CN106619216A - Essential oil microcapsule inclusion, as well as preparation method and application thereof - Google Patents
Essential oil microcapsule inclusion, as well as preparation method and application thereof Download PDFInfo
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- CN106619216A CN106619216A CN201610913737.1A CN201610913737A CN106619216A CN 106619216 A CN106619216 A CN 106619216A CN 201610913737 A CN201610913737 A CN 201610913737A CN 106619216 A CN106619216 A CN 106619216A
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- essential oil
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- Veterinary Medicine (AREA)
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- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to the technical field of chemicals for daily use, and discloses an essential oil microcapsule inclusion, as well as a preparation method and application thereof. The essential oil microcapsule inclusion is prepared from the following components in percentage by mass: 5 to 25 percent of sucrose palmitate, 4 to 12 percent of glyceryl linoleate, 1 to 5 percent of candlenut seed oil, 1 to 5 percent of squalane, 1 to 3 percent of lavender oil, 0.5 to 1.5 percent of sage clary oil, 0.5 to 1.5 percent of caprylic/capric triglyceride, 0.05 to 0.15 percent of sodium hyaluronate, 0.3 to 1 percent of carrot seed oil, 0.3 to 1 percent of parsley seed oil, 0.2 to 0.7 percent of camellia seed oil, 0.05 to 0.15 percent of Indian bdellium extract, 0.5 to 1.5 percent of phenoxyethanol and the balance of water. A multi-layer microcapsule with a plurality of bimolecular layers is prepared; the skin permeability is optimized; layer-by-layer controlled release is realized; active ingredients are released in deep layer of skin; a remarkable skincare effect is achieved.
Description
Technical field
The invention belongs to household chemicals technical field, more particularly to a kind of essential oil micro-capsule inclusion enclave and preparation method thereof with
Using.
Background technology
Essential oil is a kind of natural plant essence, the usual root extracted from plant, stem, leaf, flower, pericarp or resin, is a kind of
With including the multi-functional aromatic material including skin-protecting function.Because it typically has effumability, in production and storage and transport process
In many compositions easily loss and aoxidize, cause the organoleptic attribute of its flavor component and the change of skin-protecting function, while low water
Dissolubility also causes stable, the decentralized formulation of production highly difficult.To its storage and using bringing inconvenience.
Essential oil micro-capsule inclusion enclave is the effective means for solving these problems.Micro-capsule technique for packing is by lipid bilayer shape
Into constituted 10～1000 layers of lipid film the ultra-fine micro-capsule of Multi-layer spherical, about 1～100 μm of its diameter, essential oil is wrapped
It is rolled between multilayer lipid film, forms essential oil micro-capsule inclusion enclave.It can with the storage of effective protection essential oil isoreactivity composition, use
When open layer by layer, deep skin success discharge active component.
The content of the invention
In order to overcome the shortcoming and deficiency of above-mentioned prior art, the primary and foremost purpose of the present invention is to provide a kind of essential oil micro-capsule
Inclusion enclave.
The present invention utilizes micro-capsule package technology, will be including Lavender, Salvia japonica essential oil, carrot seed essential oil, parsley
Essential oil is rolled into the Multi-layer microcapsule of 1～100 μm of 10～1000 bilayers in interior active component, effectively realizes essential oil
Control release, and polymolecular layer can sustained release layer by layer, realize long-acting slow-release and excellent permeability.Wrapped up more by micro-capsule
Be conducive to the preservation steady in a long-term of essential oil.
Another object of the present invention is to provide a kind of preparation method of above-mentioned essential oil micro-capsule inclusion enclave.
It is still another object of the present invention to provide application of the above-mentioned essential oil micro-capsule inclusion enclave in household chemicals.
The present invention essential oil micro-capsule inclusion enclave be added in household chemicals, particularly in skin care item can deep skin into
Work(discharges active ingredients of essential oils, optimizes percutaneous permeability, and can preserve steadily in the long term in skin care item, obtains significant skin care work(
Effect.
The purpose of the present invention is realized by following proposal：
A kind of essential oil micro-capsule inclusion enclave, is prepared by the component including following mass percent：
Essential oil micro-capsule inclusion enclave of the present invention, is preferably prepared by the component including following mass percent：
In inventive formulation, the various plants essential oils of employing are the plant essences extracted from pure plant, contain number
Hundred kinds of natural organic nutrient contents and various trace elements, effect is extensive.Wherein it is classified as essential in British Pharmacopoeia magazine
Standing good medicine-Lavender, can be directly used for skin, can promote cytothesis, recover skin connective tissue, while balance
Skin surface fat secretion, sensitive skin of releiving, convergence pore, supplementary skin moisture, persistently protect skin not receive whelk powder
Thorn interference, it is used cooperatively with Salvia japonica essential oil, multi-efficiency synergy, can rapidly be penetrated into skin and be suppressed bacterium life
It is long, it is to avoid to cause skin infection to cause acne, small pox problem, with it is calm, pacify, balance skin fat secretion, shrink thick
Pore, the effect of the skin that compacts promotes cytothesis, repairs impaired skin, recovers skin vigor, greatly improves deep layer and repaiies
Multiple effect, improves the resistance of skin.Salvia japonica essential oil has anti-inflammatory, convergence skin and promotes the function of wound healing,
Any skin quality is all suitable for, there is good oil-control performance, skin enlarged pores can be restrained, recover elasticity of skin, beautification skin.Recklessly
Radish seed essential oil can improve the colour of skin, make skin consolidation flexible.Reepithelialization, the generation of pre- anti-wrinkle can be facilitated, used
Skin afterwards youthens vibrant.Parsley essential oil has promotion microcirculatory blood circulation, highlights skin complexion function.
The present invention also provides a kind of preparation method of above-mentioned essential oil micro-capsule inclusion enclave, comprises the following steps：
By sucrose palmitate, Sodium Hyaluronate, India's poponax resin extract, Phenoxyethanol mixing, stir, plus
To 70～75 DEG C, one side constant speed is persistently added dropwise water to heat, while sequentially adding Dimodan, candlenut tree seed oil, saualane, smoking clothing
Careless oil, sage clary oil, caprylic/capric triglyceride, carrot seed oil, parsley seed oil, camellia seed oil, low velocity shear stirring, cooling
To normal temperature, essential oil micro-capsule inclusion enclave is obtained.
In preparation method of the present invention, after the heating preferably first drop add water to the water yield more than or equal to sucrose palmitate, thoroughly
The total amount of bright matter acid sodium, India's poponax resin extract and Phenoxyethanol, sequentially adds other reagents.
The inventive method utilizes micro-capsule package technology, by during water is added dropwise, oil phase substance being added, due to oil
Phase/watr-proportion changes, system in the phase co-conversion of oil phase-water phase-oil phase, so as to realize will be including lavender oil, mouse
Tail grass essential oil, carrot seed oil, parsley seed oil are rolled into 1～100 μm of 10～1000 bilayers in interior active component
Multi-layer microcapsule, effectively realizes the control release of essential oil, and polymolecular layer can sustained release layer by layer, realize long-acting slow-release and excellent
Permeability.The preservation steady in a long-term of essential oil is more beneficial for by micro-capsule parcel.
The essential oil micro-capsule inclusion enclave of the present invention can be applicable in household chemicals, special in being added to household chemicals
It is not can successfully to discharge active ingredients of essential oils in deep skin in skin care item, optimizes percutaneous permeability, and can grows in skin care item
Phase stably preserves, and obtains significant skin-care effect.
The present invention has the following advantages and beneficial effect relative to prior art：
(1) essential oil micro-capsule inclusion enclave of the invention is the Multi-layer microcapsule to form multiple bilayers, effectively realizes essential oil
Control release, and polymolecular layer can sustained release layer by layer, successfully discharge active ingredients of essential oils in deep skin.
(2) essential oil micro-capsule inclusion enclave of the invention effectively optimizes the percutaneous permeability of essential oil, than the essential oil skin not wrapped up
Permeability is more preferable, so as to obtain significant skin-care effect.
(3) essential oil micro-capsule inclusion enclave of the invention is conducive to it in skin care item by the parcel to essential oil isoreactivity composition
In preservation steady in a long-term.
Description of the drawings
Fig. 1 is the structural representation of essential oil micro-capsule inclusion enclave of the present invention, wherein, 1 is water phase, and 2 is bilayer oil phase.
Specific embodiment
With reference to embodiment and accompanying drawing, the present invention is described in further detail, but embodiments of the present invention are not limited
In this.Reagent used in the following example can be obtained from commercial channel.Wherein preparation method operation is routinely grasped for this area
Make method, in addition to specified otherwise.
Embodiment 1
A kind of preparation of essential oil micro-capsule inclusion enclave, comprises the following steps：
By sucrose palmitate, Sodium Hyaluronate, India's poponax resin extract, Phenoxyethanol mixing, stir, plus
To 70～75 DEG C, one side constant speed is persistently added dropwise water to heat, while sequentially adding Dimodan, candlenut tree seed oil, saualane, smoking clothing
Careless oil, Salvia japonica essential oil, caprylic/capric triglyceride, carrot seed oil, parsley seed oil, camellia seed oil, low velocity shear stirring is cold
But normal temperature is arrived, essential oil micro-capsule inclusion enclave is obtained.Structure observation is carried out to it, its structural representation such as Fig. 1.
Wherein, the mass percent of each component is：Sucrose palmitate 15%；Dimodan 8%；Candlenut tree seed oil
3%；Saualane 3%；Lavender oil 2%；Salvia japonica essential oil 1%；Caprylic/capric triglyceride 1%；Sodium Hyaluronate 0.1%；
Carrot seed oil 0.5%；Parsley seed oil 0.5%；Camellia seed oil 0.5%；India poponax resin extract 0.1%；Phenoxyethanol
1%；Water surplus.
Embodiment 2
A kind of preparation of essential oil micro-capsule inclusion enclave, comprises the following steps：
By sucrose palmitate, Sodium Hyaluronate, India's poponax resin extract, Phenoxyethanol mixing, stir, plus
To 70～75 DEG C, one side constant speed is persistently added dropwise water to heat, while sequentially adding Dimodan, candlenut tree seed oil, saualane, smoking clothing
Careless oil, Salvia japonica essential oil, caprylic/capric triglyceride, carrot seed oil, parsley seed oil, camellia seed oil, low velocity shear stirring is cold
But normal temperature is arrived, essential oil micro-capsule inclusion enclave is obtained.
Wherein, the mass percent of each component is：Sucrose palmitate 10%；Dimodan 10%；Candlenut tree seed oil
2%；Saualane 2%；Lavender oil 2.5%；Salvia japonica essential oil 1.5%；Caprylic/capric triglyceride 1.5%；Sodium Hyaluronate
0.05%；Carrot seed oil 0.8%；Parsley seed oil 0.8%；Camellia seed oil 0.5%；India poponax resin extract 0.05%；Benzene
Oxyethanol 1%；Water surplus.
Embodiment 3
A kind of preparation of essential oil micro-capsule inclusion enclave, comprises the following steps：
By sucrose palmitate, Sodium Hyaluronate, India's poponax resin extract, Phenoxyethanol mixing, stir, plus
To 70～75 DEG C, one side constant speed is persistently added dropwise water to heat, while sequentially adding Dimodan, candlenut tree seed oil, saualane, smoking clothing
Careless oil, Salvia japonica essential oil, caprylic/capric triglyceride, carrot seed oil, parsley seed oil, camellia seed oil, low velocity shear stirring is cold
But normal temperature is arrived, essential oil micro-capsule inclusion enclave is obtained.
Wherein, the mass percent of each component is：Sucrose palmitate 20%；Dimodan 5%；Candlenut tree seed oil
4%；Saualane 4%；Lavender oil 1.5%；Salvia japonica essential oil 0.5%；Caprylic/capric triglyceride 0.5%；Sodium Hyaluronate
0.15%；Carrot seed oil 0.4%；Parsley seed oil 0.4%；Camellia seed oil 0.5%；India poponax resin extract 0.15%；Benzene
Oxyethanol 1%；Water surplus.
Embodiment 4：Comparative example
A kind of essential oil composition, is uniformly mixed with oil based on wheat-germ oil and is made.Wherein, the matter of each component
Measuring percentage is：Lavender oil 2%, Salvia japonica essential oil 1%, carrot seed oil 0.5%, parsley seed oil 0.5%, wheat-germ oil：
96%.
Embodiment 5：Performance test
By taking the essential oil micro-capsule inclusion enclave that embodiment 1 is prepared as an example, the essential oil composition of embodiment 4 as a comparison case,
In being respectively added to skin care item emulsion and cream, experimenter smears respectively the test formulations containing the essential oil micro-capsule and without this
The test formulations of essential oil micro-capsule, determine its skin moisture content growth rate after 2 hours, after continuously smearing 4 weeks daily 2 times it is determined
Skin elasticity growth rate and melanin content reduced rate, test formulations and the results are shown in Table 1～2.
Test formulations (the unit of table 1：Wt%)
The test performance parameter of table 2
| Test event | Formula 1 | Formula 2 | Formula 3 | Formula 4 | Formula 5 |
| Moisture content of skin growth rate/% | 22.7 | 43.9 | 22.7 | 52.0 | 31.5 |
| Skin elasticity growth rate/% | 16.5 | 37.0 | 17.4 | 39.6 | 23.2 |
| Dermal melanin content reduced rate/% | 2.3 | 27.0 | 2.1 | 29.1 | 9.8 |
Visible according to the test result of table 2, the emulsion and cream ratio for being added with the essential oil micro-capsule inclusion enclave of embodiment 1 is not added with
The test formulations of the essential oil micro-capsule inclusion enclave of embodiment 1, moisture content of skin growth rate, skin elasticity growth rate and melanin content drop
Low rate is obviously improved.Show that the essential oil micro-capsule inclusion enclave of embodiment 1 has good moisturizing, lifts skin elasticity and reduces skin
The function of melanin content.
Simultaneously the test data of formula 4 and formula 5 also indicates that the essential oil micro-capsule inclusion enclave of the present invention is multiple due to defining
The Multi-layer microcapsule of bilayer, effectively realizes the control release of essential oil, and polymolecular layer can sustained release layer by layer, in skin depth
Layer successfully discharges active ingredients of essential oils, and the effectively percutaneous permeability of optimization essential oil, than the essential oil percutaneous permeability that do not wrap up more
It is good, so as to obtain significant skin-care effect.Its water content, skin elasticity, reduction dermal melanin content to improving skin,
It is more more notable than the plant essential oil composition skin-care effect that embodiment 4 does not carry out micro-capsule parcel.
Above-described embodiment is the present invention preferably embodiment, but embodiments of the present invention not by above-described embodiment
Limit, other any Spirit Essences without departing from the present invention and the change, modification, replacement made under principle, combine, simplification,
Equivalent substitute mode is should be, is included within protection scope of the present invention.
Claims (6)
1. a kind of essential oil micro-capsule inclusion enclave, it is characterised in that prepared by the component including following mass percent：
2. essential oil micro-capsule inclusion enclave according to claim 1, it is characterised in that by the component including following mass percent
Prepare：
3. the preparation method of the essential oil micro-capsule inclusion enclave described in a kind of any one of claim 1～2, it is characterised in that including following
Step：
By sucrose palmitate, Sodium Hyaluronate, India's poponax resin extract, Phenoxyethanol mixing, stir, be heated to
70～75 DEG C, one side constant speed is persistently added dropwise water, while sequentially adding Dimodan, candlenut tree seed oil, saualane, lavender
Oil, sage clary oil, caprylic/capric triglyceride, carrot seed oil, parsley seed oil, camellia seed oil, low velocity shear stirring, are cooled to
Normal temperature, obtains essential oil micro-capsule inclusion enclave.
4. the preparation method of essential oil micro-capsule inclusion enclave according to claim 3, it is characterised in that：First it is added dropwise after the heating
Water is more than or equal to the total amount of sucrose palmitate, Sodium Hyaluronate, India's poponax resin extract and Phenoxyethanol to the water yield, then
Sequentially add other reagents.
5. application of the essential oil micro-capsule inclusion enclave described in any one of claim 1～2 in household chemicals.
6. application of the essential oil micro-capsule inclusion enclave described in any one of claim 1～2 in skin care item.
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| CN201610913737.1A CN106619216A (en) | 2016-10-20 | 2016-10-20 | Essential oil microcapsule inclusion, as well as preparation method and application thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112791170A (en) * | 2021-03-22 | 2021-05-14 | 广州市天芳中医医药科技有限公司 | Female vagina tightening and sensitivity traditional Chinese medicine composition, gel obtained from same and application of gel |
| CN112932998A (en) * | 2021-02-07 | 2021-06-11 | 山东省纤靓惠品牌管理有限责任公司 | Chest essential oil gel and application thereof |
| CN116942569A (en) * | 2023-09-20 | 2023-10-27 | 广东顺德芳香世家天然产品制造有限公司 | Essential oil composition containing kuquai oil and application thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112932998A (en) * | 2021-02-07 | 2021-06-11 | 山东省纤靓惠品牌管理有限责任公司 | Chest essential oil gel and application thereof |
| CN112791170A (en) * | 2021-03-22 | 2021-05-14 | 广州市天芳中医医药科技有限公司 | Female vagina tightening and sensitivity traditional Chinese medicine composition, gel obtained from same and application of gel |
| CN116942569A (en) * | 2023-09-20 | 2023-10-27 | 广东顺德芳香世家天然产品制造有限公司 | Essential oil composition containing kuquai oil and application thereof |
| CN116942569B (en) * | 2023-09-20 | 2023-12-15 | 广东顺德芳香世家天然产品制造有限公司 | Essential oil composition containing kuquai oil and application thereof |
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Application publication date: 20170510 |