CN106638111B - A kind of Packaging Box freeze proof procollagen paper material and preparation method thereof - Google Patents
A kind of Packaging Box freeze proof procollagen paper material and preparation method thereof Download PDFInfo
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- CN106638111B CN106638111B CN201611181080.0A CN201611181080A CN106638111B CN 106638111 B CN106638111 B CN 106638111B CN 201611181080 A CN201611181080 A CN 201611181080A CN 106638111 B CN106638111 B CN 106638111B
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Classifications
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H13/00—Pulp or paper, comprising synthetic cellulose or non-cellulose fibres or web-forming material
- D21H13/02—Synthetic cellulose fibres
- D21H13/04—Cellulose ethers
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H13/00—Pulp or paper, comprising synthetic cellulose or non-cellulose fibres or web-forming material
- D21H13/10—Organic non-cellulose fibres
- D21H13/20—Organic non-cellulose fibres from macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D21H13/24—Polyesters
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/03—Non-macromolecular organic compounds
- D21H17/05—Non-macromolecular organic compounds containing elements other than carbon and hydrogen only
- D21H17/06—Alcohols; Phenols; Ethers; Aldehydes; Ketones; Acetals; Ketals
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/34—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/35—Polyalkenes, e.g. polystyrene
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/675—Oxides, hydroxides or carbonates
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/10—Packing paper
Abstract
The invention discloses a kind of freeze proof procollagen paper materials of Packaging Box, it is made of the raw material of following weight parts: aluminium isopropoxide 5-7, maleic anhydride 1-1.5, ethylene glycol 2-3, stannic oxide 0.1-0.2, alkanolamide 0.5-1, triethanolamine borate 2-3, polyester fiber 10-14, rice straw pulp 70-80, styrene 10-12, bamboo pulp 20-30, fatty alcohol polyoxyethylene ether 0.5-1, zirconium carbonate ammonium 0.7-1, abienol 3-5, naphthenic soap 0.5-1, nonyl phenol 0.1-0.2, sp-800.1-0.3, cumyl peroxide 0.07-0.1, zinc pyrithione 0.8-1, diphenyl-imidazole quinoline 0.4-1, sodium carbonate 1-2, cyanogen propyl methocel 4-7.The ethylene glycol that the present invention is added also effectively raises the frost resistance of body paper material, improves the comprehensive performance of finished product.
Description
Technical field
The present invention relates to body paper field of material technology more particularly to a kind of freeze proof procollagen paper material of Packaging Box and its
Preparation method.
Background technique
In recent years, it with the continuous improvement of people's living standards, the use scope of Packaging Box is also increasingly wider, not only wraps
Traditional household items are included, further include various aquatic products, fresh, chemicals etc., this requires Packaging Box to have preferably
Protective value, traditional Packaging Box some is using materials such as velveteens, these manufactured paper pulp fiber length are longer, and fiber is very curved
Song, poor dimensional stability, and there is very strong water imbibition, it encounters moist environment and is easy for damaging, meanwhile, paper material conduct
One of common used material is closely related field of living with people, is all likely to be exposed Packaging Box everywhere in people's life.Cause
This, various diseases caused by the propagation of harmful bacteria in Packaging Box use process, protect the health of human body in order to prevent,
Health is ground, it is also necessary that researching and developing, which has the Packaging Box of anti-microbial property, therefore we just need constantly to improve
The comprehensive performance of Packaging Box meets it in the use of each packaging field, improves the use environment of safety and environmental protection.
Summary of the invention
The object of the invention is to remedy the disadvantages of known techniques, provides a kind of Packaging Box freeze proof procollagen paper wood
Material and preparation method thereof.
The present invention is achieved by the following technical solutions.
A kind of freeze proof procollagen paper material of Packaging Box, it is made of the raw material of following weight parts:
Aluminium isopropoxide 5-7, maleic anhydride 1-1.5, ethylene glycol 2-3, stannic oxide 0.1-0.2, alkanolamide 0.5-
1, triethanolamine borate 2-3, polyester fiber 10-14, rice straw pulp 70-80, styrene 10-12, bamboo pulp 20-30, poly alkyl alcohol
Ethylene oxide ether 0.5-1, zirconium carbonate ammonium 0.7-1, abienol 3-5, naphthenic soap 0.5-1, nonyl phenol 0.1-0.2, sp-800.1-
0.3, cumyl peroxide 0.07-0.1, zinc pyrithione 0.8-1, diphenyl-imidazole quinoline 0.4-1, sodium carbonate 1-2, cyanogen propyl
Methylcellulose 4-7.
A kind of preparation method of the freeze proof procollagen paper material of Packaging Box, comprising the following steps:
(1) above-mentioned nonyl phenol is added in the dehydrated alcohol of 17-20 times of its weight, is stirred evenly, increase temperature 47-
50 DEG C, above-mentioned fatty alcohol polyoxyethylene ether is added, insulated and stirred 3-4 minutes, obtains alcohol dispersion liquid；
(2) above-mentioned cyanogen propyl methocel is added in the deionized water of 30-40 times of its weight, stirs evenly, adds
Enter above-mentioned alkanolamide, 600-700 revs/min stirring 10-15 minutes, obtain fiber dispersion；
(3) above-mentioned aluminium isopropoxide is added in fiber dispersion, is stirred evenly, above-mentioned maleic anhydride is added, risen
High-temperature is 35-40 DEG C, and insulated and stirred 20-30 minutes, above-mentioned sodium carbonate is added, and increasing temperature is 51-60 DEG C, insulated and stirred
40-50 minutes, above-mentioned zirconium carbonate ammonium is added, stirs to room temperature, obtains fibre modification colloidal sol；
(4) above-mentioned cumyl peroxide is added in above-mentioned alcohol dispersion liquid, is stirred evenly, obtain initiator alcohol liquid；
(5) above-mentioned diphenyl-imidazole quinoline, styrene are mixed, are added in the dehydrated alcohol of 30-40 times of mixture weight,
It stirs evenly, above-mentioned initiator alcohol liquid is added, increasing temperature is 65-70 DEG C, and above-mentioned zinc pyrithione, insulated and stirred 1-2 is added
Hour, obtain polymer alcohol liquid；
(6) above-mentioned fibre modification colloidal sol, polymer alcohol liquid are mixed, is stirred evenly, above-mentioned sp-80 is added, increase temperature
It is 70-75 DEG C, insulated and stirred 30-40 minutes, above-mentioned naphthenic soap is added, stirs evenly, obtain polymer sol dispersion liquid；
(7) above-mentioned polymer sol dispersion liquid is mixed with remaining each raw material, stirs evenly, be added in beater, beats
Slurry, keep the temperature 20-30 minutes at 60-70 DEG C, is discongested, defibrination, adds water to solid content as 4-6%, is manufactured paper with pulp molding by paper machine,
Dehydration, drying, obtains body paper material.
The invention has the advantages that
The present invention uses aluminium isopropoxide for presoma, and fiber dispersion is added, and obtains that viscosity is higher, toughness is preferably molten
Obtained polymer is effectively mixed with the colloidal sol then using styrene as monomer, obtains polymer sol dispersion liquid by glue,
The dispersion liquid can effectively improve dispersibility of the filler between slurry, improve the compatibility of each raw material, improve finished product body paper material
The toughness of material, the ethylene glycol that the present invention is added also effectively raise the frost resistance of body paper material, improve the comprehensive of finished product
Energy.
Specific embodiment
It is the embodiment of the present invention one below.
A kind of freeze proof procollagen paper material of Packaging Box, it is made of the raw material of following weight parts:
Aluminium isopropoxide 5, maleic anhydride 1, ethylene glycol 2, stannic oxide 0.1, alkanolamide 0.5, triethanolamine boric acid
Ester 2, polyester fiber 10, rice straw pulp 70, styrene 10, bamboo pulp 20, fatty alcohol polyoxyethylene ether 0.5, zirconium carbonate ammonium 0.7, rosin
Alcohol 3, naphthenic soap 0.5, nonyl phenol 0.1, sp-80 0.1, cumyl peroxide 0.07, zinc pyrithione 0.8, diphenyl
Imidazoline 0.4, sodium carbonate 1, cyanogen propyl methocel 4.
It is the embodiment of the present invention two below.
A kind of freeze proof procollagen paper material of Packaging Box, it is made of the raw material of following weight parts:
Aluminium isopropoxide 6, maleic anhydride 1.3, ethylene glycol 2.5, stannic oxide 0.15, alkanolamide 0.7, triethanolamine
Borate 2.5, polyester fiber 13, rice straw pulp 75, styrene 11, bamboo pulp 23, fatty alcohol polyoxyethylene ether 0.7, zirconium carbonate ammonium
0.8, abienol 4, naphthenic soap 0.7, nonyl phenol 0.13, sp-80 0.2, cumyl peroxide 0.09, zinc pyrithione
0.9, diphenyl-imidazole quinoline 0.6, sodium carbonate 1.3, cyanogen propyl methocel 5.
It is the embodiment of the present invention three below.
A kind of freeze proof procollagen paper material of Packaging Box, it is made of the raw material of following weight parts:
Aluminium isopropoxide 7, maleic anhydride 1.5, ethylene glycol 3, stannic oxide 0.2, alkanolamide 1, triethanolamine boric acid
Ester 3, polyester fiber 14, rice straw pulp 80, styrene 12, bamboo pulp 30, fatty alcohol polyoxyethylene ether 1, zirconium carbonate ammonium 1, abienol 5,
Naphthenic soap 1, nonyl phenol 0.2, sp-80 0.3, cumyl peroxide 0.1, zinc pyrithione 1, diphenyl-imidazole quinoline 1,
Sodium carbonate 2, cyanogen propyl methocel 7.
A kind of preparation method of the freeze proof procollagen paper material of Packaging Box, comprising the following steps:
(1) above-mentioned nonyl phenol is added in the dehydrated alcohol of 17 times of its weight, is stirred evenly, increase 47 DEG C of temperature,
Above-mentioned fatty alcohol polyoxyethylene ether is added, insulated and stirred 3 minutes, obtains alcohol dispersion liquid；
(2) above-mentioned cyanogen propyl methocel is added in the deionized water of 30 times of its weight, is stirred evenly, in addition
Alkanolamide is stated, 600 revs/min are stirred 10 minutes, and fiber dispersion is obtained；
(3) above-mentioned aluminium isopropoxide is added in fiber dispersion, is stirred evenly, above-mentioned maleic anhydride is added, risen
High-temperature is 35 DEG C, and insulated and stirred 20 minutes, above-mentioned sodium carbonate is added, and increasing temperature is 51 DEG C, insulated and stirred 40 minutes, is added
Above-mentioned zirconium carbonate ammonium stirs to room temperature, obtains fibre modification colloidal sol；
(4) above-mentioned cumyl peroxide is added in above-mentioned alcohol dispersion liquid, is stirred evenly, obtain initiator alcohol liquid；
(5) above-mentioned diphenyl-imidazole quinoline, styrene are mixed, is added in 30 times of mixture weight of dehydrated alcohol, stirs
It mixes uniformly, above-mentioned initiator alcohol liquid is added, increasing temperature is 65 DEG C, and above-mentioned zinc pyrithione is added, insulated and stirred 1 hour, obtains
Polymer alcohol liquid；
(6) above-mentioned fibre modification colloidal sol, polymer alcohol liquid are mixed, is stirred evenly, above-mentioned sp is added, increasing temperature is 70
DEG C, insulated and stirred 30 minutes, above-mentioned naphthenic soap is added, stirs evenly, obtains polymer sol dispersion liquid；
(7) above-mentioned polymer sol dispersion liquid is mixed with remaining each raw material, stirs evenly, be added in beater, beats
Slurry, keep the temperature 20 minutes at 60 DEG C, is discongested, defibrination, and adding water to solid content is 4%, is manufactured paper with pulp molding by paper machine, dehydration, baking
It is dry, obtain body paper material.
Claims (1)
1. a kind of freeze proof procollagen paper material of Packaging Box, which is characterized in that the freeze proof colloidal sol body paper of the Packaging Box
Material is made of the raw material of following weight parts:
Aluminium isopropoxide 5-7, maleic anhydride 1-1.5, ethylene glycol 2-3, stannic oxide 0.1-0.2, alkanolamide 0.5-1, three
Ethanol amine borate 2-3, polyester fiber 10-14, rice straw pulp 70-80, styrene 10-12, bamboo pulp 20-30, fatty alcohol polyoxy second
Alkene ether 0.5-1, zirconium carbonate ammonium 0.7-1, abienol 3-5, naphthenic soap 0.5-1, nonyl phenol 0.1-0.2, sp-800.1-0.3,
Cumyl peroxide 0.07-0.1, zinc pyrithione 0.8-1, diphenyl-imidazole quinoline 0.4-1, sodium carbonate 1-2, cyanogen hydroxypropyl methyl
Cellulose 4-7；
Preparation method the following steps are included:
(1) above-mentioned nonyl phenol is added in the dehydrated alcohol of 17-20 times of its weight, is stirred evenly, increase temperature 47-50
DEG C, above-mentioned fatty alcohol polyoxyethylene ether is added, insulated and stirred 3-4 minutes, obtains alcohol dispersion liquid；
(2) above-mentioned cyanogen propyl methocel is added in the deionized water of 30-40 times of its weight, is stirred evenly, in addition
State alkanolamide, 600-700 revs/min stirring 10-15 minutes, obtain fiber dispersion；
(3) above-mentioned aluminium isopropoxide is added in fiber dispersion, is stirred evenly, above-mentioned maleic anhydride is added, increase temperature
Degree is 35-40 DEG C, and insulated and stirred 20-30 minutes, above-mentioned sodium carbonate is added, and increasing temperature is 51-60 DEG C, insulated and stirred 40-50
Minute, above-mentioned zirconium carbonate ammonium is added, stirs to room temperature, obtains fibre modification colloidal sol；
(4) above-mentioned cumyl peroxide is added in above-mentioned alcohol dispersion liquid, is stirred evenly, obtain initiator alcohol liquid；
(5) above-mentioned diphenyl-imidazole quinoline, styrene are mixed, is added in the dehydrated alcohol of 30-40 times of mixture weight, stirred
Uniformly, it is added above-mentioned initiator alcohol liquid, increasing temperature is 65-70 DEG C, it is added above-mentioned zinc pyrithione, insulated and stirred 1-2 hours,
Obtain polymer alcohol liquid；
(6) above-mentioned fibre modification colloidal sol, polymer alcohol liquid are mixed, is stirred evenly, above-mentioned sp-80 is added, raising temperature is 70-
75 DEG C, insulated and stirred 30-40 minutes, above-mentioned naphthenic soap is added, stirs evenly, obtain polymer sol dispersion liquid；
(7) above-mentioned polymer sol dispersion liquid is mixed with remaining each raw material, stirs evenly, be added in beater, is beaten,
20-30 minutes are kept the temperature at 60-70 DEG C, is discongested, defibrination, adding water to solid content is 4-6%, is manufactured paper with pulp molding by paper machine, it is dehydrated,
Drying, obtains body paper material.
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| CN201611181080.0A CN106638111B (en) | 2016-12-20 | 2016-12-20 | A kind of Packaging Box freeze proof procollagen paper material and preparation method thereof |
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| CN201611181080.0A CN106638111B (en) | 2016-12-20 | 2016-12-20 | A kind of Packaging Box freeze proof procollagen paper material and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108221471A (en) * | 2018-01-22 | 2018-06-29 | 王家浩 | A kind of polymer modification paper making pulp |
| CN108193548A (en) * | 2018-02-02 | 2018-06-22 | 朱子涵 | A kind of antibacterial yellowing-resistant paper making pulp |
| CN110093609B (en) * | 2019-05-07 | 2021-05-04 | 北京赛福贝特能源技术服务有限公司 | Method for improving frost resistance of unsaturated higher fatty acid imidazoline corrosion inhibitor |
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| US6349826B1 (en) * | 1997-06-30 | 2002-02-26 | Kimberly-Clark Worldwide, Inc. | Medical packaging fabric with improved bacteria barrier |
| CN101591148A (en) * | 2008-11-21 | 2009-12-02 | 中材高新材料股份有限公司 | The preparation method of alumina coat on quartz fibre surface |
| CN104927233A (en) * | 2015-06-04 | 2015-09-23 | 当涂县华艺金属制品有限公司 | Weather-proof durable plastic door window |
| CN105332315A (en) * | 2015-11-05 | 2016-02-17 | 义乌市义南纸业有限公司 | Food wrapper with antibacterial and bacteriostatic effects and preparation method thereof |
| CN106012688A (en) * | 2016-07-26 | 2016-10-12 | 浙江恒达新材料股份有限公司 | Preparation process for medical antibacterial packing paper |
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2016
- 2016-12-20 CN CN201611181080.0A patent/CN106638111B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6349826B1 (en) * | 1997-06-30 | 2002-02-26 | Kimberly-Clark Worldwide, Inc. | Medical packaging fabric with improved bacteria barrier |
| CN101591148A (en) * | 2008-11-21 | 2009-12-02 | 中材高新材料股份有限公司 | The preparation method of alumina coat on quartz fibre surface |
| CN104927233A (en) * | 2015-06-04 | 2015-09-23 | 当涂县华艺金属制品有限公司 | Weather-proof durable plastic door window |
| CN105332315A (en) * | 2015-11-05 | 2016-02-17 | 义乌市义南纸业有限公司 | Food wrapper with antibacterial and bacteriostatic effects and preparation method thereof |
| CN106012688A (en) * | 2016-07-26 | 2016-10-12 | 浙江恒达新材料股份有限公司 | Preparation process for medical antibacterial packing paper |
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Effective date of registration: 20201014 Address after: 524400 Zhanjiang City, Guangdong Province, Lianjiang City, Jiuzhou River economic development test area, Hejiang bridge head of Hejiang River Patentee after: LIANJIANG JUNLONG PACKING Co.,Ltd. Address before: Dong Qiao Zhen Miao Cun, Haishu District 315000 Zhejiang Shijiu city in Ningbo Province Patentee before: NINGBO BLUESTAR PACKAGING PRINTING Co.,Ltd. |
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