CN106624456B - A kind of three submerged-arc welding Special pad solder flux of FCB method and preparation method thereof - Google Patents
A kind of three submerged-arc welding Special pad solder flux of FCB method and preparation method thereof Download PDFInfo
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- CN106624456B CN106624456B CN201611068794.0A CN201611068794A CN106624456B CN 106624456 B CN106624456 B CN 106624456B CN 201611068794 A CN201611068794 A CN 201611068794A CN 106624456 B CN106624456 B CN 106624456B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/36—Selection of non-metallic compositions, e.g. coatings, fluxes; Selection of soldering or welding materials, conjoint with selection of non-metallic compositions, both selections being of interest
- B23K35/362—Selection of compositions of fluxes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/40—Making wire or rods for soldering or welding
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Abstract
The present invention provides a kind of three submerged-arc welding Special pad solder flux of FCB method, including the following raw material component according to parts by weight: 26~30 parts of MgO;8~15 parts of CaO;Al2O310~15 parts;TiO218~25 parts;SiO28~15 parts;5~10 parts of BaO;5~10 parts of MnO;Li24~5 parts of O;0.5~1.0 part of high-temperature resin;And inevitable impurity.The present invention also provides the liner solder flux preparation method.Three submerged-arc welding Special pad solder flux moisture absorptions of FCB method of the invention are small, appearance of weld is good, the removability of slag is excellent, bead crack sensibility is small, cooperate MCJH10Mn2 welding wire for submerged-arc welding in 36mm FCB method welding process below, with welding technological properties such as good de- slag, anti-stomatas and there is good cracking resistance, appearance of weld is good, weld reinforcement is no more than 3mm, I grade of qualification of x-ray inspection.
Description
Technical field
The invention belongs to technical field of welding materials, and in particular to a kind of three submerged-arc welding Special pad solder flux of FCB method and
Preparation method.
Background technique
In Modern Shipbuilding, welding is a very crucial technique, it not only has very big shadow to the build guality of hull
It rings, and to productivity is improved, shortens shipbuilding period and play very big effect.One side welding with back formation Lincoln weld is 20 generation
It records a noise source analysis new technology the growing up seventies, has been widely used at present, because it eliminates turn, overhead welding etc.
Process is conducive to tissue production line, improves the turnover rate and welding productivity of platform, thus is widely used in countries in the world and makes
Shipping agency industry.Occur it was verified that one side welding with back formation Lincoln weld adapts to modern shipbuilding needs.
Flux copper-gasket method single side Lincoln weld (i.e. FCB method) is one kind of one side welding with back formation Lincoln weld,
Since it has many advantages, such as to can be used big welding conditions, not high to matching requirements is widely used in major shipyard.
The country is relatively more for the associated welds material and its STUDY ON THE WELDING of FCB method, but always exists some skills
Problem in art not can avoid, and the bead formed on back mainly welded is bad, and it is difficult that the back side takes off slag, and is easy to make in back of weld
At transversal crack, probability of doing over again is very high.
Summary of the invention
The purpose of the present invention is overcoming the sealing run occurred in existing FCB method use process molding more convex, it is difficult to take off slag
There is the technical issues of transversal crack with back of weld.
For this purpose, the present invention provides a kind of three submerged-arc welding Special pad solder flux of FCB method, including according to parts by weight as
Lower raw material components:
26~30 parts of MgO;
8~15 parts of CaO;
Al2O310~15 parts;
TiO218~25 parts;
SiO28~15 parts;
5~10 parts of BaO;
5~10 parts of MnO;
Li24~5 parts of O;
0.5~1.0 part of high-temperature resin;And inevitable impurity.
Further, the granularity of above-mentioned liner solder flux is 12~60 mesh.
Further, the basicity of above-mentioned liner solder flux is 1.5~2.5.
Further, the content of above-mentioned impurity is no more than the 1.5% of liner solder flux gross mass.
In addition, the present invention also provides the preparation method of three submerged-arc welding Special pad solder flux of above-mentioned FCB method, including it is as follows
Step:
1) above-mentioned liner solder flux raw material components sorting is pressed, coarse crushing, fine crushing, levigation processing are carried out after raw material is rechecked,
It is processed into pulvis, and matches weighing stock according to raw material components parts by weight.
2) raw material ready in step 1) is added in dry blender and carries out dry stirring, then by powder after mixing evenly
Wet blender is added in material, and waterglass is added and carries out wet stirring, stirs.
3) expecting of stirring evenly is sent into pelletizer to be granulated, obtains granular liner solder flux.
4) the granular liner solder flux produced is sent into after heated-air drying drying oven and carries out drying and processing, go mistake after moisture removal
Sieve, control pad solder flux granule size and are sent into sintering furnace and is sintered.
5) through inspection, sieving, packaging, storage after coming out and cooling down.
Further, above-mentioned steps 2) in waterglass be lithium silicate, and lithium silicate quality be powder quality 15~
25%。
Preferably, above-mentioned lithium silicate quality is the 20% of powder quality.
Further, above-mentioned steps 4) in drying oven drying temperature be 150~200 DEG C;Sintering temperature in sintering furnace
400~500 DEG C, sintering time 0.5~1.5 hour.
Preferably, above-mentioned steps 4) in sintering time be 1 hour.
Further, above-mentioned steps 4) in enter sintering furnace liner solder flux granule size be 12~60 mesh.
The each component design principle of three submerged-arc welding Special pad solder flux of FCB method in the present invention:
MgO main function is slag making, improves the fusing point of slag, so as to improve appearance of weld, reduces the reinforcement of weld seam.This hair
In bright embodiment, MgO is added in the form of fused magnesite.The amount ranges of fused magnesite are 26~30 parts, and dosage is less than
At 26 parts, solder flux fusing point is lower, and welding slag is diluter, and weld seam is easy leakage and falls into;When its dosage is greater than 30 parts, flux basicity is excessive, weld seam
De- slag is difficult, and slag fusing point is too high, and weld seam protection is bad.
Al2O3Main function is basicity, setting temperature and the viscosity for adjusting slag, to preferably protect weld seam, and is improved
Slag detachability.In the present invention, Al2O3Amount ranges be 10~15 parts, when dosage is less than 10 parts, slag is diluter, and molten iron can be from
Sealing run evolution causes sealing run molding bad;When its dosage is greater than 15 parts, slag is relatively viscous, and weld seam easy to form is ventilative
The defects of bad and generation slag inclusion.
BaO mainly plays slag making, its presence can improve the removability of slag of weld seam.In the present invention, the dosage of BaO
Range is 5~10 parts, when dosage is less than 5 parts, and the de- slag of slag is bad, and processing performance is poor;When its dosage is greater than 10 parts, slag alkali
Degree is big, and welding technological properties is poor.
Li2O mainly plays a part of to reduce solder flux moisture absorption, its presence can make solder flux moisture absorption low, weld
When reduce weld seam in diffusible hydrogen, to reduce crack sensitivity.In the present invention, Li2The amount ranges of O are 4~5 parts,
When dosage is less than 4 parts, solder flux moisture absorption is high, and bead crack is sensitive;When its dosage is greater than 5 parts, processing performance is poor.
High-temperature resin, which mainly passes through resin heating process, makes it generate solidification, prevents molten iron from leaking, and guarantees weld seam
Molding.In the present invention, the amount ranges of high-temperature resin are 0.5~1.0 part, when dosage is less than 0.5 part, in the welding process
Molten iron is easy leakage, causes appearance of weld poor;When its dosage is greater than 1.0 parts, weld porosity is more.High temperature resin of the present invention is heat
Solidity phenolic resin, 150 degree of solidification temperature or more.
Compared with prior art, beneficial effects of the present invention:
(1) three submerged-arc welding Special pad solder flux of this FCB method provided by the invention are suitable by being added into solder flux
MgO and Al2O3It improves the fusing point of welding slag, and uses TiO2Substitute part SiO2The basicity of solder flux and the viscosity of slag are adjusted, is made
Weld seam has good appearance of weld and weld reinforcement, and weld reinforcement is no more than 3mm, and reduces the Si content in weld seam;And
Due to SiO in solder flux2Content is less, to improve the toughness and crack resistance of weld seam.
(2) it joined appropriate high-temperature resin in three submerged-arc welding Special pad solder flux of this FCB method provided by the invention, lead to
Crossing high-temperature resin heating process makes it generate solidification, prevents molten iron from leaking, ensure that appearance of weld.
(3) lithium water glass is used in the preparation method of three submerged-arc welding Special pad solder flux of this FCB method provided by the invention
Glass and Li2O is handled, and the anti-moisture absorption capacity of solder flux is enhanced, and reduces the content of diffusible hydrogen, to further enhance weldering
The cracking resistance of seam.
The present invention is described in further details below with reference to attached drawing.
Detailed description of the invention
Fig. 1 is the preparation method process flow chart of three submerged-arc welding Special pad solder flux of FCB method of the present invention.
Fig. 2 is the appearance of weld figure after being welded using liner solder flux in embodiment 1.
Fig. 3 is the appearance of weld figure after being welded using liner solder flux in embodiment 2.
Fig. 4 is the appearance of weld figure after being welded using liner solder flux in embodiment 3.
Fig. 5 is the appearance of weld figure after being welded using liner solder flux in embodiment 4.
Fig. 6 is the appearance of weld figure after being welded using existing same model welding with backing agent.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts all other
Embodiment shall fall within the protection scope of the present invention.
Embodiment 1:
A kind of three submerged-arc welding Special pad solder flux of FCB method are present embodiments provided, it is as follows including according to parts by weight
Raw material components: 30 parts of MgO;8 parts of CaO;Al2O310 parts;TiO225 parts;SiO28 parts;5 parts of BaO;7.5 parts of MnO;Li2O
5 parts;1.0 parts of high-temperature resin;And inevitable impurity.Wherein, the basicity of the liner solder flux is 1.5.
As shown in Figure 1, the preparation process of three submerged-arc welding Special pad solder flux of the FCB method is as follows: above-mentioned raw materials are rechecked
Afterwards, the processes such as coarse crushing, fine crushing, levigation are carried out, the pulvis of various criterion granularity is processed into.After sieving according to it is above-mentioned be formulated into
Row proportion weighing, then puts into and carries out dry stirring in dry blender, and powder after mixing evenly is put into wet blender, and powder is added
The lithium silicate of quality 20% carries out wet stirring, stirs, and expecting of being stirred is sent into pelletizer and is granulated, and produces
Granular liner solder flux drying oven is sent into after heated-air drying, 150~200 DEG C at a temperature of dried, after removing moisture removal
Sieving, the liner solder flux of 12~60 mesh of Control granularity are sent into sintering furnace and are sintered, and 400~500 DEG C of sintering temperature, sintering time
1.5 hours or so, through inspection, sieving, packaging, storage after coming out and cooling down, complete liner solder flux production process.
After the present embodiment liner solder flux drying obtained, water content 0.02% is opened wide dew and sets water content after 4 hours
It is 0.035%, shows that the liner solder flux moisture absorption can be good.
Before welding, the same type of liner solder flux and existing day Benshen steel group made from the present embodiment is padded into solder flux
Carry out soldering test after 300 DEG C dry 2 hours respectively, cooperation MCJH10Mn2 welding wire carry out three single face welding and double faces of FCB method at
Type welding, it is as shown in Figure 2 and Figure 6 that the two sealing run forms result difference.Through detecting, the present embodiment liner solder flux back obtained
Face appearance of weld is good, and weld reinforcement is no more than 3mm, I grade of qualification of radiographic inspection, hence it is evident that is better than existing same type welding with backing
Agent.
Embodiment 2:
A kind of three submerged-arc welding Special pad solder flux of FCB method are present embodiments provided, it is as follows including according to parts by weight
Raw material components: 26 parts of MgO;15 parts of CaO;Al2O310 parts;TiO218 parts;SiO215 parts;5 parts of BaO;5 parts of MnO;Li2O
4 parts;0.5 part of high-temperature resin;And inevitable impurity.Wherein, the basicity of the liner solder flux is 1.5.
As shown in Figure 1, the preparation process of three submerged-arc welding Special pad solder flux of the FCB method is as follows: above-mentioned raw materials are rechecked
Afterwards, the processes such as coarse crushing, fine crushing, levigation are carried out, the pulvis of various criterion granularity is processed into.After sieving according to it is above-mentioned be formulated into
Row proportion weighing, then puts into and carries out dry stirring in dry blender, and powder after mixing evenly is put into wet blender, and powder is added
The lithium silicate of quality 25% carries out wet stirring, stirs, and expecting of being stirred is sent into pelletizer and is granulated, and produces
Granular liner solder flux drying oven is sent into after heated-air drying, 150~200 DEG C at a temperature of dried, after removing moisture removal
Sieving, the liner solder flux of 12~60 mesh of Control granularity are sent into sintering furnace and are sintered, and 400~500 DEG C of sintering temperature, sintering time
1 hour or so, through inspection, sieving, packaging, storage after coming out and cooling down, complete liner solder flux production process.
After the present embodiment liner solder flux drying obtained, water content 0.015% is opened wide dew and sets water content after 4 hours
It is 0.041%, shows that the liner solder flux moisture absorption can be good.
Before welding, the same type of liner solder flux and existing day Benshen steel group made from the present embodiment is padded into solder flux
Carry out soldering test after 300 DEG C dry 2 hours respectively, cooperation MCJH10Mn2 welding wire carry out three single face welding and double faces of FCB method at
Type welding, it is as shown in Figure 3 and Figure 6 that the two sealing run forms result difference.Through detecting, the present embodiment liner solder flux back obtained
Face appearance of weld is good, and weld reinforcement is no more than 3mm, I grade of qualification of radiographic inspection, hence it is evident that is better than existing same type welding with backing
Agent.
Embodiment 3:
A kind of three submerged-arc welding Special pad solder flux of FCB method are present embodiments provided, it is as follows including according to parts by weight
Raw material components: 26 parts of MgO;8 parts of CaO;Al2O315 parts;TiO218 parts;SiO28 parts;10 parts of BaO;10 parts of MnO;Li2O
4 parts;0.5 part of high-temperature resin;And inevitable impurity.Wherein, the basicity of the liner solder flux is 2.5.
As shown in Figure 1, the preparation process of three submerged-arc welding Special pad solder flux of the FCB method is as follows: above-mentioned raw materials are rechecked
Afterwards, the processes such as coarse crushing, fine crushing, levigation are carried out, the pulvis of various criterion granularity is processed into.After sieving according to it is above-mentioned be formulated into
Row proportion weighing, then puts into and carries out dry stirring in dry blender, and powder after mixing evenly is put into wet blender, and powder is added
The lithium silicate of quality 15% carries out wet stirring, stirs, and expecting of being stirred is sent into pelletizer and is granulated, and produces
Granular liner solder flux drying oven is sent into after heated-air drying, 150~200 DEG C at a temperature of dried, after removing moisture removal
Sieving, the liner solder flux of 12~60 mesh of Control granularity are sent into sintering furnace and are sintered, and 400~500 DEG C of sintering temperature, sintering time
0.5 hour or so, through inspection, sieving, packaging, storage after coming out and cooling down, complete liner solder flux production process.
After the present embodiment liner solder flux drying obtained, water content 0.025% is opened wide dew and sets water content after 4 hours
It is 0.050%, shows that the liner solder flux moisture absorption can be good.
Before welding, the same type of liner solder flux and existing day Benshen steel group made from the present embodiment is padded into solder flux
Carry out soldering test after 300 DEG C dry 2 hours respectively, cooperation MCJH10Mn2 welding wire carry out three single face welding and double faces of FCB method at
Type welding, it is as shown in Figure 4 and Figure 6 that the two sealing run forms result difference.Through detecting, the present embodiment liner solder flux back obtained
Face appearance of weld is good, and weld reinforcement is no more than 3mm, I grade of qualification of radiographic inspection, hence it is evident that is better than existing same type welding with backing
Agent.
Embodiment 4:
A kind of three submerged-arc welding Special pad solder flux of FCB method are present embodiments provided, it is as follows including according to parts by weight
Raw material components: 28 parts of MgO;12 parts of CaO;Al2O312 parts;TiO220 parts;SiO29 parts;6 parts of BaO;8 parts of MnO;Li2O 4
Part;0.5 part of high-temperature resin;And inevitable impurity.Wherein, the basicity of the liner solder flux is 1.9.
As shown in Figure 1, the preparation process of three submerged-arc welding Special pad solder flux of the FCB method is as follows: above-mentioned raw materials are rechecked
Afterwards, the processes such as coarse crushing, fine crushing, levigation are carried out, the pulvis of various criterion granularity is processed into.After sieving according to it is above-mentioned be formulated into
Row proportion weighing, then puts into and carries out dry stirring in dry blender, and powder after mixing evenly is put into wet blender, and powder is added
The lithium silicate of quality 20% carries out wet stirring, stirs, and expecting of being stirred is sent into pelletizer and is granulated, and produces
Granular liner solder flux drying oven is sent into after heated-air drying, 150~200 DEG C at a temperature of dried, after removing moisture removal
Sieving, the liner solder flux of 12~60 mesh of Control granularity are sent into sintering furnace and are sintered, and 400~500 DEG C of sintering temperature, sintering time
1 hour or so, through inspection, sieving, packaging, storage after coming out and cooling down, complete liner solder flux production process.
After the present embodiment liner solder flux drying obtained, water content 0.025% is opened wide dew and sets water content after 4 hours
It is 0.050%, shows that the liner solder flux moisture absorption can be good.
Before welding, the same type of liner solder flux and existing day Benshen steel group made from the present embodiment is padded into solder flux
Carry out soldering test after 300 DEG C dry 2 hours respectively, cooperation MCJH10Mn2 welding wire carry out three single face welding and double faces of FCB method at
Type welding, it is as shown in Figure 5 and Figure 6 that the two sealing run forms result difference.Through detecting, the present embodiment liner solder flux back obtained
Face appearance of weld is good, and weld reinforcement is no more than 3mm, I grade of qualification of radiographic inspection, hence it is evident that is better than existing same type welding with backing
Agent.
In conclusion three submerged-arc welding Special pad solder flux moisture absorptions of this FCB method provided by the invention are small, appearance of weld
Good, the removability of slag is excellent, and bead crack sensibility is small, cooperates MCJH10Mn2 welding wire for submerged-arc welding in 36mm FCB method welding process below
In, with welding technological properties such as good de- slag, anti-stomatas and there is good cracking resistance, appearance of weld is good, weld seam
Reinforcement is no more than 3mm, I grade of qualification of x-ray inspection.
The foregoing examples are only illustrative of the present invention, does not constitute the limitation to protection scope of the present invention, all
It is within being all belonged to the scope of protection of the present invention with the same or similar design of the present invention.
Claims (10)
1. a kind of three submerged-arc welding Special pad solder flux of FCB method, it is characterised in that: including the following raw material component according to parts by weight:
26~30 parts of MgO;
8~15 parts of CaO;
Al2O310~15 parts;
TiO218~25 parts;
SiO28~15 parts;
5~10 parts of BaO;
5~10 parts of MnO;
Li24~5 parts of O;
0.5~1.0 part of high-temperature resin;And inevitable impurity;
Wherein, the high-temperature resin is thermosetting phenolic resin.
2. three submerged-arc welding Special pad solder flux of FCB method as described in claim 1, it is characterised in that: the liner solder flux
Granularity is 12~60 mesh.
3. three submerged-arc welding Special pad solder flux of FCB method as described in claim 1, it is characterised in that: the liner solder flux
Basicity is 1.5~2.5.
4. three submerged-arc welding Special pad solder flux of FCB method as described in claim 1, it is characterised in that: the content of the impurity
No more than the 1.5% of liner solder flux gross mass.
5. such as the preparation method of three submerged-arc welding Special pad solder flux of the described in any item FCB methods of Claims 1 to 4, feature
It is: includes the following steps:
1) above-mentioned liner solder flux raw material components sorting is pressed, coarse crushing, fine crushing, levigation processing, processing are carried out after raw material is rechecked
Weighing stock is matched at pulvis, and according to raw material components parts by weight;
2) raw material ready in step 1) is added in dry blender and carries out dry stirring, then add powder after mixing evenly
Enter wet blender, and waterglass is added and carries out wet stirring, stirs;
3) expecting of stirring evenly is sent into pelletizer to be granulated, obtains granular liner solder flux;
4) the granular liner solder flux produced is sent into after heated-air drying drying oven and carries out drying and processing, be sieved after removing moisture removal,
Control pads solder flux granule size and is sent into sintering furnace and is sintered;
5) through inspection, sieving, packaging, storage after coming out and cooling down.
6. the preparation method of three submerged-arc welding Special pad solder flux of FCB method as claimed in claim 5, it is characterised in that: described
Waterglass is lithium silicate in step 2), and lithium silicate quality is the 15~25% of powder quality.
7. the preparation method of three submerged-arc welding Special pad solder flux of FCB method as claimed in claim 6, it is characterised in that: described
Lithium silicate quality is the 20% of powder quality.
8. the preparation method of three submerged-arc welding Special pad solder flux of FCB method as claimed in claim 5, it is characterised in that: described
The drying temperature of drying oven is 150~200 DEG C in step 4);400~500 DEG C of sintering temperature in sintering furnace, sintering time 0.5
~1.5 hours.
9. the preparation method of three submerged-arc welding Special pad solder flux of FCB method as claimed in claim 8, it is characterised in that: described
Sintering time is 1 hour in step 4).
10. the preparation method of three submerged-arc welding Special pad solder flux of FCB method as claimed in claim 5, it is characterised in that: described
The liner solder flux granule size for entering sintering furnace in step 4) is 12~60 mesh.
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CN109290699A (en) * | 2018-10-23 | 2019-02-01 | 东莞理工学院 | A kind of overlay film liner solder flux of single face welding and double face shaping and preparation method thereof |
CN109332897A (en) * | 2018-12-27 | 2019-02-15 | 长沙理工大学 | A kind of cut deal method for laser welding |
CN110790569A (en) * | 2019-11-06 | 2020-02-14 | 山东聚力焊接材料有限公司 | Welding ceramic liner capable of preventing weld cracks and preparation method thereof |
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