree of Ageing evaluation method, can be according to objective reliability
The measure numerical value of dielectric constant high, by being scaled acid number, knows the replacing period of grease.
That is, the present invention can provide a kind of aging meter of grease and grease Degree of Ageing evaluation method, even if (fried in food materials
Thing) in the condition such as moisture difference in the case of, it is also possible to arbitrarily set by user with acid number (AV values) as index
The Degree of Ageing of grease, can easily know the replacing period of grease according to the repeatability of stabilization.
Brief description of the drawings
Fig. 1 is the block diagram of the structure for representing the aging meter of grease of the invention.
Fig. 2 is the chart of the relation between the dielectric constant and acid number (AV values) for representing grease.
Fig. 3 is the flow chart for illustrating grease Degree of Ageing evaluation method of the invention.
Specific embodiment
Hereinafter, with reference to the accompanying drawings of the aging meter of grease of the invention and the implementation method of grease Degree of Ageing evaluation method.
[summary of the structure of the aging meter of grease of the invention]
Fig. 1 is the block diagram of the structure for representing the aging meter of grease of the invention.
The aging meter of the grease is the dielectric constant for determining sample grease, and AV values (acid number) are calculated according to its measurement result
Device.
As shown in figure 1, the aging meter of the grease possesses as the CPU1 of control unit.CPU1 controls are surveyed as dielectric constant
The dielectric constant sensor 2 of order unit.Dielectric constant sensor 2 has and is immersed in comb electrodes in sample grease, by
Apply alternating voltage between the comb electrodes, the impedance of sample grease can be determined according to the change of frequency.According to the impedance
Measurement result, the dielectric constant of sample grease can be calculated.
Additionally, CPU1 controls are processed the input signal from the input unit 4 as the input unit 4 of input block.
In addition to AV values (acid number), additionally it is possible to be input into the instructions such as various numerical value, pattern selection to input unit 4.
Also, CPU1 is controlled as the memory 3 of memory cell.The storage of memory 3 is determined by dielectric constant sensor 2
Dielectric constant, AV values (acid number), other the various numerical value of input for going out.
Additionally, computing circuit 5 of the CPU1 controls as arithmetic element.Computing circuit 5 is carried out based on storage in memory 3
The computing of dielectric constant and AV values (acid number), other various computings.
Additionally, CPU1 is connected with liquid crystal display part 6.Liquid crystal display part 6 shows the AV being input into by the user of the device
The various information such as value (acid number), other various numerical value, the operation result based on computing circuit 5.
[grease Degree of Ageing evaluation method (action of the aging meter of grease) of the invention]
Fig. 2 is the chart of the relation between the dielectric constant and acid number (AV values) for representing grease.
(a) in Fig. 2 be represent the dielectric constant of the grease in fried shop (1), fried shop (2) and fried shop (3) with
The chart of the relation between acid number (AV values).
(b) in Fig. 2 is the dielectric constant for representing the grease in tempura shop, Japanese restaurant, butcher's and supermarket
With the chart of the relation between acid number (AV values).
Additionally, in Fig. 2, transverse axis represents TPM values, the TPM values are the values related to the dielectric constant of grease.Therefore, the Fig. 2
Show the relation between the dielectric constant and acid number (AV values) of grease.
As shown in Fig. 2 the relation between the dielectric constant of grease and AV values is because of the water in food materials to be processed (Fried Fishes)
The conditions such as point content and it is different.That is, it is linear near when the relation between the dielectric constant to grease and AV values carries out linear approximation
It is different because shop is different like the slope of formula.It is thought that because the species of Fried Fishes, heat time have differences.For example,
In the case that fried amount and frequency are high fried shop as shown in (a) in Fig. 2, compared to its shown in (b) in Fig. 2
His shop, relative to the increase of dielectric constant, the increased ratio of AV values is big, the slope steepness of linear approximation formula.
Additionally, during grease is aging, not observed because of the increase of AV values with as described curve
Tendency, the experimental data in each shop can approximately be showed by straight line.When observation deviate from the point of straight line proximal line, make
AV values then have the error of ± 0.5 or ± 1.0 degree.As the main cause of error, it is believed that because by the color of grease come
Measurement accuracy, data are drawn again, the behaviour in service of grease is different etc..Even if considering these errors, it is also possible to pass through
Straight line approximately shows the increase of the AV values in the ageing process of grease.
Fig. 3 is the flow chart for illustrating grease Degree of Ageing evaluation method of the invention.
The aging meter of the grease performs grease Degree of Ageing evaluation side of the invention by being acted as shown in Figure 3
Method.
That is, when the instruction that setting pattern starts is input into, CPU1 starts to perform setting pattern (setting work in step st1
Sequence), step st2 is proceeded to, if the acid number (AV of grease is not used0) it is 0, determine dielectric constant (D now0), and store (note
Record) in memory 3.
Then, step st3 is proceeded to, the grease in the replacing period (operating limit) under specific grease behaviour in service is determined
Dielectric constant (D100), together with acid number (AV now100) together storage (record) in memory 3.By acid-base titration etc.
Assay method asks for acid number (AV now100)。
Specific grease behaviour in service, refers to fried shop (1), fried shop (2), fried shop (3), tempura shop, Japanese meal
The behaviour in service of the grease in shop, butcher's and supermarket Deng Ge shops, it is believed that if then grease makes in identical shop
It is constant with situation.
Then, step st4 is proceeded to, when the instruction that mode determination starts is input into, CPU1 starts execution mode determination and (sets
Determine operation), step st5 is proceeded to, determine the dielectric constant (D of sample greasen), and by its measurement result (Dn) storage (record)
In memory 3.
Then, step st6, CPU1 are proceeded to according to the dielectric constant for storing (record) in memory 3 under setting pattern
(D0, D100) and acid number (AV100), by computing circuit 5 by following arithmetic expression, calculate the acid number (AV of sample greasen)。
AVn=AV100×{(Dn-D0)/(D100-D0)}
Then, the acid number that step st7, CPU1 show calculated sample grease by liquid crystal display part 6 is proceeded to
(AVn)。
[another example (1) of operation method]
In the aging meter of the grease, can be by the acid number (AV of the grease in the period of replacing100) it is defined as 100.In this case,
According to the dielectric constant (D of the sample grease for determiningn) acid number (AV of sample grease that calculatesn) represent until changing period
Untill percentage.
[another example (2) of operation method]
In the aging meter of the grease, can be by the unused state S of sample grease0With replacing period (operating limit) S100
In grease dielectric constant, i.e. S0Dielectric constant D0With S100Dielectric constant D100Between for example carry out 100 deciles, and set
Determine scale.Additionally, the numerical value for so carrying out decile can not be 100.
That is, it is such as following, it is defined as 1 degree:δD。
1 degree:δD=(D100-D0)/100。
If Degree of Ageing is defined as into An, then measured value D as follows according to dielectric constantnTo ask for Degree of Ageing An。
An=(Dn-D0)/δD。
Therefore, if Dn=D0, then An=0, if Dn=D100, then An=100.
Industrial utilizability
The present invention be applied to the grease of the state by evaluating grease it is aging based on and grease Degree of Ageing evaluation method.
Symbol description
1 CPU、
2 dielectric constant sensors,
3 memories,
4 input units,
5 computing circuits.
Claims (4)
1. the aging meter of a kind of grease, it is characterised in that
The aging meter of the grease possesses:
Dielectric Coefficient unit, its dielectric constant for determining sample grease;
Memory cell, the dielectric constant that its storage is determined by the Dielectric Coefficient unit;
Input block, its input acid number, and the acid number storage that will be input into is in the memory unit;
Arithmetic element, it carries out the computing based on the dielectric constant and acid number stored in the memory cell;And
Control unit, it is to the Dielectric Coefficient unit, the input block, the memory cell and the arithmetic element
It is controlled,
Under setting pattern, the acid number of unused grease is AV by described control unit00 is set to, the dielectric constant for determining now is
D0And store in the memory cell, the dielectric constant for determining the grease in the replacing period under specific grease behaviour in service is
D100, it is AV together with acid number now100It is collectively stored in the memory cell,
Under mode determination, the dielectric constant that described control unit determines sample grease is Dn, it is D by its measurement resultnStorage exists
In the memory cell, according to storing the dielectric constant i.e. D in the memory cell under the setting pattern0、D100And acid
Value is AV100, arithmetic expression [AV is passed through by the arithmetic elementn=AV100×{(Dn-D0)/(D100-D0)], calculate the sample
The acid number of grease is AVn。
2. the aging meter of grease according to claim 1, it is characterised in that
Acid number by the grease in the period of replacing is AV100It is defined as 100.
3. a kind of grease Degree of Ageing evaluation method, it is characterised in that
In operation is set, the acid number by unused grease is AV00 is set to, the dielectric constant for determining now is D0And remembered
Record, the dielectric constant of the grease in the replacing period under the specific grease behaviour in service of measure is D100, it is together with acid number now
AV100Recorded together,
In mensuration operation, the dielectric constant for determining sample grease is Dn, it is according to the dielectric constant recorded in the setting operation
D0、D100It is AV with acid number100, by arithmetic expression [AVn=AV100×{(Dn-D0)/(D100-D0)], calculate the sample grease
Acid number is AVn。
4. grease Degree of Ageing evaluation method according to claim 3, it is characterised in that
Acid number by the grease in the period of replacing is AV100It is defined as 100.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/JP2015/064074 WO2016185524A1 (en) | 2015-05-15 | 2015-05-15 | Oil degradation meter and method for evaluating oil degradation |
Publications (2)
Publication Number | Publication Date |
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CN106716118A true CN106716118A (en) | 2017-05-24 |
CN106716118B CN106716118B (en) | 2020-03-24 |
Family
ID=57319694
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201580049990.0A Active CN106716118B (en) | 2015-05-15 | 2015-05-15 | Grease aging meter and grease aging degree evaluation method |
Country Status (7)
Country | Link |
---|---|
US (1) | US10429332B2 (en) |
EP (1) | EP3296729B1 (en) |
JP (1) | JP6435565B2 (en) |
KR (1) | KR101975308B1 (en) |
CN (1) | CN106716118B (en) |
TW (1) | TWI574004B (en) |
WO (1) | WO2016185524A1 (en) |
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WO2019165734A1 (en) * | 2018-02-27 | 2019-09-06 | 江南大学 | Rapid combined detection device for detecting deterioration degree of frying oil and detection method therefor |
CN110554172A (en) * | 2019-06-06 | 2019-12-10 | 上海传一电子科技有限公司 | Portable lubricating oil state check out test set |
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JP6471300B1 (en) * | 2018-08-21 | 2019-02-20 | 株式会社アタゴ | Oil degradation degree measuring method and oil degradation detection device |
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JP7525757B1 (en) | 2023-03-07 | 2024-07-30 | 株式会社J-オイルミルズ | Grease management device, grease management system, grease management method, and grease management display device |
WO2024185247A1 (en) * | 2023-03-07 | 2024-09-12 | 株式会社J-オイルミルズ | Oil/fat management device, oil/fat management system, oil/fat management method, and oil/fat management display device |
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JPWO2016185524A1 (en) | 2017-07-06 |
WO2016185524A1 (en) | 2016-11-24 |
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JP6435565B2 (en) | 2018-12-12 |
US10429332B2 (en) | 2019-10-01 |
CN106716118B (en) | 2020-03-24 |
KR101975308B1 (en) | 2019-05-07 |
EP3296729B1 (en) | 2020-11-25 |
EP3296729A1 (en) | 2018-03-21 |
TWI574004B (en) | 2017-03-11 |
US20170276629A1 (en) | 2017-09-28 |
EP3296729A4 (en) | 2019-02-27 |
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