CN106629910A - Demulsifying and purifying agent, and preparation method thereof - Google Patents
Demulsifying and purifying agent, and preparation method thereof Download PDFInfo
- Publication number
- CN106629910A CN106629910A CN201611165059.1A CN201611165059A CN106629910A CN 106629910 A CN106629910 A CN 106629910A CN 201611165059 A CN201611165059 A CN 201611165059A CN 106629910 A CN106629910 A CN 106629910A
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- parts
- trichloride
- aluminium
- sewage
- calcium chloride
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/40—Devices for separating or removing fatty or oily substances or similar floating material
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
Abstract
The invention discloses a demulsifying and purifying agent, and a preparation method thereof. The demulsifying and purifying agent consists of the following components in parts by mass: 2 to 4 parts of a sewage purifying agent, 10 to 15 parts of diatomite, 16 to 18 parts of natural soap powder, 4 to 6 parts of polyferric sulfate, 6 to 8 parts of soybean phospholipid, 6 to 8 parts of aluminum trichloride hexahydrate, 5 to 9 parts of copper ions, 5 to 7 parts of anhydrous calcium chloride, 6 to 8 parts of ferric trichloride, 6 to 10 parts of octadecyl methacrylate, 20 to 30 parts of poly aluminium chloride and 2 to 4 parts of anionic polyacrylamide. The demulsifying and purifying agent is good in sewage treatment effect and small in investment, guarantees personal safety, reduces production cost, saves energy, saves work time and realizes ecological and environmental-friendly safety production operation.
Description
Technical field
The present invention relates to filth disposal technical field, in particular to a kind of demulsification clarifier and preparation method thereof.
Background technology
Auto manufacturing and mechanical industry, need in process of production a large amount of emulsions and the cleaning agent for adopting, itself
The main polluted factors that environment can be caused of chemical constitution, typically process high concentrated organic wastewater, use calcium chloride and
Oxidant, i.e. hydrochloric acid and sulfuric acid, it has the disadvantage：
1. process is more complicated, less efficient, high cost；
2. invest big, operation difficulty is high, safety print is suffered from many.
The content of the invention
The invention provides a kind of demulsification clarifier and preparation method thereof, its good sewage processing effect of the invention, invest little,
Ensure personal safety, reduce production cost, energy saving saves man-hour, realize ecological, environmental protectiveization safety in production operation.
For achieving the above object, the present invention provides following technical scheme：
A kind of demulsification clarifier and preparation method thereof, is made up of following mass fraction formula components：The net 2-4 parts of sewage, silicon
Diatomaceous earth 10-15 part, natural soap powder 16-18 parts, bodied ferric sulfate 4-6 parts, soybean lecithin 6-8 parts, six trichloride hydrate aluminium 6-8
Part, copper ion 5-9 parts, anhydrous calcium chloride 5-7 parts, ferric trichloride 6-8 parts, the fat 6-10 parts of methacrylic acid 18, polyaluminium
Aluminium 20-30 parts, PAMA 2-4 parts.
Further：It is made up of following mass fraction formula components：Sewage is net 2 parts, 10 parts of diatomite, 16 parts of natural soap powder,
4 parts of bodied ferric sulfate, 6 parts of soybean lecithin, 6 parts of six trichloride hydrate aluminium, 5 parts of copper ion, 5 parts of anhydrous calcium chloride, ferric trichloride 6
Part, 6 parts of 18 fat of methacrylic acid, 20 parts of aluminium polychloride, 2 parts of PAMA.
Further：It is made up of following mass fraction formula components：Sewage is net 3 parts, 12.5 parts of diatomite, natural soap powder 17
Part, 5 parts of bodied ferric sulfate, 7 parts of soybean lecithin, 7 parts of six trichloride hydrate aluminium, 7 parts of copper ion, 6 parts of anhydrous calcium chloride, tri-chlorination
7 parts of iron, 8 parts of 18 fat of methacrylic acid, 25 parts of aluminium polychloride, 3 parts of PAMA.
Further：It is made up of following mass fraction formula components：Sewage is net 4 parts, 15 parts of diatomite, 18 parts of natural soap powder,
6 parts of bodied ferric sulfate, 8 parts of soybean lecithin, 8 parts of six trichloride hydrate aluminium, 9 parts of copper ion, 7 parts of anhydrous calcium chloride, ferric trichloride 8
Part, 10 parts of 18 fat of methacrylic acid, 30 parts of aluminium polychloride, 4 parts of PAMA.
Further：Preparation method of the present invention has following steps：
Step one, by sewage is net, bodied ferric sulfate and six trichloride hydrate aluminium are to entering in mixer, then pour anhydrous chlorination into
Calcium simultaneously adds 50% water of four kinds of raw material summations, is sufficiently stirred for, and mixing speed is per minute 60 turns, it is ensured that solid constituent is thorough
Bottom is dissolved, retention time 2-3 hour；
Step 2, add ferric trichloride and continue to stir, mixing speed 50-80 per minute turns, the time is half -1 hour, is stopped
Machine 6-10 hours；
Step 3, surplus stock is added to continue to stir mixing speed 50-80 per minute and turn step 2 gained, the time is
Partly -1 hour, 6-10 hours are shut down, filter and load product packaging barrel.
The invention has the beneficial effects as follows：Its good sewage processing effect of the invention, invests little, it is ensured that personal safety, reduces life
Cost is produced, energy saving saves man-hour, realize ecological, environmental protectiveization safety in production operation.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the invention, rather than the embodiment of whole.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all
Belong to the scope of protection of the invention.
Embodiment one：
A kind of demulsification clarifier is made up of following mass fraction formula components：The net 2-4 parts of sewage, diatomite 10-15 parts, day
So soap powder 16-18 parts, bodied ferric sulfate 4-6 parts, soybean lecithin 6-8 parts, six trichloride hydrate aluminium 6-8 parts, copper ion 5-9 parts,
Anhydrous calcium chloride 5-7 parts, ferric trichloride 6-8 parts, the fat 6-10 parts of methacrylic acid 18, aluminium polychloride 20-30 parts, anion
Polyacrylamide 2-4 parts.
Embodiment two：
A kind of demulsification clarifier is made up of following mass fraction formula components：Sewage is net 2 parts, 10 parts of diatomite, natural soap
16 parts of powder, 4 parts of bodied ferric sulfate, 6 parts of soybean lecithin, 6 parts of six trichloride hydrate aluminium, 5 parts of copper ion, 5 parts of anhydrous calcium chloride, three
6 parts of iron chloride, 6 parts of 18 fat of methacrylic acid, 20 parts of aluminium polychloride, 2 parts of PAMA.
Embodiment three：
A kind of demulsification clarifier is made up of following mass fraction formula components：Sewage is net 3 parts, 12.5 parts of diatomite, natural
17 parts of soap powder, 5 parts of bodied ferric sulfate, 7 parts of soybean lecithin, 7 parts of six trichloride hydrate aluminium, 7 parts of copper ion, 6 parts of anhydrous calcium chloride,
7 parts of ferric trichloride, 8 parts of 18 fat of methacrylic acid, 25 parts of aluminium polychloride, 3 parts of PAMA.
Example IV：
A kind of demulsification clarifier is made up of following mass fraction formula components：Sewage is net 4 parts, 15 parts of diatomite, natural soap
18 parts of powder, 6 parts of bodied ferric sulfate, 8 parts of soybean lecithin, 8 parts of six trichloride hydrate aluminium, 9 parts of copper ion, 7 parts of anhydrous calcium chloride, three
8 parts of iron chloride, 10 parts of 18 fat of methacrylic acid, 30 parts of aluminium polychloride, 4 parts of PAMA.
Embodiment five：
A kind of preparation method preparation method of demulsification clarifier comprises the steps：
Step one, by sewage is net, bodied ferric sulfate and six trichloride hydrate aluminium are to entering in mixer, then pour anhydrous chlorination into
Calcium simultaneously adds 50% water of four kinds of raw material summations, is sufficiently stirred for, and mixing speed is per minute 60 turns, it is ensured that solid constituent is thorough
Bottom is dissolved, retention time 2-3 hour；
Step 2, add ferric trichloride and continue to stir, mixing speed 50-80 per minute turns, the time is half -1 hour, is stopped
Machine 6-10 hours；
Step 3, surplus stock is added to continue to stir mixing speed 50-80 per minute and turn step 2 gained, the time is
Partly -1 hour, 6-10 hours are shut down, filter and load product packaging barrel.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity those skilled in the art should
Using specification as an entirety, the technical scheme in each embodiment can also Jing it is appropriately combined, form those skilled in the art
Understandable other embodiment.
Claims (5)
1. a kind of demulsification clarifier, it is characterised in that：It is made up of following mass fraction formula components：
The net 2-4 parts of sewage, diatomite 10-15 parts, natural soap powder 16-18 parts, bodied ferric sulfate 4-6 parts, soybean lecithin 6-8 parts,
Six trichloride hydrate aluminium 6-8 parts, copper ion 5-9 parts, anhydrous calcium chloride 5-7 parts, ferric trichloride 6-8 parts, methacrylic acid 18
Fat 6-10 parts, aluminium polychloride 20-30 parts, PAMA 2-4 parts.
2. a kind of demulsification clarifier according to claim 1, it is characterised in that：By following mass fraction formula components group
Into：
Sewage is net 2 parts, 10 parts of diatomite, 16 parts of natural soap powder, 4 parts of bodied ferric sulfate, 6 parts of soybean lecithin, six trichloride hydrates
6 parts of aluminium, 5 parts of copper ion, 5 parts of anhydrous calcium chloride, 6 parts of ferric trichloride, 6 parts of 18 fat of methacrylic acid, 20 parts of aluminium polychloride,
2 parts of PAMA.
3. a kind of demulsification clarifier according to claim 1, it is characterised in that：By following mass fraction formula components group
Into：
Sewage is net 3 parts, 12.5 parts of diatomite, 17 parts of natural soap powder, 5 parts of bodied ferric sulfate, 7 parts of soybean lecithin, six hydration trichlorines
Change 7 parts of aluminium, 7 parts of copper ion, 6 parts of anhydrous calcium chloride, 7 parts of ferric trichloride, 8 parts of 18 fat of methacrylic acid, aluminium polychloride 25
Part, 3 parts of PAMA.
4. a kind of demulsification clarifier according to claim 1, it is characterised in that：By following mass fraction formula components group
Into：
Sewage is net 4 parts, 15 parts of diatomite, 18 parts of natural soap powder, 6 parts of bodied ferric sulfate, 8 parts of soybean lecithin, six trichloride hydrates
8 parts of aluminium, 9 parts of copper ion, 7 parts of anhydrous calcium chloride, 8 parts of ferric trichloride, 10 parts of 18 fat of methacrylic acid, aluminium polychloride 30
Part, 4 parts of PAMA.
5. a kind of a kind of preparation method of demulsification clarifier according to claim 1, it is characterised in that：Including following step
Suddenly：
Step one, by sewage is net, bodied ferric sulfate and six trichloride hydrate aluminium are to entering in mixer, then pour anhydrous calcium chloride into simultaneously
50% water of four kinds of raw material summations is added, is sufficiently stirred for, mixing speed is per minute 60 turns, it is ensured that solid constituent is thoroughly molten
Solution, retention time 2-3 hour；
Step 2, add ferric trichloride and continue to stir, mixing speed 50-80 per minute turns, the time is half -1 hour, shuts down 6-
10 hours；
Step 3, surplus stock is added to continue to stir mixing speed 50-80 per minute and turn step 2 gained, the time is little for half -1
When, 6-10 hours are shut down, filter and load product packaging barrel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611165059.1A CN106629910A (en) | 2016-12-16 | 2016-12-16 | Demulsifying and purifying agent, and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611165059.1A CN106629910A (en) | 2016-12-16 | 2016-12-16 | Demulsifying and purifying agent, and preparation method thereof |
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| CN106629910A true CN106629910A (en) | 2017-05-10 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201611165059.1A Pending CN106629910A (en) | 2016-12-16 | 2016-12-16 | Demulsifying and purifying agent, and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109020107A (en) * | 2018-06-19 | 2018-12-18 | 辽宁兴望源环保科技有限公司 | Greasy filth demulsification three phase separation agent and its preparation process |
| CN109794080A (en) * | 2019-03-07 | 2019-05-24 | 中国科学院兰州化学物理研究所 | It is a kind of can magnetic recovery composite diatomite demulsifying material preparation method and application |
| CN110040810A (en) * | 2019-05-08 | 2019-07-23 | 扬州宏平精工设备有限公司 | A kind of environment-friendly type fluorescence sewage-treating agent |
| CN113967466A (en) * | 2021-11-25 | 2022-01-25 | 吉林省正达环保工程有限公司 | Preparation method of sodium hypochlorite composite adsorbent |
| CN114014420A (en) * | 2021-11-25 | 2022-02-08 | 吉林省正达环保工程有限公司 | Preparation method of ferric trichloride composite solution water purifying agent |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101113028A (en) * | 2007-06-07 | 2008-01-30 | 上海忠诚环保科技有限公司 | Method for preparing demulsification clarifier |
| CN101139115A (en) * | 2007-08-21 | 2008-03-12 | 马冬兰 | Composite emulsion breaking scavenging agnet and preparation method thereof |
-
2016
- 2016-12-16 CN CN201611165059.1A patent/CN106629910A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101113028A (en) * | 2007-06-07 | 2008-01-30 | 上海忠诚环保科技有限公司 | Method for preparing demulsification clarifier |
| CN101139115A (en) * | 2007-08-21 | 2008-03-12 | 马冬兰 | Composite emulsion breaking scavenging agnet and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109020107A (en) * | 2018-06-19 | 2018-12-18 | 辽宁兴望源环保科技有限公司 | Greasy filth demulsification three phase separation agent and its preparation process |
| CN109794080A (en) * | 2019-03-07 | 2019-05-24 | 中国科学院兰州化学物理研究所 | It is a kind of can magnetic recovery composite diatomite demulsifying material preparation method and application |
| CN110040810A (en) * | 2019-05-08 | 2019-07-23 | 扬州宏平精工设备有限公司 | A kind of environment-friendly type fluorescence sewage-treating agent |
| CN113967466A (en) * | 2021-11-25 | 2022-01-25 | 吉林省正达环保工程有限公司 | Preparation method of sodium hypochlorite composite adsorbent |
| CN114014420A (en) * | 2021-11-25 | 2022-02-08 | 吉林省正达环保工程有限公司 | Preparation method of ferric trichloride composite solution water purifying agent |
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