CN106669572B - A kind of reaction kettle - Google Patents
A kind of reaction kettle Download PDFInfo
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- CN106669572B CN106669572B CN201611194056.0A CN201611194056A CN106669572B CN 106669572 B CN106669572 B CN 106669572B CN 201611194056 A CN201611194056 A CN 201611194056A CN 106669572 B CN106669572 B CN 106669572B
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- reaction kettle
- inlet
- pipette
- ontology
- stirring wheel
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00245—Avoiding undesirable reactions or side-effects
- B01J2219/00252—Formation of deposits other than coke
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Present patent application belongs to the general chemical method and its special equipment technical field for making liquid and liquid reactions, specifically disclose a kind of reaction kettle, including reaction kettle ontology, it is provided with heating chamber on the side wall of reaction kettle ontology, heating chamber side is equipped with water filling port, reaction kettle is originally wound with pipette in vitro, pipette one end is equipped with funnel shaped inlet, the first check valve is equipped at inlet, the other end of pipette is equipped with liquid outlet, inlet and liquid outlet are respectively positioned on reaction kettle body interior, and the vertical distance of liquid outlet and reaction kettle body bottom portion is 1~3cm；Reaction kettle body upper part can be threaded connection with kettle cover, and through-hole is provided on kettle cover, agitating shaft is combined in through-hole, driving device is equipped at the top of agitating shaft, shaft bottom eccentric setting has stirring wheel, stirring wheel to be correspondingly arranged with inlet, and when stirring wheel turns to radius maximum squeezes inlet.Compared with prior art, it may be implemented that the material in reaction kettle is sufficiently stirred and is evenly heated.
Description
Technical field
The invention belongs to make the general chemical method of liquid and liquid reactions；And its special equipment technical field.
Background technology
The present reaction kettles for being used to prepare printing and dyeing assistant most of on the market are not provided with agitating device so that the object of reaction
Material stirring is insufficient and uneven, and it is slow that this just directly results in reaction speed, and reacts not exclusively, wastes resource, improves life
Cost is produced, and some reaction mediums after reaction in tank under residual easily corrode, and affect consersion unit, cannot improve economic effect
Benefit.
To solve the above-mentioned problems, Chinese utility model patent CN203123964U discloses one kind and being used to prepare printing and dyeing
The reaction unit of auxiliary agent is equipped with the agitating shaft being inserted into can body on cover, and agitating shaft bottom end is equipped with anchor blade,
It realizes the stirring to material, accelerates reaction speed.
Above-mentioned reaction unit realizes stirring and mixing to material only by the mode for adding agitating shaft, but is installing
When agitating shaft, in order to avoid agitating shaft scratches reaction kettle bottom in whipping process, the bottom of general agitating shaft will not be with reaction kettle
Bottom contacts, therefore in the whipping process of agitating shaft, agitating shaft can not stir reaction kettle substrate material, can not be in reaction kettle
Material is adequately stirred.
During chemical reaction in simultaneous reactions kettle, it is sometimes desirable to the certain heating environment of needs, tradition is only
Can realize the heating to material by being heated to tank body, heating speed is slow and tank in temperature of charge it is uneven, be unfavorable for anti-
That answers is smoothed out.
Invention content
The purpose of the present invention is to provide a kind of reaction kettle, may be implemented the material in reaction kettle be sufficiently stirred and
It is evenly heated.
In order to achieve the above object, base case of the invention provides a kind of reaction kettle, including reaction kettle ontology, reaction kettle
Heating chamber is provided in the side wall of ontology, heating chamber side is equipped with the water filling port for filling hot water, and reaction kettle is originally wound in vitro
Pipette, pipette one end are equipped with funnel shaped inlet, are equipped with the first check valve at inlet, the other end of pipette is equipped with
Liquid outlet, inlet and liquid outlet are respectively positioned on reaction kettle body interior, and the vertical distance of liquid outlet and reaction kettle body bottom portion
For 1~3cm；Reaction kettle body upper part is threaded with kettle cover, and through-hole is provided on kettle cover, and agitating shaft is combined in through-hole, stirring
Driving device is equipped at the top of axis, shaft bottom eccentric setting has stirring wheel, and stirring wheel is opposite with inlet, and stirring wheel rotates
Inlet is squeezed when to radius maximum.
The principle of this base case is：When preparing using this reaction kettle, kettle cover is rotated first, and kettle cover rotation is removed,
Then material is poured into reaction kettle body interior, it would be desirable to which the material of hybrid reaction, which is all added after reaction kettle ontology, again will
Kettle cover covers on reaction kettle ontology, and rotates and tighten.
Start driving device to start to work, while hot water is injected to from water filling port to heating chamber, it is intrinsic to reaction kettle
Material is heated, and the intrinsic material of reaction kettle is made to reach the temperature of reaction, and driving device drives agitating shaft to start to rotate, stirs
It mixes and drives stirring wheel rotation while shaft rotation is moved, liquid material when stirring wheel rotates in impact reaction kettle, and liquid is raised
It rises, the liquid that stirring wheel raises is sent into inlet.
The first check valve is opened at this time, and liquid enters pipette, and as stirring wheel rotates, when rotation will produce wind and pour into suction
Liquid in pipette is pressed to liquid outlet by liquid pipe, while stirring wheel can squeeze into when stirring wheel turns to radius maximum
Liquid mouth accelerates the liquid rate of outflow of liquid outlet.
Since the vertical distance of liquid outlet and reaction kettle body bottom portion is 1~3cm, then the liquid of liquid outlet outflow will be direct
It is contacted with the liquid material of the bottom, forms stirring action using liquid outflow alluvium material, so that material is mixed more abundant.
The advantageous effect of this base case is：1, in this programme simultaneously eccentric setting stirring wheel and pipette, will react
The liquid of kettle ontology sucks pipette, and causes to stir to substrate material using the liquid mobilization of liquid outlet, avoids object
Expect that bottom becomes retention layer, liquid is stirred under the collective effect of agitating shaft and liquid outlet, stirring is more uniform；Simultaneously
Inlet is squeezed using stirring wheel, accelerating liquid flow velocity enhances the agitaion to bottom liquid.
2, heating water bath is carried out to material using heating chamber in this programme, reaction kettle ontology is uniformly heated, inhales simultaneously
Liquid pipe is wrapped on reaction kettle ontology, ensures that the liquid in pipette can also be heated, while by the liquid in the pipette after heating
Body discharges into reaction kettle ontology, can accelerate the heating speed of material, improves reaction efficiency.
Scheme two：This is the preferred of basic scheme, and the outlet end of the pipette is equipped with cleaning and manages, and cleaning pipe is equipped with
Second check valve cleans and is provided with several scuppers on pipe, and cleaning pipe is bonded with reaction kettle inner body wall.
After the intrinsic material reaction of reaction kettle is complete, the hot water in heating chamber is poured out from water filling port, and will fallen
Hot water out pours into reaction kettle ontology again, and the water in reaction kettle is squeezed into pipette by stirring wheel rotation, and first is unidirectional at this time
Valve and the second check valve are opened, and water enters cleaning pipe from pipette, and inner wall of the water directly from scupper along reaction kettle flows down, clearly
The inner wall of clean reaction kettle ontology.
The hot water after use is directly utilized, avoids the wilful waste of water resource, while entire cleaning process is not required to very important person
Hand enters reaction kettle ontology, and chemical substance is avoided to injure human body.
Scheme three：This is preferred for scheme two, and the cleaning pipe is positioned at the middle and upper part of reaction kettle ontology.
The intrinsic material of reaction kettle is typically in the lower part of reaction kettle ontology, then what is be contaminated is typically also reaction kettle
The lower part of ontology, therefore the water cleaned in pipe helps to clean under overhead stream, improves clean validity.
Scheme four：This is preferred for scheme three, and the reaction kettle ontology is externally provided with vibrator.
In cleaning, Vibration on Start-up device can improve cleaning capacity.
Scheme five：This is the preferred of basic scheme, and gasket is equipped between the reaction kettle ontology and kettle cover.
The leakproofness for improving reaction kettle avoids the pernicious gas generated during material reaction from drifting in air, to people
Body damages.
Scheme six：This is the preferred of basic scheme, and the through-hole is opened in side of the kettle cover close to inlet.
Ensure that stirring wheel can effectively squeeze inlet in rotation process, enhancing liquid pipette flowing velocity,
Improve stirring action of the liquid outlet to substrate material.
Description of the drawings
Fig. 1 is a kind of structural schematic diagram of reaction kettle of the embodiment of the present invention.
Specific implementation mode
Below by specific implementation mode, the present invention is described in further detail：
Reference numeral in Figure of description includes：Reaction kettle ontology 10, kettle cover 11, heating chamber 12, water filling port 13, imbibition
Pipe 20, liquid outlet 21, inlet 22, cleaning pipe 23, agitating shaft 30, motor 40, stirring wheel 50, vibrator 60.
Embodiment
Substantially as shown in Fig. 1：A kind of reaction kettle, including reaction kettle ontology 10, be provided on the wall of reaction kettle ontology 10 plus
Hot chamber 12, heating chamber 12 is interior to be full of hot water, and 12 right end of heating chamber is integrally formed with water filling port 13；Reaction kettle external spiral is wound with suction
Liquid pipe 20,20 right end of pipette are equipped with the first check valve, inlet 22 is in a left side integrally formed with inlet 22 at inlet 22
Wide right narrow infundibulate, 20 left end of pipette is integrally formed with the cleaning pipe 23 of vertical liquid outlet 21 and annular, liquid outlet 21
With reactor bottom distance and 1cm, cleaning pipe 23 is mounted on the inner wall of reaction kettle, and is cleaned and be equipped with second on pipe 23 unidirectionally
Valve.
10 top of reaction kettle ontology is threaded with kettle cover 11, and sealing is equipped between kettle cover 11 and reaction kettle ontology 10
Pad, 11 right part of kettle cover offer through-hole, and agitating shaft 30 is combined in through-hole, and 30 top of agitating shaft is equipped with motor 40, agitating shaft
30 bottoms are eccentrically mounted to have stirring wheel 50, inlet 22 to be correspondingly arranged with stirring wheel 50, and stirring wheel 50 squeezes inlet when stirring
22,10 bottom of reaction kettle ontology is equipped with vibrator 60.
When preparing using this reaction kettle, kettle cover 11 is rotated first, the rotation of kettle cover 11 is removed, then to reaction kettle ontology 10
Material is poured into inside, it would be desirable to which the material of hybrid reaction, which is all added reaction kettle ontology 10 and later again covers kettle cover 11, to react
On kettle ontology 10, and rotates and tighten.
When material in reaction kettle starts reaction, starts motor 40 and work, while to from water filling port 13 to 12 note of heating chamber
Enter hot water, heating water bath is carried out to the material in reaction kettle ontology 10, motor 40 drives agitating shaft 30 to start to rotate, agitating shaft 30
Stirring wheel 50 is driven to start to rotate while rotation, liquid material when stirring wheel 50 rotates in impact reaction kettle, and by liquid
Body raises.
Since inlet 22 and stirring wheel 50 are correspondingly arranged, then the liquid that stirring wheel 50 raises will enter pipette 20,
The first check valve is opened at this time, the second closed check valve, due to 50 eccentric setting of stirring wheel, when to turn to radius big for stirring wheel 50
Side and inlet 22 when contacting, stirring wheel 50 will squeeze inlet 22, to by the liquid of pipette 20 to liquid outlet 21
It squeezes, and is finally flowed out from liquid outlet 21, since the bottom of liquid outlet 21 and reaction kettle ontology 10 is close, when liquid is from going out liquid
When mouth 21 flows out, directly contacted with the liquid material of the bottom, as liquid is constantly flowed out from liquid outlet 21, to the bottom
Liquid carry out flow-disturbing, cause to stir, to make material mix more fully.
After the material reaction in reaction kettle ontology 10 is complete, kettle cover 11 is removed again, by the object in reaction kettle ontology 10
Material export is collected, while the hot water in heating chamber 12 being poured out from water filling port 13, and the hot water poured out is poured into instead again
Kettle ontology 10 is answered, kettle cover 11 is then covered, same to start motor 40, motor 40 drives stirring wheel 50 to rotate, will be in reaction kettle
Water squeezes into pipette 20, and the first check valve and the second check valve are opened at this time, and water enters cleaning pipe 23, cleaning from pipette 20
Several scuppers are provided in pipe 23, inner wall of the water directly from scupper along reaction kettle ontology 10 flows down, while Vibration on Start-up device 60,
Make reaction kettle ontology 10 start to vibrate, to achieve the purpose that clean reaction kettle ontology 10, kettle cover 11 is removed after cleaning, it will
Water pours out completion cleaning, does not have to human hand and cleans, chemical substance is avoided to injure human body.
Above-described is only the embodiment of the present invention, and the common sense such as well known concrete structure and characteristic are not made herein in scheme
Excessive description.It, without departing from the structure of the invention, can be with it should be pointed out that for those skilled in the art
Several modifications and improvements are made, these should also be considered as protection scope of the present invention, these all do not interfere with what the present invention was implemented
Effect and patent practicability.The scope of protection required by this application should be based on the content of the claims, in specification
The records such as specific implementation mode can be used for explaining the content of claim.
Claims (6)
1. a kind of reaction kettle, including reaction kettle ontology, which is characterized in that be provided with heating chamber in the side wall of reaction kettle ontology, heat
Chamber side is equipped with the water filling port for filling hot water, and reaction kettle is originally wound with pipette in vitro, and pipette one end is equipped with infundibulate
Inlet, the first check valve is equipped at inlet, the other end of pipette is equipped with liquid outlet, and inlet and liquid outlet are respectively positioned on
Reaction kettle body interior, and the vertical distance of liquid outlet and reaction kettle body bottom portion is 1~3cm；Reaction kettle body upper part screw thread
It is connected with kettle cover, through-hole is provided on kettle cover, agitating shaft is combined in through-hole, driving device, agitating shaft bottom are equipped at the top of agitating shaft
Portion's eccentric setting has stirring wheel, and stirring wheel is opposite with inlet, and when stirring wheel turns to radius maximum squeezes inlet.
2. a kind of reaction kettle according to claim 1, it is characterised in that：The outlet end of the pipette is equipped with cleaning
Pipe, cleaning pipe are equipped with the second check valve, clean and are provided with several scuppers on pipe, and cleaning pipe is bonded with reaction kettle inner body wall.
3. a kind of reaction kettle according to claim 2, it is characterised in that：The cleaning pipe is located in reaction kettle ontology
Portion.
4. a kind of reaction kettle according to claim 3, it is characterised in that：The reaction kettle ontology is externally provided with vibrator.
5. a kind of reaction kettle according to claim 1, it is characterised in that：It is equipped between the reaction kettle ontology and kettle cover close
Packing.
6. a kind of reaction kettle according to claim 1, it is characterised in that：The through-hole is opened in kettle cover close to inlet
Side.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611194056.0A CN106669572B (en) | 2016-12-21 | 2016-12-21 | A kind of reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611194056.0A CN106669572B (en) | 2016-12-21 | 2016-12-21 | A kind of reaction kettle |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106669572A CN106669572A (en) | 2017-05-17 |
| CN106669572B true CN106669572B (en) | 2018-09-21 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611194056.0A Active CN106669572B (en) | 2016-12-21 | 2016-12-21 | A kind of reaction kettle |
Country Status (1)
| Country | Link |
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| CN (1) | CN106669572B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108579120B (en) * | 2018-02-09 | 2021-05-14 | 山东中医药大学 | Automatic ultrasonic extraction equipment |
| CN108355373B (en) * | 2018-02-09 | 2021-05-14 | 山东中医药大学 | Automatic microwave extraction equipment |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3847805A (en) * | 1972-12-07 | 1974-11-12 | Illinois Water Treatment Co | Ion exchange vessel |
| JP4980547B2 (en) * | 2000-09-22 | 2012-07-18 | アルファ ラバル タンク イクィップメント アクティーゼルスカブ | Method and processing plant for processing a batch of liquid |
| CN103521159A (en) * | 2013-10-31 | 2014-01-22 | 罗江晨明生物制品有限公司 | Reaction kettle |
| AT515881B1 (en) * | 2014-05-20 | 2020-01-15 | Geolyth Mineral Tech Gmbh | Sequential continuous mixing plant |
| CN104492338A (en) * | 2014-12-25 | 2015-04-08 | 常州商瑞服饰有限公司 | Interruption type spraying device |
| CN205253055U (en) * | 2015-12-24 | 2016-05-25 | 重庆凌峰橡塑制品有限公司 | Resin production reation kettle |
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2016
- 2016-12-21 CN CN201611194056.0A patent/CN106669572B/en active Active
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| Publication number | Publication date |
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| CN106669572A (en) | 2017-05-17 |
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Effective date of registration: 20190819 Address after: 102600 Unit 403, Unit 1, 15th Floor, Changfengyuan, Huangcun Town, Daxing District, Beijing Patentee after: Dong Jinhuan Address before: 400052 Building 8-1, District C, Jiulongpo District, Jiulongpo District, Jiulongpo District, Chongqing Patentee before: Chongqing Demengte Technical Development Co., Ltd. |
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Effective date of registration: 20191216 Address after: 276600 West Six Road, East Huaihai Second Road, Junan Economic Development Zone, Linyi City, Shandong Province Patentee after: Shandong Peak-tech New Material Co., Ltd. Address before: 102600 Unit 403, Unit 1, 15th Floor, Changfengyuan, Huangcun Town, Daxing District, Beijing Patentee before: Dong Jinhuan |
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