CN106623429A - Rolling forming method for low-oxygen-content aero titanium alloy precision thin sheet - Google Patents

Rolling forming method for low-oxygen-content aero titanium alloy precision thin sheet Download PDF

Info

Publication number
CN106623429A
CN106623429A CN201610921646.2A CN201610921646A CN106623429A CN 106623429 A CN106623429 A CN 106623429A CN 201610921646 A CN201610921646 A CN 201610921646A CN 106623429 A CN106623429 A CN 106623429A
Authority
CN
China
Prior art keywords
rolling
titanium alloy
low
oxygen content
aero titanium
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610921646.2A
Other languages
Chinese (zh)
Inventor
过冬
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201610921646.2A priority Critical patent/CN106623429A/en
Publication of CN106623429A publication Critical patent/CN106623429A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B3/00Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metals
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B1/00Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations
    • B21B1/22Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling plates, strips, bands or sheets of indefinite length
    • B21B1/30Metal-rolling methods or mills for making semi-finished products of solid or profiled cross-section; Sequence of operations in milling trains; Layout of rolling-mill plant, e.g. grouping of stands; Succession of passes or of sectional pass alternations for rolling plates, strips, bands or sheets of indefinite length in a non-continuous process
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/16Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
    • C22F1/18High-melting or refractory metals or alloys based thereon
    • C22F1/183High-melting or refractory metals or alloys based thereon of titanium or alloys based thereon

Abstract

The invention discloses a rolling forming method for a low-oxygen-content aero titanium alloy precision thin sheet. According to the rolling forming method, impregnation is performed on a primarily rolled sheet, which is primarily rolled and degreased, with an impregnation liquid containing specific ingredients, and further recrystallization annealing and secondary rolling are conducted. The rolling forming method particularly comprises the following steps: taking an aero titanium alloy sheet as the raw materials, performing twenty-high rolling, degreasing, impregnating, performing recrystallization annealing, conducting secondary cold rolling by a twenty-high rolling mill, degreasing, performing stress relief annealing, performing stretcher straightening, longitudinally cutting/transversely cutting, examining, packaging and the like. The titanium alloy precision thin sheet has the thickness tolerance of +/- 0.003 mm, the camber of 0.1-0.25 mm/1 m, the surface quality of No.3, and the grain size of 7-8 level, and is uniformly distributed in internal stress, free from anisotropism and excellent in follow-up plastic formability. The rolling forming method is simple and easy, low in cost and high in product quality and production efficiency.

Description

The method for rolling and molding of low-oxygen content aero titanium alloy precision sheet
Technical field
The present invention relates to a kind of rolling processing method of aero titanium alloy precision sheet, specifically a kind of hypoxia contains The method for rolling and molding of amount aero titanium alloy precision sheet.
Background technology
To ensure that aircraft body structure has enough strength and stiffness, and mitigate architecture quality, generally using specific strength, The high material of specific stiffness.In terms of housing construction material, the same aluminium alloy of advanced composite material, high strength steel, titanium alloy together by It is classified as four big structure materials.Titanium alloy material because intensity is high, lightweight, damage tolerance is high and the features such as good corrosion resistance, one Directly it is that instead of the desired metallic material of steel in aircaft configuration.With the raising of aircraft speed, titanium alloy answering on body It is main to make aircraft rear body and composite element joint, beam etc. with substantially increase, at present using it is most be Ti-6Al- 4V.Titanium alloy can make various thin plates, foil, tubing and silk material, replace 30CrMnSiA etc., be a kind of more satisfactory sheet metal Load-carrying member material.At present the U.S. applies on the aircrafts such as B-1b, F-15, F-16, F-18, F-22.In F-22 construction weights The proportion very little that traditional steel and aluminium alloy is accounted for, and 41% titanium alloy and 27% composite have been used in a large number, this is favourable In the stealth and thermostability that improve aircraft, mitigate body weight, increase cylinder block strength.In state-of-the art seating plane --- it is empty On objective A380, the consumption of titanium alloy increases to 10% from the 5%~7% of original duty visitor's aero-structure weight.
The conventional version of aircraft body structure has eyelid covering frame structure, integral panel structure, honeycomb interlayer or fills out Feed collet Rotating fields, pressurising shell structure etc..In recent years, the flight speed of aircraft is from subsonic speed to the even high ultrasound of supersonic speed Speed development.When Mach 2 ship 2~3, aircraft surface temperature is up to 200 DEG C~300 DEG C.For this purpose, many components of aircraft, Such as housing, fuel tank, air intake duct, empennage and trouserss skeleton select in a large number titanium alloy.The U.S. adopts Ti-6Al-4V titanium alloys The structural members such as fuel tank, air intake duct, the empennage of battleax cruise missile of thin plate manufacture, quality mitigates 20%~35%, manufacturing expenses With 20%~60% can be reduced.As eyelid covering frame structure, integral panel structure, honeycomb interlayer or stuffing sandwich structure, pressurising The importance of the titanium-alloy thin-plate material of shell structure raw material is highlighted all the more.
Because aviation titanium alloy material rolling performance is poor, in addition domestic manufacturer's rolling technique, equipment fall behind, using fire more The aero titanium alloy thin plate of the domestic thickness≤1mm (especially below 0.8mm) of secondary hot rolling and cladding ply rolling technique productions and state There is larger quality gap in outer like product, generally existing content of surface oxygen is high, microscopic structure is poor, surface smoothness is low, thickness The shortcomings of deviation is big.In follow-up titanium alloy member forming process, usually can cause thin plate panel beating/pipe crimping, welding performance it is poor, Superplastic forming is poor, fatigue strength is poor, causes the aerospace vehicle titanium alloy member dimensional accuracy such as aircraft, guided missile unmanageable Technical barrier.
The B of CN 101817015 disclose a kind of method for rolling and molding of low-oxygen content aero titanium alloy precision sheet, its It is raw material that thickness is adopted for the aero titanium alloy plate of 1-5mm, through once cold rolling rolling, defat, recrystallization annealing, secondary cold-rolling Rolling, defat, stress relief annealing, strength is aligned, and rip cutting/crosscutting, inspection, packaging and storage obtain low-oxygen content aero titanium alloy Precision sheet finished product.But, the thickness deviation of the low-oxygen content aero titanium alloy precision sheet finished product is still larger, ± 0.005mm, camber is larger, and in 0.3-1mm/1m, and crystal grain is still relatively thick, in follow-up titanium alloy member forming process, still There are problems that welding performance is poor, superplastic forming is poor, fatigue strength.
The content of the invention
For the above-mentioned problems in the prior art, it is an object of the invention to provide a kind of low-oxygen content aero titanium alloy The method for rolling and molding of precision sheet.The light sheet combination property of the method roll forming is superior, its thickness deviation for ± 0.003mm, camber 0.1-0.25mm/1m, surface quality is NO.3, and grain size reaches 7-8 levels, fully meets Aero-Space The performance need of device construction material, and production method is simple, low cost, efficiency high.
The purpose of the present invention is achieved through the following technical solutions:
A kind of method for rolling and molding of low-oxygen content aero titanium alloy precision sheet, the method for rolling and molding passes through two Secondary mill cold rolling, and in once cold rolling rolling and after the completion of defat, impregnated with specific impregnation liquid, obtain Low-oxygen content aero titanium alloy precision sheet, comprises the following steps that:
1) raw material prepares, and it is raw material to adopt thickness for the aero titanium alloy plate of 1-5mm;
2) raw material is carried out into mill once cold rolling rolling, obtains just rolling sheets;
3) by first rolling sheets defat;
4) using impregnation liquid to defat after first rolling sheets impregnate;
5) by dipping after first rolling sheets recrystallization annealing is carried out under reduction or inert atmosphere protection, cool down;
6) by recrystallization annealing after first rolling sheets carry out mill secondary cold-rolling rolling, obtain light sheet;
7) by the light sheet defat for obtaining;
8) light sheet after defat is carried out into stress relief annealing under reduction or inert atmosphere protection, is cooled down;
9) light sheet after stress relief annealing is carried out into stretcher leveling, rip cutting/crosscutting, inspection, packaging and storage, obtains hypoxia Content aero titanium alloy precision sheet finished product.
Preferably, step 1) in, aero titanium alloy board raw material is TC4 or TA15.
Preferably, step 4) in, impregnation liquid into being grouped into Ti (SO4)260-65g/L, BiCl350-60g/L, Fe3O40.02-0.04g/L, La2O36-8.5g/L, balance of water.
Preferably, Ti (SO4)2Content be 60-65g/L, for example can be 60g/L, 62g/L, 63g/L, 64g/L or 65g/L Deng.
Preferably, BiCl3Content be 50-60g/L, for example can be 50g/L, 52g/L, 55g/L, 57.5g/L or 60g/L Deng.
Preferably, Fe3O4Content be 0.02-0.04g/L, for example can for 0.02g/L, 0.03g/L, 0.035g/L or 0.04g/L etc..
Preferably, La2O3Content be 6-8.5g/L, for example can be for 6g/L, 7g/L, 7.5g/L, 8g/L or 8.5g/L etc..
Preferably, step 4) dipping temperature be 70-85 DEG C, for example can be 70 DEG C, 73 DEG C, 75 DEG C, 78 DEG C, 80 DEG C or 85 DEG C etc..
Preferably, step 4) time of dipping is 4-9h, for example can be for 4h, 5h, 6.5h, 7.5h, 8h or 9h etc..
Preferably, step 5) recrystallization annealing temperature be 800-830 DEG C.
Preferably, step 5) recrystallization annealing time be 15-25 minutes.
Preferably, step 6) in, the work roll surface roughness of mill is controlled at Ra0.2-0.3 μm, 20 rollers Milling train secondary cold-rolling pass deformation rate 50-65%.
Preferably, step 8) in stress relief annealing temperature be 550-620 DEG C, minute time 15-20 of stress relief annealing.
Compared with prior art, the invention has the advantages that:
The present invention is impregnated by the impregnation liquid using special component to the first rolling sheets once rolled and after defat, and Further recrystallization annealing, secondary rolling so that the low-oxygen content aero titanium alloy precision sheet combination property for obtaining is superior, Its thickness deviation is ± 0.003mm, and camber 0.1-0.25mm/1m, surface quality is NO.3, and grain size reaches 7-8 levels, fully Meet the performance need of aerospace vehicle construction material.Production method is simple, low cost, efficiency high.
Description of the drawings
Fig. 1 is the process chart of the present invention.
Specific embodiment
Further illustrate technical scheme below in conjunction with the accompanying drawings and by specific embodiment.
Embodiment 1
Adopt thickness for 5mm cold rolling 2B surfaces TC4 titanium-alloy thin-plates be raw material, the rolling of Jing mills, defat, Dipping, bright annealing, mill secondary cold-rolling, defat, bright annealing, stretcher leveling, rip cutting/crosscutting, check, be packaged into The operations such as storehouse are made.Wherein, impregnation liquid into being grouped into:Ti(SO4)260g/L, BiCl360g/L, Fe3O40.02g/L, La2O38.5g/L, balance of water;The temperature of dipping is 70 DEG C, and the time of dipping is 9h;Work in mill secondary cold-rolling It is Ra0.2 μm to make roll surface roughness, pass deformation rate 65%;Recrystallization annealing temperature is 800 DEG C, temperature retention time 25 minutes, Protection of reducing atmosphere, quick cooling;Stress relief annealing temperature is 550 DEG C, temperature retention time 20 minutes, protection of reducing atmosphere, quickly Cooling.Obtained low-oxygen content aero titanium alloy precision sheet surface does not have the surface contamination layers such as any oxygen-rich layer, α layers, Internal stress is evenly distributed, and without anisotropy, follow-up plastic formability is good.Its thickness is 0.8mm ± 0.003mm, and camber is 0.1mm/1m, surface quality is No.3, and grain size reaches 7 grades.
Embodiment 2
Adopt thickness for 3mm cold rolling 2B surfaces TC4 titanium-alloy thin-plates be raw material, the rolling of Jing mills, defat, Dipping, bright annealing, mill secondary cold-rolling, defat, bright annealing, stretcher leveling, rip cutting/crosscutting, check, be packaged into The operations such as storehouse are made.Wherein, impregnation liquid into being grouped into:Ti(SO4)265g/L, BiCl350g/L, Fe3O40.04g/L, La2O36g/L, balance of water;The temperature of dipping is 85 DEG C, and the time of dipping is 4h;Work in mill secondary cold-rolling Roll surface roughness is Ra0.3 μm, pass deformation rate 50%;Recrystallization annealing temperature is 830 DEG C, temperature retention time 15 minutes, also Former atmosphere protection, quick cooling;Stress relief annealing temperature is 620 DEG C, temperature retention time 15 minutes, protection of reducing atmosphere, fast quickly cooling But.Obtained low-oxygen content aero titanium alloy precision sheet surface should not have the surface contamination layers such as any oxygen-rich layer, α layers, Internal stress is evenly distributed, and without anisotropy, follow-up plastic formability is good.Its thickness is 0.5mm ± 0.003mm, and camber is 0.15mm/1m, surface quality is No.3, and grain size reaches 8 grades.
Embodiment 3
It is raw material that thickness is adopted for the TA15 titanium-alloy thin-plates on the cold rolling 2B surfaces of 1mm, and Jing mills are rolled, taken off Fat, dipping, bright annealing, mill secondary cold-rolling, defat, bright annealing, stretcher leveling, rip cutting/crosscutting, inspection, bag Load the operations such as storehouse to make.Wherein, impregnation liquid into being grouped into:Ti(SO4)262g/L, BiCl355g/L, Fe3O4 0.03g/L, La2O37.5g/L, balance of water;The temperature of dipping is 78 DEG C, and the time of dipping is 5h;Mill is secondary cold Work roll surface roughness in rolling is Ra0.25 μm, pass deformation rate 60%;Recrystallization annealing temperature is 815 DEG C, during insulation Between 20 minutes, protection of reducing atmosphere, quick cooling;Stress relief annealing temperature is 590 DEG C, temperature retention time 17 minutes, reducing atmosphere Protection, quick cooling.Obtained low-oxygen content aero titanium alloy precision sheet surface should be without any oxygen-rich layer, α layers etc. Surface contamination layer, internal stress is evenly distributed, and without anisotropy, follow-up plastic formability is good.Its thickness is 0.3mm ± 0.003mm, Camber is 0.2mm/1m, and surface quality is No.3, and grain size reaches 7 grades.
Embodiment 4
It is raw material that thickness is adopted for the TA15 titanium-alloy thin-plates on the cold rolling 2B surfaces of 1mm, and Jing mills are rolled, taken off Fat, dipping, bright annealing, mill secondary cold-rolling, defat, bright annealing, stretcher leveling, rip cutting/crosscutting, inspection, bag Load the operations such as storehouse to make.Wherein, impregnation liquid into being grouped into:Ti(SO4)263g/L, BiCl356g/L, Fe3O4 0.025g/L, La2O37g/L, balance of water;The temperature of dipping is 77 DEG C, and the time of dipping is 6h;Mill is secondary cold Work roll surface roughness in rolling is Ra0.28 μm, pass deformation rate 55%;Recrystallization annealing temperature is 820 DEG C, during insulation Between 20 minutes, protection of reducing atmosphere, quick cooling;Stress relief annealing temperature is 610 DEG C, temperature retention time 16 minutes, reducing atmosphere Protection, quick cooling.Obtained low-oxygen content aero titanium alloy precision sheet surface should be without any oxygen-rich layer, α layers etc. Surface contamination layer, internal stress is evenly distributed, and without anisotropy, follow-up plastic formability is good.Its thickness is 0.4mm ± 0.003mm, Camber is 0.22mm/1m, and surface quality is No.3, and grain size reaches 8 grades.
Production method of the present invention is simple, low cost, the low-oxygen content aero titanium alloy precision sheet synthesis for obtaining Superior performance, fully meets the performance need of aerospace vehicle construction material.
Applicant states that the present invention illustrates the method detailed of the present invention, but the present invention not office by above-described embodiment It is limited to above-mentioned method detailed, that is, does not mean that the present invention has to rely on above-mentioned method detailed and could implement.Art Technical staff it will be clearly understood that any improvement in the present invention, the equivalence replacement and auxiliary element to each raw material of product of the present invention Addition, selection of concrete mode etc., within the scope of all falling within protection scope of the present invention and disclosure.

Claims (10)

1. a kind of method for rolling and molding of low-oxygen content aero titanium alloy precision sheet, it is characterised in that methods described includes Following steps:
1) raw material prepares, and it is raw material to adopt thickness for the aero titanium alloy plate of 1-5mm;
2) raw material is carried out into mill once cold rolling rolling, obtains just rolling sheets;
3) by first rolling sheets defat;
4) using impregnation liquid to defat after first rolling sheets impregnate;
5) sheet material after dipping is carried out into recrystallization annealing under reduction or inert atmosphere protection, is cooled down;
6) by recrystallization annealing after first rolling sheets carry out mill secondary cold-rolling rolling, obtain light sheet;
7) by the light sheet defat for obtaining;
8) light sheet after defat is carried out into stress relief annealing under reduction or inert atmosphere protection, is cooled down;
9) light sheet after stress relief annealing is carried out into stretcher leveling, rip cutting/crosscutting, inspection, packaging and storage, obtains low oxygen content Aero titanium alloy precision sheet finished product.
2. the method for rolling and molding of low-oxygen content aero titanium alloy precision sheet according to claim 1, its feature exists In, the impregnation liquid into being grouped into:Ti(SO4)260-65g/L, BiCl350-60g/L, Fe3O40.02-0.04g/L, La2O36-8.5g/L, balance of water.
3. the method for rolling and molding of low-oxygen content aero titanium alloy precision sheet according to claim 1, its feature exists In the temperature of the dipping is 70 DEG C -85 DEG C.
4. the method for rolling and molding of low-oxygen content aero titanium alloy precision sheet according to claim 1, its feature exists In the time of the dipping is 4-9h.
5. the method for rolling and molding of the low-oxygen content aero titanium alloy precision sheet according to any one of claim 1-4, Characterized in that, the temperature of the recrystallization annealing is 800-830 DEG C.
6. the method for rolling and molding of the low-oxygen content aero titanium alloy precision sheet according to any one of claim 1-5, Characterized in that, the time of the recrystallization annealing is 15-25 minutes.
7. the method for rolling and molding of the low-oxygen content aero titanium alloy precision sheet according to any one of claim 1-6, Characterized in that, in the mill secondary cold-rolling operation of rolling, the work roll surface roughness control of mill At Ra0.2-0.3 μm, mill secondary cold-rolling pass deformation rate 50-65%.
8. the method for rolling and molding of low-oxygen content aero titanium alloy precision sheet according to claim 1, its feature exists In the temperature of the stress relief annealing is 550-620 DEG C.
9. the method for rolling and molding of low-oxygen content aero titanium alloy precision sheet according to claim 1, its feature exists In the time of the stress relief annealing is 15-20 minutes.
10. the method for rolling and molding of the low-oxygen content aero titanium alloy precision sheet according to any one of claim 1-9, Characterized in that, the aero titanium alloy board raw material is TC4 or TA15.
CN201610921646.2A 2016-10-21 2016-10-21 Rolling forming method for low-oxygen-content aero titanium alloy precision thin sheet Pending CN106623429A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610921646.2A CN106623429A (en) 2016-10-21 2016-10-21 Rolling forming method for low-oxygen-content aero titanium alloy precision thin sheet

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610921646.2A CN106623429A (en) 2016-10-21 2016-10-21 Rolling forming method for low-oxygen-content aero titanium alloy precision thin sheet

Publications (1)

Publication Number Publication Date
CN106623429A true CN106623429A (en) 2017-05-10

Family

ID=58855559

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610921646.2A Pending CN106623429A (en) 2016-10-21 2016-10-21 Rolling forming method for low-oxygen-content aero titanium alloy precision thin sheet

Country Status (1)

Country Link
CN (1) CN106623429A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108994077A (en) * 2018-06-13 2018-12-14 昆明理工大学 A kind of anisotropic milling method of weakening TC4 titanium alloy plate
CN113714286A (en) * 2021-08-31 2021-11-30 西北有色金属研究院 Preparation method of TA15 titanium alloy thin strip
CN114798798A (en) * 2022-04-24 2022-07-29 陕西创能新材料科技有限公司 Preparation method of TB8 titanium alloy plate

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101322977A (en) * 2008-07-25 2008-12-17 武钢集团昆明钢铁股份有限公司 Coil cold rolling industrial pure titanium plate coil
CN101665938A (en) * 2009-09-30 2010-03-10 华南理工大学 Preparation method of high anti-corrosion zinc coat titanium salt protective film
CN101817015A (en) * 2010-03-25 2010-09-01 江苏呈飞精密合金股份有限公司 Method for rolling and molding low-oxygen content aero titanium alloy precision sheet
CN102310314A (en) * 2011-07-01 2012-01-11 云南钛业股份有限公司 Processing method of titanium and titanium alloy strip coils
JP2012218010A (en) * 2011-04-05 2012-11-12 Nippon Steel Corp Shape measuring method in hot rolling of steel sheet and steel plate, and hot-rolling method of the same
CN103409781A (en) * 2013-08-05 2013-11-27 青岛农业大学 Preparation method for bismuth titanate film layer on basis of micro-arc oxidation technology
CN103706636A (en) * 2013-12-20 2014-04-09 湖南湘投金天钛金属有限公司 Method for producing metal titanium roll with thickness not more than 0.3mm through twenty-roller cold rolling unit
JP2014121725A (en) * 2012-12-21 2014-07-03 Jfe Steel Corp Plate thickness control method and plate thickness control device
CN104178757A (en) * 2014-08-08 2014-12-03 东北大学 Chromium-free composite passivator for hot-dip galvanized steel sheet and preparation and application methods of composite passivator
CN105154859A (en) * 2015-10-16 2015-12-16 首钢总公司 Weathering steel surface rust layer stabilization treating agent
CN105414178A (en) * 2015-12-10 2016-03-23 湖南湘投金天钛金属有限公司 Machining method for de-stressing thin pure titanium strip coils

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101322977A (en) * 2008-07-25 2008-12-17 武钢集团昆明钢铁股份有限公司 Coil cold rolling industrial pure titanium plate coil
CN101665938A (en) * 2009-09-30 2010-03-10 华南理工大学 Preparation method of high anti-corrosion zinc coat titanium salt protective film
CN101817015A (en) * 2010-03-25 2010-09-01 江苏呈飞精密合金股份有限公司 Method for rolling and molding low-oxygen content aero titanium alloy precision sheet
JP2012218010A (en) * 2011-04-05 2012-11-12 Nippon Steel Corp Shape measuring method in hot rolling of steel sheet and steel plate, and hot-rolling method of the same
CN102310314A (en) * 2011-07-01 2012-01-11 云南钛业股份有限公司 Processing method of titanium and titanium alloy strip coils
JP2014121725A (en) * 2012-12-21 2014-07-03 Jfe Steel Corp Plate thickness control method and plate thickness control device
CN103409781A (en) * 2013-08-05 2013-11-27 青岛农业大学 Preparation method for bismuth titanate film layer on basis of micro-arc oxidation technology
CN103706636A (en) * 2013-12-20 2014-04-09 湖南湘投金天钛金属有限公司 Method for producing metal titanium roll with thickness not more than 0.3mm through twenty-roller cold rolling unit
CN104178757A (en) * 2014-08-08 2014-12-03 东北大学 Chromium-free composite passivator for hot-dip galvanized steel sheet and preparation and application methods of composite passivator
CN105154859A (en) * 2015-10-16 2015-12-16 首钢总公司 Weathering steel surface rust layer stabilization treating agent
CN105414178A (en) * 2015-12-10 2016-03-23 湖南湘投金天钛金属有限公司 Machining method for de-stressing thin pure titanium strip coils

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108994077A (en) * 2018-06-13 2018-12-14 昆明理工大学 A kind of anisotropic milling method of weakening TC4 titanium alloy plate
CN108994077B (en) * 2018-06-13 2019-09-27 昆明理工大学 A kind of anisotropic milling method of weakening TC4 titanium alloy plate
CN113714286A (en) * 2021-08-31 2021-11-30 西北有色金属研究院 Preparation method of TA15 titanium alloy thin strip
CN113714286B (en) * 2021-08-31 2022-07-05 西北有色金属研究院 Preparation method of TA15 titanium alloy thin strip
CN114798798A (en) * 2022-04-24 2022-07-29 陕西创能新材料科技有限公司 Preparation method of TB8 titanium alloy plate
CN114798798B (en) * 2022-04-24 2024-04-12 陕西创能新材料科技有限公司 Preparation method of TB8 titanium alloy plate

Similar Documents

Publication Publication Date Title
CN101817015B (en) Method for rolling and molding low-oxygen content aero titanium alloy precision sheet
Boyer et al. Materials considerations for aerospace applications
CN104759625B (en) A kind of material and the method that use laser 3D printing technique to prepare aluminum alloy junction component
CN106623429A (en) Rolling forming method for low-oxygen-content aero titanium alloy precision thin sheet
CN101652240B (en) Method for hybrid composite panel systems
Lequeu et al. Engineering for the future: weight saving and cost reduction initiatives
Li et al. The shot peen forming of fiber metal laminates based on the aluminum-lithium alloy: Deformation characteristics
CN114367611B (en) Magnesium alloy revolving body structural member and preparation process thereof
CN102021296A (en) Method for rolling and forming low-oxygen-content pure-titanium precise thin strip coiled material
CN110977108A (en) Ti2Electric arc additive manufacturing method of AlNb-based alloy structural member and device used by same
Grechnikov et al. A manufacturability improvement of glass-fiber reinforced aluminum laminate by forming an effective crystallographic texture in V95 alloy sheets
EP3056579B1 (en) Method for manufacturing anodized aluminum alloy parts without surface discoloration
CN106513457A (en) Preparation method for near-beta titanium alloy disc spring
Baranov et al. The research of the cold rolling modes for plates of aluminum alloy sparingly doped with scandium
Hu et al. Carbon Fiber Breakage Mechanism in Aluminum (Al)/Carbon Fibers (CFs) Composite Sheet during Accumulative Roll Bonding (ARB) Process
CN109487185A (en) A kind of progressive creep age forming technique of Complex Aluminum Alloy component
Teichmann et al. Buckling of sandwich cylinders under axial compression
Chernikov et al. Research of different processes for forming fiber metal laminates
CN106890851B (en) A kind of magnesium-based composite board and the milling method for regulating and controlling magnesium-based composite board texture
Glushchenkov et al. Electro-magnetic forming of fiber metal laminates
Zheng et al. The effect of laser shock peening on the microstructure and High-Temperature mechanical properties of AZ31 alloy
Wu et al. Microstructure, mechanical properties and post-weld heat treatments of dissimilar laser-welded Ti 2 AlNb/Ti60 sheet
CN109365640A (en) A kind of lightweight magnesium alloy instrument support product ausforming method
Erisov et al. Structure and anisotropy of the mechanical properties of hot-and cold-rolled semi-finished products from aluminium-lithium alloys
CN109161759A (en) A method of improving magnesium alloy plate punching performance

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20170510

WD01 Invention patent application deemed withdrawn after publication