CN106630667A - An anti-glare (AG) glass processing process adopting silicon oxide sedimentation - Google Patents
An anti-glare (AG) glass processing process adopting silicon oxide sedimentation Download PDFInfo
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- CN106630667A CN106630667A CN201510725839.6A CN201510725839A CN106630667A CN 106630667 A CN106630667 A CN 106630667A CN 201510725839 A CN201510725839 A CN 201510725839A CN 106630667 A CN106630667 A CN 106630667A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
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- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
- C03C17/23—Oxides
- C03C17/25—Oxides by deposition from the liquid phase
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/006—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character
- C03C17/007—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character containing a dispersed phase, e.g. particles, fibres or flakes, in a continuous phase
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
- C03C17/23—Oxides
- C03C17/25—Oxides by deposition from the liquid phase
- C03C17/253—Coating containing SnO2
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
- C03C17/23—Oxides
- C03C17/25—Oxides by deposition from the liquid phase
- C03C17/256—Coating containing TiO2
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/21—Oxides
- C03C2217/213—SiO2
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/21—Oxides
- C03C2217/23—Mixtures
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/70—Properties of coatings
- C03C2217/73—Anti-reflective coatings with specific characteristics
- C03C2217/732—Anti-reflective coatings with specific characteristics made of a single layer
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/70—Properties of coatings
- C03C2217/77—Coatings having a rough surface
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/11—Deposition methods from solutions or suspensions
- C03C2218/111—Deposition methods from solutions or suspensions by dipping, immersion
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/11—Deposition methods from solutions or suspensions
- C03C2218/116—Deposition methods from solutions or suspensions by spin-coating, centrifugation
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/11—Deposition methods from solutions or suspensions
- C03C2218/118—Deposition methods from solutions or suspensions by roller-coating
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- Geochemistry & Mineralogy (AREA)
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Abstract
An anti-glare (AG) glass processing process adopting silicon oxide sedimentation belongs to anti-glare (AG) glass processing processes of a new generation. The process is a result of research and experiments on various problems of traditional sand blasting, spraying and acid corrosion methods. The process includes preparing a sedimentation solution, pretreating glass, coating the glass with the sedimentation solution through a leaching manner or a spin-coating manner, a roller-coating manner or a spraying manner, and after a certain period of time of sedimentation, forming a dense anti-glare film having a certain degree of roughness on the surface of the glass through drying, sintering and other types of after-treatment. Compared with traditional processes, the process has obvious advantages, is free of pollution, high in production quality and stable in production and can completely replace present three traditional processes.
Description
Technical field
The invention belongs to glass post-processing field, belongs to anti-dazzle glas processing technique of new generation
Technical background
AG is the abbreviation of Anti-glare (anti-glare), when ambient is radiated on undressed glass surface, due to the reflection of glass surface, makes one not seeing glass Inner appearances below.When some electronic display units are used such as under light or sunlight, the content of screen can not be often seen.Anti-glare is by the process to glass surface improving this reflecting properties to light of glass so that glass content below is clearly got up.
Anti-dazzle principle is that glass surface is processed, and makes surface become rough whole, and this irregular glass surface can make irradiation light diffuse-reflectance above, so that the content of screen display is apparent from.
AG anti-dazzle glases should have a field
1st, electronic display screen, electronic touch screen
2nd, illuminate, mount a picture
3rd, photovoltaic generation
4th, top-grade furniture, house ornamentation, high-grade building
Existing glass carries out the method for the anti-dazzle processing of AG mainly following three kinds
1st, sand-blast
It is exactly that this technique is developed by glass frosting technology, and this is the anti-dazzle glas processing method of earliest period by glass surface hacking with corundum fine and smooth enough, it is characterized in that process velocity is very slow, surface roughness is uneven, poor product quality, it is impossible to meet the needs that electronic product is developed rapidly.This technique is substantially superseded.
2nd, low-temp. spraying coating
Exactly mix some transparent grains for possessing reflective functions with Polyester Paint, be sprayed on glass surface, then toast drying and aggregate into anti-dazzle face.This method production efficiency is high, and equipment is simple, pollutes not serious, it is but product surface hardness is low, also easily aging, be not suitable for electronic touch screen and outdoor equipment (such as electric advertisement screen, photovoltaic generation etc.), it is only applicable to as mounted a picture and some less demanding fields.
3rd, Fluohydric acid. etching (method is invaded in abbreviation acid)
Exactly mixed with Fluohydric acid. and some adjuvants, process is eroded to glass surface, glass surface becomes coarse because weathering, so that glass surface reaches antiglare effect.The characteristics of this method is to produce the higher product of mass, no matter case hardness, resistance to elevated temperatures, ageing-resistant performance, roughness, mist degree, and the indices such as light transmittance can meet the needs of modern electronic product.The anti-dazzle glas that electron trade is used at present is exactly mainly this technique productions.
The subject matter of this technique is that one is seriously polluted, and Fluohydric acid. and its side-product are all reluctant pollutant, and Fluohydric acid. is harmful to environmental and human health impacts.All it is difficult to obtain environmentally friendly license passport using the enterprise of this technique at present.Two are, unstable product quality is not only affected by liquor strength, are also affected by environment temperature and humidity change, and so as to cause finished product rate low, production cost is high.Three are, the anti-dazzle glas of this technique productions possesses hydrophilic due to anti-dazzle face, easily more mouldy than simple glass, is difficult long-time storage.Four are, this technique cannot be applied to the increasing ultra-thin glass field of current consumption.
For the problem of three of the above traditional handicraft, SiO deposition AG anti-dazzle glas processing technique is we have invented
The content of the invention
The ultimate principle of SiO deposition AG anti-dazzle glas processing technique is, using liquid phase deposition, to deposit last layer in glass surface and possess the dense film that the oxidized silicon of certain roughness is combined with glass surface with chemical bond, so as to form anti-dazzle face.Its technical process is as follows：
1st, prepare deposition liquid
With silicic acid, metasilicic acid, sodium silicate, potassium silicate, methyl silicate, silester, sodium metasilicate, potassium metasilicate, metasilicic acid ethyl ester, metasilicic acid methyl ester, methyl acetate, after one or more of ethyl acetate mix by a certain percentage, with suitable quantity of water under the conditions of certain environment, methanol, ethanol, acetone, one or more solvents in carbon tetrachloride fuse, add appropriate additive again under certain environment, the acting as of additive slows down agent, accelerator, binding agent, dispersant and agent can be sent out, additive is from oxalic acid respectively, hydrochloric acid, sulphuric acid, phosphoric acid, acetic acid, potassium hydroxide, sodium hydroxide, sodium phosphate, potassium phosphate, n-butyl alcohol, isobutanol, sec-butyl alcohol, choose in the reagents such as the tert-butyl alcohol.The solution for preparing forms qualified coating liquid under the conditions of certain environment, according to the requirement of different cultivars antiglare effect, appropriate suspensible nano material can be added, it is aluminium oxide, Zinc Oxide, stannum oxide, titanium oxide, one or more mixture in silicon oxide respectively, medicinal liquid can be standby after preparing.
2nd, glass pre-treatment
Glass unpack after through cutting, edging, clean, select, it is standby.
3rd, coating deposition liquid
Under the conditions of certain environment, the deposition liquid for preparing is coated uniformly on glass surface, forms anti-dazzle deposition film, after coating deposition liquid, need the deposition process of certain hour.
The method of coating deposition liquid includes：1st, extraction, is exactly in glass immersion deposition liquid, and to keep certain hour, then glass is enhanced from medicinal liquid with certain speed, so as to form certain thickness film in glass surface.2nd, spin-coating method, exactly fixes glass on one disk, and glass and disk are rotated with certain speed together, and the heart presses certain speed by medicinal liquid drip on glass in glass, and as glass rotates, medicinal liquid can be uniformly distributed and hold, and form film.3rd, rolling method, is exactly the soft roller with similar sponge on glass, with the rotation and the movement of glass of soft roller, medicinal liquid is coated uniformly on glass surface and forms film 4, spraying process, is exactly, in glass surface, to form film with spray gun medicinal liquid even application.Four kinds of methods of the above need to choose different painting methods according to the anti-dazzle glas of different cultivars.
4th, post processing
After deposition certain hour, you can glass is dried, between 10 minutes to 8 hours, drying temperature is between 30 DEG C to 100 DEG C for drying time.
After drying, you can enter sintering furnace, between 150 DEG C to 650 DEG C, sintering time is between 10 minutes to 8 hours for sintering temperature.
The organic substance volatilization of the glass surface after sintering, what is stayed are the films that fine and close exquisiteness possesses that the oxidized silicon of certain roughness is linked with chemical bond and glass surface.
5th, technique and products characteristics
As silicon oxide is that, than simple glass transparency more preferably material, inherently possess certain effect for reducing visible reflectance, therefore can effectively improve the transparency of glass.Transparency be simple glass 87% or so, Jing test, Jing this technique processing after transparency bring up to 92% or so.
As silicon oxide and glass surface are that, with chemical bonds, therefore the firmness of antiglare film is not less than the intensity of glass itself.
As the hardness of inorganic material in silicon oxide and film itself is more than glass hard (HRC65Yi Shang), therefore anti-dazzle surface hardness more than the hardness of glass itself, Jing tests anti-dazzle surface hardness and can reach more than 7h.
Due to using silicon oxide deposition method, therefore anti-dazzle face can be finer and smoother, Jing tests, and the roughness in the anti-dazzle face of anti-dazzle glas of this technique processing is between 0.1-0.2 microns.
Because the anti-dazzle glas of SiO deposition production, property indices all meet or exceed acid and invade method, production process does not pollute, and there will not be pollutant generation, so being anti-dazzle glas processing technique of new generation.
Claims (2)
1. the claims in the present invention are to adopt SiO deposition to be formed with certain roughness in glass surface and be oxidized silicon with chemistry
The dense film that key is combined with glass surface, reaches the technical scheme that glass surface possesses antiglare effect.
2. the claims in the present invention are machining process, i.e.,：
Prepare deposition liquid：With silicic acid, metasilicic acid, sodium silicate, potassium silicate, methyl silicate, silester, sodium metasilicate, metasilicic acid
The one of which such as potassium, metasilicic acid ethyl ester, metasilicic acid methyl ester, methyl acetate, ethyl acetate, or wherein several reagents are by a definite proportion
Example mixing, it is molten with one or more solvents in suitable quantity of water, methanol, ethanol, acetone, carbon tetrachloride under the conditions of certain environment
Close, then appropriate additive is added under certain environment, the acting as of additive slows down agent, accelerator, binding agent, dispersant
And volatilizer, additive be respectively from oxalic acid, hydrochloric acid, sulphuric acid, phosphoric acid, acetic acid, potassium hydroxide, sodium hydroxide, sodium phosphate,
Choose in the reagents such as potassium phosphate, n-butyl alcohol, isobutanol, sec-butyl alcohol, the tert-butyl alcohol.The solution for preparing shape under the conditions of certain environment
Into qualified deposition liquid, according to the requirement of different cultivars antiglare effect, appropriate suspensible nano material can be added, respectively
It is aluminium oxide, Zinc Oxide, stannum oxide, titanium oxide, one or more mixing in silicon oxide, medicinal liquid can be standby after preparing.
Glass pre-treatment：Glass unpack after through cutting, edging, clean, select, it is standby.
Coating deposition liquid：Under the conditions of certain environment, the deposition liquid for preparing is coated uniformly on glass surface, forms anti-dazzle deposition film,
The deposition process of certain hour is needed after deposition film coating.The method of coating deposition liquid includes：1st, extraction, exactly soaks glass
Enter to deposit in liquid, and keep certain hour, then glass is enhanced from medicinal liquid with certain speed, so as in glass surface
Form certain thickness film.2nd, spin-coating method, exactly fixes glass on one disk, and glass and disk are together with certain speed
Rotation, and the heart presses certain speed by medicinal liquid drip on glass in glass, as glass rotates, medicinal liquid can be uniformly distributed and hold,
Form film.3rd, rolling method, is exactly the soft roller with similar sponge on glass, with the rotation of soft roller, medicinal liquid is coated uniformly on
Glass surface forms film 4, spraying process, is exactly, in glass surface, to form film with spray gun medicinal liquid even application.Four kinds of sides of the above
Method chooses different methods according to the performance requirement of different quality anti-dazzle glases.
Post processing：After deposition certain hour, you can glass is dried, between 10 minutes to 8 hours, drying temperature exists drying time
Between 30 DEG C to 100 DEG C.
After drying, you can sintering, between 150 DEG C to 650 DEG C, sintering time is between 10 minutes to 8 hours for sintering temperature.
Glass surface after sintering organic substance volatilization, stay be fine and close exquisiteness possess certain roughness be oxidized silicon with chemical bond with
The film that glass surface combines.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510725839.6A CN106630667A (en) | 2015-11-02 | 2015-11-02 | An anti-glare (AG) glass processing process adopting silicon oxide sedimentation |
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| CN201510725839.6A CN106630667A (en) | 2015-11-02 | 2015-11-02 | An anti-glare (AG) glass processing process adopting silicon oxide sedimentation |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107500556A (en) * | 2017-07-31 | 2017-12-22 | 重庆市中光电显示技术有限公司 | Long acting antibiotic anti-dazzle protective glass for touch-screen and preparation method thereof |
| CN107500562A (en) * | 2017-07-31 | 2017-12-22 | 重庆市中光电显示技术有限公司 | A kind of high grade of transparency glass for touch-screen and preparation method thereof |
| CN107540240A (en) * | 2017-07-31 | 2018-01-05 | 重庆市中光电显示技术有限公司 | A kind of antifouling anti-dazzle shows glass and preparation method thereof |
| CN108298830A (en) * | 2018-04-10 | 2018-07-20 | 深圳市格络光电有限公司 | A kind of preparation method and antibacterial glare proof glass of antibacterial anti-dazzle treatment fluid |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103466958A (en) * | 2013-09-22 | 2013-12-25 | 四川世创达电子科技有限公司 | Anti-dazzle method for optical glass by wet process |
| CN103979800A (en) * | 2014-03-31 | 2014-08-13 | 广州视睿电子科技有限公司 | Antidazzle toughened glass and preparation method thereof |
| CN104877290A (en) * | 2015-06-08 | 2015-09-02 | 西安钧盛新材料科技有限公司 | Preparation method for anti-glare material and anti-glare glass product |
-
2015
- 2015-11-02 CN CN201510725839.6A patent/CN106630667A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103466958A (en) * | 2013-09-22 | 2013-12-25 | 四川世创达电子科技有限公司 | Anti-dazzle method for optical glass by wet process |
| CN103979800A (en) * | 2014-03-31 | 2014-08-13 | 广州视睿电子科技有限公司 | Antidazzle toughened glass and preparation method thereof |
| CN104877290A (en) * | 2015-06-08 | 2015-09-02 | 西安钧盛新材料科技有限公司 | Preparation method for anti-glare material and anti-glare glass product |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107500556A (en) * | 2017-07-31 | 2017-12-22 | 重庆市中光电显示技术有限公司 | Long acting antibiotic anti-dazzle protective glass for touch-screen and preparation method thereof |
| CN107500562A (en) * | 2017-07-31 | 2017-12-22 | 重庆市中光电显示技术有限公司 | A kind of high grade of transparency glass for touch-screen and preparation method thereof |
| CN107540240A (en) * | 2017-07-31 | 2018-01-05 | 重庆市中光电显示技术有限公司 | A kind of antifouling anti-dazzle shows glass and preparation method thereof |
| CN108298830A (en) * | 2018-04-10 | 2018-07-20 | 深圳市格络光电有限公司 | A kind of preparation method and antibacterial glare proof glass of antibacterial anti-dazzle treatment fluid |
| CN108298830B (en) * | 2018-04-10 | 2021-07-13 | 深圳市格络新材科技有限公司 | Preparation method of antibacterial anti-glare treatment liquid and antibacterial anti-glare glass |
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Application publication date: 20170510 |