CN106630549A - Melted glass vacuumizing and defoaming device and method thereof - Google Patents

Melted glass vacuumizing and defoaming device and method thereof Download PDF

Info

Publication number
CN106630549A
CN106630549A CN201611030686.4A CN201611030686A CN106630549A CN 106630549 A CN106630549 A CN 106630549A CN 201611030686 A CN201611030686 A CN 201611030686A CN 106630549 A CN106630549 A CN 106630549A
Authority
CN
China
Prior art keywords
smelting furnace
furnace
glass
vacuum extractor
vacuumizing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201611030686.4A
Other languages
Chinese (zh)
Other versions
CN106630549B (en
Inventor
邓浩
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chongqing huabinwei Glass Co.,Ltd.
Original Assignee
Chongqing Zhaofeng Galssware Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chongqing Zhaofeng Galssware Co Ltd filed Critical Chongqing Zhaofeng Galssware Co Ltd
Priority to CN201611030686.4A priority Critical patent/CN106630549B/en
Publication of CN106630549A publication Critical patent/CN106630549A/en
Application granted granted Critical
Publication of CN106630549B publication Critical patent/CN106630549B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B5/00Melting in furnaces; Furnaces so far as specially adapted for glass manufacture
    • C03B5/16Special features of the melting process; Auxiliary means specially adapted for glass-melting furnaces
    • C03B5/225Refining

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Glass Melting And Manufacturing (AREA)

Abstract

The invention belongs to the technical field of glass production, and in particular relates to a melted glass vacuumizing and defoaming device and a method thereof. The device comprises a melting furnace and an extrusion mechanism, wherein combustion chambers are formed in the periphery and bottom of the melting furnace; a combustion engine is fixedly arranged on one side of the bottom of the melting furnace; a furnace lid is arranged on the top of the melting furnace; a first connecting pipe penetrates through the furnace lid; a first vacuumizing device is connected to one side, which is far away from the furnace lid, of the first connecting pipe; the extrusion mechanism comprises a siphon; the opening end of the siphon penetrates through the side wall of the melting furnace and is arranged in the melting furnace; and a molding furnace is arranged below the opening end of the siphon. The problem that the quality of glass products is influenced by bubbles produced in the process of melting the molten glass in the melting furnace is solved.

Description

Melten glass vacuumizing and defoaming devices and methods therefor
Technical field
The invention belongs to field of glass production technology, more particularly to a kind of melten glass vacuumizing and defoaming device and its side Method.
Background technology
The manufacturing process of glass is generally divided into following steps:Dispensing, found, be molded, four master operations of annealing.Wherein match somebody with somebody The composition of the starting material employed in material step, weight proportion determine the key property and quality of the glass produced; The equipment founded, be molded and anneal etc. used in step, the process conditions for being adopted then determine produced glass Whether the quality and technical requirements of finished glass disclosure satisfy that.
Melting process is the physical-chemical reaction process of a complexity, comprising silicate formation stages, glass formation stages, Clarification homogenizing stage, wherein clarification stage are the processes that bubble is eliminated.Raise viscosity of glass metal drop with temperature in this course Low, equilibrium establishment between physical dissolution and chemically combined gas in gas and glass metal, makes visible in the gas, kiln in bubble Bubble floats on metal level and is eliminated.
The patent of invention of the B of Authorization Notice No. CN 103848556 discloses a kind of improved glass-melting furnace, and the device includes Smelting furnace, the surrounding of smelting furnace and bottom are provided with combustion chamber, and regenerator, the regenerator are provided with the outside of the smelting furnace surrounding combustion chamber Outside be provided with heat-insulating room, the side of the combustion chamber of the bottom is provided with combustor, and the afterbody of the combustor is provided with blower fan, institute The upper end for stating smelting furnace is provided with lid, and the upper lid is provided with extrusion device, and the lower end of the extrusion device is placed in molten through upper lid In stove, the extrusion device for being placed in smelting furnace is formed around screen pack, is connected with the extrusion device being placed in smelting furnace Ascending pipe, the ascending pipe is connected by connecting tube through upper lid with vacuum extractor, and the device can be collected in combustion process Heat, reused, saved the energy, using extrusion device and the pattern of ascending pipe, not only overcome liquation itself from The difficulty of liquid is difficult out again, and the screen pack on extrusion device can also play a part of to isolate impurity, improve the clean rate of liquation; But the device arranges extrusion device during founding to glass, only on bell, facilitate the derivation of liquation, it is right The bubble produced in smelting furnace fusion process is not processed, and has bubble to cause the glassware of final manufacture in glass melts Middle generation bubble, affects the quality of glassware.
The content of the invention
The present invention in order to solve smelting furnace in glass melts fusion process in produce bubble can affect glassware quality Problem, there is provided a kind of melten glass vacuumizing and defoaming device and the side by the device to melten glass vacuumizing and defoaming Method.
In order to achieve the above object, first foundation scheme of the invention provides a kind of melten glass vacuumizing and defoaming device, Including smelting furnace and extrusion mechanism, the surrounding of smelting furnace and bottom are provided with combustion chamber, and the bottom of smelting furnace is provided with combustor, the top of smelting furnace Portion is provided with bell, and through there is the first connecting tube on bell, the first connecting tube is connected with the first vacuum means away from one end of bell Put, extrusion mechanism includes siphon pipe, siphon pipe openend is placed in smelting furnace through furnace sidewall, and the siphonal port of export is connected with Forming furnace.
The principle of this base case is:Smelting furnace is used for placing preparing glass charge, and combustor is used for furnace heats, smelting furnace four Energy produced by combustor burning can quickly be passed to smelting furnace by the combustion chamber of week and bottom;On bell first vacuumizes Device can pass through to vacuumize the effect for reaching bubble removing to the glass melts in smelting furnace, and its cardinal principle be:In glass In melting process, as the viscosity of the rising glass melts of temperature is reduced, according to Stokes' law, the rate of climb of bubble with The radius squared of bubble is directly proportional, and is inversely proportional to viscosity of glass metal, and due to the first vacuum extractor on bell it is constantly right Smelting furnace is vacuumized, and the air pressure in stove gradually increases less than the air pressure in bubble, the bubble diameter in glass melts, therefore, With the continuous rising constantly vacuumized with glass melts temperature of the first vacuum extractor on bell, bubble diameter constantly increases With the continuous reduction of liquation viscosity so that bubble is quickly floated on glass melts surface, until bubbles burst disappears;Smelting furnace one The siphon pipe of side extrusion mechanism, applies siphon principle, by vacuumizing generation to the siphon pipe air-breathing near forming furnace one end Negative pressure, the glass melts in glass-melting furnace are sucked in forming furnace.
The beneficial effect of this base case is:1st, this device is passed through by arranging the first vacuum extractor on bell Smelting furnace is vacuumized can be so that the bubble in glass melts constantly swells until rupture so that glass melts fusion process is produced Bubble substantially all burst;2nd, the siphon pipe in this device extrusion mechanism, make use of siphon principle, can by glass melts from Derive in glass-melting furnace, whole device solves the bubble produced in the glass melts fusion process in smelting furnace can affect glass system The problem of product quality.
Scheme two:Scheme is preferred based on this, and siphonal material is platinum.Beneficial effect:The siphon of platinum material Pipe resistance to corrosion is strong.
Scheme three:This is preferred for scheme two, and the first connecting tube is the thin-walled rubber pipe of quality of rubber materials.Beneficial effect:It is thin First connecting tube of wall quality of rubber materials is flexible, cheap, the first connecting tube of flexible material and the connection of vacuum extractor It is convenient, fast.
Scheme four:This is preferred for scheme three, and also including the second connecting tube, second connecting tube one end is connected with siphon pipe, The other end is connected with the second vacuum extractor.Beneficial effect:Glass melts in a furnace are gone after bubble, can be by rubber hose The vacuum extractor of connection is arranged on siphon pipe, siphon pipe is vacuumized by vacuum extractor, by the glass in smelting furnace Glass liquation is imported in forming furnace and is molded.
Scheme five:This is preferred for scheme four, and the side wall of smelting furnace is made up of castable refractory.Beneficial effect:Founding is resistance to The furnace sidewall of fiery Material texture is all not susceptible to chemical reaction with Acidity of Aikalinity slag at high temperature, it is to avoid glass melting process In corrosion to furnace wall.
Second base case:Using the method for melten glass vacuumizing and defoaming device deaeration, comprise the following steps:
The first step:It is placed in batch mixer after the preparing glass charge for having configured is weighed and is well mixed, the preparing glass charge for mixing is put In smelting furnace, open combustor and the preparing glass charge in smelting furnace is heated, heating-up temperature is in 1300 ~ 1600 ゜ C;
Second step:, the first vacuum extractor being then turned on bell carries out taking out true by the first vacuum extractor to smelting furnace Sky, closes the first vacuum extractor when vacuum reaches 22mmHg, inside furnace pressurize 30 minutes;
3rd step:The second vacuum extractor is opened, siphon pipe is vacuumized by the second vacuum extractor, in treating smelting furnace Glass melts take the second vacuum extractor away when flowing to forming furnace by siphon pipe.
The principle of this base case is:The preparing glass charge for having configured is mixed after weighing in batch mixer, can be made Obtain preparing glass charge to be well mixed, the preparing glass charge being well mixed is placed in into smelting furnace, and melted at a temperature of 1300 ~ 1600 ゜ C Change, the temperature fullys meet the fusing point of glass so that the glass in smelting furnace is in molten condition;For the glass under molten condition Liquation is vacuumized, when vacuum reaches 22mmHg, because the air pressure in glass blister is more than the air pressure in smelting furnace, glass Bubble in liquation constantly rises so that bubble constantly swells, until rupture;Second vacuum extractor carries out taking out true to siphon pipe Sky, based on siphon principle, the liquation in smelting furnace is imported in forming furnace from smelting furnace.Beneficial effect:Can be made by the method for operating Bubble in glass melts swells to rupture and the glass melts gone after bubble can be exported in forming furnace and is molded.
Description of the drawings
Fig. 1 is melten glass vacuumizing and defoaming schematic device of the present invention.
Specific embodiment
Below by specific embodiment, the present invention is further detailed explanation:
Reference in Figure of description includes:
First vacuum extractor 10, bell 11, siphon pipe 12, forming furnace 13, combustor 14, combustion chamber 15, smelting furnace 16, first connect Adapter 17, the second vacuum extractor 18, the second connecting tube 19.
Embodiment one:Melten glass vacuumizing and defoaming device as shown in Figure 1, including smelting furnace 16, the surrounding of smelting furnace 16 and Bottom is provided with combustion chamber 15, and combustor 14 is installed in the left side of the bottom of smelting furnace 16, and the top of smelting furnace 16 has been bolted bell 11, first vacuum extractor 10 is connected by first connecting tube of thin-walled 17 of quality of rubber materials on bell 11, the right side of smelting furnace 16 is consolidated Surely the siphon pipe 12 of the platinum material of inverted U is connected, the left end of siphon pipe 12 is placed in smelting furnace 16 through the side wall of smelting furnace 16, siphon Forming furnace 13 is placed in the right-hand member lower section of pipe 12, and the position of forming furnace 13 is less than smelting furnace 16.
When melten glass is founded, the charger sheet that designs is first according to by silica and other chemical substances(Soda ash, stone Lime stone and quartz)Weigh, the material after weighing is placed in pulverizer and is crushed, the preparing glass charge after crushing is stirred rearmounted In smelting furnace 16, open combustor 14 and the preparing glass charge in smelting furnace 16 is heated so as to which heating and temperature control is in 1550- 1600℃;The control valve of the first vacuum extractor 10 on bell 11 is then turned on, an observation window can be set on bell 11, Bubble in smelting furnace 16 is seen disappears substantially, and till glass melts no longer bubbling, the whole pumpdown time is about controlled in 3-4 Individual hour, the flow on the first vacuum extractor 10 when vacuum reaches 22mmHg can be closed and be kept for 30 minutes;Will Second vacuum extractor 18 on the right side of siphon pipe 12 is connected on the siphon pipe 12 of forming furnace 13 by the second connecting tube 19, is opened Second vacuum extractor 18 is aspirated to siphon pipe 12, treats that the glass melts in smelting furnace 16 flow to forming furnace by siphon pipe 12 Take second vacuum extractor 18 of the one end of siphon pipe 12 when 13 away so that glass melts constantly flow to forming furnace 13.
Using the method for melten glass vacuumizing and defoaming device deaeration, comprise the following steps:
The first step:Prepare preparing glass charge according to the formula list for designing, after the preparing glass charge for having configured is weighed batch mixer is placed in In be well mixed, the preparing glass charge for mixing is placed in smelting furnace 16, open combustor 14 preparing glass charge in smelting furnace 16 is entered Row heating, heating-up temperature is in 1300 ~ 1600 ゜ C;
Second step:, the first vacuum extractor 10 being then turned on bell 11 entered by the first vacuum extractor 10 to smelting furnace 16 Row is vacuumized, and when vacuum reaches 22mmHg the first vacuum extractor 10 is closed and kept for 30 minutes, is closed first and is taken out true Empty device 10;
3rd step:The second vacuum extractor 18 is opened, siphon pipe 12 is vacuumized by the second vacuum extractor 18, it is fusion Glass melts in stove 16 take the second vacuum extractor 18 away when flowing to forming furnace.
By the melten glass vacuumizing and defoaming device to glassware obtained in the glass melts after deaeration, surface is basic Without bubble, made by glassware quality be greatly improved.
Above-described is only embodiments of the invention, and the general knowledge here such as known concrete structure and characteristic is not made in scheme Excessive description.It should be pointed out that for a person skilled in the art, on the premise of without departing from present configuration, can be with Some deformations and improvement are made, these should also be considered as protection scope of the present invention, these are implemented all without the impact present invention Effect and practical applicability.This application claims protection domain should be defined by the content of its claim, in specification Specific embodiment etc. records the content that can be used for explaining claim.

Claims (6)

1. melten glass vacuumizing and defoaming device, including smelting furnace and extrusion mechanism, the surrounding of the smelting furnace and bottom are provided with burning Room, it is characterised in that the bottom of the smelting furnace is provided with combustor, is provided with bell at the top of the smelting furnace, pass through on the bell The first connecting tube is installed with, first connecting tube is connected with the first vacuum extractor, the extrusion mechanism away from one end of bell Including siphon pipe, the siphon pipe openend is placed in smelting furnace through furnace sidewall, and the siphon pipe port of export is connected with forming furnace.
2. melten glass vacuumizing and defoaming device as claimed in claim 1, it is characterised in that the siphonal material is Platinum.
3. melten glass vacuumizing and defoaming device as claimed in claim 2, it is characterised in that first connecting tube is rubber The thin-walled rubber pipe of material.
4. melten glass vacuumizing and defoaming device as claimed in claim 3, it is characterised in that also including the second connecting tube, institute State second connecting tube one end to be connected with siphon pipe, the other end is connected with the second vacuum extractor.
5. melten glass vacuumizing and defoaming device as claimed in claim 4, it is characterised in that the side wall of the smelting furnace is by founding Refractory material is made.
6. the method that usage right requires the melten glass vacuumizing and defoaming device deaeration described in 1, comprises the following steps:
The first step:It is placed in batch mixer after the preparing glass charge for having configured is weighed and is well mixed, the preparing glass charge for mixing is put In smelting furnace, open combustor and the preparing glass charge in smelting furnace is heated, heating-up temperature is in 1300 ~ 1600 ゜ C;
Second step:The first vacuum extractor on bell is opened, smelting furnace is vacuumized by the first vacuum extractor, true Reciprocal of duty cycle closes the first vacuum extractor when reaching 22mmHg, inside furnace pressurize 30 minutes;
3rd step:The second vacuum extractor is opened, siphon pipe is vacuumized by the second vacuum extractor, in treating smelting furnace Glass melts take the second vacuum extractor away when flowing to forming furnace by siphon pipe.
CN201611030686.4A 2016-11-22 2016-11-22 Melten glass vacuumizing and defoaming devices and methods therefor Active CN106630549B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611030686.4A CN106630549B (en) 2016-11-22 2016-11-22 Melten glass vacuumizing and defoaming devices and methods therefor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611030686.4A CN106630549B (en) 2016-11-22 2016-11-22 Melten glass vacuumizing and defoaming devices and methods therefor

Publications (2)

Publication Number Publication Date
CN106630549A true CN106630549A (en) 2017-05-10
CN106630549B CN106630549B (en) 2019-03-15

Family

ID=58808568

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611030686.4A Active CN106630549B (en) 2016-11-22 2016-11-22 Melten glass vacuumizing and defoaming devices and methods therefor

Country Status (1)

Country Link
CN (1) CN106630549B (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201250175Y (en) * 2008-08-25 2009-06-03 京东方科技集团股份有限公司 Discharging device of glass furnace
CN201933137U (en) * 2010-12-30 2011-08-17 重庆硏镁科技有限公司 Vacuum magnesium alloy melting device
CN103848556A (en) * 2012-11-28 2014-06-11 沈国宝 Improved glass melting furnace
CN204714688U (en) * 2015-06-02 2015-10-21 重庆市盛源安全节能玻璃有限公司 A kind of glass-melting furnace

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201250175Y (en) * 2008-08-25 2009-06-03 京东方科技集团股份有限公司 Discharging device of glass furnace
CN201933137U (en) * 2010-12-30 2011-08-17 重庆硏镁科技有限公司 Vacuum magnesium alloy melting device
CN103848556A (en) * 2012-11-28 2014-06-11 沈国宝 Improved glass melting furnace
CN204714688U (en) * 2015-06-02 2015-10-21 重庆市盛源安全节能玻璃有限公司 A kind of glass-melting furnace

Also Published As

Publication number Publication date
CN106630549B (en) 2019-03-15

Similar Documents

Publication Publication Date Title
CN103951158B (en) The vacuum fusion stove of a kind of infrared glass and found system and method
CN1326803C (en) Hollow cast ceramic core and its preparation method
CN102485971B (en) Vitreous silica crucible
CN206828356U (en) A kind of platinum channel
CN104603082B (en) Purposes based on the castable refractory of aluminum oxide, zirconium dioxide and silica and this material
CN103624237A (en) Magnesium alloy counter-gravity casting device and method
CN113754247B (en) Method for producing glass substrate by utilizing platinum channel
CN104370438A (en) Molten glass clarifying and homogenizing device and method
CN208362171U (en) A kind of energy saving kiln
CN111360239B (en) Baking method and device for submerged nozzle
CN113860704B (en) High borosilicate glass smelting pot
TW201714840A (en) Apparatus and method for manufacturing glass sheet capable of uniformly heating the molten glass in a clarification tube without disturbing the flow of the gas in the gas phase space
CN105177333B (en) A kind of smelting apparatus of anti-oxidant tin soldering alloys and preparation method thereof
CZ299360B6 (en) Vacuum degassing apparatus for molten glass and method to rise temperatures of vacuum degassing vessel
JP7127587B2 (en) Alkali-free glass substrate
CN113772930B (en) Quartz crucible preparation device and method for reducing dehydroxylation in quartz crucible
CN104556633A (en) Preparation method and preparation device for chalcogenide glass
CN106630549A (en) Melted glass vacuumizing and defoaming device and method thereof
CN107572785A (en) Vial manufacture craft
CN106555224A (en) A kind of production method and production equipment of monocrystal silicon
CN203741207U (en) Vacuum melting furnace and founding system of infrared glass
CN111811274A (en) Advanced composite material test furnace
CN110204176A (en) The microwave of glass batch is pre- to be melted and then full melting technology and its equipment
CN206589087U (en) A kind of common casting zirconia-corundum refractory brick foamed bricks casting equipment
CN205014832U (en) Electromagnetic stirring formula aluminum mixing vessel

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20200617

Address after: Lot e1-01 / 01, Baisha Industrial Park, Jiangjin District, Chongqing

Patentee after: Chongqing huabinwei Glass Co.,Ltd.

Address before: 401532 Chongqing Qingping Hechuan town of Willow Village

Patentee before: CHONGQING ZHAOFENG GLASSWARE Co.,Ltd.