CN106634565A - Method for preparing transparent heat-protecting glass coating - Google Patents
Method for preparing transparent heat-protecting glass coating Download PDFInfo
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- CN106634565A CN106634565A CN201610918964.3A CN201610918964A CN106634565A CN 106634565 A CN106634565 A CN 106634565A CN 201610918964 A CN201610918964 A CN 201610918964A CN 106634565 A CN106634565 A CN 106634565A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- C08L2205/00—Polymer mixtures characterised by other features
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Abstract
The invention relates to a method for preparing a transparent heat-protecting glass coating and belongs to the technical field of preparation of glass coatings. The preparation method disclosed by the invention comprises the following steps: fermenting earthworm skin according to the characteristic that the earthworm skin is not adhered with any soil in the soil, and obtaining anti-fouling components in the skin; grinding thermal insulation matters such as talcum powder, magnesium silicate and the like, mixing with xanthan gum and the like so as to obtain slurry; mixing the slurry, the earthworm fermentation product, hollow glass microspheres and the like so as to obtain a base material; mixing the base material with various aids, so as to obtain the transparent heat-protecting glass coating. The transparent heat-protecting glass coating prepared by the invention is high in water resistance, high in wear resistance, high in anti-fouling ability, high in impact resistance and excellent thermal insulation property. The method disclosed by the invention is easy to operate and convenient for industrial production.
Description
Technical field
The present invention relates to a kind of preparation method of transparent heat insulating glass coating, belongs to glass coating preparing technical field.
Background technology
Glass is widely used as building glass window, glass door, glass curtain wall, motor-vehicle glass window etc., and window is heat turnover
Passage, the heat radiation of sunlight passes through window-glass to heating indoor;The heat-proof quality of glass is energy-saving to the world with great
Contribution.For energy saving, people take various measures to solve the heat-insulating problem of glass.Tradition solves the problems, such as glass heat-proof
Mainly there is three approach, one is to use glass heat-proof pad pasting, but the price of general every square metre of 200-600 unit of import thermal isolation film is too
Height, only uses at present on high-grade car;Two is to use thermal reflecting coating, and by reflectance coating emitting heat quantity, but this product is saturating
Photosensitiveness is poor so as to cannot extensive utilization;Three is LOW-E glass, has domestic manufacturer to produce at present, and equipment and investing huge is runed into
Originally surging to cause per square of wooden price at 150 yuan or so, expensive price constrains the use of user.In recent years, based on material
The development of science and nanometer technology, people begin one's study using transparent heat-insulated nano paint to improve the heat-proof quality of glass.Thoroughly
Bright nano heat insulating coating, there is high-transmission rate to visible ray and there is good reflection near infrared light and ultraviolet light, intercept or
Absorption.The coating is applied into building or vehicle glass, indoor lighting has not both been interfered with, air-conditioning can be suitably reduced again
Alleviating energy crisis and energy-conserving and environment-protective are had great importance by load.
At present, the research with regard to transparent heat insulating glass coating is concentrated mainly on the country such as American-European-Japanese, and research emphasis are mainly
The selection of inorganic functional material, such as ITO(Tin indium oxide)、ATO(Antimony oxidation tin)TiO2(Titanium dioxide)Deng.General principle is profit
With the spectral selection of such nano material, i.e., reflectivity near infrared light and ultraviolet light and to the highly transmissive of visible ray
Property.Nano material is initially formed into the aqueous or solvent-borne type slurry of stable dispersion, is then reapplied in coating, obtain have every
The multifunctional nano coating of hot property.But such insulating glass coating also be present in some practical applications:On the one hand, by
The reflection near infrared ray is based only upon in its mechanism of heat insulation, 70% near-infrared shielding rate is reached, effect of heat insulation need to be improved;
On the other hand, due to being to be applied to open air, at present disclosed transparent heat insulating glass coating is in resistance to water, ultraviolet aging resistance, resistance to
The aspect performances such as mill property have also been short of.
The content of the invention
The technical problem to be solved:For current transparent heat insulating glass coating generally existing resistance to water, wear-resisting
Property, the poor problem of pollution resistance, there is provided a kind of preparation method of bright insulating glass coating, the present invention is first according to earthworm in soil
In earth, its epidermis but without any soil, ferments to earthworm epidermis, obtains its intraepidermal antifoulant composition, then by talcum powder,
The heat-insulated material such as magnesium silicate is crushed, then is mixed with xanthans etc., obtains slurry, then by slurry, Lumbricus fermented product with it is hollow
After the mixing such as glass microsphere, base-material is obtained, after base-material is mixed with various auxiliary agents, you can obtain transparent heat insulating glass coating, this
Invention prepare transparent heat insulating glass water-resistant coating it is good, wearability is good, stain resistance is strong and excellent in cushion effect, heat-insulated
Excellent performance, the present invention is simple to operate, it is easy to industrialized production.
To solve above-mentioned technical problem, the technical solution used in the present invention is:
(1)300~400g earthworms are taken, it is dissected, gone to its surface and deionized water is cleaned 3~5 times, by its surface certainly
After so drying, in being placed in fermentation tank, 500~600mL deionized waters and 6~8g dusty yeasts are sequentially added, at 30~40 DEG C
Sealing and fermenting 6~8 days, fermentation ends are warming up to 90~100 DEG C, stirring 5~10min of sterilizing, collect zymotic fluid, be placed in from
In scheming, 20~30min is centrifuged under 4000~5000r/min, collects supernatant, and be spray-dried, obtain dried object,
I.e. Lumbricus fermented product, standby;
(2)Weigh 60~80g talcum powder, 10~15g magnesium silicates, 20~30g calcium carbonate, 8~12g barium sulfate and 10~20g electric
Gas stone is added in pulverizer to be crushed, and crosses 80~100 mesh sieves, obtains mixed-powder, and mixed-powder is added in beaker,
Add 300~400mL deionized waters, 6~8g xanthans and 3~5g neopelexes, stirring mixing 10~
20min, obtains slurry;
(3)Count by weight, weigh 20~30 parts of steps(1)Standby Lumbricus fermented product, 50~60 parts of above-mentioned slurries, 10~
20 parts of hollow glass micro-balls, 30~40 parts of methyl phenyl silicone resins, 8~12 parts of cellulose whiskers, 3~5 parts of silicon carbide whiskers, plus
Enter in beaker, 20~30min of magnetic agitation obtains base-material;
(4)Count by weight, weigh 60~70 parts of above-mentioned base-materials, 6~8 parts of carboxymethylcellulose calciums, 3~5 parts of poly dimethyl silicon
Oxygen alkane, 1~3 part of ethoxylated dodecyl alcohol, 6~8 parts of butyl glycol ethers, 8~12 parts of methyl silicon sodium alcoholates and 80~90 parts go from
Sub- water, in being added to mixer, stirs 30~40min, you can obtain transparent heat insulating glass coating.
The application process of the present invention:With alcohol wipe glass surface it is dirty after, take transparent heat-insulated glass obtained in the present invention
Glass coating, 1 is pressed by it with water:10 mixing, after 10~20min of stirring, even application controls spray gun with glass in glass surface
Distance is 100~120mm, and coating thickness is surface drying by 6~8mm, 30~40min, and 4~5h can be absolutely dry.After testing, this
After the transparent heat insulating glass coating spraying of bright preparation, light transmittance is 80~85%.
Compared with additive method, Advantageous Effects are the present invention:
(1)The transparent heat insulating glass water-resistant coating for preparing of the invention is good, wearability is good, stain resistance is strong, and shock resistance is strong
Degree is high, heat-proof quality is excellent;
(2)The main preparation process of the present invention is simple, required low cost.
Specific embodiment
300~400g earthworms are taken first, it is dissected, go to its surface and deionized water is cleaned 3~5 times, by it
After surface is dried naturally, in being placed in fermentation tank, 500~600mL deionized waters and 6~8g dusty yeasts are sequentially added, 30~
Sealing and fermenting 6~8 days, fermentation ends at 40 DEG C, are warming up to 90~100 DEG C, and stirring 5~10min of sterilizing collects zymotic fluid, and
It is placed in a centrifuge, 20~30min is centrifuged under 4000~5000r/min, collect supernatant, and be spray-dried, obtains
Dried object, i.e. Lumbricus fermented product, it is standby;
Weigh 60~80g talcum powder, 10~15g magnesium silicates, 20~30g calcium carbonate, 8~12g barium sulfate and 10~20g tourmaline
It is added in pulverizer and is crushed, cross 80~100 mesh sieves, obtain mixed-powder, mixed-powder is added in beaker, then adds
Enter 300~400mL deionized waters, 6~8g xanthans and 3~5g neopelexes, stirring 10~20min of mixing is obtained
To slurry;Count by weight, weigh 20~30 parts of standby Lumbricus fermented products, 50~60 parts of above-mentioned slurries, 10~20 parts of skies
Heart glass microsphere, 30~40 parts of methyl phenyl silicone resins, 8~12 parts of cellulose whiskers, 3~5 parts of silicon carbide whiskers, are added to burning
In cup, 20~30min of magnetic agitation obtains base-material;Count by weight, weigh 60~70 parts of above-mentioned base-materials, 6~8 parts of carboxylic first
Base cellulose, 3~5 parts of dimethyl silicone polymers, 1~3 part of ethoxylated dodecyl alcohol, 6~8 parts of butyl glycol ethers, 8~12 parts
Methyl silicon sodium alcoholate and 80~90 parts of deionized waters, in being added to mixer, stir 30~40min, you can obtain transparent heat-insulated glass
Glass coating.
Example 1
300g earthworms being taken first, it being dissected, gone to its surface and deionized water is cleaned 3 times, its surface is dried naturally
Afterwards, it is placed in fermentation tank, sequentially adds 500mL deionized waters and 6g dusty yeasts, sealing and fermenting 6 days at 30 DEG C, fermentation knot
Beam, is warming up to 90 DEG C, and stirring sterilizing 5min collects zymotic fluid, in being placed in centrifuge, 20min is centrifuged under 4000r/min,
Supernatant is collected, and is spray-dried, obtain dried object, i.e. Lumbricus fermented product, it is standby;Weigh 60g talcum powder, 10g silicic acid
Magnesium, 20g calcium carbonate, 8g barium sulfate and 10g tourmaline are added in pulverizer and are crushed, and cross 80 mesh sieves, obtain mixed-powder,
Mixed-powder is added in beaker, 300mL deionized waters, 6g xanthans and 3g neopelexes is added, is stirred
Mixing 10min, obtains slurry;Count by weight, weigh 20 parts of standby Lumbricus fermented products, 50 parts of above-mentioned slurries, 10 parts of skies
Heart glass microsphere, 30 parts of methyl phenyl silicone resins, 8 parts of cellulose whiskers, 3 parts of silicon carbide whiskers, in being added to beaker, magnetic force is stirred
20min is mixed, base-material is obtained;Count by weight, weigh 60 parts of above-mentioned base-materials, 6 parts of carboxymethylcellulose calciums, 3 parts of poly dimethyl silicon
Oxygen alkane, 1 part of ethoxylated dodecyl alcohol, 6 parts of butyl glycol ethers, 8 parts of methyl silicon sodium alcoholates and 80 parts of deionized waters, are added to stirring
In machine, 30min is stirred, you can obtain transparent heat insulating glass coating.
The application process of the present invention:With alcohol wipe glass surface it is dirty after, take transparent heat-insulated glass obtained in the present invention
Glass coating, 1 is pressed by it with water:10 mixing, after stirring 10min, even application controls the distance of spray gun and glass in glass surface
For 100mm, coating thickness is surface drying by 6mm, 30min, and 4h can be absolutely dry.After testing, the transparent heat-insulated glass that prepared by the present invention
After the spraying of glass coating, light transmittance is 80%.
Example 2
400g earthworms being taken first, it being dissected, gone to its surface and deionized water is cleaned 5 times, its surface is dried naturally
Afterwards, it is placed in fermentation tank, then adds 600mL deionized waters and 8g dusty yeasts successively, sealing and fermenting 8 days at 40 DEG C, fermentation ends,
100 DEG C are warming up to, stirring sterilizing 10min collects zymotic fluid, in being placed in centrifuge, 30min is centrifuged under 5000r/min, receives
Collection supernatant, and be spray-dried, dried object, i.e. Lumbricus fermented product are obtained, it is standby;Weigh 80g talcum powder, 15g magnesium silicates,
30g calcium carbonate, 12g barium sulfate and 20g tourmaline are added in pulverizer and are crushed, and cross 100 mesh sieves, obtain mixed-powder,
Mixed-powder is added in beaker, 400mL deionized waters, 8g xanthans and 5g neopelexes is added, is stirred
Mixing 20min, obtains slurry;Count by weight, weigh 30 parts of standby Lumbricus fermented products, 60 parts of above-mentioned slurries, 20 parts of skies
Heart glass microsphere, 40 parts of methyl phenyl silicone resins, 12 parts of cellulose whiskers, 5 parts of silicon carbide whiskers, in being added to beaker, magnetic force
Stirring 30min, obtains base-material;Count by weight, weigh 70 parts of above-mentioned base-materials, 8 parts of carboxymethylcellulose calciums, 5 parts of poly dimethyls
Siloxanes, 3 parts of ethoxylated dodecyl alcohols, 8 parts of butyl glycol ethers, 12 parts of methyl silicon sodium alcoholates and 90 parts of deionized waters, are added to
In mixer, 40min is stirred, you can obtain transparent heat insulating glass coating.
The application process of the present invention:With alcohol wipe glass surface it is dirty after, take transparent heat-insulated glass obtained in the present invention
Glass coating, 1 is pressed by it with water:10 mixing, after stirring 15min, even application controls the distance of spray gun and glass in glass surface
For 110mm, coating thickness is surface drying by 7mm, 35min, and 4.5h can be absolutely dry.After testing, what prepared by the present invention is transparent heat-insulated
After glass coating spraying, light transmittance is 83%.
Example 3
350g earthworms being taken first, it being dissected, gone to its surface and deionized water is cleaned 4 times, its surface is dried naturally
Afterwards, it is placed in fermentation tank, sequentially adds 550mL deionized waters and 7g dusty yeasts, sealing and fermenting 7 days at 35 DEG C, fermentation knot
Beam, is warming up to 95 DEG C, and stirring sterilizing 8min collects zymotic fluid, in being placed in centrifuge, 25min is centrifuged under 4500r/min,
Supernatant is collected, and is spray-dried, obtain dried object, i.e. Lumbricus fermented product, it is standby;Weigh 70g talcum powder, 13g silicic acid
Magnesium, 25g calcium carbonate, 10g barium sulfate and 15g tourmaline are added in pulverizer and are crushed, and cross 90 mesh sieves, obtain mixed powder
End, mixed-powder is added in beaker, adds 350mL deionized waters, 7g xanthans and 4g neopelexes, is stirred
Mixing 15min is mixed, slurry is obtained;Count by weight, weigh 25 parts of standby Lumbricus fermented products, 55 parts of above-mentioned slurries, 15 parts
Hollow glass micro-ball, 35 parts of methyl phenyl silicone resins, 10 parts of cellulose whiskers, 4 parts of silicon carbide whiskers, in being added to beaker, magnetic
Power stirs 25min, obtains base-material;Count by weight, weigh 65 parts of above-mentioned base-materials, 7 parts of carboxymethylcellulose calciums, 4 parts of poly- diformazans
Radical siloxane, 2 parts of ethoxylated dodecyl alcohols, 7 parts of butyl glycol ethers, 10 parts of methyl silicon sodium alcoholates and 85 parts of deionized waters, add
To in mixer, 35min is stirred, you can obtain transparent heat insulating glass coating.
The application process of the present invention:With alcohol wipe glass surface it is dirty after, take transparent heat-insulated glass obtained in the present invention
Glass coating, 1 is pressed by it with water:10 mixing, after stirring 20min, even application controls the distance of spray gun and glass in glass surface
For 120mm, coating thickness is surface drying by 8mm, 40min, and 5h can be absolutely dry.After testing, the transparent heat-insulated glass that prepared by the present invention
After the spraying of glass coating, light transmittance is 85%.
Claims (1)
1. a kind of preparation method of transparent heat insulating glass coating, it is characterised in that concrete preparation process is:
(1)300~400g earthworms are taken, it is dissected, gone to its surface and deionized water is cleaned 3~5 times, by its surface certainly
After so drying, in being placed in fermentation tank, 500~600mL deionized waters and 6~8g dusty yeasts are sequentially added, at 30~40 DEG C
Sealing and fermenting 6~8 days, fermentation ends are warming up to 90~100 DEG C, stirring 5~10min of sterilizing, collect zymotic fluid, be placed in from
In scheming, 20~30min is centrifuged under 4000~5000r/min, collects supernatant, and be spray-dried, obtain dried object,
I.e. Lumbricus fermented product, standby;
(2)Weigh 60~80g talcum powder, 10~15g magnesium silicates, 20~30g calcium carbonate, 8~12g barium sulfate and 10~20g electric
Gas stone is added in pulverizer to be crushed, and crosses 80~100 mesh sieves, obtains mixed-powder, and mixed-powder is added in beaker,
Add 300~400mL deionized waters, 6~8g xanthans and 3~5g neopelexes, stirring mixing 10~
20min, obtains slurry;
(3)Count by weight, weigh 20~30 parts of steps(1)Standby Lumbricus fermented product, 50~60 parts of above-mentioned slurries, 10~
20 parts of hollow glass micro-balls, 30~40 parts of methyl phenyl silicone resins, 8~12 parts of cellulose whiskers, 3~5 parts of silicon carbide whiskers, plus
Enter in beaker, 20~30min of magnetic agitation obtains base-material;
(4)Count by weight, weigh 60~70 parts of above-mentioned base-materials, 6~8 parts of carboxymethylcellulose calciums, 3~5 parts of poly dimethyl silicon
Oxygen alkane, 1~3 part of ethoxylated dodecyl alcohol, 6~8 parts of butyl glycol ethers, 8~12 parts of methyl silicon sodium alcoholates and 80~90 parts go from
Sub- water, in being added to mixer, stirs 30~40min, you can obtain transparent heat insulating glass coating.
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102020898A (en) * | 2010-10-28 | 2011-04-20 | 华南理工大学 | Nanometer transparent heat insulation coating and preparation method thereof |
US20120040179A1 (en) * | 2009-04-30 | 2012-02-16 | Bakul Champaklal Dave | Anti-Reflective and Anti-Soiling Coatings with Self-Cleaning Properties |
CN102391778A (en) * | 2011-09-05 | 2012-03-28 | 北京首创纳米科技有限公司 | Colored transparent heat insulation glass coating and preparation method thereof |
CN104610825A (en) * | 2015-01-27 | 2015-05-13 | 东南大学 | Heat insulation coating and preparation method thereof |
CN105860689A (en) * | 2016-05-05 | 2016-08-17 | 郭迎庆 | Preparation method of non-smooth surface anti-drag liquid material |
-
2016
- 2016-10-21 CN CN201610918964.3A patent/CN106634565A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20120040179A1 (en) * | 2009-04-30 | 2012-02-16 | Bakul Champaklal Dave | Anti-Reflective and Anti-Soiling Coatings with Self-Cleaning Properties |
CN102020898A (en) * | 2010-10-28 | 2011-04-20 | 华南理工大学 | Nanometer transparent heat insulation coating and preparation method thereof |
CN102391778A (en) * | 2011-09-05 | 2012-03-28 | 北京首创纳米科技有限公司 | Colored transparent heat insulation glass coating and preparation method thereof |
CN104610825A (en) * | 2015-01-27 | 2015-05-13 | 东南大学 | Heat insulation coating and preparation method thereof |
CN105860689A (en) * | 2016-05-05 | 2016-08-17 | 郭迎庆 | Preparation method of non-smooth surface anti-drag liquid material |
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Application publication date: 20170510 |