CN106675866A - Zirconium phosphate germicidal soap and preparation method thereof - Google Patents
Zirconium phosphate germicidal soap and preparation method thereof Download PDFInfo
- Publication number
- CN106675866A CN106675866A CN201710051427.8A CN201710051427A CN106675866A CN 106675866 A CN106675866 A CN 106675866A CN 201710051427 A CN201710051427 A CN 201710051427A CN 106675866 A CN106675866 A CN 106675866A
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- Prior art keywords
- zirconium phosphate
- parts
- germicidal
- soapses
- component
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
- C11D9/18—Water-insoluble compounds
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention relates to the technical field of chemicals for daily use, and in particular relates to a zirconium phosphate germicidal soap and a preparation method thereof. Raw materials comprise grease, a saponifying agent, zirconium phosphate and water. By adding zirconium phosphate into the zirconium phosphate germicidal soap, the sterilizing property can be effectively enhanced, and the soap is free of irritation to skin and can be used for cleaning skin and clothes and the like. The clothes after washing do not need to be disposed, so that the soap is free of environmental pollution. The preparation method is simple and easy to operate.
Description
Technical field
The present invention relates to household chemicals technical field, in particular to zirconium phosphate germicidal soapses and preparation method thereof.
Background technology
Zirconium phosphate compound is the class Multifunction mesoporous material that developed recently gets up, and is famous layered solid
One of material of most study in sour material family.Zirconium phosphate itself have solid acid catalysis function and using inner layer space as
Reactor, because reactant or product shape are different, causes them to pass in and out the dynamic process of interlayer difference, so as in catalytic reaction
During there is shape selective.Because zirconium phosphate has good chemistry, heat stability and mechanical strength, and can provide
Sizable specific surface area, so having very big application prospect in effective catalyst direction.The catalytic performance of zirconium phosphate not only exists
In the acidity of itself, prior is other objects（Or column-supporting agent）The composite obtained after embedding people.On the one hand, make
The acid geometrical property and Shape-selective that there is adjustable degeneration, pore passage structure is improved of zirconium phosphate；On the other hand, zirconium phosphate can be with
All kinds of different active substances are introduced by various means, to prepare the catalyst and catalyst carrier of different purposes so as to have
There is composite catalyzing performance, therefore the research to this kind of composite will have very vast potential for future development.
But at present, zirconium phosphate is applied among soap the announcement that do not appear in the newspapers.
The content of the invention
The present invention proposes a kind of zirconium phosphate germicidal soapses, can effectively lift the sterilizing function of common soap, and to skin
Skin is non-stimulated.
To achieve these goals, the technical solution adopted in the present invention is that zirconium phosphate germicidal soapses, its raw material includes oil
Fat, saponifier, zirconium phosphate, water.
Further, in zirconium phosphate germicidal soapses raw material, by weight, oils and fatss：Zirconium phosphate=25~35：1.
Preferably, described saponifier is sodium hydroxide.
Preferably, described oils and fatss are using one or more combination in natural plant grease.
Preferably, the one kind in the zirconium phosphate germicidal soapses, its raw material includes by weight：Petiolus Trachycarpi oil 600~
700 parts, 300~400 parts of Oleum Cocois, 300~400 parts of salad oil, 75~125 parts of Semen pruni armeniacae oil, 120~180 parts of olive oil, hydrogen
200~270 parts of sodium oxide, 400~530 parts of water, 35~65 parts of zirconium phosphate.
Preferably, the one kind in the zirconium phosphate germicidal soapses, its raw material includes by weight：650 parts of Petiolus Trachycarpi oil,
350 parts of Oleum Cocois, 350 parts of salad oil, 100 parts of Semen pruni armeniacae oil, 150 parts of olive oil, 234.5 parts of sodium hydroxide, 469 parts of water, phosphorus
50 parts of sour zirconium.
Preferably, can also include that various fumet, lubricant etc. are all kinds of in described zirconium phosphate germicidal soapses raw material
Additive.
A kind of method for preparing zirconium phosphate germicidal soapses as above, comprises the following steps：
1. oils and fatss are heated under stirring 45~50 DEG C, component A is obtained standby；
2. water is mixed with saponifier, saponifier is fully melted, obtain component B standby；
3. component A and zirconium phosphate are added in component B, are stirred, obtained soap lye and enter mould.
Further, the step 3. in first component A is added in component B after mix homogeneously, add zirconium phosphate.
Further, 3. middle mixing time is 35~45min to the step.
Further, the described mould mode that enters is：The soap lye is poured into after mould and wraps up mould with towel.
Further, the step 3. in enter after mould step also include the demoulding with ventilation storage.
Preferably, the ventilation resting period is 25~35 days.
Zirconium phosphate germicidal soapses of the present invention are added zirconium phosphate, can effectively lift bactericidal property, and to skin
It is non-stimulated to can be used for cleaning skin and medicated clothing etc., and the waste water washed after shield need not process environmentally safe.And preparation method
Simply, it is easily operated.
Specific embodiment
The present invention is described in further detail below by specific embodiment.
Embodiment 1：A kind of zirconium phosphate germicidal soapses, its raw material includes by weight：650 parts of Petiolus Trachycarpi oil, Oleum Cocois 350
Part, 350 parts of salad oil, 100 parts of Semen pruni armeniacae oil, 150 parts of olive oil, 234.5 parts of sodium hydroxide, 469 parts of water, 50 parts of zirconium phosphate.
The various additives such as various fumet, lubricant can also be included in described zirconium phosphate germicidal soapses raw material.
Zirconium phosphate germicidal soapses as above are prepared, is comprised the following steps：
1. oils and fatss are heated under stirring 45~50 DEG C, component A is obtained standby；
2. water is mixed with sodium hydroxide, sodium hydroxide is fully melted, obtain component B standby；
3. component A and zirconium phosphate are added in component B, are stirred, obtained soap lye and enter mould.
The step 3. in first component A is added in component B after mix homogeneously, add zirconium phosphate, the step 3. in
Mixing time is 35~45min, and the described mould mode that enters is：The soap lye is poured into after mould and wraps up mould with towel, enter mould
Also include the demoulding with ventilation storage after step.The ventilation resting period is 30 days.
Embodiment 2：A kind of zirconium phosphate germicidal soapses, its raw material includes by weight：600 parts of Petiolus Trachycarpi oil, Oleum Cocois 300
Part, 300 parts of salad oil, 75 parts of Semen pruni armeniacae oil, 120 parts of olive oil, 200 parts of sodium hydroxide, 400 parts of water, 65 parts of zirconium phosphate.
Zirconium phosphate germicidal soapses as above are prepared, is comprised the following steps：
1. oils and fatss are heated under stirring 45~50 DEG C, component A is obtained standby；
2. water is mixed with sodium hydroxide, sodium hydroxide is fully melted, obtain component B standby；
3. component A and zirconium phosphate are added in component B, are stirred, obtained soap lye and enter mould.
The step 3. in first component A is added in component B after mix homogeneously, add zirconium phosphate, the step 3. in
Mixing time is 35~45min, and the described mould mode that enters is：The soap lye is poured into after mould and wraps up mould with towel, enter mould
Also include the demoulding with ventilation storage after step.The ventilation resting period is 35 days.
Embodiment 3：A kind of zirconium phosphate germicidal soapses, its raw material includes by weight：700 parts of Petiolus Trachycarpi oil, Oleum Cocois 400
Part, 400 parts of salad oil, 125 parts of Semen pruni armeniacae oil, 180 parts of olive oil, 270 parts of sodium hydroxide, 530 parts of water, 35 parts of zirconium phosphate.
Zirconium phosphate germicidal soapses as above are prepared, is comprised the following steps：
1. oils and fatss are heated under stirring 45~50 DEG C, component A is obtained standby；
2. water is mixed with sodium hydroxide, sodium hydroxide is fully melted, obtain component B standby；
3. component A and zirconium phosphate are added in component B, are stirred, obtained soap lye and enter mould.
To enter also include after mould step the demoulding with ventilation storage.The ventilation resting period is 25 days
Embodiment 4：A kind of zirconium phosphate germicidal soapses, its raw material includes seed of Camelliasinensis(L.)Ktzel oil, sodium hydroxide, zirconium phosphate, water.By weight
Meter, seed of Camelliasinensis(L.)Ktzel oil：Zirconium phosphate=30：1.Described saponifier is sodium hydroxide.
Zirconium phosphate germicidal soapses as above are prepared, is comprised the following steps：
1. seed of Camelliasinensis(L.)Ktzel oil is heated under stirring 45~50 DEG C, obtains component A standby；
2. water is mixed with sodium hydroxide, sodium hydroxide is fully melted, obtain component B standby；
3. component A and zirconium phosphate are added in component B, are stirred, obtained soap lye and enter mould.
The step 3. in first component A is added in component B after mix homogeneously, add zirconium phosphate, the step 3. in
Mixing time is 35~45min, and the described mould mode that enters is：The soap lye is poured into after mould and wraps up mould with towel, enter mould
Also include the demoulding with ventilation storage after step.The ventilation resting period is 30 days.
Embodiment 5：A kind of zirconium phosphate germicidal soapses, its raw material include seed of Camelliasinensis(L.)Ktzel oil, Oleum Ricini, Radix Oenotherae erythrosepalae oil, cheese pears
Fruit oil, sodium hydroxide, zirconium phosphate, water.By weight, compound lard total amount：Zirconium phosphate=25：1.Described zirconium phosphate sterilization
The various additives such as various fumet, lubricant can also be included in soap.
Zirconium phosphate germicidal soapses as above are prepared, is comprised the following steps：
1. oils and fatss mixing is heated under stirring 45~50 DEG C, obtains component A standby；
2. water is mixed with saponifier, saponifier is fully melted, obtain component B standby；
3. component A and zirconium phosphate are added in component B, are stirred, obtained soap lye and enter mould.
The step 3. in first component A is added in component B after mix homogeneously, add zirconium phosphate, described enters mould side
Formula is：The soap lye is poured into after mould and wraps up mould with towel, to enter also include after mould step the demoulding with ventilation storage.Ventilation is deposited
The time is put for 25 days.
Embodiment 6：A kind of zirconium phosphate germicidal soapses, its raw material includes Oleum Vitis viniferae, hazelnut oil, Jojoba oil, hydroxide
Sodium, zirconium phosphate, water.By weight, compound lard total amount：Zirconium phosphate=35：1.Described saponifier is sodium hydroxide.
Zirconium phosphate germicidal soapses as above are prepared, is comprised the following steps：
1. oils and fatss mixing is heated under stirring 45~50 DEG C, obtains component A standby；
2. water is mixed with saponifier, saponifier is fully melted, obtain component B standby；
3. component A and zirconium phosphate are added in component B, are stirred, obtained soap lye and enter mould.
To enter also include after mould step the demoulding with ventilation storage.The ventilation resting period is 35 days.
Embodiment 7：A kind of zirconium phosphate germicidal soapses, its raw material includes waste oil, sodium hydroxide, zirconium phosphate, water.By weight
Part meter, waste oil：Zirconium phosphate=30：1.Described waste oil is the waste oil after decolouring, washing, deodorization, sterilisation step.
Described saponifier is sodium hydroxide.
Zirconium phosphate germicidal soapses as above are prepared, is comprised the following steps：
1. waste oil oil is heated under stirring 45~50 DEG C, obtains component A standby；
2. water is mixed with sodium hydroxide, sodium hydroxide is fully melted, obtain component B standby；
3. component A and zirconium phosphate are added in component B, are stirred, obtained soap lye and enter mould.
The preferred embodiments of the present invention are the foregoing is only, the present invention is not limited to, for the skill of this area
For art personnel, there can be various modifications and variations in the spirit and principles in the present invention, the modification of these equivalents or replacement etc.,
It is all contained within protection scope of the present invention.
Claims (10)
1. zirconium phosphate germicidal soapses, it is characterised in that its raw material includes oils and fatss, saponifier, zirconium phosphate, water.
2. zirconium phosphate germicidal soapses according to claim 1, it is characterised in that in raw material, by weight, oils and fatss：Phosphorus
Sour zirconium=25~35：1.
3. zirconium phosphate germicidal soapses according to claim 1, it is characterised in that：Described saponifier is sodium hydroxide.
4. zirconium phosphate germicidal soapses according to claim 1 and 2, it is characterised in that：Described oils and fatss adopt natural plants
One or more combination in oils and fatss.
5. zirconium phosphate germicidal soapses according to claim 1 or 2 or 3, it is characterised in that in the zirconium phosphate germicidal soapses
One kind, its raw material includes by weight：600~700 parts of Petiolus Trachycarpi oil, 300~400 parts of Oleum Cocois, salad oil 300~400
Part, 75~125 parts of Semen pruni armeniacae oil, 120~180 parts of olive oil, 200~270 parts of sodium hydroxide, 400~530 parts of water, zirconium phosphate
35~65 parts.
6. zirconium phosphate germicidal soapses according to claim 5, it is characterised in that the one kind in zirconium phosphate germicidal soapses, its
Raw material includes by weight：650 parts of Petiolus Trachycarpi oil, 350 parts of Oleum Cocois, 350 parts of salad oil, 100 parts of Semen pruni armeniacae oil, olive oil
150 parts, 234.5 parts of sodium hydroxide, 469 parts of water, 50 parts of zirconium phosphate.
7. the method that one kind prepares the zirconium phosphate germicidal soapses as described in claim 1-6 is any, comprises the following steps：
1. oils and fatss are heated under stirring 45~50 DEG C, component A is obtained standby；
2. water is mixed with saponifier, saponifier is fully melted, obtain component B standby；
3. component A and zirconium phosphate are added in component B, are stirred, obtained soap lye and enter mould.
8. the preparation method of a kind of zirconium phosphate germicidal soapses according to claim 7, it is characterised in that：The step 3. in
First component A is added in component B after mix homogeneously, zirconium phosphate is added.
9. the preparation method of a kind of zirconium phosphate germicidal soapses according to claim 7, it is characterised in that：Described enters mould side
Formula is：The soap lye is poured into after mould and wraps up mould with towel.
10. the preparation method of a kind of zirconium phosphate germicidal soapses according to claim 7, it is characterised in that：The step is 3.
In to enter after mould step also include the demoulding with ventilation storage.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710051427.8A CN106675866A (en) | 2017-01-23 | 2017-01-23 | Zirconium phosphate germicidal soap and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710051427.8A CN106675866A (en) | 2017-01-23 | 2017-01-23 | Zirconium phosphate germicidal soap and preparation method thereof |
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| CN106675866A true CN106675866A (en) | 2017-05-17 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710051427.8A Pending CN106675866A (en) | 2017-01-23 | 2017-01-23 | Zirconium phosphate germicidal soap and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107177428A (en) * | 2017-07-27 | 2017-09-19 | 绵竹市天骄农业开发有限公司 | A kind of preparation method of basic zirconium phosphate handmade soap |
| CN107267311A (en) * | 2017-06-26 | 2017-10-20 | 绵竹市天骄农业开发有限公司 | A kind of basic zirconium phosphate liquid detergent and preparation method thereof |
| CN107287057A (en) * | 2017-06-26 | 2017-10-24 | 绵竹市天骄农业开发有限公司 | A kind of antibacterial manual soap powder of basic zirconium phosphate and preparation method thereof |
| CN107312655A (en) * | 2017-07-27 | 2017-11-03 | 绵竹市天骄农业开发有限公司 | A kind of basic zirconium phosphate handmade soap |
| CN107338119A (en) * | 2017-07-26 | 2017-11-10 | 绵竹市天骄农业开发有限公司 | A kind of grease dirt cleaning agent |
| CN107384627A (en) * | 2017-07-26 | 2017-11-24 | 绵竹市天骄农业开发有限公司 | A kind of basic zirconium phosphate cleaning agent |
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| CN102911816A (en) * | 2012-11-14 | 2013-02-06 | 沈阳信达信息科技有限公司 | Super fatted soap and production method thereof |
| CN105713744A (en) * | 2016-01-26 | 2016-06-29 | 孟根森 | Cleaning and treating agent for textile fabrics |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1519304A (en) * | 2003-01-24 | 2004-08-11 | 谢家忠 | Nano bactericidal detergent with no phosphor |
| CN101005762A (en) * | 2004-07-13 | 2007-07-25 | 出光技优股份有限公司 | Antibacterial composition, antibacterial molding, solution containing antibacterial composition, detergent, surface of tatami mat and tatami mat |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107267311A (en) * | 2017-06-26 | 2017-10-20 | 绵竹市天骄农业开发有限公司 | A kind of basic zirconium phosphate liquid detergent and preparation method thereof |
| CN107287057A (en) * | 2017-06-26 | 2017-10-24 | 绵竹市天骄农业开发有限公司 | A kind of antibacterial manual soap powder of basic zirconium phosphate and preparation method thereof |
| CN107338119A (en) * | 2017-07-26 | 2017-11-10 | 绵竹市天骄农业开发有限公司 | A kind of grease dirt cleaning agent |
| CN107384627A (en) * | 2017-07-26 | 2017-11-24 | 绵竹市天骄农业开发有限公司 | A kind of basic zirconium phosphate cleaning agent |
| CN107177428A (en) * | 2017-07-27 | 2017-09-19 | 绵竹市天骄农业开发有限公司 | A kind of preparation method of basic zirconium phosphate handmade soap |
| CN107312655A (en) * | 2017-07-27 | 2017-11-03 | 绵竹市天骄农业开发有限公司 | A kind of basic zirconium phosphate handmade soap |
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Application publication date: 20170517 |