CN106669877A - Multifunctional heating device for heating reaction - Google Patents
Multifunctional heating device for heating reaction Download PDFInfo
- Publication number
- CN106669877A CN106669877A CN201710028823.9A CN201710028823A CN106669877A CN 106669877 A CN106669877 A CN 106669877A CN 201710028823 A CN201710028823 A CN 201710028823A CN 106669877 A CN106669877 A CN 106669877A
- Authority
- CN
- China
- Prior art keywords
- reaction bulb
- heating device
- heating
- base
- bath
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L7/00—Heating or cooling apparatus; Heat insulating devices
- B01L7/02—Water baths; Sand baths; Air baths
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01L—CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- B01L9/00—Supporting devices; Holding devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Clinical Laboratory Science (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses a multifunctional heating device for a heating reaction. The multifunctional heating device comprises a water bath kettle; a flask rack is arranged above the water bath kettle; a plurality of through holes used for holding reaction flasks are formed in the flask rack; in the process of the heating reaction, necks of the reaction flasks are fixed with the flask rack by means of the through holes; bodies of the reaction flasks are positioned in the water bath kettle; a stirring rack is arranged above the flask rack, and stirring rods which are matched with the through holes in a one-to-one way are arranged on the stirring rack; the flask rack and the stirring rack are connected to a first telescopic pillar; the lower end of the first telescopic pillar is vertically connected with a first base, and the first base is arranged parallel to the ground. After the multifunctional heating device is adopted, no heating device is added, a plurality of reactions can be carried out at the same time on the same heating device while lower cost is maintained, and the yield of target products is increased.
Description
Technical field
The present invention relates to a kind of reaction unit, and in particular to a kind of multi-function heating device for reacting by heating.
Background technology
Into atom, atom rearranges the process of combination producing novel substance, referred to as chemical reaction to the cracking of molecules.In the reaction
The discoloration that is often accompanied by emitting light and heat generates precipitate etc., judge one react be whether the foundation of chemical reaction be to react whether to generate
New material.Oil, chemical industry, medicine and other fields can be related to a large amount of chemical reactions, and chemical reaction includes that exothermic reaction, heating are anti-
Should, need to use heater in reacting by heating, carrying out heating to reactant can increase reaction rate.
Generally, in chemistry, the research of medicine and other fields, it is required for every day carrying out substantial amounts of chemical reaction,
And it is current, the production of each material is individually carried out, and most reaction needs heating, and heating, can simultaneously with stirring
Effectively increase reaction rate；Therefore, in the case of heater, agitating device limited amount, multiple experiments can not be simultaneously
Carry out, the research to novel substances such as medicine, chemical substances and throughput rate can be affected.
The content of the invention
The technical problem to be solved is in the case of heater, agitating device limited amount, it is impossible to same
When prepare substantial amounts of target product, it is therefore intended that a kind of multi-function heating device for reacting by heating is provided, is solved in heating
In the case of device, agitating device limited amount, it is identical or different current so as to prepare in a large number that realization carries out multiple reactions simultaneously
The problem of product.
The present invention is achieved through the following technical solutions：
A kind of multi-function heating device for reacting by heating, including water-bath, the water-bath top is provided with bottle stand,
The through hole of multiple placing response bottles is provided with bottle stand, during reacting by heating, reaction bulb bottleneck is fixed by through hole with bottle stand,
Reaction bulb body is located in water-bath, and puddle support is provided with above bottle stand, is provided with the puddle support and is matched somebody with somebody one by one with through hole
The stirring rod of set, the bottle stand, puddle support are both connected on the first telescopic mast, and the lower end of the first telescopic mast is vertically connected with first
Base, first base placement parallel to the ground.
In the present invention, a heater can carry out heating simultaneously to multiple reactions simultaneously, and multiple reactions are carried out simultaneously
The throughput rate of target product can be increased, the present invention does not increase the quantity of heater, and production cost does not increase；This
Each reaction bulb has corresponding stirring rod in bright, realizes heated and stirred integration, and reaction rate can be significantly increased；This
Water-bath is used for heating in water bath in invention, and water-bath has the function of heated at constant temperature, reactant will not be caused the feelings of bumping occur
Condition, bottle stand is used to fix reaction bulb, and when needing to use reaction bulb, the bottleneck of reaction bulb through through hole and then is fixed reaction bulb
On bottle stand, turn to have the reaction bulb body of reactant in water-bath；It is anti-after can cleaning when reaction bulb need not be used
Bottle is answered to be placed on the through hole top of bottle stand, bottle stand serves storage effect；In course of reaction, stirring rod is displaced downwardly in reaction bulb
The inside of reactant, stirring rod Stirring accelerates reaction rate；First telescopic mast is used to adjust bottle stand, puddle support and water-bath
The distance of pot；First base fixes the first sound telescopic mast for support.
Second base is connected with below the water-bath, the second base is connected with water-bath by the second telescopic mast
Connect.Second telescopic mast is used to adjust the height of water-bath so that the reactant in reaction bulb reaches most suitable heating location.The
Two bases play support fixation to the second telescopic mast.
The through hole top is provided with the fixed block of fixed reaction bulb, offers on the fixed block and is worn for reaction bulb bottleneck
The aperture crossed, the diameter with diameter greater than reaction bulb bottleneck of aperture, aperture and reaction bulb bottleneck inscribe, the aperture is same with through hole
Central shaft.Fixed block is used to fix reaction bulb with bottle stand, bottleneck and the aperture inscribe of reaction bulb, is contacted with aperture by bottleneck
The rubbing action in face so that fixed block can fix reaction bulb.
The stirring rod adopt driven stirring rod, the stirring rod be located at through hole central axis, stirring rod it is straight
Footpath is much smaller than reaction bulb bottleneck diameter.All stirring rod are both connected on a motor, and the motor is arranged in first base,
The button of controlled motor startup is provided with first base.Stirring rod electric stirring, it is time saving and energy saving, although electric stirring cost ratio
Manpower stirs high cost, but, driven stirring rod can well control stir speed (S.S.) by motor, and stir speed (S.S.) compares manpower
Stirring is fast, and from meeting faster, yield is bigger for reaction rate.
The present invention compared with prior art, has the following advantages and advantages：
1st, a kind of yield of the multi-function heating device for reacting by heating of the present invention is high, and the present invention is not increasing plus hot charging
Put, in the case of the relatively low cost of holding, multiple reactions can simultaneously be carried out on a heater, increased target product
Volume of production；
2nd, a kind of multi-function heating device for reacting by heating of the present invention is simple to operate, and the present invention only needs to react
Bottle, stirring rod are arranged in place, open the i.e. achievable heated and stirred one of switch of water-bath, control stirring rod motor
Body；
3rd, a kind of multi-function heating device low cost for reacting by heating of the present invention, the low cost of the present invention, practicality
It is high.
Description of the drawings
Accompanying drawing described herein is used for providing further understanding the embodiment of the present invention, constitutes of the application
Point, do not constitute the restriction to the embodiment of the present invention.In the accompanying drawings：
Fig. 1 is schematic structural view of the invention.
Labelling and corresponding parts title in accompanying drawing：
1- water-baths, 2- bottle stands, 3- stirring rod, 4- puddle supports, the telescopic masts of 5- first, 6- first bases, 7- second bases,
The telescopic masts of 8- second, 9- fixed blocks.
Specific embodiment
To make the object, technical solutions and advantages of the present invention become more apparent, with reference to embodiment and accompanying drawing, to this
Invention is described in further detail, and the exemplary embodiment of the present invention and its explanation are only used for explaining the present invention, do not make
For limitation of the invention.
Embodiment 1
As shown in figure 1, a kind of multi-function heating device for reacting by heating of the present invention, including water-bath 1, the water-bath
The top of pot 1 is provided with bottle stand 2, and the through hole of multiple placing response bottles, during reacting by heating, reaction bulb bottle are provided with bottle stand 2
Neck is fixed by through hole with bottle stand 2, and reaction bulb body is located in water-bath 1, and the top of bottle stand 2 is provided with puddle support 4, described to stir
Mix and the stirring rod 3 supporting one by one with through hole be provided with frame 4, the bottle stand 2, puddle support 4 are both connected on the first telescopic mast 5,
The lower end of the first telescopic mast 5 is vertically connected with first base 6, the placement parallel to the ground of the first base 6.The through hole top
Be provided with the fixed block 9 of fixed reaction bulb, offer the aperture passed through for reaction bulb bottleneck on the fixed block 9, aperture it is straight
Footpath is more than the diameter of reaction bulb bottleneck, aperture and reaction bulb bottleneck inscribe, the aperture and the same central shaft of through hole.The stirring rod
3 adopt driven stirring rod, the stirring rod 3 to be located at the central axis of through hole, and the diameter of stirring rod 3 is much smaller than reaction bulb bottle
Neck diameter.All stirring rod 3 are both connected on a motor, and the motor is arranged in first base 6, is set in first base 6
It is equipped with the button of controlled motor startup.
Water-bath is used for heating in water bath in the present invention, and water-bath has the function of heated at constant temperature, reactant will not be caused to go out
The situation of existing bumping, bottle stand is used to fix reaction bulb, and when needing to use reaction bulb, then the bottleneck of reaction bulb will through through hole
Reaction bulb is fixed on bottle stand, is turned to have the reaction bulb body of reactant in water-bath；Need not using reaction bulb when, can be by
Reaction bulb after cleaning is placed on the through hole top of bottle stand, and bottle stand serves storage effect；In course of reaction, stirring rod is moved down
The inside of reactant into reaction bulb, stirring rod Stirring accelerates reaction rate；First telescopic mast is used to adjust bottle stand, stir
Mix the distance of frame and water-bath；First base fixes the first sound telescopic mast for support.Fixed block is used for reaction bulb and bottle stand
It is fixed, bottleneck and the aperture inscribe of reaction bulb, by the rubbing action of bottleneck and aperture contact surface so that fixed block can be fixed
Reaction bulb.Stirring rod electric stirring, it is time saving and energy saving, although electric stirring cost stirs high cost than manpower, driven stirring rod
Stir speed (S.S.) can well be controlled by motor, and stir speed (S.S.) is faster than manpower stirring, reaction rate from can faster, yield
It is bigger, install convenient low using a motor cost.
Embodiment 2
Based on embodiment 1, the lower section of the water-bath 1 is connected with second base 7, and the second base 7 is led to water-bath
Cross the second telescopic mast 8 to connect.Second telescopic mast is used to adjust the height of water-bath so that the reactant in reaction bulb reaches and most closes
Suitable heating location.Second base plays support fixation to the second telescopic mast.
Above-described specific embodiment, has been carried out further to the purpose of the present invention, technical scheme and beneficial effect
Describe in detail, should be understood that the specific embodiment that the foregoing is only the present invention, be not intended to limit the present invention
Protection domain, all any modification, equivalent substitution and improvements within the spirit and principles in the present invention, done etc. all should include
Within protection scope of the present invention.
Claims (5)
1. a kind of multi-function heating device for reacting by heating, including water-bath (1), it is characterised in that the water-bath (1)
Top is provided with bottle stand (2), and the through hole of multiple placing response bottles, during reacting by heating, reaction bulb bottle are provided with bottle stand (2)
Neck is fixed with bottle stand (2) by through hole, and reaction bulb body is located in water-bath (1), and bottle stand is provided with puddle support above (2)
(4), the stirring rod (3) supporting one by one with through hole is provided with the puddle support (4), the bottle stand (2), puddle support (4) connect
It is connected on the first telescopic mast (5), the lower end of the first telescopic mast (5) is vertically connected with first base (6), the first base (6)
Placement parallel to the ground.
2. a kind of multi-function heating device for reacting by heating according to claim 1, it is characterised in that the water-bath
Second base (7) is connected with below pot (1), the second base (7) is connected with water-bath by the second telescopic mast (8).
3. a kind of multi-function heating device for reacting by heating according to claim 2, it is characterised in that the through hole
Top is provided with the fixed block (9) of fixed reaction bulb, and on the fixed block (9) aperture passed through for reaction bulb bottleneck is offered,
The diameter with diameter greater than reaction bulb bottleneck of aperture, aperture and reaction bulb bottleneck inscribe, the aperture and the same central shaft of through hole.
4. a kind of multi-function heating device for reacting by heating according to claim 3, it is characterised in that the stirring
Rod (3) adopts driven stirring rod, and positioned at the central axis of through hole, the diameter of stirring rod (3) is much smaller than the stirring rod (3)
Reaction bulb bottleneck diameter.
5. a kind of multi-function heating device for reacting by heating according to claim 4, it is characterised in that all stirrings
Rod (3) is both connected on a motor, and the motor is arranged in first base (6), and control electricity is provided with first base (6)
The button that machine starts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710028823.9A CN106669877A (en) | 2017-01-16 | 2017-01-16 | Multifunctional heating device for heating reaction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710028823.9A CN106669877A (en) | 2017-01-16 | 2017-01-16 | Multifunctional heating device for heating reaction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106669877A true CN106669877A (en) | 2017-05-17 |
Family
ID=58859065
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710028823.9A Withdrawn CN106669877A (en) | 2017-01-16 | 2017-01-16 | Multifunctional heating device for heating reaction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106669877A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112275345A (en) * | 2020-10-31 | 2021-01-29 | 张晓东 | Net type combined beaker bracket and beaker moving device |
-
2017
- 2017-01-16 CN CN201710028823.9A patent/CN106669877A/en not_active Withdrawn
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112275345A (en) * | 2020-10-31 | 2021-01-29 | 张晓东 | Net type combined beaker bracket and beaker moving device |
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| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20170517 |