CN106635397A - Method for semi-refined linseed oil - Google Patents

Method for semi-refined linseed oil Download PDF

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Publication number
CN106635397A
CN106635397A CN201710088656.7A CN201710088656A CN106635397A CN 106635397 A CN106635397 A CN 106635397A CN 201710088656 A CN201710088656 A CN 201710088656A CN 106635397 A CN106635397 A CN 106635397A
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Prior art keywords
oil
raw material
control
controlled
semi
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Pending
Application number
CN201710088656.7A
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Chinese (zh)
Inventor
张立宁
梁国兵
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wuzhong City Ningxia Su Crisp Muslim Grain And Oil Industry And Trade Co Ltd
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Wuzhong City Ningxia Su Crisp Muslim Grain And Oil Industry And Trade Co Ltd
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Application filed by Wuzhong City Ningxia Su Crisp Muslim Grain And Oil Industry And Trade Co Ltd filed Critical Wuzhong City Ningxia Su Crisp Muslim Grain And Oil Industry And Trade Co Ltd
Priority to CN201710088656.7A priority Critical patent/CN106635397A/en
Publication of CN106635397A publication Critical patent/CN106635397A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/02Pretreatment
    • C11B1/04Pretreatment of vegetable raw material
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00Production of fats or fatty oils from raw materials
    • C11B1/06Production of fats or fatty oils from raw materials by pressing
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/001Refining fats or fatty oils by a combination of two or more of the means hereafter

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Microbiology (AREA)
  • Fats And Perfumes (AREA)
  • Edible Oils And Fats (AREA)

Abstract

The invention belongs to the field of oil processing and particularly relates to a method for semi-refined linseed oil. The method comprises the steps of cleaning working procedure, parching, cooling, crushing, mixing, pressing, filtering, degreasing, secondary filtering, dewaxing, filtering for the third time and filling. The method disclosed by the invention has the beneficial effects that unique characteristics of linseed oil raw materials can be greatly retained by adopting an advanced production technique, alpha-linolenic acid in the raw materials can be greatly prevented from being damaged, the oil pump capacity can be improved, and production benefits are increased.

Description

A kind of method of semi-refined siritch
Technical field
The invention belongs to Oil processing field, and in particular to a kind of method of semi-refined siritch.
Background technology
Siritch, also known as linseed oil, is a kind of ancient edible oil, and it is the fat squeezed from Hu section plant sesame seed Fat oil.The happiness of flax natural disposition is cold cold-resistant, is adapted to be grown in western part, Northern cold arid area, in recent years, with entering for science and technology Step, the nutritive value and health care of linseed cause the concern of many field scientists such as medical treatment, food, agricultural.In a large number Result of study show that linseed oil is a kind of high quality food oil, rich in alpha-linolenic acid and various unrighted acids, in human body It is interior to be directly translated into DHA and EPA.Containing 48% leukotrienes in linseed oil, this is highest in vegetable oil, with reparation more The unrighted acid chain of neencephalon neuron membrane, play brain tonic, promote intelligence, reducing blood lipid, platelet aggregation-against, expansion parteriole and Antithrombotic etc..
In traditional vegetable oil production technique, typically do not go to control the temperature parameter in expressing process, cause linseed The reduction of alpha-linolenic acid content in oil, the present invention utilizes modern industry automated control technology, rationally, accurately controls production Each link, alpha-linolenic acid is not damaged in reservation raw material as much as possible, contains the alpha-linolenic acid in linseed oil and measures To raising, while improving oil quality, increase productivity effect.
The content of the invention
The invention aims to solve the deficiencies in the prior art part, there is provided a kind of method of semi-refined siritch.
To achieve these goals, the present invention is realized in the following way:
A kind of method of semi-refined siritch, it is characterised in that comprise the following steps that:
(1) cleaning process:Using the impurity such as cleaning sieve and the iron, stone grass, the soil that go in magnetic machine removing raw material.
(2) parch:In adding raw materials into frying equipment so as to which thermally equivalent carries out frying, temperature control is fried at 200 DEG C Time control processed is controlled at 45-55 kilogram in 40-50 minutes, raw material.
(3) cool down:Shady place being placed on through the raw material of parch and adopting the natural type of cooling, paved, THICKNESS CONTROL is in 2- 5cm, prevents dust impurity pollution, cool time from controlling in 10-12 hours.
(4) crush:Raw material after cooling is crushed using steel mill equipment, grume is ground into, cleaning is then charged into Container in.
(5) mix:Grume greasy filth after crushing is placed in mixer, being proportionally added into the water of 7 ﹪ -9 ﹪ is carried out Even stirring, mixing time was controlled in 15-20 minutes.
(6) squeeze:Squeezing will be carried out using hydraulic oil press through mixed raw material and obtain crude oil, raw material will be filtered with clean Cloth presses mold thickness sized packages, by hydraulic oil press Stress control in 75-85Mpa.
(7) filter:The crude oil obtained after squeezing is filtered by leaf filter equipment, to remove crude oil in it is miscellaneous Matter.
(8) degreasing:Crude oil after filtration is loaded in fining pot, volume controlled is entered in 1.5-2T using water-bath furnace apparatus Row heating is stirred simultaneously, and mixing speed is 60 revs/min, 10 ﹪ saline solutions is added when oil temperature rises to 65 DEG C, uniformly Spray in fining pot, spray time control in 28-30 minutes, the temperature control of 10 ﹪ saline solutions at 75-85 DEG C, quality control In 18-22Kg, when oil temperature rises to again 80 DEG C, continue to stir, mixing time control stops heating in 12-15 minutes, until Till having edible vegetable oil to discharge.
(9) secondary filter:Edible vegetable oil after degreasing is carried out into secondary filter using plate filter, is filtered out miscellaneous in edible vegetable oil Matter.
(10) dewax:Edible vegetable oil is delivered in refrigerator carries out cooling process, and control temperature is less than 0 DEG C, is proportionally added into 50Kg/t pearl salt is stirred, and mixing time is controlled in 40-50min.
(11) three filtrations:The fluid after dewaxing is filtered using leaf filter, except the impurity in deoiling, is obtained Product oil.
(12) it is canned.
Preferably, acid number content is 0.1-0.5KOHmg/g in semi-refined siritch, and peroxide value is 1.0-5.0mmol/ Kg, moisture and volatile matter content is 0.02-0.1 ﹪.
Preferably, frying equipment rotating speed is controlled at 20-50 rev/min during parch.
The beneficial effects of the present invention is:Can be peculiar in greatly reservation siritch raw material using advanced production technology Feature, can greatly retain alpha-linolenic acid in raw material and not be damaged, it is possible to increase oil pump capacity, increase productivity effect.
Description of the drawings
Fig. 1 is a kind of flow chart of the method for semi-refined siritch of the present invention;
Specific embodiment
Below in conjunction with drawings and Examples, the present invention is described in detail, and described embodiment is only the present invention one Section Example, rather than the embodiment of whole.Based on the embodiment in the present invention, those of ordinary skill in the art are not doing Go out resulting other embodiments on the premise of creative work, belong to the scope that the present invention is protected.
As illustrated, a kind of method of semi-refined siritch, comprises the following steps that:
(1) cleaning process:Using the impurity such as cleaning sieve and the iron, stone grass, the soil that go in magnetic machine removing raw material.
(2) parch:In adding raw materials into frying equipment so as to which thermally equivalent carries out frying, temperature control is fried at 200 DEG C Time control processed is controlled at 45-55 kilogram in 40-50 minutes, raw material.
(3) cool down:Shady place being placed on through the raw material of parch and adopting the natural type of cooling, paved, THICKNESS CONTROL is in 2- 5cm, prevents dust impurity pollution, cool time from controlling in 10-12 hours.
(4) crush:Raw material after cooling is crushed using steel mill equipment, grume is ground into, cleaning is then charged into Container in.
(5) mix:Grume greasy filth after crushing is placed in mixer, being proportionally added into the water of 7 ﹪ -9 ﹪ is carried out Even stirring, mixing time was controlled in 15-20 minutes.
(6) squeeze:Squeezing will be carried out using hydraulic oil press through mixed raw material and obtain crude oil, raw material will be filtered with clean Cloth presses mold thickness sized packages, by hydraulic oil press Stress control in 75-85Mpa.
(7) filter:The crude oil obtained after squeezing is filtered by leaf filter equipment, to remove crude oil in it is miscellaneous Matter.
(8) degreasing:Crude oil after filtration is loaded in fining pot, volume controlled is entered in 1.5-2T using water-bath furnace apparatus Row heating is stirred simultaneously, and mixing speed is 60 revs/min, 10 ﹪ saline solutions is added when oil temperature rises to 65 DEG C, uniformly Spray in fining pot, spray time control in 28-30 minutes, the temperature control of 10 ﹪ saline solutions at 75-85 DEG C, quality control In 18-22Kg, when oil temperature rises to again 80 DEG C, continue to stir, mixing time control stops heating in 12-15 minutes, until Till having edible vegetable oil to discharge.
(9) secondary filter:Edible vegetable oil after degreasing is carried out into secondary filter using plate filter, is filtered out miscellaneous in edible vegetable oil Matter.
(10) dewax:Edible vegetable oil is delivered in refrigerator carries out cooling process, and control temperature is less than 0 DEG C, is proportionally added into 50Kg/t pearl salt is stirred, and mixing time is controlled in 40-50min.
(11) three filtrations:The fluid after dewaxing is filtered using leaf filter, except the impurity in deoiling, is obtained Product oil.
(12) it is canned.
Acid number content is 0.1-0.5KOHmg/g in the semi-refined siritch, and peroxide value is 1.0-5.0mmol/kg, Moisture and volatile matter content is 0.02-0.1 ﹪.
Frying equipment rotating speed is controlled at 20-50 rev/min during the parch.
Embodiment 1:
A kind of method of semi-refined siritch of the present invention, comprises the following steps that:
(1) cleaning process:Using the impurity such as cleaning sieve and the iron, stone grass, the soil that go in magnetic machine removing raw material.
(2) parch:In adding raw materials into frying equipment so as to which thermally equivalent carries out frying, temperature control is fried at 200 DEG C Time control processed is controlled at 45-55 kilogram in 40-50 minutes, raw material.
(3) cool down:Shady place being placed on through the raw material of parch and adopting the natural type of cooling, paved, THICKNESS CONTROL is in 2- 5cm, prevents dust impurity pollution, cool time from controlling in 10-12 hours.
(4) crush:Raw material after cooling is crushed using steel mill equipment, grume is ground into, cleaning is then charged into Container in.
(5) mix:Grume greasy filth after crushing is placed in mixer, the water for being proportionally added into 7 ﹪ is uniformly stirred Mix, mixing time was controlled in 15-20 minutes.
(6) squeeze:Squeezing will be carried out using hydraulic oil press through mixed raw material and obtain crude oil, raw material will be filtered with clean Cloth presses mold thickness sized packages, by hydraulic oil press Stress control in 75-85Mpa.
(7) filter:The crude oil obtained after squeezing is filtered by leaf filter equipment, to remove crude oil in it is miscellaneous Matter.
(8) degreasing:Crude oil after filtration is loaded in fining pot, volume controlled is entered in 1.5-2T using water-bath furnace apparatus Row heating is stirred simultaneously, and mixing speed is 60 revs/min, 10 ﹪ saline solutions is added when oil temperature rises to 65 DEG C, uniformly Spray in fining pot, spray time control in 28-30 minutes, the temperature control of 10 ﹪ saline solutions at 75-85 DEG C, quality control In 18Kg, when oil temperature rises to again 80 DEG C, continue to stir, mixing time control stops heating, until having in 12-15 minutes Till edible vegetable oil is discharged.
(9) secondary filter:Edible vegetable oil after degreasing is carried out into secondary filter using plate filter, is filtered out miscellaneous in edible vegetable oil Matter.
(10) dewax:Edible vegetable oil is delivered in refrigerator carries out cooling process, and control temperature is less than 0 DEG C, is proportionally added into 50Kg/t pearl salt is stirred, and mixing time is controlled in 40-50min.
(11) three filtrations:The fluid after dewaxing is filtered using leaf filter, except the impurity in deoiling, is obtained Product oil.
(12) it is canned.
Using the squeezing sunflower oil prepared by above-mentioned processing technology, its acid number is 0.5KOHmg/g, and peroxide value is 1.4mmol/kg, moisture and volatile matter content content is 0.06%.
Embodiment 2:
A kind of method of semi-refined siritch of the present invention, comprises the following steps that:
(1) cleaning process:Using the impurity such as cleaning sieve and the iron, stone grass, the soil that go in magnetic machine removing raw material.
(2) parch:In adding raw materials into frying equipment so as to which thermally equivalent carries out frying, temperature control is fried at 200 DEG C Time control processed is controlled at 45-55 kilogram in 40-50 minutes, raw material.
(3) cool down:Shady place being placed on through the raw material of parch and adopting the natural type of cooling, paved, THICKNESS CONTROL is in 2- 5cm, prevents dust impurity pollution, cool time from controlling in 10-12 hours.
(4) crush:Raw material after cooling is crushed using steel mill equipment, grume is ground into, cleaning is then charged into Container in.
(5) mix:Grume greasy filth after crushing is placed in mixer, the water for being proportionally added into 8 ﹪ is uniformly stirred Mix, mixing time was controlled in 15-20 minutes.
(6) squeeze:Squeezing will be carried out using hydraulic oil press through mixed raw material and obtain crude oil, raw material will be filtered with clean Cloth presses mold thickness sized packages, by hydraulic oil press Stress control in 75-85Mpa.
(7) filter:The crude oil obtained after squeezing is filtered by leaf filter equipment, to remove crude oil in it is miscellaneous Matter.
(8) degreasing:Crude oil after filtration is loaded in fining pot, volume controlled is entered in 1.5-2T using water-bath furnace apparatus Row heating is stirred simultaneously, and mixing speed is 60 revs/min, 10 ﹪ saline solutions is added when oil temperature rises to 65 DEG C, uniformly Spray in fining pot, spray time control in 28-30 minutes, the temperature control of 10 ﹪ saline solutions at 75-85 DEG C, quality control In 20Kg, when oil temperature rises to again 80 DEG C, continue to stir, mixing time control stops heating, until having in 12-15 minutes Till edible vegetable oil is discharged.
(9) secondary filter:Edible vegetable oil after degreasing is carried out into secondary filter using plate filter, is filtered out miscellaneous in edible vegetable oil Matter.
(10) dewax:Edible vegetable oil is delivered in refrigerator carries out cooling process, and control temperature is less than 0 DEG C, is proportionally added into 50Kg/t pearl salt is stirred, and mixing time is controlled in 40-50min.
(11) three filtrations:The fluid after dewaxing is filtered using leaf filter, except the impurity in deoiling, is obtained Product oil.
(12) it is canned.
Using the squeezing sunflower oil prepared by above-mentioned processing technology, its acid number is 0.2KOHmg/g, and peroxide value is 1.0mmol/kg, moisture and volatile matter content content is 0.05%.
A kind of method of semi-refined siritch of the present invention is compared with semi-refined siritch in prior art with production effect The high advantage of good, oil quality, effectively solves the deficiencies in the prior art part, and the present invention can greatly retain siritch Alpha-linolenic acid in raw material is not damaged, it is possible to increase oil pump capacity, increases productivity effect.

Claims (3)

1. a kind of method of semi-refined siritch, it is characterised in that comprise the following steps that:
(1) cleaning process:Using the impurity such as cleaning sieve and the iron, stone grass, the soil that go in magnetic machine removing raw material.
(2) parch:In adding raw materials into frying equipment so as to which thermally equivalent carries out frying, temperature control at 200 DEG C, during frying Between control in 40-50 minutes, raw material control at 45-55 kilogram.
(3) cool down:Shady place being placed on through the raw material of parch and adopting the natural type of cooling, paved, THICKNESS CONTROL is prevented in 2-5cm Only dust impurity pollution, cool time is controlled in 10-12 hours.
(4) crush:Raw material after cooling is crushed using steel mill equipment, grume is ground into, the appearance of cleaning is then charged into In device.
(5) mix:Grume greasy filth after crushing is placed in mixer, the water for being proportionally added into 7 ﹪ -9 ﹪ is uniformly stirred Mix, mixing time was controlled in 15-20 minutes.
(6) squeeze:Squeezing will be carried out using hydraulic oil press through mixed raw material and obtain crude oil, raw material cleaning filter cloth will be pressed Mold thickness sized packages, by hydraulic oil press Stress control in 75-85Mpa.
(7) filter:The crude oil obtained after squeezing is filtered by leaf filter equipment, to remove crude oil in impurity.
(8) degreasing:Crude oil after filtration is loaded in fining pot, volume controlled carries out adding in 1.5-2T using water-bath furnace apparatus Heat is stirred simultaneously, and mixing speed is 60 revs/min, and 10 ﹪ saline solutions are added when oil temperature rises to 65 DEG C, uniform spray To in fining pot, spray time was controlled in 28-30 minutes, and at 75-85 DEG C, quality control exists the temperature control of 10 ﹪ saline solutions 18-22Kg, when oil temperature rises to again 80 DEG C, continues to stir, and mixing time control stops heating, until having in 12-15 minutes Till edible vegetable oil is discharged.
(9) secondary filter:Edible vegetable oil after degreasing is carried out into secondary filter using plate filter, the impurity in edible vegetable oil is filtered out.
(10) dewax:Edible vegetable oil is delivered in refrigerator carries out cooling process, and control temperature is less than 0 DEG C, is proportionally added into 50Kg/ T pearl salt is stirred, and mixing time is controlled in 40-50min.
(11) three filtrations:The fluid after dewaxing is filtered using leaf filter, except the impurity in deoiling, obtains finished product Oil.
(12) it is canned.
2. a kind of method of semi-refined siritch according to claim 1, it is characterised in that:Acid in the semi-refined siritch Value content is 0.1-0.5KOHmg/g, and peroxide value is 1.0-5.0mmol/kg, and moisture and volatile matter content is 0.02-0.1 ﹪.
3. a kind of method of semi-refined siritch according to claim 1, it is characterised in that:Frying during the parch sets Standby rotating speed is controlled at 20-50 rev/min.
CN201710088656.7A 2017-02-20 2017-02-20 Method for semi-refined linseed oil Pending CN106635397A (en)

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Application Number Priority Date Filing Date Title
CN201710088656.7A CN106635397A (en) 2017-02-20 2017-02-20 Method for semi-refined linseed oil

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107312621A (en) * 2017-08-21 2017-11-03 宁夏兴灵粮油有限公司 A kind of linseed oil preparation system
CN108504446A (en) * 2018-04-24 2018-09-07 鞠振霞 A kind of siritch method of refining that can protect omega 3
CN108795570A (en) * 2018-07-04 2018-11-13 宁夏马氏兄弟粮油产业发展有限公司 A kind of siritch filter method and system

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4411499C1 (en) * 1994-04-05 1995-10-26 Allkraft Futtermittel Gmbh Use of natural cold-pressed linseed oil
CN103215118A (en) * 2013-05-13 2013-07-24 宁夏吴忠市国军清真食品有限公司 Cold-pressing method of linseed oil
CN103740458A (en) * 2014-01-26 2014-04-23 刘武综 Method for preparing vegetable oil
CN103937595A (en) * 2014-04-23 2014-07-23 宁夏吴忠市伊盛达粮油有限公司 Linseed oil refining production system
CN106010769A (en) * 2016-07-13 2016-10-12 甘肃长清生物科技有限责任公司 Production method for hot pressed linseed oil

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4411499C1 (en) * 1994-04-05 1995-10-26 Allkraft Futtermittel Gmbh Use of natural cold-pressed linseed oil
CN103215118A (en) * 2013-05-13 2013-07-24 宁夏吴忠市国军清真食品有限公司 Cold-pressing method of linseed oil
CN103740458A (en) * 2014-01-26 2014-04-23 刘武综 Method for preparing vegetable oil
CN103937595A (en) * 2014-04-23 2014-07-23 宁夏吴忠市伊盛达粮油有限公司 Linseed oil refining production system
CN106010769A (en) * 2016-07-13 2016-10-12 甘肃长清生物科技有限责任公司 Production method for hot pressed linseed oil

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107312621A (en) * 2017-08-21 2017-11-03 宁夏兴灵粮油有限公司 A kind of linseed oil preparation system
CN108504446A (en) * 2018-04-24 2018-09-07 鞠振霞 A kind of siritch method of refining that can protect omega 3
CN108795570A (en) * 2018-07-04 2018-11-13 宁夏马氏兄弟粮油产业发展有限公司 A kind of siritch filter method and system

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Application publication date: 20170510